DTA measure 2gyors Date: 2026224:1132 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.29 s Mass = 968.000 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3379 -4.7826 459.5578 464.3403 433.3832 3.9464 -4.7980 459.5519 464.3499 433.6219 5.5343 -4.8087 459.5658 464.3745 433.8174 7.1429 -4.8177 459.5648 464.3825 433.9340 8.7564 -4.8252 459.5684 464.3936 433.9331 10.3598 -4.8358 459.5828 464.4186 433.8655 11.9836 -4.8455 459.6296 464.4751 433.7062 13.5716 -4.8489 459.6432 464.4921 433.4317 15.1804 -4.8563 459.6745 464.5308 433.1327 16.7838 -4.8658 459.6892 464.5550 432.7331 18.3921 -4.8775 459.7077 464.5852 432.2488 20.0006 -4.8783 459.7328 464.6111 431.7008 21.6039 -4.8805 459.7291 464.6096 431.1933 23.2125 -4.8835 459.7190 464.6025 430.7004 24.8313 -4.8801 459.7026 464.5827 430.2336 26.4396 -4.8803 459.6868 464.5671 429.7802 28.0483 -4.8875 459.7120 464.5994 429.3472 29.6566 -4.8869 459.6903 464.5772 428.9692 31.2600 -4.8899 459.6950 464.5849 428.6136 32.8735 -4.8930 459.6612 464.5541 428.3668 34.4769 -4.8895 459.6370 464.5265 428.1992 36.1060 -4.8929 459.6070 464.4999 428.0920 37.7093 -4.8982 459.5728 464.4710 427.9825 39.3229 -4.9007 459.5300 464.4307 427.9425 40.9264 -4.9049 459.5028 464.4077 427.9779 42.5399 -4.9056 459.4364 464.3421 428.0258 44.1280 -4.9061 459.4134 464.3194 428.0308 45.7364 -4.9100 459.3634 464.2734 428.0427 47.3398 -4.9169 459.3248 464.2418 427.9969 48.9689 -4.9196 459.2827 464.2023 427.9561 50.5774 -4.9255 459.2347 464.1602 427.8473 52.1859 -4.9235 459.1908 464.1143 427.6864 53.7894 -4.9272 459.1757 464.1029 427.4972 55.3979 -4.9319 459.1276 464.0595 427.2174 56.9961 -4.9408 459.1106 464.0514 426.9589 58.5945 -4.9475 459.0566 464.0041 426.6632 60.1979 -4.9488 459.0278 463.9766 426.3058 61.8013 -4.9516 458.9750 463.9266 425.9214 63.4048 -4.9549 458.8953 463.8502 425.5329 65.0030 -4.9579 458.8166 463.7745 425.1677 66.6115 -4.9624 458.7224 463.6848 424.8329 68.1996 -4.9693 458.6505 463.6198 424.4927 69.8081 -4.9660 458.6011 463.5672 424.2000 71.4114 -4.9647 458.5177 463.4824 423.9254 73.0201 -4.9643 458.4381 463.4024 423.6836 74.6235 -4.9695 458.3402 463.3097 423.4873 76.2269 -4.9693 458.2692 463.2384 423.3062 77.8354 -4.9703 458.1772 463.1475 423.1235 79.4386 -4.9708 458.1415 463.1123 422.9855 81.0473 -4.9688 458.0659 463.0347 422.8656 82.6508 -4.9738 458.0244 462.9982 422.7623 84.2591 -4.9762 457.9297 462.9059 422.6216 85.8626 -4.9785 457.7869 462.7654 422.5158 87.4815 -4.9775 457.7092 462.6867 422.4050 89.0899 -4.9821 457.6335 462.6156 422.2983 90.6986 -4.9869 457.5708 462.5578 422.2072 92.2919 -4.9896 457.5179 462.5074 422.0962 93.8953 -4.9892 457.3928 462.3820 421.9460 95.5036 -4.9905 457.2594 462.2499 421.7746 97.1123 -4.9920 457.1407 462.1328 421.5218 98.7206 -4.9878 457.0275 462.0153 421.2755 100.3446 -4.9874 456.9294 461.9168 420.9942 101.9530 -4.9838 456.8329 461.8167 420.7038 103.5615 -4.9920 456.7638 461.7557 420.4337 105.1700 -4.9957 456.6895 461.6852 420.1310 106.7733 -4.9961 456.5292 461.5253 419.8307 108.3818 -4.9939 456.4214 461.4154 419.5580 109.9901 -4.9952 456.3324 461.3276 419.2510 111.5834 -4.9983 456.2368 461.2351 419.0072 113.2021 -4.9964 456.1126 461.1090 418.7768 114.8209 -4.9970 456.0118 461.0088 418.5177 116.4191 -4.9970 455.9158 460.9129 418.2906 118.0276 -4.9968 455.7929 460.7896 418.1059 119.6360 -4.9916 455.6379 460.6296 417.8855 121.2344 -4.9929 455.5071 460.5000 417.6923 122.8428 -4.9980 455.4054 460.4034 417.5166 124.4410 -5.0000 455.2772 460.2772 417.3429 126.0445 -4.9958 455.1559 460.1516 417.1949 127.6479 -4.9931 455.0184 460.0115 417.0323 129.2514 -4.9888 454.9033 459.8922 416.8633 130.8548 -4.9887 454.8010 459.7897 416.6802 132.4579 -4.9984 454.6717 459.6701 416.5410 134.0614 -5.0015 454.5509 459.5525 416.3650 135.6696 -5.0015 454.4219 459.4234 416.2044 137.2885 -4.9934 454.2799 459.2733 416.0122 138.8971 -4.9924 454.1433 459.1357 415.8421 140.5004 -4.9945 454.0129 459.0074 415.6326 142.1039 -4.9933 453.8389 458.8322 415.4356 143.7125 -4.9879 453.6867 458.6745 415.2122 145.3156 -4.9818 453.5452 458.5270 414.9419 146.9243 -4.9806 453.3601 458.3408 414.7261 148.5120 -4.9825 453.2517 458.2341 414.4670 150.1360 -4.9856 453.1232 458.1087 414.2222 151.7394 -4.9830 452.9702 457.9532 413.9621 153.3529 -4.9839 452.7964 457.7803 413.7029 154.9564 -4.9841 452.6792 457.6632 413.4350 156.5596 -4.9787 452.5490 457.5278 413.2029 158.1734 -4.9762 452.3884 457.3645 412.9759 159.7768 -4.9704 452.2645 457.2349 412.7459 161.4056 -4.9706 452.1079 457.0785 412.5211 162.9938 -4.9726 451.9576 456.9302 412.3391 164.6074 -4.9714 451.8283 456.7996 412.1297 166.2106 -4.9662 451.6839 456.6501 411.9782 167.8244 -4.9655 451.4866 456.4520 411.8105 169.4275 -4.9637 451.3224 456.2860 411.6415 171.0360 -4.9627 451.1633 456.1259 411.4681 172.6241 -4.9572 451.0089 455.9662 411.2860 174.2325 -4.9561 450.8374 455.7935 411.1164 175.8564 -4.9531 450.7161 455.6691 410.9316 177.4648 -4.9519 450.5115 455.4634 410.7499 179.0681 -4.9521 450.3489 455.3009 410.5177 180.6819 -4.9472 450.1930 455.1401 410.2679 182.2853 -4.9432 449.9949 454.9381 410.0593 183.8835 -4.9400 449.8568 454.7968 409.8582 185.4766 -4.9362 449.7122 454.6484 409.6496 187.0749 -4.9349 449.5625 454.4974 409.4210 188.6938 -4.9373 449.4068 454.3442 409.1976 190.2815 -4.9350 449.2235 454.1584 408.9687 191.8851 -4.9329 449.0237 453.9566 408.7367 193.4885 -4.9274 448.8238 453.7512 408.5455 195.0918 -4.9210 448.6964 453.6173 408.3171 196.6951 -4.9182 448.5330 453.4513 408.0645 198.3035 -4.9153 448.3764 453.2918 407.8144 199.9069 -4.9127 448.2203 453.1330 407.5800 201.5000 -4.9103 448.0241 452.9344 407.3586 203.1186 -4.9089 447.8626 452.7714 407.1370 204.7273 -4.9048 447.7258 452.6305 406.9634 206.3305 -4.8985 447.5735 452.4721 406.7724 207.9339 -4.8953 447.4264 452.3217 406.5922 209.5425 -4.8889 447.2484 452.1373 406.4223 211.1456 -4.8881 447.0548 451.9429 406.2404 212.7541 -4.8838 446.8514 451.7352 406.0438 214.3728 -4.8883 446.6593 451.5476 405.8333 215.9865 -4.8833 446.4837 451.3669 405.6406 217.5898 -4.8801 446.3609 451.2410 405.4408 219.1983 -4.8763 446.2126 451.0889 405.2044 220.8018 -4.8766 446.0115 450.8881 404.9967 222.4154 -4.8763 445.8270 450.7032 404.7923 224.0188 -4.8679 445.6263 450.4942 404.5983 225.6274 -4.8609 445.4577 450.3186 404.3764 227.2356 -4.8569 445.2784 450.1353 404.1745 228.8393 -4.8537 445.0632 449.9168 403.9878 230.4530 -4.8504 444.9037 449.7541 403.7548 232.0564 -4.8419 444.7280 449.5699 403.4935 233.6701 -4.8344 444.5260 449.3603 403.2458 235.2735 -4.8330 444.3148 449.1478 402.9993 236.8871 -4.8300 444.1529 448.9829 402.8093 238.5060 -4.8279 444.0029 448.8308 402.5694 240.1146 -4.8248 443.8147 448.6395 402.3677 241.7181 -4.8222 443.6141 448.4363 402.1395 243.3315 -4.8192 443.4289 448.2481 401.9159 244.9351 -4.8168 443.2435 448.0603 401.6943 246.5436 -4.8106 443.0732 447.8838 401.5107 248.1470 -4.8045 442.8609 447.6654 401.2985 249.7659 -4.7998 442.6874 447.4872 401.1001 251.3693 -4.7974 442.5262 447.3236 400.9107 252.9674 -4.7923 442.3632 447.1555 400.7380 254.5709 -4.7872 442.1755 446.9627 400.5395 256.1745 -4.7858 442.0176 446.8034 400.3366 257.7623 -4.7848 441.8169 446.6017 400.1321 259.3709 -4.7773 441.5951 446.3724 399.9372 260.9741 -4.7711 441.3784 446.1495 399.7545 262.5673 -4.7674 441.1487 445.9161 399.5138 264.1861 -4.7680 440.9639 445.7319 399.3002 265.7894 -4.7672 440.8171 445.5843 399.1067 267.3980 -4.7596 440.6100 445.3696 398.8806 268.9911 -4.7522 440.4368 445.1890 398.6544 270.5995 -4.7451 440.2444 444.9896 398.4699 272.2030 -4.7413 440.0589 444.8002 398.2680 273.8061 -4.7378 439.8367 444.5745 398.0450 275.4095 -4.7317 439.6369 444.3686 397.8127 277.0180 -4.7339 439.4584 444.1923 397.6282 278.6368 -4.7256 439.3027 444.0283 397.4209 280.2454 -4.7220 439.1253 443.8472 397.1778 281.8485 -4.7175 438.8958 443.6133 396.9857 283.4418 -4.7114 438.7026 443.4140 396.7853 285.0503 -4.7080 438.4580 443.1660 396.5905 286.6588 -4.7059 438.2665 442.9725 396.3773 288.2673 -4.7022 438.1294 442.8316 396.1749 289.8759 -4.6995 437.9464 442.6459 395.9514 291.4793 -4.6993 437.7471 442.4464 395.7088 293.0929 -4.6910 437.5958 442.2868 395.4575 294.6963 -4.6863 437.3608 442.0470 395.2798 296.2996 -4.6814 437.1441 441.8255 395.0889 297.9083 -4.6771 436.9620 441.6391 394.8792 299.5116 -4.6690 436.7874 441.4564 394.6495 301.1253 -4.6628 436.5881 441.2508 394.4166 302.7286 -4.6607 436.3565 441.0172 394.2280 304.3575 -4.6536 436.1568 440.8104 394.0075 305.9610 -4.6472 435.9842 440.6314 393.7566 307.5696 -4.6415 435.7926 440.4341 393.5311 309.1730 -4.6398 435.5963 440.2361 393.3040 310.7868 -4.6330 435.3922 440.0252 393.0620 312.3901 -4.6258 435.1761 439.8019 392.8675 313.9729 -4.6229 434.9657 439.5886 392.6967 315.5764 -4.6216 434.7428 439.3644 392.4787 317.1901 -4.6177 434.5408 439.1585 392.2557 318.7935 -4.6098 434.3289 438.9386 392.0401 320.4020 -4.6038 434.1316 438.7353 391.8569 322.0055 -4.6002 433.9521 438.5523 391.6657 323.6088 -4.5949 433.6934 438.2883 391.4796 325.2124 -4.5885 433.5004 438.0889 391.2829 326.8159 -4.5831 433.3290 437.9121 391.0466 328.4241 -4.5755 433.1412 437.7167 390.8483 330.0226 -4.5733 432.9649 437.5382 390.6537 331.6311 -4.5694 432.7813 437.3507 390.4440 333.2395 -4.5648 432.5501 437.1149 390.2263 334.8481 -4.5639 432.3239 436.8878 390.0165 336.4516 -4.5597 432.0961 436.6558 389.7937 338.0549 -4.5492 431.8991 436.4483 389.5767 339.6635 -4.5368 431.7335 436.2703 389.3744 341.2824 -4.5314 431.5420 436.0734 389.2166 342.8906 -4.5226 431.3078 435.8304 389.0134 344.4941 -4.5187 431.1246 435.6433 388.8041 346.1075 -4.5143 430.9366 435.4509 388.6129 347.7109 -4.5111 430.7428 435.2539 388.3533 349.3245 -4.5029 430.5491 435.0521 388.1055 350.9279 -4.4978 430.3352 434.8330 387.8495 352.5415 -4.4930 430.1404 434.6334 387.6221 354.1448 -4.4907 429.9413 434.4319 387.4063 355.7688 -4.4898 429.7010 434.1909 387.1795 357.3721 -4.4867 429.5340 434.0208 386.9459 358.9858 -4.4778 429.3239 433.8017 386.7673 360.5739 -4.4704 429.0979 433.5684 386.5442 362.2029 -4.4657 428.8842 433.3499 386.3291 363.8061 -4.4590 428.6988 433.1578 386.1035 365.4096 -4.4484 428.4938 432.9422 385.8891 367.0233 -4.4398 428.2745 432.7143 385.6376 368.6266 -4.4335 428.0584 432.4919 385.4523 370.2403 -4.4253 427.8228 432.2481 385.2693 371.8435 -4.4248 427.5882 432.0130 385.0593 373.4574 -4.4176 427.3749 431.7925 384.8224 375.0609 -4.4217 427.1580 431.5797 384.6119 376.6694 -4.4137 426.9524 431.3661 384.4424 378.2676 -4.4080 426.7814 431.1895 384.2662 379.8711 -4.4013 426.6401 431.0414 384.0899 381.4744 -4.3927 426.4498 430.8425 383.9244 383.0726 -4.3871 426.1965 430.5836 383.7332 384.6608 -4.3760 426.0103 430.3864 383.5760 386.2639 -4.3688 425.7846 430.1533 383.3534 387.8623 -4.3665 425.5817 429.9482 383.1538 389.4709 -4.3655 425.3961 429.7616 382.9533 391.0895 -4.3578 425.1813 429.5392 382.7431 392.6776 -4.3549 424.9583 429.3133 382.5210 394.2861 -4.3519 424.7543 429.1061 382.2841 395.8895 -4.3476 424.5749 428.9225 382.0578 397.4980 -4.3416 424.3608 428.7024 381.8122 399.1013 -4.3358 424.1293 428.4652 381.5291 400.7099 -4.3299 423.8926 428.2225 381.2916 402.3031 -4.3217 423.6900 428.0117 381.0665 403.9114 -4.3193 423.4826 427.8019 380.8308 405.5303 -4.3123 423.3027 427.6150 380.6133 407.1334 -4.3049 423.1118 427.4167 380.4079 408.7420 -4.3077 422.9007 427.2085 380.1936 410.3455 -4.2998 422.6641 426.9639 379.9797 411.9539 -4.2884 422.4525 426.7410 379.7793 413.5573 -4.2759 422.2491 426.5250 379.6118 415.1709 -4.2662 422.0743 426.3405 379.4113 416.7896 -4.2610 421.8446 426.1056 379.2115 418.3983 -4.2567 421.6114 425.8682 378.9932 420.0016 -4.2535 421.3637 425.6172 378.7764 421.6255 -4.2460 421.1478 425.3938 378.5811 423.2188 -4.2453 420.9372 425.1825 378.3694 424.8273 -4.2388 420.7314 424.9702 378.1807 426.4358 -4.2321 420.5172 424.7493 378.0140 428.0545 -4.2239 420.2951 424.5190 377.8576 429.6631 -4.2255 420.0922 424.3177 377.6348 431.2664 -4.2204 419.9107 424.1311 377.4398 432.8750 -4.2163 419.7243 423.9406 377.2329 434.4833 -4.2084 419.5294 423.7378 377.0146 436.0919 -4.2003 419.2974 423.4977 376.8462 437.7004 -4.1962 419.0737 423.2699 376.6086 439.3396 -4.1877 418.8514 423.0391 376.3948 440.9278 -4.1798 418.6451 422.8249 376.1429 442.5309 -4.1761 418.4542 422.6303 375.9063 444.1293 -4.1693 418.2601 422.4293 375.7103 445.7328 -4.1644 418.0573 422.2217 375.4794 447.3411 -4.1547 417.8145 421.9693 375.2169 448.9445 -4.1485 417.5991 421.7475 375.0124 450.5581 -4.1474 417.4135 421.5609 374.7996 452.1666 -4.1451 417.2348 421.3799 374.5654 453.7700 -4.1373 417.0316 421.1690 374.3343 455.3630 -4.1324 416.8062 420.9386 374.0875 456.9665 -4.1318 416.5588 420.6906 373.8584 458.5698 -4.1220 416.3020 420.4240 373.6224 460.1781 -4.1112 416.1404 420.2516 373.4349 461.7816 -4.1052 415.9405 420.0457 373.2218 463.4054 -4.1005 415.6966 419.7971 373.0339 465.0089 -4.0902 415.5048 419.5950 372.8410 466.6174 -4.0817 415.3005 419.3822 372.6509 468.2206 -4.0778 415.0999 419.1777 372.4885 469.8344 -4.0752 414.8548 418.9300 372.3276 471.4429 -4.0724 414.6248 418.6973 372.1363 473.0514 -4.0636 414.4171 418.4807 371.9100 474.6549 -4.0544 414.2289 418.2833 371.7161 476.2788 -4.0552 414.0212 418.0764 371.4944 477.8873 -4.0505 413.8105 417.8610 371.2821 479.5009 -4.0437 413.6100 417.6537 371.0680 481.1091 -4.0421 413.3862 417.4282 370.8278 482.7178 -4.0427 413.1672 417.2100 370.5915 484.3260 -4.0386 412.9683 417.0069 370.3683 485.9346 -4.0302 412.7846 416.8148 370.1368 487.5534 -4.0232 412.5499 416.5730 369.9440 489.1670 -4.0183 412.3132 416.3316 369.7114 490.7704 -4.0108 412.1263 416.1371 369.4881 492.3790 -4.0007 411.9209 415.9216 369.2645 493.9824 -3.9923 411.7029 415.6952 369.0728 495.5960 -3.9839 411.4972 415.4811 368.8859 497.1994 -3.9765 411.2716 415.2481 368.6872 498.8231 -3.9686 411.0663 415.0348 368.4494 500.4318 -3.9586 410.8424 414.8010 368.2788 502.0401 -3.9565 410.6299 414.5864 368.0677 503.6436 -3.9482 410.4295 414.3777 367.8603 505.2471 -3.9428 410.2049 414.1477 367.6265 506.8504 -3.9358 410.0155 413.9513 367.4145 508.4538 -3.9263 409.8143 413.7406 367.2252 510.0571 -3.9257 409.5644 413.4902 367.0213 511.6605 -3.9217 409.3939 413.3156 366.7591 513.2588 -3.9209 409.1717 413.0927 366.5354 514.8670 -3.9111 408.9468 412.8579 366.3236 516.4655 -3.9032 408.7639 412.6671 366.1338 518.0689 -3.8986 408.5707 412.4693 365.9118 519.6773 -3.8917 408.3466 412.2383 365.6564 521.2808 -3.8900 408.1331 412.0232 365.4469 522.9044 -3.8876 407.9245 411.8121 365.2164 524.4925 -3.8831 407.7407 411.6238 364.9711 526.1010 -3.8760 407.5408 411.4169 364.7799 527.7094 -3.8647 407.3319 411.1966 364.5941 529.3179 -3.8565 407.1204 410.9769 364.4095 530.9211 -3.8505 406.9006 410.7511 364.2012 532.5246 -3.8450 406.6788 410.5238 364.0286 534.1333 -3.8370 406.3974 410.2344 363.8567 535.7570 -3.8313 406.1843 410.0157 363.6836 537.3656 -3.8221 405.9868 409.8089 363.4413 538.9586 -3.8209 405.7956 409.6165 363.2398 540.5671 -3.8160 405.5941 409.4101 363.0495 542.1706 -3.8125 405.3999 409.2124 362.8233 543.7791 -3.8101 405.1495 408.9596 362.5973 545.3876 -3.8026 404.9463 408.7490 362.3763 546.9964 -3.7928 404.7412 408.5340 362.1431 548.6153 -3.7832 404.5267 408.3099 361.9359 550.2236 -3.7784 404.3389 408.1173 361.7120 551.8271 -3.7753 404.1519 407.9271 361.4731 553.4358 -3.7775 403.9178 407.6954 361.2659 555.0440 -3.7722 403.7068 407.4791 361.0630 556.6526 -3.7647 403.4983 407.2631 360.8735 558.2610 -3.7552 403.2554 407.0106 360.6594 559.8798 -3.7503 403.0389 406.7892 360.4468 561.4779 -3.7463 402.8021 406.5484 360.2516 563.0915 -3.7428 402.5513 406.2940 360.0570 564.6950 -3.7387 402.3703 406.1091 359.8748 566.3084 -3.7310 402.1662 405.8973 359.6640 567.9119 -3.7234 401.9475 405.6709 359.4370 569.5153 -3.7119 401.7776 405.4896 359.2418 571.1185 -3.7091 401.5441 405.2533 359.0197 572.7374 -3.7051 401.3157 405.0208 358.8239 574.3356 -3.6988 401.1384 404.8372 358.5898 575.9390 -3.6959 400.9393 404.6352 358.3675 577.5271 -3.6946 400.7103 404.4049 358.1664 579.1251 -3.6838 400.4657 404.1494 357.9422 580.7338 -3.6753 400.2538 403.9290 357.7103 582.3373 -3.6691 400.0673 403.7364 357.5089 583.9456 -3.6622 399.8445 403.5066 357.2564 585.5645 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