DTA measure 1Cu_meres Date: 202541:1550 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 755.09 s Mass = 967.400 mg data_number = 1879 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.4840 -0.9075 238.5229 239.4305 268.3721 0.9655 -0.9053 238.6455 239.5508 268.3491 1.3440 -0.9038 238.7392 239.6430 268.3336 1.7020 -0.9024 238.8268 239.7292 268.3146 2.1220 -0.9005 238.9307 239.8312 268.2914 2.5625 -0.8983 239.0381 239.9364 268.2679 2.9200 -0.8971 239.1247 240.0218 268.2481 3.2990 -0.8947 239.2240 240.1186 268.2305 3.7185 -0.8925 239.3280 240.2205 268.2090 4.1595 -0.8910 239.4385 240.3295 268.1821 4.5170 -0.8896 239.5287 240.4183 268.1620 4.8750 -0.8882 239.6209 240.5090 268.1425 5.3775 -0.8861 239.7479 240.6340 268.1107 5.7350 -0.8842 239.8332 240.7174 268.0922 6.0930 -0.8823 239.9231 240.8054 268.0751 6.5335 -0.8802 240.0284 240.9086 268.0431 6.9535 -0.8786 240.1271 241.0056 268.0141 7.3115 -0.8773 240.2118 241.0891 267.9896 7.6900 -0.8755 240.3059 241.1815 267.9616 8.1720 -0.8738 240.4192 241.2931 267.9271 8.5500 -0.8722 240.5087 241.3809 267.9006 8.9080 -0.8703 240.5948 241.4650 267.8760 9.3485 -0.8685 240.6995 241.5680 267.8455 9.7680 -0.8664 240.7979 241.6643 267.8177 10.1260 -0.8654 240.8823 241.7476 267.7913 10.5045 -0.8636 240.9707 241.8342 267.7670 10.9860 -0.8606 241.0887 241.9494 267.7343 11.3440 -0.8594 241.1738 242.0332 267.7084 11.7230 -0.8578 241.2625 242.1203 267.6837 12.1635 -0.8556 241.3659 242.2216 267.6543 12.5830 -0.8537 241.4701 242.3238 267.6243 12.9410 -0.8523 241.5565 242.4088 267.5970 13.3195 -0.8507 241.6471 242.4977 267.5718 13.7390 -0.8491 241.7447 242.5938 267.5442 14.1590 -0.8472 241.8433 242.6906 267.5151 14.5375 -0.8454 241.9334 242.7789 267.4922 14.9160 -0.8437 242.0211 242.8648 267.4700 15.3980 -0.8409 242.1330 242.9739 267.4351 15.7555 -0.8389 242.2198 243.0588 267.4160 16.1340 -0.8374 242.3068 243.1442 267.3925 16.5540 -0.8358 242.4024 243.2382 267.3669 16.9735 -0.8329 242.4984 243.3313 267.3454 17.3520 -0.8308 242.5849 243.4157 267.3226 17.7100 -0.8297 242.6681 243.4978 267.3012 18.1920 -0.8273 242.7765 243.6038 267.2745 18.5705 -0.8254 242.8633 243.6887 267.2529 18.9490 -0.8232 242.9482 243.7714 267.2307 19.3690 -0.8212 243.0436 243.8648 267.2058 19.7885 -0.8191 243.1375 243.9566 267.1842 20.1670 -0.8172 243.2243 244.0414 267.1634 20.5250 -0.8157 243.3068 244.1225 267.1456 21.0065 -0.8135 243.4168 244.2303 267.1320 21.3850 -0.8118 243.5065 244.3183 267.1145 21.7635 -0.8097 243.5889 244.3986 267.0966 22.1830 -0.8079 243.6833 244.4912 267.0817 22.6030 -0.8059 243.7753 244.5812 267.0687 22.9815 -0.8045 243.8580 244.6625 267.0542 23.3390 -0.8029 243.9415 244.7444 267.0401 23.8215 -0.8010 244.0464 244.8474 267.0268 24.2000 -0.7995 244.1310 244.9304 267.0163 24.5580 -0.7984 244.2122 245.0106 267.0049 24.9980 -0.7968 244.3087 245.1055 266.9968 25.4180 -0.7952 244.4031 245.1983 266.9887 25.7965 -0.7938 244.4896 245.2834 266.9789 26.1540 -0.7921 244.5702 245.3623 266.9731 26.6365 -0.7899 244.6800 245.4699 266.9634 27.0145 -0.7885 244.7648 245.5533 266.9573 27.3935 -0.7869 244.8442 245.6311 266.9512 27.8130 -0.7857 244.9382 245.7239 266.9502 28.2330 -0.7844 245.0345 245.8188 266.9498 28.6115 -0.7830 245.1171 245.9001 266.9515 28.9690 -0.7816 245.1940 245.9756 266.9500 29.4510 -0.7800 245.3032 246.0832 266.9559 29.8295 -0.7786 245.3858 246.1643 266.9631 30.2085 -0.7776 245.4687 246.2463 266.9714 30.6280 -0.7759 245.5609 246.3367 266.9818 31.0480 -0.7745 245.6525 246.4270 266.9910 31.4265 -0.7730 245.7358 246.5088 267.0038 31.7840 -0.7723 245.8177 246.5900 267.0141 32.2660 -0.7699 245.9237 246.6936 267.0304 32.6445 -0.7686 246.0060 246.7745 267.0451 33.0230 -0.7669 246.0814 246.8483 267.0649 33.4430 -0.7649 246.1715 246.9364 267.0830 33.8625 -0.7635 246.2580 247.0215 267.1045 34.2410 -0.7628 246.3421 247.1049 267.1252 34.5990 -0.7620 246.4188 247.1808 267.1468 35.0810 -0.7599 246.5223 247.2823 267.1779 35.4595 -0.7592 246.6020 247.3613 267.2029 35.8380 -0.7585 246.6803 247.4388 267.2237 36.2580 -0.7577 246.7693 247.5270 267.2607 36.6775 -0.7572 246.8583 247.6154 267.2964 37.0560 -0.7565 246.9361 247.6926 267.3265 37.4140 -0.7562 247.0097 247.7659 267.3576 37.8960 -0.7546 247.1119 247.8665 267.4037 38.2745 -0.7540 247.1886 247.9426 267.4409 38.6530 -0.7537 247.2679 248.0215 267.4839 39.0730 -0.7527 247.3573 248.1100 267.5297 39.4925 -0.7515 247.4429 248.1944 267.5775 39.8715 -0.7503 247.5239 248.2741 267.6211 40.2290 -0.7497 247.5995 248.3492 267.6659 40.7320 -0.7487 247.7055 248.4542 267.7297 41.0895 -0.7478 247.7795 248.5273 267.7785 41.4675 -0.7471 247.8527 248.5997 267.8328 41.8875 -0.7461 247.9400 248.6861 267.8917 42.3075 -0.7457 248.0292 248.7748 267.9530 42.6860 -0.7452 248.1061 248.8513 268.0122 43.0645 -0.7450 248.1869 248.9320 268.0707 43.5460 -0.7440 248.2858 249.0298 268.1486 43.9045 -0.7444 248.3599 249.1043 268.2093 44.2825 -0.7440 248.4423 249.1862 268.2773 44.7030 -0.7437 248.5307 249.2744 268.3506 45.1225 -0.7435 248.6191 249.3625 268.4272 45.5010 -0.7440 248.6963 249.4403 268.4973 45.8795 -0.7436 248.7738 249.5174 268.5698 46.3610 -0.7437 248.8754 249.6191 268.6575 46.7195 -0.7440 248.9472 249.6912 268.7285 47.0975 -0.7443 249.0233 249.7677 268.8049 47.5175 -0.7441 249.1066 249.8507 268.8915 47.9375 -0.7442 249.1886 249.9328 268.9820 48.3160 -0.7439 249.2645 250.0084 269.0635 48.6945 -0.7443 249.3410 250.0853 269.1430 49.1760 -0.7446 249.4374 250.1820 269.2484 49.5345 -0.7448 249.5100 250.2548 269.3298 49.9125 -0.7453 249.5856 250.3309 269.4204 50.3330 -0.7461 249.6713 250.4174 269.5195 50.7525 -0.7465 249.7554 250.5019 269.6207 51.1310 -0.7470 249.8353 250.5823 269.7148 51.5095 -0.7470 249.9079 250.6549 269.8098 51.9910 -0.7473 250.0003 250.7476 269.9319 52.3495 -0.7473 250.0724 250.8196 270.0236 52.7280 -0.7478 250.1472 250.8950 270.1205 53.1685 -0.7483 250.2362 250.9845 270.2370 53.5880 -0.7491 250.3164 251.0655 270.3500 53.9460 -0.7499 250.3851 251.1350 270.4476 54.3245 -0.7509 250.4575 251.2084 270.5518 54.8060 -0.7518 250.5552 251.3069 270.6887 55.1645 -0.7518 250.6261 251.3779 270.7901 55.5425 -0.7528 250.7026 251.4554 270.8986 55.9830 -0.7535 250.7926 251.5461 271.0274 56.4030 -0.7545 250.8754 251.6299 271.1531 56.7605 -0.7556 250.9445 251.7000 271.2602 57.1395 -0.7562 251.0191 251.7753 271.3794 57.6210 -0.7584 251.1129 251.8713 271.5248 58.0000 -0.7597 251.1849 251.9446 271.6404 58.3575 -0.7610 251.2518 252.0128 271.7464 58.7980 -0.7624 251.3325 252.0949 271.8875 59.2180 -0.7637 251.4134 252.1771 272.0230 59.5755 -0.7647 251.4880 252.2527 272.1381 59.9540 -0.7659 251.5670 252.3329 272.2573 60.4360 -0.7677 251.6667 252.4344 272.4198 60.8140 -0.7692 251.7394 252.5085 272.5421 61.1725 -0.7704 251.8118 252.5822 272.6565 61.6130 -0.7718 251.8995 252.6713 272.8056 62.0330 -0.7730 251.9800 252.7531 272.9462 62.3905 -0.7739 252.0473 252.8211 273.0665 62.7690 -0.7756 252.1221 252.8977 273.1953 63.2715 -0.7778 252.2187 252.9965 273.3665 63.6290 -0.7796 252.2903 253.0699 273.4872 63.9875 -0.7813 252.3628 253.1442 273.6107 64.4275 -0.7827 252.4490 253.2317 273.7636 64.8480 -0.7846 252.5299 253.3145 273.9102 65.2055 -0.7858 252.6005 253.3863 274.0344 65.5840 -0.7871 252.6744 253.4615 274.1646 66.0040 -0.7890 252.7558 253.5448 274.3111 66.4235 -0.7904 252.8371 253.6275 274.4631 66.8020 -0.7912 252.9084 253.6996 274.5990 67.1805 -0.7927 252.9833 253.7759 274.7294 67.6620 -0.7953 253.0806 253.8759 274.8991 68.0205 -0.7973 253.1496 253.9469 275.0239 68.3990 -0.7993 253.2221 254.0214 275.1602 68.8190 -0.8017 253.3007 254.1024 275.3090 69.2385 -0.8040 253.3824 254.1864 275.4590 69.6170 -0.8064 253.4535 254.2599 275.5888 69.9750 -0.8090 253.5203 254.3293 275.7129 70.3945 -0.8112 253.6001 254.4114 275.8611 70.8350 -0.8141 253.6870 254.5012 276.0180 71.1930 -0.8163 253.7570 254.5733 276.1401 71.5710 -0.8177 253.8294 254.6471 276.2774 72.0530 -0.8202 253.9208 254.7410 276.4506 72.4315 -0.8222 253.9944 254.8167 276.5839 72.7890 -0.8243 254.0664 254.8907 276.7092 73.2090 -0.8270 254.1490 254.9760 276.8560 73.6495 -0.8290 254.2319 255.0610 277.0076 74.0075 -0.8318 254.3061 255.1379 277.1294 74.3655 -0.8341 254.3772 255.2113 277.2554 74.8680 -0.8374 254.4767 255.3141 277.4355 75.2260 -0.8396 254.5465 255.3862 277.5608 75.6040 -0.8422 254.6240 255.4662 277.6945 75.9625 -0.8447 254.6953 255.5400 277.8163 76.4645 -0.8481 254.7945 255.6425 277.9873 76.8225 -0.8499 254.8642 255.7141 278.1092 77.1800 -0.8527 254.9351 255.7878 278.2346 77.6205 -0.8552 255.0237 255.8789 278.3885 78.0410 -0.8576 255.1110 255.9685 278.5336 78.4190 -0.8598 255.1877 256.0475 278.6624 78.7770 -0.8624 255.2571 256.1196 278.7829 79.2795 -0.8657 255.3587 256.2244 278.9511 79.6370 -0.8682 255.4326 256.3007 279.0712 79.9950 -0.8708 255.5064 256.3772 279.1910 80.4355 -0.8739 255.5944 256.4683 279.3344 80.8550 -0.8767 255.6792 256.5559 279.4704 81.2135 -0.8793 255.7487 256.6280 279.5844 81.5920 -0.8817 255.8242 256.7059 279.7080 82.0740 -0.8852 255.9194 256.8046 279.8618 82.4520 -0.8877 255.9909 256.8786 279.9802 82.8100 -0.8902 256.0606 256.9508 280.0926 83.1885 -0.8918 256.1299 257.0217 280.2093 83.6705 -0.8956 256.2285 257.1241 280.3587 84.0280 -0.8980 256.3018 257.1998 280.4679 84.4065 -0.9004 256.3737 257.2741 280.5790 84.8475 -0.9034 256.4622 257.3657 280.7095 85.2670 -0.9063 256.5441 257.4505 280.8352 85.6250 -0.9085 256.6159 257.5244 280.9371 86.0035 -0.9109 256.6935 257.6045 281.0441 86.4850 -0.9147 256.7881 257.7028 281.1820 86.8430 -0.9180 256.8588 257.7767 281.2839 87.2215 -0.9207 256.9394 257.8601 281.3895 87.6625 -0.9244 257.0286 257.9529 281.5157 88.0820 -0.9279 257.1171 258.0450 281.6326 88.4405 -0.9306 257.1896 258.1202 281.7279 88.8185 -0.9336 257.2646 258.1982 281.8265 89.3010 -0.9365 257.3626 258.2991 281.9562 89.6585 -0.9396 257.4367 258.3764 282.0505 90.0370 -0.9428 257.5113 258.4541 282.1515 90.4775 -0.9460 257.5994 258.5454 282.2626 90.8975 -0.9493 257.6821 258.6314 282.3635 91.2555 -0.9518 257.7525 258.7043 282.4556 91.6340 -0.9548 257.8248 258.7796 282.5508 92.0540 -0.9580 257.9042 258.8623 282.6582 92.4735 -0.9610 257.9897 258.9507 282.7584 92.8525 -0.9639 258.0686 259.0325 282.8457 93.2310 -0.9667 258.1467 259.1134 282.9289 93.7130 -0.9703 258.2453 259.2156 283.0382 94.0705 -0.9728 258.3144 259.2872 283.1208 94.4490 -0.9758 258.3918 259.3676 283.2016 94.8690 -0.9792 258.4802 259.4594 283.2934 95.2885 -0.9829 258.5654 259.5483 283.3822 95.6675 -0.9860 258.6382 259.6243 283.4628 96.0460 -0.9891 258.7105 259.6996 283.5440 96.5280 -0.9932 258.8072 259.8004 283.6441 96.8855 -0.9962 258.8817 259.8779 283.7144 97.2640 -0.9989 258.9584 259.9574 283.7922 97.6840 -1.0026 259.0458 260.0484 283.8730 98.1035 -1.0057 259.1316 260.1373 283.9531 98.4820 -1.0088 259.2058 260.2146 284.0266 98.8605 -1.0116 259.2820 260.2936 284.0953 99.3430 -1.0155 259.3840 260.3995 284.1777 99.7210 -1.0184 259.4607 260.4790 284.2445 100.0790 -1.0214 259.5336 260.5551 284.3077 100.4575 -1.0242 259.6148 260.6389 284.3728 100.9390 -1.0278 259.7115 260.7394 284.4526 101.2970 -1.0305 259.7843 260.8148 284.5144 101.6755 -1.0334 259.8656 260.8990 284.5724 102.1165 -1.0364 259.9478 260.9842 284.6371 102.5360 -1.0394 260.0367 261.0761 284.6998 102.8940 -1.0419 260.1113 261.1532 284.7543 103.2725 -1.0439 260.1850 261.2289 284.8116 103.7540 -1.0471 260.2813 261.3284 284.8808 104.1330 -1.0497 260.3589 261.4086 284.9370 104.4905 -1.0520 260.4360 261.4880 284.9846 104.9310 -1.0554 260.5232 261.5786 285.0457 105.3510 -1.0584 260.6108 261.6692 285.0993 105.7090 -1.0606 260.6810 261.7416 285.1440 106.0875 -1.0634 260.7573 261.8207 285.1902 106.5690 -1.0661 260.8596 261.9258 285.2501 106.9480 -1.0689 260.9379 262.0069 285.2957 107.3055 -1.0709 261.0096 262.0806 285.3355 107.7460 -1.0738 261.0999 262.1737 285.3844 108.1660 -1.0763 261.1879 262.2642 285.4320 108.5240 -1.0787 261.2604 262.3392 285.4710 108.9230 -1.0808 261.3424 262.4232 285.5113 109.3430 -1.0833 261.4307 262.5140 285.5527 109.7835 -1.0857 261.5189 262.6047 285.5991 110.1410 -1.0879 261.5935 262.6813 285.6317 110.5200 -1.0904 261.6747 262.7651 285.6661 110.9400 -1.0928 261.7600 262.8528 285.7057 111.3805 -1.0953 261.8551 262.9504 285.7421 111.7380 -1.0971 261.9270 263.0241 285.7715 112.0960 -1.0987 262.0004 263.0991 285.7995 112.5985 -1.1019 262.1023 263.2041 285.8376 112.9560 -1.1034 262.1742 263.2776 285.8636 113.3350 -1.1048 262.2502 263.3551 285.8925 113.7550 -1.1072 262.3370 263.4443 285.9202 114.1955 -1.1098 262.4295 263.5393 285.9520 114.5530 -1.1115 262.5004 263.6120 285.9778 114.9110 -1.1132 262.5697 263.6829 285.9982 115.4135 -1.1156 262.6706 263.7862 286.0234 115.7720 -1.1173 262.7415 263.8588 286.0453 116.1500 -1.1193 262.8189 263.9382 286.0668 116.6320 -1.1215 262.9175 264.0390 286.0882 117.0105 -1.1232 262.9935 264.1167 286.1112 117.3680 -1.1251 263.0653 264.1903 286.1274 117.7260 -1.1266 263.1444 264.2710 286.1472 118.2285 -1.1293 263.2453 264.3746 286.1683 118.5870 -1.1303 263.3215 264.4519 286.1844 118.9650 -1.1315 263.3991 264.5306 286.2000 119.3850 -1.1328 263.4852 264.6180 286.2172 119.8255 -1.1345 263.5730 264.7074 286.2360 120.1830 -1.1359 263.6455 264.7814 286.2510 120.5620 -1.1377 263.7212 264.8590 286.2646 121.0435 -1.1397 263.8187 264.9584 286.2828 121.4225 -1.1408 263.8945 265.0353 286.2957 121.7800 -1.1424 263.9677 265.1102 286.3103 122.1995 -1.1445 264.0535 265.1981 286.3238 122.6400 -1.1459 264.1433 265.2892 286.3366 123.0185 -1.1475 264.2248 265.3722 286.3502 123.3760 -1.1488 264.2987 265.4475 286.3622 123.8580 -1.1507 264.3929 265.5436 286.3760 124.2365 -1.1521 264.4675 265.6196 286.3833 124.5945 -1.1541 264.5421 265.6962 286.3896 125.0145 -1.1558 264.6287 265.7845 286.3989 125.4545 -1.1578 264.7178 265.8756 286.4106 125.8330 -1.1588 264.7966 265.9555 286.4195 126.1910 -1.1595 264.8730 266.0324 286.4251 126.6730 -1.1614 264.9741 266.1355 286.4320 127.0515 -1.1626 265.0510 266.2135 286.4434 127.4090 -1.1643 265.1262 266.2905 286.4524 127.8290 -1.1660 265.2104 266.3763 286.4619 128.2695 -1.1678 265.2996 266.4673 286.4770 128.6480 -1.1692 265.3744 266.5436 286.4837 129.0060 -1.1700 265.4473 266.6173 286.4938 129.4875 -1.1712 265.5446 266.7158 286.5009 129.8660 -1.1729 265.6204 266.7934 286.5023 130.2240 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