DTA measure 1Pb2_meres Date: 202541:1744 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.75 s Mass = 967.400 mg data_number = 1071 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3388 -0.8197 218.5648 219.3845 207.4418 3.9368 -0.8208 218.5758 219.3967 207.3513 5.5499 -0.8213 218.5837 219.4050 207.2674 7.1373 -0.8221 218.5963 219.4183 207.1992 8.7454 -0.8239 218.6081 219.4320 207.1427 10.3479 -0.8244 218.6106 219.4350 207.0998 11.9611 -0.8261 218.6142 219.4403 207.0702 13.5640 -0.8285 218.6200 219.4484 207.0518 15.1719 -0.8310 218.6263 219.4572 207.0310 16.7800 -0.8324 218.6307 219.4632 207.0363 18.3830 -0.8349 218.6281 219.4630 207.0574 19.9860 -0.8371 218.6353 219.4725 207.1021 21.5994 -0.8398 218.6321 219.4718 207.1635 23.2024 -0.8419 218.6313 219.4732 207.2425 24.8106 -0.8453 218.6312 219.4765 207.3354 26.4341 -0.8490 218.6253 219.4743 207.4499 28.0266 -0.8522 218.6218 219.4740 207.5845 29.6349 -0.8558 218.6148 219.4706 207.7331 31.2479 -0.8595 218.6136 219.4731 207.8976 32.8508 -0.8634 218.6159 219.4792 208.0816 34.4639 -0.8678 218.6129 219.4807 208.2911 36.0668 -0.8717 218.6136 219.4854 208.5226 37.6749 -0.8769 218.6121 219.4890 208.7722 39.2984 -0.8819 218.6031 219.4850 209.0348 40.8856 -0.8865 218.5975 219.4841 209.3131 42.4990 -0.8927 218.5975 219.4902 209.6198 44.1019 -0.8990 218.5956 219.4946 209.9299 45.7149 -0.9056 218.5972 219.5028 210.2634 47.4161 -0.9121 218.5968 219.5090 210.6324 49.0191 -0.9183 218.5948 219.5131 210.9925 50.6323 -0.9237 218.5942 219.5179 211.3670 52.2456 -0.9303 218.5981 219.5284 211.7565 53.9418 -0.9379 218.5958 219.5337 212.1711 55.5393 -0.9450 218.6062 219.5511 212.5654 57.1526 -0.9532 218.6136 219.5668 212.9712 58.7609 -0.9611 218.6237 219.5848 213.3823 60.3690 -0.9690 218.6321 219.6011 213.7957 61.9670 -0.9774 218.6462 219.6236 214.2074 63.5646 -0.9854 218.6632 219.6486 214.6227 65.2296 -0.9945 218.6825 219.6769 215.0490 66.9049 -1.0049 218.7037 219.7085 215.4810 68.5490 -1.0143 218.7321 219.7465 215.9045 70.1521 -1.0229 218.7519 219.7748 216.3088 71.7910 -1.0330 218.7806 219.8135 216.7082 73.4303 -1.0423 218.8001 219.8424 217.0980 75.0384 -1.0509 218.8150 219.8660 217.4698 76.6363 -1.0602 218.8407 219.9009 217.8321 78.2493 -1.0695 218.8624 219.9319 218.1904 79.8368 -1.0777 218.8910 219.9687 218.5348 81.4448 -1.0855 218.9231 220.0087 218.8714 83.0528 -1.0934 218.9605 220.0539 219.1845 84.6764 -1.1011 218.9935 220.0947 219.4984 86.2845 -1.1085 219.0287 220.1372 219.7939 87.8873 -1.1169 219.0734 220.1903 220.0698 89.4901 -1.1239 219.1211 220.2450 220.3338 91.0830 -1.1313 219.1659 220.2972 220.5908 92.6961 -1.1380 219.2115 220.3495 220.8319 94.3043 -1.1445 219.2543 220.3989 221.0650 95.9124 -1.1518 219.3041 220.4559 221.2826 97.5100 -1.1579 219.3502 220.5081 221.4854 99.1335 -1.1641 219.3968 220.5609 221.6799 100.7364 -1.1697 219.4562 220.6259 221.8524 102.3495 -1.1759 219.5184 220.6943 222.0216 103.9576 -1.1818 219.5799 220.7616 222.1749 105.5656 -1.1872 219.6427 220.8299 222.3206 107.1736 -1.1930 219.7053 220.8983 222.4536 108.7713 -1.1974 219.7637 220.9611 222.5850 110.3793 -1.2012 219.8259 221.0271 222.6967 112.0031 -1.2057 219.8968 221.1025 222.7997 113.6111 -1.2091 219.9730 221.1822 222.8883 115.2141 -1.2122 220.0376 221.2498 222.9870 116.8274 -1.2156 220.1105 221.3261 223.0739 118.5753 -1.2183 220.1885 221.4067 223.1596 120.4001 -1.2206 220.2676 221.4882 223.2384 122.0290 -1.2222 220.3491 221.5712 223.3056 123.6784 -1.2245 220.4295 221.6540 223.3708 125.3380 -1.2262 220.5116 221.7378 223.4402 126.9980 -1.2266 220.5947 221.8212 223.5137 128.6474 -1.2274 220.6813 221.9087 223.5766 130.3225 -1.2274 220.7600 221.9874 223.6409 132.1118 -1.2274 220.8516 222.0790 223.7164 133.7869 -1.2280 220.9388 222.1668 223.7860 135.4000 -1.2283 221.0229 222.2512 223.8500 136.9824 -1.2285 221.1101 222.3385 223.9333 138.5905 -1.2289 221.1934 222.4223 224.0143 140.2089 -1.2289 221.2819 222.5108 224.0910 141.8221 -1.2283 221.3700 222.5983 224.1735 143.4251 -1.2276 221.4615 222.6891 224.2582 145.0333 -1.2258 221.5550 222.7809 224.3602 146.6360 -1.2245 221.6420 222.8665 224.4670 148.2494 -1.2231 221.7267 222.9498 224.5805 149.8519 -1.2224 221.8062 223.0286 224.7005 151.4446 -1.2205 221.8959 223.1164 224.8334 153.0681 -1.2184 221.9887 223.2071 224.9809 154.6761 -1.2166 222.0781 223.2948 225.1290 156.2843 -1.2160 222.1673 223.3833 225.2904 157.8873 -1.2139 222.2566 223.4705 225.4617 159.5005 -1.2125 222.3455 223.5580 225.6436 161.0878 -1.2107 222.4403 223.6509 225.8419 162.6960 -1.2089 222.5352 223.7441 226.0471 164.3040 -1.2073 222.6231 223.8304 226.2561 165.9275 -1.2053 222.7146 223.9199 226.4874 167.5356 -1.2042 222.8143 224.0185 226.7223 169.1383 -1.2039 222.9212 224.1251 226.9703 170.7516 -1.2033 223.0229 224.2262 227.2234 172.3544 -1.2030 223.1209 224.3239 227.4856 173.9621 -1.2027 223.2216 224.4243 227.7494 175.5704 -1.2025 223.3177 224.5202 228.0304 177.1631 -1.2015 223.4119 224.6134 228.3207 178.7866 -1.2023 223.5144 224.7167 228.6212 180.3895 -1.2022 223.6155 224.8178 228.9215 181.9876 -1.2012 223.7189 224.9201 229.2284 183.5905 -1.2012 223.8209 225.0220 229.5424 185.1881 -1.2002 223.9253 225.1255 229.8575 186.7856 -1.2001 224.0283 225.2284 230.1715 188.3935 -1.2011 224.1444 225.3455 230.4962 190.0016 -1.2020 224.2536 225.4556 230.8205 191.5993 -1.2037 224.3595 225.5632 231.1360 193.2073 -1.2047 224.4680 225.6727 231.4589 194.8101 -1.2054 224.5810 225.7864 231.7777 196.4130 -1.2063 224.6967 225.9029 232.0977 198.0264 -1.2075 224.8224 226.0299 232.4107 199.6238 -1.2090 224.9421 226.1511 232.7162 201.2216 -1.2110 225.0598 226.2709 233.0229 202.8194 -1.2132 225.1767 226.3899 233.3289 204.4430 -1.2145 225.3020 226.5164 233.6304 206.0511 -1.2168 225.4259 226.6427 233.9275 207.6593 -1.2183 225.5466 226.7650 234.2189 209.2623 -1.2199 225.6744 226.8943 234.5048 210.8598 -1.2212 225.8015 227.0227 234.7815 212.4626 -1.2223 225.9257 227.1480 235.0565 214.0708 -1.2241 226.0465 227.2706 235.3210 215.6788 -1.2246 226.1795 227.4041 235.5789 217.3024 -1.2263 226.3186 227.5449 235.8348 218.9106 -1.2276 226.4502 227.6778 236.0781 220.5135 -1.2288 226.5912 227.8200 236.3072 222.1268 -1.2295 226.7339 227.9634 236.5330 223.7296 -1.2298 226.8741 228.1039 236.7510 225.3376 -1.2306 227.0096 228.2402 236.9664 226.9459 -1.2319 227.1473 228.3792 237.1678 228.5694 -1.2314 227.2916 228.5230 237.3674 230.1775 -1.2310 227.4363 228.6673 237.5541 231.7804 -1.2313 227.5782 228.8095 237.7370 233.3938 -1.2318 227.7262 228.9579 237.9151 234.9813 -1.2321 227.8760 229.1081 238.0862 236.6050 -1.2317 228.0248 229.2565 238.2539 238.1975 -1.2309 228.1676 229.3986 238.4121 239.8366 -1.2296 228.3222 229.5517 238.5631 241.4445 -1.2296 228.4769 229.7065 238.7094 243.0474 -1.2295 228.6249 229.8544 238.8578 244.6606 -1.2289 228.7749 230.0038 239.0014 246.2585 -1.2277 228.9323 230.1600 239.1382 247.8461 -1.2257 229.0869 230.3126 239.2736 249.4438 -1.2245 229.2417 230.4662 239.4059 251.0416 -1.2245 229.3980 230.6225 239.5298 252.6653 -1.2241 229.5527 230.7768 239.6587 254.2734 -1.2218 229.7041 230.9259 239.7847 255.8711 -1.2216 229.8550 231.0766 239.9091 257.4533 -1.2212 230.0131 231.2343 240.0287 259.0563 -1.2205 230.1769 231.3974 240.1530 260.6694 -1.2198 230.3366 231.5564 240.2882 262.2673 -1.2189 230.4957 231.7146 240.4257 263.8751 -1.2179 230.6618 231.8797 240.5608 265.4938 -1.2178 230.8257 232.0435 240.6963 267.0863 -1.2167 230.9776 232.1942 240.8295 268.6943 -1.2149 231.1344 232.3493 240.9739 270.3024 -1.2132 231.2937 232.5068 241.1202 271.9054 -1.2127 231.4525 232.6652 241.2720 273.5084 -1.2109 231.6098 232.8207 241.4262 275.1009 -1.2092 231.7673 232.9765 241.5875 276.7089 -1.2072 231.9252 233.1325 241.7543 278.3169 -1.2063 232.0917 233.2980 241.9261 279.9403 -1.2049 232.2562 233.4612 242.1000 281.5430 -1.2033 232.4327 233.6361 242.2820 283.1561 -1.2025 232.6004 233.8029 242.4796 284.7488 -1.2028 232.7589 233.9617 242.6778 286.3566 -1.2025 232.9202 234.1227 242.8767 287.9645 -1.2043 233.0826 234.2869 243.0914 289.5676 -1.2039 233.2554 234.4594 243.3054 291.1809 -1.2032 233.4209 234.6241 243.5239 292.7993 -1.2031 233.5897 234.7928 243.7496 294.3970 -1.2023 233.7613 234.9636 243.9784 296.0049 -1.2021 233.9262 235.1282 244.2100 297.6128 -1.2024 234.0905 235.2930 244.4453 299.2156 -1.2020 234.2658 235.4678 244.6873 300.8290 -1.2016 234.4376 235.6392 244.9356 302.4373 -1.2018 234.6096 235.8114 245.1868 304.0296 -1.2027 234.7804 235.9831 245.4394 305.6426 -1.2037 234.9540 236.1577 245.7022 307.2611 -1.2036 235.1350 236.3386 245.9707 308.8694 -1.2032 235.3090 236.5122 246.2325 310.4671 -1.2043 235.4778 236.6821 246.4979 312.0699 -1.2062 235.6498 236.8559 246.7611 313.6679 -1.2067 235.8211 237.0279 247.0347 315.2809 -1.2066 235.9972 237.2038 247.3132 316.8630 -1.2073 236.1662 237.3736 247.5846 318.4659 -1.2081 236.3355 237.5436 247.8556 320.0844 -1.2100 236.5138 237.7239 248.1302 321.6926 -1.2114 236.6950 237.9064 248.4056 323.2903 -1.2121 236.8733 238.0854 248.6811 324.8985 -1.2140 237.0518 238.2658 248.9507 326.5065 -1.2164 237.2348 238.4512 249.2247 328.0938 -1.2179 237.4139 238.6318 249.4850 329.7018 -1.2205 237.5896 238.8101 249.7494 331.3048 -1.2220 237.7673 238.9894 250.0155 332.9283 -1.2242 237.9552 239.1794 250.2763 334.5310 -1.2263 238.1428 239.3691 250.5376 336.1393 -1.2282 238.3227 239.5508 250.7819 337.7425 -1.2297 238.5061 239.7358 251.0235 339.3555 -1.2315 238.6990 239.9306 251.2687 340.9583 -1.2334 238.8852 240.1185 251.5124 342.5661 -1.2352 239.0716 240.3068 251.7502 344.1900 -1.2376 239.2607 240.4984 251.9934 345.7980 -1.2392 239.4501 240.6893 252.2248 347.4060 -1.2417 239.6505 240.8922 252.4505 349.0088 -1.2433 239.8396 241.0828 252.6669 350.6221 -1.2451 240.0351 241.2802 252.8817 352.2251 -1.2462 240.2293 241.4755 253.0918 353.8335 -1.2482 240.4172 241.6654 253.2902 355.4569 -1.2497 240.6073 241.8570 253.5019 357.0649 -1.2516 240.7987 242.0503 253.6993 358.6729 -1.2540 240.9919 242.2459 253.8820 360.2759 -1.2558 241.1842 242.4400 254.0673 361.8893 -1.2569 241.3766 242.6335 254.2550 363.4871 -1.2572 241.5688 242.8261 254.4303 365.1004 -1.2579 241.7684 243.0263 254.6081 366.7033 -1.2592 241.9715 243.2307 254.7757 368.3268 -1.2598 242.1752 243.4350 254.9481 369.9401 -1.2611 242.3766 243.6378 255.1259 371.5430 -1.2615 242.5809 243.8425 255.2955 373.1564 -1.2615 242.7792 244.0407 255.4594 374.7386 -1.2629 242.9807 244.2436 255.6184 376.3361 -1.2653 243.1778 244.4431 255.7867 377.9391 -1.2669 243.3771 244.6440 255.9411 379.5371 -1.2675 243.5782 244.8457 256.0965 381.1506 -1.2685 243.7876 245.0561 256.2548 382.7586 -1.2692 243.9910 245.2602 256.4101 384.3564 -1.2696 244.1986 245.4681 256.5619 385.9646 -1.2698 244.3995 245.6692 256.7179 387.5621 -1.2700 244.5959 245.8659 256.8696 389.1703 -1.2699 244.7890 246.0589 257.0292 390.7629 -1.2708 244.9865 246.2572 257.1884 392.3601 -1.2709 245.1858 246.4567 257.3487 393.9840 -1.2702 245.3925 246.6627 257.5182 395.5869 -1.2710 245.5928 246.8638 257.6887 397.1895 -1.2724 245.7902 247.0626 257.8630 398.8029 -1.2730 245.9923 247.2653 258.0377 400.4058 -1.2737 246.1968 247.4705 258.2107 402.0136 -1.2745 246.4016 247.6761 258.3891 403.6111 -1.2749 246.6049 247.8798 258.5705 405.2138 -1.2749 246.8089 248.0838 258.7557 406.8375 -1.2754 247.0100 248.2854 258.9490 408.4455 -1.2769 247.2106 248.4874 259.1514 410.0535 -1.2780 247.4170 248.6951 259.3506 411.6614 -1.2790 247.6157 248.8947 259.5615 413.2641 -1.2799 247.8153 249.0952 259.7714 414.8776 -1.2813 248.0202 249.3016 259.9826 416.4806 -1.2832 248.2186 249.5018 260.2014 418.0886 -1.2857 248.4268 249.7125 260.4244 419.7120 -1.2874 248.6271 249.9145 260.6526 421.3203 -1.2886 248.8281 250.1167 260.8883 422.9128 -1.2908 249.0318 250.3225 261.1251 424.5158 -1.2932 249.2406 250.5338 261.3646 426.1291 -1.2951 249.4472 250.7423 261.6084 427.7323 -1.2975 249.6566 250.9541 261.8565 429.3401 -1.3000 249.8579 251.1580 262.1119 430.9635 -1.3033 250.0608 251.3641 262.3771 432.5716 -1.3064 250.2753 251.5818 262.6305 434.1953 -1.3087 250.4876 251.7963 262.8889 435.8756 -1.3118 250.7020 252.0138 263.1620 437.4889 -1.3147 250.9082 252.2229 263.4305 439.0864 -1.3171 251.1165 252.4337 263.6985 440.6891 -1.3201 251.3242 252.6442 263.9647 442.2868 -1.3235 251.5244 252.8480 264.2238 443.8845 -1.3271 251.7280 253.0551 264.4805 445.5081 -1.3302 251.9407 253.2710 264.7476 447.1110 -1.3337 252.1518 253.4855 265.0002 448.7139 -1.3374 252.3648 253.7022 265.2581 450.2961 -1.3413 252.5694 253.9107 265.5186 451.9199 -1.3451 252.7839 254.1290 265.7730 453.5230 -1.3486 252.9880 254.3366 266.0292 455.1104 -1.3524 253.1951 254.5475 266.2866 456.7131 -1.3564 253.4113 254.7676 266.5395 458.3366 -1.3598 253.6283 254.9881 266.7800 459.9449 -1.3637 253.8354 255.1991 267.0358 461.5996 -1.3664 254.0568 255.4232 267.2797 463.2591 -1.3685 254.2747 255.6433 267.5195 464.8776 -1.3713 254.4878 255.8591 267.7574 466.4701 -1.3744 254.7044 256.0788 267.9832 468.0781 -1.3779 254.9178 256.2957 268.2033 469.6861 -1.3815 255.1386 256.5201 268.4246 471.3096 -1.3856 255.3662 256.7517 268.6448 472.9126 -1.3877 255.5765 256.9642 268.8523 474.5259 -1.3897 255.7926 257.1823 269.0647 476.1290 -1.3919 256.0101 257.4019 269.2712 477.7371 -1.3939 256.2279 257.6219 269.4714 479.3453 -1.3964 256.4442 257.8405 269.6751 480.9531 -1.3991 256.6604 258.0595 269.8761 482.5766 -1.4016 256.8774 258.2790 270.0738 484.1794 -1.4044 257.0946 258.4991 270.2608 485.7929 -1.4083 257.3127 258.7210 270.4435 487.3959 -1.4112 257.5272 258.9385 270.6220 489.0036 -1.4144 257.7493 259.1636 270.7956 490.6115 -1.4171 257.9646 259.3817 270.9687 492.2196 -1.4190 258.1882 259.6072 271.1424 493.8436 -1.4201 258.4164 259.8364 271.3116 495.4363 -1.4224 258.6321 260.0545 271.4727 497.0444 -1.4248 258.8489 260.2737 271.6384 498.6521 -1.4269 259.0737 260.5007 271.8068 500.2551 -1.4285 259.2974 260.7259 271.9675 501.8686 -1.4305 259.5186 260.9491 272.1335 503.4713 -1.4334 259.7381 261.1714 272.2952 505.0689 -1.4353 259.9609 261.3962 272.4512 506.6871 -1.4377 260.1843 261.6221 272.6175 508.2900 -1.4394 260.4069 261.8463 272.7862 509.8984 -1.4404 260.6340 262.0744 272.9485 511.4963 -1.4422 260.8484 262.2906 273.1171 513.0940 -1.4443 261.0659 262.5103 273.2831 514.7023 -1.4462 261.2804 262.7266 273.4570 516.3104 -1.4478 261.5028 262.9506 273.6400 517.8925 -1.4492 261.7215 263.1707 273.8108 519.5163 -1.4511 261.9498 263.4009 273.9968 521.1191 -1.4540 262.1737 263.6276 274.1787 522.7325 -1.4562 262.3986 263.8548 274.3558 524.3354 -1.4576 262.6133 264.0709 274.5396 525.9384 -1.4594 262.8277 264.2870 274.7285 527.5464 -1.4614 263.0442 264.5057 274.9237 529.1545 -1.4629 263.2627 264.7256 275.1222 530.7729 -1.4651 263.4842 264.9493 275.3278 532.3861 -1.4686 263.7093 265.1779 275.5324 533.9890 -1.4711 263.9280 265.3990 275.7430 535.6021 -1.4739 264.1496 265.6236 275.9587 537.2051 -1.4764 264.3631 265.8395 276.1765 538.7976 -1.4789 264.5758 266.0547 276.3985 540.4108 -1.4817 264.7928 266.2745 276.6220 542.0136 -1.4843 265.0064 266.4907 276.8491 543.6375 -1.4863 265.2191 266.7054 277.0807 545.2455 -1.4895 265.4341 266.9236 277.3143 546.8535 -1.4931 265.6512 267.1443 277.5501 548.4618 -1.4962 265.8699 267.3661 277.7804 550.0645 -1.4995 266.0877 267.5873 278.0175 551.6774 -1.5024 266.3094 267.8118 278.2569 553.2855 -1.5054 266.5273 268.0328 278.4991 554.9038 -1.5077 266.7439 268.2516 278.7439 556.5170 -1.5094 266.9659 268.4753 278.9893 558.1303 -1.5123 267.1843 268.6966 279.2390 559.7331 -1.5159 267.4052 268.9211 279.4861 561.3464 -1.5202 267.6219 269.1421 279.7368 562.9543 -1.5247 267.8404 269.3651 279.9919 564.5623 -1.5289 268.0563 269.5852 280.2480 566.1859 -1.5329 268.2834 269.8164 280.5051 567.7836 -1.5378 268.4983 270.0361 280.7565 569.3864 -1.5428 268.7123 270.2552 281.0053 570.9841 -1.5459 268.9287 270.4746 281.2535 572.5868 -1.5501 269.1499 270.7000 281.5007 574.1950 -1.5541 269.3688 270.9230 281.7499 575.7979 -1.5588 269.5953 271.1540 281.9928 577.4161 -1.5641 269.8109 271.3749 282.2341 579.0194 -1.5699 270.0307 271.6005 282.4756 580.6221 -1.5752 270.2576 271.8328 282.7109 582.2251 -1.5796 270.4871 272.0668 282.9468 583.8333 -1.5825 270.7076 272.2901 283.1807 585.4363 -1.5866 270.9302 272.5169 283.4057 587.0388 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