DTA measure 2felle1 Date: 2025917:90 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.48 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2943 -0.6887 235.6701 236.3587 275.8950 2.0915 -0.6865 235.9547 236.6413 275.8017 2.8785 -0.6850 236.2338 236.9188 275.6814 3.7065 -0.6851 236.4975 237.1826 275.5420 4.4730 -0.6881 236.7268 237.4149 275.3716 5.3208 -0.6850 237.0273 237.7123 275.1800 6.0973 -0.6831 237.2971 237.9802 275.0239 6.9150 -0.6789 237.5697 238.2486 274.7908 7.7123 -0.6781 237.8181 238.4962 274.5375 8.5095 -0.6782 238.0613 238.7395 274.3406 9.3273 -0.6752 238.3218 238.9970 274.1057 10.0938 -0.6755 238.5429 239.2185 273.8825 10.9215 -0.6723 238.8037 239.4761 273.6505 11.6873 -0.6738 239.0172 239.6910 273.4210 12.5460 -0.6700 239.3140 239.9840 273.2341 13.3023 -0.6673 239.5493 240.2167 273.1101 14.1405 -0.6599 239.8445 240.5044 272.9791 14.9275 -0.6558 240.0754 240.7312 272.8981 15.7238 -0.6525 240.3127 240.9651 272.8559 16.5518 -0.6489 240.5808 241.2297 272.8484 17.3183 -0.6451 240.8294 241.4745 272.8482 18.1770 -0.6446 241.0883 241.7329 272.9075 18.9435 -0.6415 241.3356 241.9771 273.0486 19.7715 -0.6401 241.6131 242.2532 273.2401 20.5688 -0.6390 241.8552 242.4942 273.4697 21.3650 -0.6352 242.0922 242.7274 273.7632 22.1623 -0.6322 242.3508 242.9830 274.1019 22.9595 -0.6309 242.6342 243.2651 274.4731 23.7875 -0.6321 242.8861 243.5182 274.9086 24.5540 -0.6342 243.1112 243.7453 275.3598 25.4023 -0.6342 243.3627 243.9969 275.8648 26.1783 -0.6359 243.6292 244.2651 276.3560 26.9960 -0.6396 243.8558 244.4954 276.8683 27.7933 -0.6441 244.0711 244.7152 277.3345 28.5905 -0.6454 244.2946 244.9400 277.8237 29.4493 -0.6504 244.5366 245.1870 278.3508 30.1840 -0.6537 244.7704 245.4241 278.7803 31.0325 -0.6562 245.0034 245.6596 279.2664 31.8400 -0.6621 245.2222 245.8844 279.6783 32.6270 -0.6656 245.4632 246.1288 280.0919 33.4140 -0.6641 245.7287 246.3929 280.4412 34.2210 -0.6661 245.9721 246.6383 280.7717 35.0383 -0.6713 246.2094 246.8807 281.0826 35.7945 -0.6801 246.4229 247.1030 281.3149 36.6635 -0.6900 246.6556 247.3457 281.5219 37.4198 -0.6917 246.8537 247.5454 281.6929 38.2375 -0.6959 247.0963 247.7922 281.8453 39.0450 -0.7016 247.3354 248.0371 281.9489 39.8313 -0.7063 247.5593 248.2655 281.9886 40.6590 -0.7122 247.7641 248.4763 281.9817 41.4255 -0.7156 247.9829 248.6985 281.9590 42.2843 -0.7159 248.2547 248.9706 281.9215 43.0508 -0.7197 248.4959 249.2156 281.8556 43.8683 -0.7238 248.7212 249.4450 281.7647 44.6750 -0.7270 248.9775 249.7044 281.6568 45.4620 -0.7292 249.2342 249.9634 281.5316 46.2900 -0.7293 249.4504 250.1798 281.3495 47.0565 -0.7343 249.6565 250.3908 281.1680 47.9153 -0.7387 249.8901 250.6288 280.9718 48.6813 -0.7400 250.0975 250.8375 280.8300 49.4985 -0.7341 250.3176 251.0517 280.6529 50.3060 -0.7319 250.5577 251.2896 280.4733 51.0930 -0.7339 250.8083 251.5422 280.3182 51.9210 -0.7371 251.0542 251.7913 280.1479 52.6870 -0.7402 251.2548 251.9950 280.0061 53.5453 -0.7425 251.4535 252.1961 279.8966 54.3118 -0.7426 251.6708 252.4134 279.8260 55.1295 -0.7426 251.8981 252.6407 279.8365 55.9370 -0.7433 252.1499 252.8932 279.8498 56.7240 -0.7426 252.3657 253.1083 279.8873 57.5520 -0.7411 252.5631 253.3042 279.9673 58.3185 -0.7420 252.7753 253.5172 280.0811 59.1773 -0.7380 252.9812 253.7192 280.2797 59.9428 -0.7396 253.1932 253.9328 280.4703 60.7708 -0.7391 253.4359 254.1750 280.7018 61.5680 -0.7364 253.6103 254.3467 280.9556 62.3653 -0.7376 253.8453 254.5829 281.2480 63.1933 -0.7382 254.0738 254.8120 281.5808 63.9495 -0.7412 254.2701 255.0113 281.9113 64.8073 -0.7501 254.5300 255.2801 282.3341 65.5635 -0.7548 254.7152 255.4700 282.7542 66.3915 -0.7555 254.9376 255.6931 283.2030 67.1580 -0.7594 255.1589 255.9182 283.6460 67.9758 -0.7632 255.3799 256.1431 284.1056 68.7730 -0.7670 255.6262 256.3932 284.5191 69.5703 -0.7702 255.8481 256.6183 284.9168 70.3880 -0.7726 256.0505 256.8231 285.3278 71.1538 -0.7807 256.2501 257.0308 285.7141 72.0123 -0.7905 256.4744 257.2649 286.1259 72.7788 -0.7967 256.6705 257.4673 286.4580 73.5965 -0.8010 256.8489 257.6499 286.7708 74.4040 -0.8028 257.0605 257.8633 287.0622 75.1905 -0.8031 257.2887 258.0917 287.3063 76.0180 -0.8058 257.5205 258.3263 287.5118 76.7845 -0.8072 257.7358 258.5430 287.6381 77.6330 -0.8125 257.9533 258.7658 287.7990 78.3995 -0.8167 258.1647 258.9814 287.8870 79.2275 -0.8211 258.3493 259.1704 287.9611 79.9828 -0.8255 258.5360 259.3614 288.0532 80.8415 -0.8301 258.7525 259.5826 288.0870 81.6080 -0.8334 258.9666 259.7999 288.0680 82.4360 -0.8319 259.1918 260.0237 288.0523 83.2230 -0.8355 259.3996 260.2351 287.9894 84.0303 -0.8392 259.6411 260.4803 287.9115 84.8473 -0.8452 259.8365 260.6817 287.7927 85.6138 -0.8499 260.0258 260.8757 287.6774 86.4725 -0.8547 260.2551 261.1098 287.5115 87.2390 -0.8580 260.4381 261.2962 287.3706 88.0670 -0.8624 260.6131 261.4755 287.2330 88.8538 -0.8670 260.7976 261.6646 287.1368 89.6605 -0.8721 261.0102 261.8822 287.0540 90.4783 -0.8741 261.2296 262.1037 286.9007 91.2448 -0.8719 261.4199 262.2918 286.8161 92.1035 -0.8752 261.6316 262.5068 286.6763 92.8700 -0.8799 261.7955 262.6754 286.5795 93.6978 -0.8821 261.9919 262.8739 286.5300 94.4945 -0.8820 262.2098 263.0918 286.4987 95.2915 -0.8840 262.4112 263.2952 286.5390 96.0888 -0.8877 262.6229 263.5106 286.6069 96.8860 -0.8913 262.8121 263.7034 286.6941 97.7038 -0.8943 262.9835 263.8778 286.7989 98.4703 -0.8978 263.1669 264.0647 286.9481 99.3183 -0.8966 263.3887 264.2852 287.1314 100.0843 -0.8950 263.5885 264.4834 287.3555 100.9123 -0.8961 263.7952 264.6912 287.6383 101.6993 -0.9042 263.9578 264.8620 287.9521 102.4965 -0.9058 264.1301 265.0359 288.2663 103.2938 -0.9054 264.3275 265.2329 288.6399 104.0910 -0.9079 264.5293 265.4372 289.0144 104.9080 -0.9180 264.7444 265.6624 289.4109 105.6845 -0.9219 264.9618 265.8837 289.8214 106.5330 -0.9248 265.1564 266.0812 290.2813 107.2995 -0.9268 265.3427 266.2695 290.6586 108.1275 -0.9291 265.5433 266.4724 291.0735 108.9248 -0.9329 265.7671 266.7000 291.4844 109.7215 -0.9406 265.9415 266.8821 291.8656 110.5388 -0.9524 266.0929 267.0453 292.1878 111.3155 -0.9590 266.2745 267.2335 292.4988 112.1640 -0.9651 266.4926 267.4578 292.8505 112.9100 -0.9691 266.6685 267.6376 293.1225 113.7585 -0.9755 266.8792 267.8547 293.4360 114.5350 -0.9781 267.0461 268.0242 293.6577 115.3520 -0.9835 267.2187 268.2022 293.8325 116.1493 -0.9889 267.4000 268.3889 293.9802 116.9465 -0.9932 267.6102 268.6035 294.1472 117.7745 -0.9949 267.7967 268.7916 294.2476 118.5410 -0.9979 268.0043 269.0021 294.2922 119.3895 -1.0007 268.1925 269.1932 294.3208 120.1655 -1.0070 268.3311 269.3381 294.3373 120.9830 -1.0135 268.5602 269.5736 294.3209 121.7803 -1.0181 268.7660 269.7840 294.2808 122.5775 -1.0232 268.9736 269.9968 294.1989 123.4055 -1.0285 269.1537 270.1822 294.1295 124.1720 -1.0350 269.3207 270.3557 294.0693 125.0300 -1.0368 269.4909 270.5277 293.9657 125.7963 -1.0407 269.7214 270.7621 293.8632 126.6243 -1.0446 269.9399 270.9846 293.7449 127.4215 -1.0465 270.1382 271.1847 293.6144 128.2085 -1.0442 270.3368 271.3810 293.5237 129.0058 -1.0458 270.4919 271.5377 293.4250 129.8030 -1.0492 270.6649 271.7141 293.3297 130.6203 -1.0586 270.8850 271.9436 293.2470 131.3965 -1.0586 271.0480 272.1066 293.1965 132.2450 -1.0591 271.2223 272.2814 293.1744 133.0013 -1.0597 271.4238 272.4835 293.1542 133.8395 -1.0635 271.6163 272.6798 293.1643 134.6265 -1.0643 271.8229 272.8872 293.2095 135.4238 -1.0692 271.9910 273.0602 293.2762 136.2518 -1.0705 272.1673 273.2378 293.3450 137.0080 -1.0741 272.3518 273.4259 293.4219 137.8663 -1.0794 272.5482 273.6276 293.5709 138.6323 -1.0822 272.7138 273.7960 293.7560 139.4603 -1.0866 272.8911 273.9777 294.0360 140.2575 -1.0899 273.0483 274.1382 294.3040 141.0445 -1.0905 273.2001 274.2906 294.5765 141.8828 -1.0971 273.3825 274.4796 294.9318 142.6383 -1.1000 273.5201 274.6201 295.2801 143.4660 -1.1033 273.7266 274.8299 295.7030 144.2325 -1.1047 273.9059 275.0106 296.0707 145.0913 -1.1099 274.1477 275.2576 296.4799 145.8578 -1.1140 274.3313 275.4453 296.8807 146.6858 -1.1203 274.5246 275.6449 297.3150 147.4828 -1.1265 274.7406 275.8670 297.7083 148.2793 -1.1356 274.9283 276.0638 298.1103 149.1073 -1.1356 275.0806 276.2162 298.4594 149.8738 -1.1420 275.2488 276.3907 298.7975 150.7325 -1.1503 275.4138 276.5642 299.1253 151.4990 -1.1553 275.5847 276.7400 299.3835 152.3168 -1.1635 275.7770 276.9404 299.6385 153.0925 -1.1690 275.9519 277.1209 299.8889 153.9410 -1.1738 276.1490 277.3227 300.0923 154.7075 -1.1775 276.3239 277.5013 300.2381 155.5355 -1.1822 276.4592 277.6414 300.3713 156.3430 -1.1871 276.6108 277.7979 300.4764 157.1290 -1.1890 276.7883 277.9773 300.5360 157.9570 -1.1956 277.0044 278.2000 300.5843 158.7235 -1.2023 277.1830 278.3853 300.5962 159.5925 -1.2059 277.3827 278.5886 300.5969 160.3488 -1.2087 277.5850 278.7937 300.5652 161.1665 -1.2151 277.7505 278.9656 300.5176 161.9525 -1.2215 277.9449 279.1664 300.4755 162.7805 -1.2271 278.1324 279.3595 300.4251 163.5470 -1.2317 278.2991 279.5308 300.3649 164.3750 -1.2404 278.5018 279.7422 300.2886 165.1620 -1.2429 278.6451 279.8880 300.1853 165.9593 -1.2426 278.8031 280.0457 300.0966 166.7870 -1.2414 278.9616 280.2030 299.9874 167.5425 -1.2447 279.1135 280.3583 299.9097 168.4115 -1.2481 279.2638 280.5119 299.8409 169.1370 -1.2499 279.4183 280.6681 299.7605 169.9958 -1.2519 279.6312 280.8831 299.6733 170.7623 -1.2555 279.7968 281.0523 299.6220 171.5800 -1.2587 279.9865 281.2452 299.6305 172.3770 -1.2592 280.1265 281.3857 299.6376 173.1735 -1.2636 280.3128 281.5764 299.6813 174.0015 -1.2611 280.4929 281.7539 299.7587 174.7680 -1.2629 280.6344 281.8973 299.8855 175.6165 -1.2682 280.8488 282.1170 300.0454 176.3933 -1.2715 281.0376 282.3091 300.2266 177.2110 -1.2739 281.2127 282.4866 300.4226 178.0083 -1.2714 281.3855 282.6569 300.6236 178.8045 -1.2734 281.5633 282.8367 300.8462 179.6325 -1.2739 281.7320 283.0059 301.1733 180.3990 -1.2818 281.9199 283.2017 301.4945 181.2475 -1.2817 282.0734 283.3551 301.8621 182.0243 -1.2843 282.2246 283.5089 302.1867 182.8420 -1.2828 282.4174 283.7002 302.5616 183.6393 -1.2884 282.5857 283.8741 302.9330 184.4360 -1.2918 282.7568 284.0486 303.3112 185.2738 -1.3001 282.9470 284.2471 303.6710 186.0300 -1.3070 283.1022 284.4091 304.0203 186.8888 -1.3128 283.2800 284.5927 304.4012 187.6553 -1.3195 283.4505 284.7699 304.7216 188.4833 -1.3244 283.6013 284.9257 305.0410 189.2805 -1.3247 283.7765 285.1013 305.3537 190.0675 -1.3307 283.9468 285.2775 305.6244 190.8745 -1.3417 284.1217 285.4634 305.8597 191.6610 -1.3530 284.2572 285.6102 306.0706 192.4890 -1.3637 284.4379 285.8016 306.2482 193.2555 -1.3684 284.5968 285.9652 306.3888 194.1040 -1.3703 284.7962 286.1665 306.5462 194.8703 -1.3688 284.9311 286.2999 306.6552 195.6975 -1.3745 285.1091 286.4836 306.7486 196.4948 -1.3828 285.2985 286.6812 306.7618 197.2818 -1.3870 285.4830 286.8700 306.7722 198.0790 -1.3905 285.6593 287.0498 306.8101 198.8763 -1.3920 285.8231 287.2151 306.7939 199.6935 -1.3966 285.9769 287.3735 306.7666 200.4595 -1.3992 286.0976 287.4968 306.7602 201.3183 -1.4069 286.2570 287.6639 306.6933 202.0848 -1.4083 286.4527 287.8610 306.6197 202.9025 -1.4159 286.6419 288.0578 306.5573 203.7100 -1.4201 286.8439 288.2640 306.4740 204.4970 -1.4242 287.0102 288.4343 306.3956 205.3245 -1.4268 287.1744 288.6012 306.2933 206.0905 -1.4272 287.3264 288.7536 306.2317 206.9185 -1.4290 287.5220 288.9510 306.1947 207.6850 -1.4230 287.6801 289.1030 306.1659 208.5335 -1.4220 287.8425 289.2645 306.1700 209.3103 -1.4192 288.0025 289.4217 306.1350 210.1275 -1.4196 288.1574 289.5771 306.1583 210.9243 -1.4233 288.3273 289.7507 306.1948 211.7215 -1.4271 288.5020 289.9291 306.2591 212.5495 -1.4273 288.6883 290.1156 306.3235 213.3365 -1.4304 288.8172 290.2477 306.4200 214.1543 -1.4340 288.9951 290.4291 306.5598 214.9198 -1.4381 289.1372 290.5753 306.6786 215.7785 -1.4383 289.3466 290.7849 306.8833 216.5450 -1.4368 289.5033 290.9401 307.0989 217.3730 -1.4368 289.6570 291.0938 307.3419 218.1703 -1.4393 289.8337 291.2730 307.6351 218.9675 -1.4407 290.0264 291.4671 307.9452 219.7640 -1.4467 290.1760 291.6227 308.2704 220.5610 -1.4503 290.3354 291.7857 308.5916 221.3788 -1.4574 290.4970 291.9544 308.9419 222.1555 -1.4631 290.6555 292.1185 309.2793 223.0040 -1.4715 290.8373 292.3088 309.6797 223.7705 -1.4739 290.9755 292.4494 310.0245 224.5985 -1.4764 291.0979 292.5742 310.3851 225.3950 -1.4777 291.2204 292.6981 310.7034 226.1920 -1.4844 291.3639 292.8484 311.0011 227.0098 -1.4900 291.5580 293.0480 311.3254 227.7763 -1.4948 291.7131 293.2079 311.5906 228.6350 -1.5010 291.9102 293.4112 311.8516 229.3913 -1.5055 292.0824 293.5879 312.0379 230.2188 -1.5109 292.2810 293.7918 312.2503 231.0155 -1.5151 292.4679 293.9830 312.4107 231.8025 -1.5218 292.6000 294.1219 312.5565 232.5998 -1.5272 292.7299 294.2571 312.7072 233.3970 -1.5306 292.9243 294.4549 312.7824 234.2148 -1.5359 293.0893 294.6252 312.8462 234.9915 -1.5381 293.2277 294.7658 312.9199 235.8395 -1.5451 293.4303 294.9755 312.9882 236.6055 -1.5510 293.5995 295.1505 313.0104 237.4335 -1.5554 293.7785 295.3339 313.0181 238.2308 -1.5605 293.9105 295.4709 313.0014 239.0280 -1.5672 294.0579 295.6251 312.9757 239.8458 -1.5687 294.2488 295.8175 312.9677 240.6225 -1.5700 294.4156 295.9856 312.9333 241.4708 -1.5707 294.6056 296.1763 312.8524 242.2365 -1.5744 294.7519 296.3263 312.8138 243.0645 -1.5790 294.9400 296.5190 312.7822 243.8618 -1.5845 295.0940 296.6786 312.7306 244.6590 -1.5903 295.2314 296.8218 312.6780 245.4768 -1.5926 295.3495 296.9421 312.6580 246.2535 -1.5916 295.5004 297.0920 312.6115 247.1020 -1.5925 295.6845 297.2769 312.5946 247.8678 -1.5934 295.8855 297.4789 312.6057 248.6955 -1.5994 296.0517 297.6512 312.6089 249.4723 -1.6010 296.2201 297.8211 312.6292 250.2900 -1.6012 296.3807 297.9819 312.6943 251.0873 -1.6016 296.5303 298.1319 312.7565 251.8845 -1.6017 296.6830 298.2847 312.8555 252.7115 -1.6000 296.8133 298.4133 313.0278 253.4780 -1.6007 296.9418 298.5426 313.1907 254.3163 -1.6062 297.1179 298.7242 313.3862 255.0930 -1.6083 297.2719 298.8801 313.5775 255.9415 -1.6114 297.4311 299.0425 313.8541 256.7183 -1.6150 297.5902 299.2052 314.1369 257.5360 -1.6245 297.7522 299.3767 314.4625 258.3230 -1.6299 297.8499 299.4798 314.7774 259.1195 -1.6346 297.9974 299.6320 315.1089 259.9473 -1.6405 298.1398 299.7803 315.4425 260.7035 -1.6429 298.2954 299.9383 315.7938 261.5623 -1.6442 298.4440 300.0882 316.1545 262.3288 -1.6472 298.6001 300.2472 316.4854 263.1465 -1.6534 298.7882 300.4416 316.7976 263.9438 -1.6571 298.9250 300.5821 317.1083 264.7410 -1.6602 299.0978 300.7580 317.3985 265.5578 -1.6642 299.2598 300.9240 317.6902 266.3345 -1.6686 299.4246 301.0932 317.9112 267.1830 -1.6722 299.5900 301.2621 318.1467 267.9495 -1.6783 299.7694 301.4477 318.3674 268.7775 -1.6860 299.9531 301.6392 318.5605 269.5748 -1.6929 300.1224 301.8153 318.7218 270.3710 -1.6978 300.3017 301.9995 318.8757 271.1888 -1.7078 300.4899 302.1977 318.9927 271.9655 -1.7134 300.6137 302.3271 319.0697 272.8140 -1.7160 300.7985 302.5145 319.1202 273.5803 -1.7195 300.9491 302.6686 319.1710 274.4075 -1.7253 301.1104 302.8356 319.2429 275.2048 -1.7320 301.2586 302.9906 319.2321 276.0020 -1.7388 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