DTA measure 3felle1 Date: 2025917:929 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.54 s Mass = 100.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4110 -4.6417 446.6292 451.2708 433.9958 4.0201 -4.6557 446.7408 451.3965 434.1313 5.6249 -4.6694 446.8746 451.5440 434.1218 7.2343 -4.6773 447.0073 451.6845 433.9827 8.8539 -4.6866 447.1275 451.8140 433.7588 10.4429 -4.6972 447.1549 451.8522 433.4155 12.0521 -4.7031 447.2668 451.9699 433.0001 13.6719 -4.7095 447.3429 452.0524 432.5164 15.2606 -4.7144 447.3868 452.1012 431.9755 16.8654 -4.7174 447.4606 452.1781 431.3863 18.4794 -4.7084 447.5615 452.2699 430.7737 20.0790 -4.7031 447.6167 452.3198 430.1934 21.6881 -4.7057 447.6125 452.3182 429.6355 23.3080 -4.7004 447.7021 452.4025 429.1362 24.9173 -4.6995 447.7809 452.4804 428.7244 26.5216 -4.6938 447.8215 452.5153 428.3554 28.1313 -4.6896 447.8583 452.5479 428.0845 29.7353 -4.6833 447.9408 452.6241 427.9314 31.3451 -4.6835 447.9722 452.6557 427.8347 32.9490 -4.6860 448.0161 452.7021 427.8013 34.5588 -4.6924 448.0331 452.7256 427.8129 36.1785 -4.6986 448.0816 452.7802 427.8586 37.7826 -4.6964 448.1073 452.8037 427.9523 39.3976 -4.6983 448.0858 452.7841 428.0323 41.0016 -4.6973 448.1454 452.8427 428.1203 42.6113 -4.6971 448.1382 452.8353 428.1777 44.2208 -4.7026 448.1973 452.8999 428.1186 45.8300 -4.7077 448.2452 452.9529 428.0167 47.4500 -4.7123 448.2464 452.9587 427.8429 49.0590 -4.7194 448.2824 453.0018 427.6551 50.6586 -4.7228 448.3076 453.0303 427.3332 52.2574 -4.7178 448.3130 453.0308 427.0001 53.8518 -4.7174 448.3128 453.0302 426.6336 55.4509 -4.7205 448.2742 452.9947 426.2845 57.0551 -4.7229 448.3064 453.0293 425.9001 58.6598 -4.7177 448.2954 453.0131 425.4630 60.2790 -4.7121 448.2762 452.9883 425.0688 61.8838 -4.7107 448.2877 452.9984 424.7092 63.4879 -4.7141 448.2908 453.0049 424.3221 65.0923 -4.7178 448.2984 453.0161 423.9889 66.7021 -4.7064 448.2978 453.0042 423.7329 68.3064 -4.7016 448.2983 452.9999 423.5078 69.9004 -4.7036 448.2445 452.9481 423.3278 71.5051 -4.7054 448.2030 452.9084 423.1772 73.1243 -4.7078 448.1265 452.8343 423.0429 74.7341 -4.7022 448.1086 452.8108 422.8743 76.3385 -4.7021 448.0581 452.7602 422.8036 77.9478 -4.7071 448.0444 452.7515 422.7421 79.5523 -4.7071 448.0077 452.7148 422.6539 81.1614 -4.7100 447.9928 452.7028 422.6123 82.7558 -4.7111 447.9506 452.6616 422.5472 84.3648 -4.7113 447.9316 452.6430 422.4648 85.9849 -4.7127 447.9791 452.6918 422.3508 87.5889 -4.7194 447.9056 452.6250 422.1607 89.2036 -4.7209 447.8678 452.5887 421.9799 90.8081 -4.7218 447.8069 452.5287 421.7426 92.4173 -4.7281 447.7241 452.4522 421.4932 94.0220 -4.7276 447.6835 452.4111 421.1806 95.6211 -4.7223 447.6008 452.3231 420.8654 97.2254 -4.7188 447.5349 452.2537 420.5672 98.8555 -4.7174 447.4454 452.1628 420.2495 100.4595 -4.7156 447.3758 452.0914 419.9429 102.0694 -4.7102 447.3256 452.0359 419.6331 103.6731 -4.7132 447.2577 451.9709 419.3134 105.2676 -4.7127 447.2179 451.9306 419.0552 106.8774 -4.7095 447.1863 451.8958 418.7886 108.4915 -4.7060 447.1082 451.8141 418.5752 110.0963 -4.7087 446.9993 451.7080 418.3440 111.7208 -4.7030 446.9056 451.6086 418.2001 113.3099 -4.6998 446.8173 451.5171 418.0249 114.9094 -4.6997 446.7667 451.4663 417.8396 116.5081 -4.7042 446.7006 451.4048 417.7178 118.1129 -4.7030 446.6090 451.3120 417.5780 119.7120 -4.7019 446.5427 451.2445 417.4511 121.3214 -4.7005 446.4406 451.1411 417.3234 122.9255 -4.7050 446.3832 451.0882 417.1871 124.5401 -4.7108 446.2686 450.9794 417.0004 126.1346 -4.7087 446.1499 450.8586 416.8155 127.7486 -4.7088 446.0672 450.7759 416.6668 129.3380 -4.7050 446.0206 450.7256 416.5132 130.9423 -4.7038 445.8663 450.5700 416.3153 132.5465 -4.7112 445.7936 450.5047 416.0877 134.1564 -4.7080 445.6930 450.4010 415.8665 135.7605 -4.7015 445.5778 450.2794 415.6337 137.3803 -4.7021 445.4426 450.1447 415.3718 138.9900 -4.7047 445.3535 450.0582 415.1525 140.5939 -4.7001 445.1969 449.8970 414.8704 142.2038 -4.6989 445.0976 449.7965 414.5732 143.8076 -4.6977 445.0097 449.7074 414.3012 145.4174 -4.6935 444.9063 449.5998 413.9792 147.0314 -4.6853 444.8259 449.5112 413.7111 148.6361 -4.6812 444.7039 449.3850 413.4951 150.2450 -4.6787 444.5731 449.2518 413.2971 151.8549 -4.6763 444.4489 449.1252 413.0816 153.4593 -4.6737 444.3288 449.0026 412.8699 155.0736 -4.6749 444.2109 448.8858 412.6674 156.6783 -4.6716 444.0849 448.7566 412.4707 158.2873 -4.6757 443.9530 448.6287 412.2792 159.8920 -4.6711 443.8312 448.5023 412.1317 161.5014 -4.6714 443.7011 448.3726 411.9816 163.1210 -4.6681 443.5747 448.2428 411.8113 164.7309 -4.6666 443.4233 448.0899 411.6256 166.3399 -4.6664 443.2818 447.9482 411.4529 167.9496 -4.6652 443.1415 447.8067 411.2736 169.5541 -4.6624 443.0218 447.6842 411.1220 171.1684 -4.6589 442.8664 447.5254 410.9117 172.7731 -4.6560 442.7557 447.4116 410.6900 174.3926 -4.6536 442.6160 447.2696 410.4832 176.0021 -4.6501 442.4866 447.1367 410.2520 177.5915 -4.6517 442.3459 446.9976 410.0639 179.1904 -4.6535 442.2260 446.8794 409.8240 180.7949 -4.6548 442.0807 446.7355 409.5852 182.3945 -4.6511 441.9750 446.6261 409.3286 183.9830 -4.6436 441.8543 446.4979 409.0767 185.5876 -4.6401 441.7004 446.3405 408.8458 187.1868 -4.6372 441.5682 446.2054 408.6398 188.8115 -4.6351 441.4049 446.0400 408.3936 190.4006 -4.6303 441.2575 445.8877 408.1448 192.0046 -4.6217 441.1486 445.7703 407.9303 193.6144 -4.6149 441.0163 445.6312 407.7282 195.2183 -4.6153 440.8363 445.4516 407.4897 196.8128 -4.6102 440.7081 445.3183 407.2992 198.4169 -4.6077 440.5344 445.1421 407.1033 200.0264 -4.6045 440.3920 444.9965 406.9059 201.6311 -4.6059 440.2296 444.8355 406.7208 203.2504 -4.6092 440.0656 444.6748 406.5517 204.8601 -4.6057 439.9142 444.5199 406.3641 206.4490 -4.5983 439.7559 444.3541 406.1961 208.0584 -4.5948 439.5795 444.1743 405.9906 209.6631 -4.5908 439.4506 444.0413 405.7869 211.2720 -4.5940 439.2424 443.8364 405.5498 212.8768 -4.5860 439.0973 443.6833 405.3416 214.4809 -4.5875 438.9798 443.5672 405.1398 216.1109 -4.5835 438.8197 443.4032 404.9371 217.7154 -4.5844 438.6466 443.2310 404.7890 219.3245 -4.5820 438.4885 443.0705 404.5696 220.9139 -4.5782 438.3047 442.8829 404.3227 222.5228 -4.5694 438.1164 442.6858 404.0699 224.1326 -4.5656 437.9405 442.5060 403.8312 225.7418 -4.5612 437.8234 442.3847 403.5734 227.3463 -4.5577 437.6567 442.2143 403.3529 228.9713 -4.5560 437.4789 442.0349 403.1378 230.5753 -4.5590 437.3293 441.8883 402.9231 232.1799 -4.5529 437.1472 441.7001 402.6640 233.7889 -4.5469 436.9841 441.5310 402.4238 235.3988 -4.5417 436.7871 441.3288 402.2216 237.0076 -4.5433 436.6241 441.1674 402.0017 238.6124 -4.5446 436.4533 440.9979 401.7785 240.2371 -4.5404 436.3250 440.8654 401.5729 241.8414 -4.5308 436.1736 440.7044 401.3856 243.4359 -4.5203 436.0297 440.5500 401.2216 245.0449 -4.5177 435.8755 440.3933 401.0425 246.6444 -4.5158 435.7290 440.2449 400.8475 248.2434 -4.5137 435.5127 440.0264 400.6782 249.8375 -4.5099 435.3369 439.8469 400.4955 251.4366 -4.5140 435.2123 439.7264 400.3301 253.0563 -4.5112 435.0214 439.5326 400.1742 254.6609 -4.5114 434.8118 439.3232 399.9253 256.2648 -4.5025 434.6522 439.1546 399.7320 257.8746 -4.5020 434.4372 438.9392 399.5309 259.4733 -4.4946 434.2735 438.7682 399.3133 261.0780 -4.4878 434.0851 438.5729 399.0953 262.6878 -4.4821 433.9038 438.3859 398.8746 264.3070 -4.4842 433.7351 438.2193 398.6078 265.9169 -4.4816 433.5669 438.0485 398.3697 267.5208 -4.4735 433.3787 437.8522 398.1498 269.1151 -4.4721 433.1975 437.6696 397.9423 270.7299 -4.4732 433.0290 437.5022 397.7274 272.3390 -4.4702 432.8675 437.3377 397.5060 273.9436 -4.4656 432.7064 437.1720 397.2322 275.5526 -4.4646 432.5577 437.0223 396.9910 277.1779 -4.4605 432.3695 436.8300 396.7951 278.7816 -4.4513 432.1752 436.6265 396.5841 280.3915 -4.4432 431.9848 436.4280 396.3470 281.9955 -4.4359 431.8400 436.2759 396.1599 283.5898 -4.4306 431.6228 436.0535 395.9778 285.1943 -4.4181 431.4238 435.8418 395.7668 286.8034 -4.4134 431.2228 435.6362 395.5878 288.4131 -4.4190 431.0482 435.4672 395.4228 290.0375 -4.4161 430.8763 435.2924 395.2459 291.6423 -4.4095 430.7117 435.1212 395.0590 293.2565 -4.4006 430.4846 434.8852 394.8672 294.8610 -4.3965 430.3394 434.7359 394.6803 296.4708 -4.3928 430.1723 434.5651 394.4515 298.0798 -4.3904 429.9557 434.3462 394.2260 299.6691 -4.3840 429.7914 434.1754 393.9899 301.2834 -4.3778 429.5970 433.9747 393.7424 302.9033 -4.3767 429.4195 433.7961 393.5327 304.5126 -4.3751 429.2330 433.6081 393.3321 306.1169 -4.3749 429.0386 433.4135 393.1091 307.7163 -4.3693 428.8245 433.1938 392.9116 309.3049 -4.3625 428.6479 433.0105 392.6791 310.9045 -4.3536 428.4539 432.8075 392.4566 312.5135 -4.3520 428.2454 432.5975 392.2424 314.1130 -4.3455 428.0379 432.3834 391.9930 315.7021 -4.3416 427.8920 432.2336 391.7776 317.3215 -4.3369 427.6918 432.0287 391.5759 318.9263 -4.3334 427.5388 431.8722 391.3629 320.5250 -4.3250 427.3571 431.6821 391.1530 322.1348 -4.3196 427.1732 431.4928 390.8972 323.7394 -4.3161 426.9904 431.3065 390.7137 325.3330 -4.3120 426.7697 431.0817 390.5395 326.9378 -4.3062 426.5954 430.9016 390.2999 328.5421 -4.3038 426.4047 430.7086 390.1268 330.1668 -4.3052 426.2059 430.5111 389.9005 331.7715 -4.3005 425.9924 430.2929 389.6736 333.3805 -4.2898 425.7670 430.0568 389.4682 334.9851 -4.2853 425.6090 429.8943 389.2386 336.5946 -4.2799 425.4292 429.7092 389.0200 338.1988 -4.2799 425.2882 429.5681 388.8151 339.8035 -4.2792 425.0717 429.3509 388.6003 341.4176 -4.2763 424.8416 429.1179 388.4163 343.0223 -4.2734 424.6374 428.9108 388.2720 344.6313 -4.2661 424.4560 428.7221 388.0826 346.2359 -4.2683 424.2648 428.5331 387.9108 347.8453 -4.2683 424.0224 428.2907 387.7693 349.4495 -4.2630 423.8617 428.1247 387.5630 351.0593 -4.2588 423.6798 427.9386 387.2854 352.6683 -4.2561 423.4860 427.7421 387.0494 354.2935 -4.2524 423.2237 427.4762 386.8474 355.8976 -4.2416 423.0661 427.3078 386.6202 357.5020 -4.2391 422.8920 427.1311 386.3565 359.1168 -4.2297 422.7259 426.9555 386.1299 360.7208 -4.2299 422.5402 426.7701 385.8808 362.3306 -4.2274 422.3615 426.5889 385.6132 363.9351 -4.2298 422.1547 426.3846 385.4175 365.5648 -4.2260 421.9000 426.1260 385.1686 367.1695 -4.2188 421.7004 425.9192 384.9531 368.7785 -4.2142 421.5425 425.7567 384.6719 370.3729 -4.2072 421.3570 425.5642 384.4498 371.9723 -4.1985 421.1287 425.3272 384.2409 373.5763 -4.1922 420.9351 425.1273 384.0280 375.1604 -4.1849 420.7196 424.9044 383.8211 376.7591 -4.1766 420.4868 424.6634 383.6464 378.3793 -4.1731 420.2633 424.4364 383.4384 379.9888 -4.1694 420.0708 424.2403 383.2611 381.5878 -4.1709 419.9314 424.1023 383.0875 383.1976 -4.1687 419.7171 423.8858 382.9295 384.8015 -4.1668 419.5471 423.7139 382.7388 386.3856 -4.1615 419.3813 423.5429 382.5537 387.9955 -4.1498 419.1449 423.2947 382.3930 389.5994 -4.1432 418.9032 423.0464 382.1827 391.2245 -4.1362 418.6910 422.8271 381.9279 392.8334 -4.1285 418.4701 422.5986 381.7397 394.4433 -4.1293 418.3028 422.4321 381.5031 396.0475 -4.1217 418.1129 422.2346 381.2394 397.6364 -4.1200 417.9229 422.0429 381.0158 399.2463 -4.1139 417.7236 421.8375 380.7896 400.8500 -4.1124 417.5333 421.6458 380.5823 402.4599 -4.1080 417.3147 421.4227 380.4040 404.0796 -4.1001 417.0743 421.1744 380.2013 405.6889 -4.0904 416.8825 420.9729 379.9678 407.2936 -4.0834 416.6641 420.7475 379.8171 408.8974 -4.0815 416.4592 420.5407 379.6448 410.5073 -4.0758 416.2499 420.3257 379.4496 412.1116 -4.0708 416.0486 420.1194 379.2443 413.7209 -4.0686 415.9024 419.9710 379.0515 415.3406 -4.0659 415.6884 419.7544 378.8268 416.9499 -4.0608 415.4166 419.4774 378.5471 418.5545 -4.0583 415.2569 419.3153 378.3091 420.1584 -4.0516 415.0905 419.1422 378.0467 421.7683 -4.0427 414.9369 418.9796 377.8071 423.3723 -4.0396 414.6678 418.7074 377.5589 424.9819 -4.0326 414.4178 418.4504 377.2792 426.6019 -4.0253 414.2241 418.2494 377.0593 428.2109 -4.0148 414.0554 418.0702 376.8275 429.8156 -4.0085 413.9031 417.9116 376.6425 431.4253 -4.0083 413.6955 417.7039 376.4178 433.0344 -4.0063 413.4915 417.4978 376.2307 434.6340 -3.9990 413.2964 417.2953 376.0613 436.2384 -3.9952 413.0555 417.0508 375.8423 437.8528 -3.9901 412.8568 416.8469 375.6543 439.4574 -3.9856 412.6609 416.6465 375.4898 441.0561 -3.9899 412.4568 416.4467 375.2977 442.6609 -3.9820 412.2406 416.2226 375.0818 444.2599 -3.9754 412.0285 416.0039 374.8955 445.8694 -3.9701 411.8282 415.7983 374.6703 447.4741 -3.9660 411.6335 415.5995 374.4934 449.0625 -3.9638 411.4316 415.3953 374.3172 450.6826 -3.9571 411.2189 415.1760 374.1475 452.2870 -3.9513 411.0108 414.9621 373.8986 453.8963 -3.9487 410.7519 414.7005 373.6833 455.5010 -3.9459 410.5612 414.5071 373.4739 457.1048 -3.9461 410.3448 414.2909 373.2436 458.7146 -3.9434 410.1238 414.0672 373.0110 460.3193 -3.9351 409.9693 413.9044 372.8006 461.9439 -3.9250 409.7955 413.7204 372.5980 463.5484 -3.9225 409.5818 413.5042 372.3652 465.1583 -3.9186 409.3571 413.2758 372.1715 466.7628 -3.9131 409.1769 413.0900 371.9666 468.3668 -3.9107 408.9877 412.8984 371.7640 469.9766 -3.9067 408.7739 412.6806 371.4990 471.5813 -3.8989 408.5599 412.4588 371.2827 473.2056 -3.8922 408.3603 412.2526 371.0842 474.8155 -3.8897 408.1451 412.0348 370.8589 476.4245 -3.8879 407.9038 411.7917 370.6627 478.0291 -3.8830 407.6599 411.5430 370.4325 479.6386 -3.8810 407.4621 411.3432 370.2470 481.2428 -3.8781 407.2695 411.1476 370.0177 482.8526 -3.8759 407.0726 410.9485 369.7842 484.4769 -3.8660 406.8501 410.7161 369.6148 486.0816 -3.8621 406.6224 410.4845 369.4526 487.6910 -3.8619 406.4305 410.2924 369.2320 489.2953 -3.8549 406.2517 410.1066 369.0199 490.9051 -3.8458 406.0796 409.9254 368.8386 492.5090 -3.8415 405.8786 409.7201 368.6401 494.1188 -3.8363 405.6908 409.5271 368.4352 495.7384 -3.8371 405.4870 409.3241 368.1795 497.3529 -3.8358 405.2552 409.0910 367.9133 498.9525 -3.8305 405.0740 408.9045 367.7077 500.5571 -3.8253 404.8426 408.6679 367.4869 502.1559 -3.8197 404.6821 408.5018 367.2587 503.7606 -3.8149 404.4499 408.2648 367.0744 505.3595 -3.8076 404.2394 408.0470 366.8359 506.9691 -3.8037 404.0311 407.8349 366.6662 508.5731 -3.8000 403.8140 407.6140 366.4911 510.1776 -3.7945 403.6567 407.4512 366.2832 511.7870 -3.7876 403.3944 407.1820 366.0474 513.3913 -3.7778 403.1583 406.9361 365.8162 514.9906 -3.7717 402.9316 406.7032 365.5808 516.5998 -3.7723 402.7274 406.4997 365.3189 518.2096 -3.7647 402.5349 406.2996 365.0848 519.8143 -3.7578 402.3334 406.0912 364.9063 521.4386 -3.7464 402.1587 405.9052 364.7094 523.0434 -3.7399 401.9435 405.6834 364.4877 524.6525 -3.7402 401.7171 405.4573 364.2682 526.2570 -3.7376 401.4412 405.1787 364.0521 527.8611 -3.7315 401.2532 404.9847 363.9071 529.4706 -3.7320 401.0759 404.8079 363.6779 531.0753 -3.7298 400.8552 404.5849 363.4682 532.6996 -3.7209 400.7090 404.4299 363.2455 534.3044 -3.7122 400.5396 404.2518 363.0615 535.9138 -3.7076 400.3729 404.0805 362.8396 537.5180 -3.6990 400.1837 403.8827 362.6557 539.1223 -3.6865 399.9981 403.6846 362.4210 540.7316 -3.6871 399.7403 403.4275 362.1881 542.3413 -3.6819 399.5375 403.2194 361.9920 543.9658 -3.6838 399.3638 403.0476 361.8281 545.5705 -3.6749 399.1336 402.8084 361.6153 547.1795 -3.6712 398.8922 402.5634 361.4240 548.7841 -3.6596 398.6544 402.3140 361.1900 550.3936 -3.6557 398.4500 402.1057 360.9088 552.0029 -3.6532 398.2310 401.8842 360.7013 553.6128 -3.6506 397.9959 401.6465 360.4912 555.2323 -3.6464 397.7545 401.4009 360.2799 556.8366 -3.6441 397.5601 401.2042 360.0138 558.4465 -3.6323 397.3718 401.0041 359.8037 560.0564 -3.6238 397.1674 400.7912 359.5776 561.6653 -3.6200 396.9739 400.5939 359.3649 563.2649 -3.6151 396.7932 400.4084 359.2033 564.8693 -3.6147 396.5359 400.1505 358.9985 566.4836 -3.6091 396.3478 399.9570 358.8209 568.0833 -3.6026 396.1407 399.7433 358.5998 569.6723 -3.5954 395.9315 399.5269 358.4249 571.2764 -3.5901 395.7364 399.3265 358.2156 572.8811 -3.5877 395.5194 399.1071 358.0024 574.4798 -3.5795 395.2702 398.8497 357.8619 576.0896 -3.5794 395.0702 398.6496 357.6557 577.6936 -3.5778 394.8804 398.4582 357.4364 579.3135 -3.5745 394.6517 398.2262 357.2527 580.9183 -3.5658 394.4159 397.9817 357.0136 582.5068 -3.5593 394.2509 397.8102 356.7666 584.1165 -3.5496 394.0475 397.5970 356.5306 585.7208 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