DTA measure 3gyors fel Date: 2024115:1419 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1442.76 s Mass = 958.600 mg data_number = 1796 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1668 -3.6680 415.9278 419.5958 423.7159 1.9588 -3.6628 416.1259 419.7886 423.6968 2.7498 -3.6674 416.2211 419.8885 423.6831 3.5688 -3.6599 416.4433 420.1033 423.6391 4.3270 -3.6742 416.4436 420.1178 423.7146 5.1755 -3.6670 416.5774 420.2445 423.8160 5.9635 -3.6814 416.7409 420.4223 423.7410 6.7525 -3.6825 417.0152 420.6977 423.5675 7.5710 -3.6734 417.1856 420.8590 423.6392 8.3590 -3.6715 417.3221 420.9936 423.5285 9.1785 -3.6735 417.3223 420.9957 423.5856 9.9683 -3.6757 417.6057 421.2814 423.5358 10.7593 -3.6744 417.7350 421.4094 423.5746 11.5815 -3.6711 418.0106 421.6816 423.3550 12.3430 -3.6845 418.1565 421.8410 423.3057 13.1950 -3.6864 418.3336 422.0199 423.2733 13.9865 -3.6732 418.4711 422.1443 423.1925 14.7775 -3.6890 418.5255 422.2145 423.1785 15.5998 -3.6979 418.6354 422.3334 423.1808 16.3615 -3.6721 418.9488 422.6209 422.9802 17.2140 -3.6756 419.1644 422.8400 422.7316 17.9758 -3.6872 419.1928 422.8801 422.6724 18.7978 -3.7052 419.3288 423.0340 422.6814 19.6198 -3.6995 419.4026 423.1021 422.5467 20.3815 -3.6847 419.6222 423.3070 422.4151 21.2338 -3.6851 419.7339 423.4190 422.3201 21.9955 -3.6989 419.9533 423.6522 422.1900 22.8178 -3.6960 420.0294 423.7254 422.0974 23.6398 -3.7044 420.2416 423.9460 421.9919 24.4025 -3.7079 420.3075 424.0154 421.9627 25.2548 -3.7102 420.4392 424.1494 421.8423 26.0165 -3.7134 420.5641 424.2775 421.7147 26.8388 -3.7119 420.6792 424.3911 421.6131 27.6610 -3.7014 420.8552 424.5566 421.4035 28.4235 -3.7050 421.0084 424.7134 421.3856 29.2755 -3.7082 421.1607 424.8689 421.2478 30.0675 -3.7111 421.3720 425.0831 421.1391 30.8595 -3.7107 421.3896 425.1003 421.0673 31.6818 -3.6982 421.5538 425.2520 420.7985 32.4445 -3.6986 421.6598 425.3584 420.7807 33.2965 -3.6970 421.8550 425.5519 420.7892 34.0885 -3.6945 421.9121 425.6066 420.6776 34.8790 -3.6907 421.9778 425.6685 420.5231 35.6973 -3.7013 422.1604 425.8617 420.4985 36.4860 -3.7154 422.3763 426.0917 420.3660 37.3045 -3.7102 422.5215 426.2318 420.2740 38.0930 -3.7041 422.5495 426.2536 420.2176 38.8820 -3.7087 422.6539 426.3626 420.1520 39.7003 -3.7224 422.6868 426.4092 419.9717 40.4890 -3.7075 422.8859 426.5934 419.6854 41.3083 -3.7127 422.9651 426.6779 419.7309 42.0988 -3.7137 423.0748 426.7885 419.6559 42.8905 -3.7115 423.2738 426.9853 419.5709 43.7125 -3.7232 423.3782 427.1014 419.4358 44.5035 -3.7201 423.5241 427.2442 419.4280 45.3255 -3.7258 423.5747 427.3005 419.3270 46.1175 -3.7149 423.7323 427.4471 419.1524 46.9095 -3.7164 423.8527 427.5691 419.0336 47.7315 -3.7287 423.7699 427.4986 419.0203 48.4935 -3.7318 423.9441 427.6758 418.8992 49.3455 -3.7385 424.0539 427.7924 418.9286 50.1375 -3.7255 424.1863 427.9118 418.8126 50.9295 -3.7377 424.2857 428.0234 418.6682 51.7515 -3.7332 424.3467 428.0800 418.5639 52.5135 -3.7375 424.4548 428.1924 418.5277 53.3655 -3.7417 424.5815 428.3232 418.3298 54.1575 -3.7418 424.6882 428.4301 418.2370 54.9490 -3.7405 424.7371 428.4775 418.1566 55.7718 -3.7409 424.9001 428.6409 418.0144 56.5343 -3.7427 425.0565 428.7991 417.8888 57.3865 -3.7540 425.0595 428.8135 417.8580 58.1488 -3.7426 425.1820 428.9246 417.8237 58.9708 -3.7341 425.3238 429.0579 417.5716 59.7930 -3.7465 425.3820 429.1285 417.5779 60.5555 -3.7563 425.5628 429.3191 417.4104 61.4083 -3.7571 425.5422 429.2993 417.2087 62.1705 -3.7671 425.5835 429.3505 417.3045 62.9928 -3.7489 425.7568 429.5057 417.2098 63.7848 -3.7428 425.8285 429.5713 417.0679 64.5765 -3.7729 425.8730 429.6458 416.9625 65.4293 -3.7820 425.9589 429.7409 416.7532 66.1915 -3.8047 426.0369 429.8416 416.7062 67.0120 -3.7852 426.0085 429.7937 416.7084 67.8000 -3.7838 426.1693 429.9531 416.6218 68.5880 -3.7868 426.2166 430.0034 416.5406 69.4373 -3.7872 426.2793 430.0664 416.3884 70.1960 -3.7834 426.3542 430.1376 416.2174 71.0145 -3.7808 426.4861 430.2669 416.2062 71.8033 -3.7989 426.5581 430.3570 416.1687 72.5920 -3.8068 426.6812 430.4879 415.9971 73.4410 -3.7986 426.6846 430.4832 415.8544 74.2018 -3.7985 426.6886 430.4870 415.8745 75.0223 -3.7924 426.7643 430.5567 415.7160 75.8128 -3.7997 426.8416 430.6413 415.6398 76.6045 -3.8008 426.8230 430.6238 415.5005 77.4568 -3.8127 426.8612 430.6739 415.4117 78.2185 -3.8170 426.9766 430.7937 415.3358 79.0408 -3.8260 427.0239 430.8499 415.3787 79.8328 -3.8172 427.1350 430.9522 415.2228 80.6245 -3.8314 427.2520 431.0834 415.1303 81.4468 -3.8325 427.2635 431.0960 414.9898 82.2385 -3.8577 427.3020 431.1597 414.9611 83.0608 -3.8403 427.3947 431.2349 414.8053 83.8528 -3.8511 427.5514 431.4025 414.6492 84.6445 -3.8480 427.5294 431.3774 414.6481 85.4965 -3.8242 427.6574 431.4816 414.4338 86.2585 -3.8318 427.6448 431.4766 414.3497 87.0805 -3.8468 427.6661 431.5128 414.3087 87.8725 -3.8499 427.7650 431.6149 414.2365 88.6645 -3.8461 427.8214 431.6675 413.9901 89.5165 -3.8445 427.8628 431.7073 413.9877 90.2785 -3.8465 427.7787 431.6252 413.8615 91.1013 -3.8571 427.8531 431.7102 413.8219 91.8935 -3.8596 427.9379 431.7975 413.6766 92.6855 -3.8719 427.9066 431.7784 413.5645 93.5375 -3.8779 427.9658 431.8437 413.5525 94.2993 -3.8767 428.0819 431.9586 413.3963 95.1215 -3.8768 428.1158 431.9926 413.2361 95.9430 -3.8907 428.2257 432.1164 413.1381 96.7045 -3.8868 428.1358 432.0226 413.1428 97.5575 -3.8864 428.1058 431.9922 413.0206 98.3198 -3.8759 428.2020 432.0779 412.9353 99.1400 -3.8846 428.2483 432.1329 412.9568 99.9285 -3.9119 428.3302 432.2422 412.8067 100.7175 -3.9074 428.2556 432.1629 412.6125 101.5660 -3.9069 428.4364 432.3433 412.4961 102.3235 -3.9056 428.5050 432.4105 412.4297 103.1425 -3.9050 428.4937 432.3988 412.4755 103.9310 -3.9130 428.4582 432.3712 412.3032 104.7208 -3.9028 428.4788 432.3816 412.2095 105.5698 -3.9082 428.5990 432.5072 412.1692 106.3303 -3.9260 428.6230 432.5490 412.1696 107.1505 -3.9326 428.5862 432.5188 412.0430 107.9425 -3.9217 428.6187 432.5405 411.9687 108.7340 -3.9205 428.5612 432.4817 411.6697 109.5563 -3.9325 428.7172 432.6497 411.6200 110.3483 -3.9415 428.7205 432.6620 411.5023 111.1705 -3.9431 428.7994 432.7424 411.4073 111.9623 -3.9400 428.7962 432.7361 411.2815 112.7535 -3.9429 428.7368 432.6798 411.2267 113.5763 -3.9495 428.7521 432.7017 411.1033 114.3375 -3.9516 428.7786 432.7302 411.0887 115.1903 -3.9594 428.7837 432.7431 410.9326 115.9818 -3.9627 428.8067 432.7694 410.6809 116.7735 -3.9609 428.7921 432.7530 410.6033 117.5960 -3.9635 428.9413 432.9048 410.6067 118.3575 -3.9643 429.0046 432.9690 410.5591 119.2118 -3.9727 428.9270 432.8998 410.4566 119.9745 -3.9713 428.8836 432.8549 410.3136 120.7968 -3.9822 428.8748 432.8570 410.2056 121.6188 -3.9933 429.0690 433.0623 410.1121 122.3805 -3.9977 429.1237 433.1214 409.9737 123.2328 -3.9996 429.0861 433.0857 409.9240 123.9945 -4.0088 429.1041 433.1130 409.7529 124.8165 -4.0198 429.0585 433.0782 409.7317 125.6388 -4.0105 428.9490 432.9595 409.5421 126.4005 -4.0134 428.9816 432.9950 409.4276 127.2533 -4.0169 428.9413 432.9582 409.4535 128.0155 -4.0066 428.9842 432.9908 409.2668 128.8375 -4.0156 429.0138 433.0295 409.1140 129.6595 -4.0199 429.0174 433.0373 408.9876 130.4215 -4.0271 428.9981 433.0252 408.9567 131.2735 -4.0110 428.9713 432.9824 408.9696 132.0330 -4.0248 429.0754 433.1001 408.7554 132.8510 -4.0316 429.1058 433.1374 408.6661 133.6690 -4.0479 428.9732 433.0211 408.6281 134.4270 -4.0305 428.9624 432.9929 408.5322 135.2750 -4.0426 429.0407 433.0834 408.3510 136.0630 -4.0379 429.0192 433.0571 408.2025 136.8520 -4.0456 429.0424 433.0880 408.1702 137.6703 -4.0390 429.0525 433.0915 408.0681 138.4590 -4.0550 428.9586 433.0136 407.9087 139.2798 -4.0451 429.1292 433.1743 407.7264 140.0715 -4.0638 428.9989 433.0627 407.7614 140.8635 -4.0663 429.0588 433.1251 407.6762 141.6855 -4.0668 429.1287 433.1955 407.6202 142.4775 -4.0818 429.0822 433.1640 407.4926 143.2995 -4.0890 428.9706 433.0596 407.4390 144.0915 -4.0888 428.8864 432.9752 407.3924 144.8835 -4.0853 428.9461 433.0314 407.1672 145.7055 -4.0829 428.9472 433.0300 407.1330 146.4975 -4.0746 428.9970 433.0716 407.0255 147.3195 -4.0801 429.0048 433.0849 406.9246 148.1115 -4.0986 428.7921 432.8907 406.9051 148.9035 -4.1230 428.8459 432.9689 406.7483 149.7555 -4.1229 428.9340 433.0568 406.6236 150.5175 -4.1103 428.9578 433.0681 406.5804 151.3393 -4.1152 428.8451 432.9603 406.5469 152.1313 -4.1241 428.8779 433.0021 406.3636 152.9233 -4.1272 428.8997 433.0269 406.1365 153.7750 -4.1109 428.7870 432.8979 406.1144 154.5368 -4.1349 428.7602 432.8951 406.0607 155.3588 -4.1196 428.8199 432.9395 406.0077 156.1808 -4.1258 428.7238 432.8496 405.8198 156.9425 -4.1380 428.7733 432.9113 405.8041 157.7953 -4.1541 428.6901 432.8442 405.7796 158.5575 -4.1710 428.6857 432.8567 405.5601 159.3798 -4.1591 428.7053 432.8645 405.4437 160.2020 -4.1438 428.6958 432.8396 405.4034 160.9645 -4.1599 428.7622 432.9222 405.2183 161.8168 -4.1592 428.7690 432.9282 405.0681 162.5785 -4.1675 428.7263 432.8937 405.0212 163.4008 -4.1639 428.5998 432.7637 404.9612 164.2190 -4.1614 428.6014 432.7628 404.9034 164.9770 -4.1592 428.6115 432.7707 404.7495 165.8250 -4.1486 428.6009 432.7494 404.6219 166.5830 -4.1686 428.6125 432.7810 404.4937 167.4010 -4.1700 428.4701 432.6401 404.3768 168.2193 -4.1389 428.4515 432.5904 404.2455 168.9790 -4.1446 428.4098 432.5544 404.1659 169.8285 -4.1671 428.3382 432.5053 404.1527 170.5890 -4.1700 428.2952 432.4652 404.0523 171.4108 -4.1791 428.3625 432.5416 403.9862 172.2013 -4.1802 428.3295 432.5098 403.9293 172.9918 -4.1959 428.2648 432.4607 403.6939 173.8438 -4.1774 428.2146 432.3920 403.5847 174.6055 -4.1797 428.1844 432.3641 403.5180 175.4278 -4.1922 428.1494 432.3416 403.3452 176.2198 -4.1982 428.1190 432.3172 403.2994 177.0115 -4.1916 428.1419 432.3335 403.2194 177.8338 -4.1810 428.1403 432.3213 403.0896 178.6255 -4.1968 428.1442 432.3410 402.9470 179.4478 -4.1995 428.0909 432.2904 402.8940 180.2398 -4.2029 427.9251 432.1280 402.9614 181.0315 -4.1904 427.9029 432.0933 402.8556 181.8535 -4.1976 427.7729 431.9706 402.7090 182.6455 -4.1966 427.8417 432.0383 402.5537 183.4675 -4.2118 427.8258 432.0376 402.5292 184.2595 -4.2088 427.7878 431.9966 402.3516 185.0515 -4.2118 427.7796 431.9914 402.2561 185.8738 -4.2038 427.7957 431.9995 402.0961 186.6365 -4.2191 427.7206 431.9397 402.0385 187.4885 -4.2262 427.6777 431.9039 401.8878 188.2805 -4.2214 427.6876 431.9091 401.7666 189.0735 -4.2339 427.6045 431.8384 401.7597 189.8955 -4.2409 427.4903 431.7312 401.6564 190.6573 -4.2374 427.4928 431.7302 401.4657 191.5093 -4.2402 427.4054 431.6456 401.3642 192.3015 -4.2468 427.4319 431.6786 401.3047 193.0935 -4.2491 427.3312 431.5803 401.2570 193.9163 -4.2483 427.3322 431.5805 401.0807 194.7075 -4.2471 427.2994 431.5464 401.0056 195.5295 -4.2395 427.2520 431.4916 400.8018 196.3185 -4.2418 427.2125 431.4543 400.7641 197.1070 -4.2415 427.2463 431.4878 400.5851 197.9255 -4.2281 427.2136 431.4418 400.5378 198.7138 -4.2439 427.1247 431.3687 400.4681 199.5318 -4.2567 427.0188 431.2755 400.3796 200.3200 -4.2523 427.0013 431.2535 400.3022 201.1090 -4.2576 426.8558 431.1134 400.2501 201.9575 -4.2785 426.7675 431.0459 400.1163 202.7175 -4.2585 426.7884 431.0469 399.9885 203.5390 -4.2570 426.7641 431.0211 399.7769 204.3305 -4.2550 426.6805 430.9356 399.7316 205.1225 -4.2505 426.6584 430.9089 399.6233 205.9743 -4.2696 426.6387 430.9083 399.5263 206.7365 -4.2747 426.6712 430.9459 399.4398 207.5578 -4.2896 426.5734 430.8630 399.4003 208.3505 -4.2740 426.4826 430.7566 399.3679 209.1415 -4.2721 426.5117 430.7838 399.1053 209.9940 -4.2638 426.3829 430.6467 399.0353 210.7560 -4.2675 426.4164 430.6839 399.0327 211.5778 -4.2481 426.4348 430.6829 398.8357 212.3700 -4.2863 426.3465 430.6329 398.8420 213.1615 -4.2909 426.2090 430.4999 398.6965 214.0140 -4.2859 426.1806 430.4666 398.6143 214.7755 -4.2855 426.0795 430.3650 398.5183 215.5978 -4.2740 426.0148 430.2888 398.3821 216.4198 -4.2786 426.0200 430.2986 398.2534 217.1815 -4.2685 426.0432 430.3117 398.1081 218.0338 -4.2762 425.9909 430.2671 398.0046 218.7955 -4.2707 425.8634 430.1341 397.8721 219.6178 -4.2617 425.9290 430.1906 397.6634 220.4098 -4.2765 425.6147 429.8912 397.7607 221.2015 -4.2683 425.6540 429.9224 397.6645 222.0543 -4.2827 425.5883 429.8710 397.5454 222.8165 -4.2717 425.4724 429.7441 397.4235 223.6385 -4.2710 425.4574 429.7284 397.3093 224.4305 -4.2734 425.4837 429.7571 397.1207 225.2225 -4.2528 425.4676 429.7205 396.9763 226.0750 -4.2507 425.4020 429.6527 396.8169 226.8375 -4.2684 425.3351 429.6034 396.8496 227.6595 -4.2683 425.2655 429.5338 396.8066 228.4480 -4.2684 425.1096 429.3780 396.6718 229.2368 -4.2772 424.9503 429.2275 396.7283 230.0850 -4.2753 424.9798 429.2551 396.5242 230.8430 -4.2804 424.9741 429.2545 396.4944 231.6618 -4.2766 424.9492 429.2258 396.4396 232.4505 -4.2766 424.8169 429.0935 396.3856 233.2403 -4.2685 424.7080 428.9765 396.1954 234.0900 -4.2733 424.7383 429.0116 396.0526 234.8513 -4.2715 424.7029 428.9743 395.9382 235.6715 -4.2816 424.5254 428.8069 395.8812 236.4638 -4.2745 424.5297 428.8042 395.7941 237.2553 -4.2783 424.5021 428.7804 395.6865 238.0765 -4.2737 424.4093 428.6830 395.5329 238.8685 -4.2778 424.3722 428.6500 395.3720 239.6905 -4.2876 424.2934 428.5810 395.3482 240.4828 -4.2716 424.3144 428.5860 395.1081 241.2745 -4.2710 424.2039 428.4749 395.0775 242.0965 -4.2774 424.1433 428.4206 395.0250 242.8885 -4.2685 424.1229 428.3913 394.9237 243.7105 -4.2672 424.0340 428.3012 394.8193 244.5025 -4.2653 423.9765 428.2418 394.7683 245.2945 -4.2660 423.9616 428.2276 394.6027 246.1165 -4.2729 423.8818 428.1548 394.5058 246.9085 -4.2740 423.6661 427.9401 394.4173 247.7313 -4.2772 423.6058 427.8830 394.3241 248.5235 -4.2770 423.6685 427.9454 394.1290 249.3150 -4.2519 423.6522 427.9041 394.0088 250.1370 -4.2657 423.4773 427.7430 393.9250 250.9288 -4.2701 423.4185 427.6885 393.7819 251.7508 -4.2768 423.2974 427.5742 393.7827 252.5428 -4.2767 423.1771 427.4539 393.6881 253.3345 -4.2813 423.1096 427.3909 393.6073 254.1868 -4.2612 423.0922 427.3535 393.4492 254.9485 -4.2632 423.0736 427.3368 393.4096 255.7715 -4.2816 423.0232 427.3049 393.3684 256.5638 -4.2851 422.8577 427.1428 393.2449 257.3555 -4.2749 422.7721 427.0470 393.0624 258.2083 -4.2683 422.8552 427.1235 392.9977 258.9705 -4.2617 422.7363 426.9980 392.8981 259.7928 -4.2429 422.6753 426.9181 392.8308 260.6143 -4.2638 422.5881 426.8519 392.7388 261.3730 -4.2561 422.5401 426.7962 392.6621 262.2210 -4.2603 422.5243 426.7845 392.4235 262.9793 -4.2618 422.4171 426.6789 392.3479 263.7990 -4.2648 422.3779 426.6427 392.1576 264.5873 -4.2555 422.2660 426.5215 391.9623 265.3760 -4.2435 422.1450 426.3886 392.0335 266.2250 -4.2558 422.0591 426.3149 392.0167 266.9853 -4.2544 422.0240 426.2784 391.9156 267.8058 -4.2422 421.9792 426.2214 391.7738 268.5958 -4.2653 421.9360 426.2013 391.6783 269.3875 -4.2335 421.8152 426.0487 391.5603 270.2395 -4.2371 421.8316 426.0687 391.3372 271.0015 -4.2391 421.6824 425.9214 391.3580 271.8238 -4.2375 421.6040 425.8415 391.1478 272.6158 -4.2387 421.5351 425.7738 391.0298 273.4075 -4.2517 421.5070 425.7587 391.0067 274.2298 -4.2390 421.3983 425.6373 390.9477 274.9915 -4.2363 421.3182 425.5545 390.7872 275.8438 -4.2364 421.3819 425.6183 390.7097 276.6358 -4.2359 421.3052 425.5410 390.5557 277.4275 -4.2388 421.1194 425.3582 390.4616 278.2498 -4.2205 421.1368 425.3573 390.3452 279.0715 -4.2186 421.0557 425.2743 390.1829 279.8635 -4.2198 420.9562 425.1761 390.2231 280.6855 -4.2270 420.8368 425.0638 390.0524 281.4775 -4.2305 420.8688 425.0993 390.0206 282.2995 -4.2264 420.6445 424.8709 389.8221 283.0915 -4.2188 420.6460 424.8648 389.5911 283.8835 -4.2240 420.5226 424.7466 389.6540 284.7055 -4.2029 420.4103 424.6131 389.5955 285.4975 -4.2141 420.2509 424.4650 389.4687 286.3203 -4.2134 420.2272 424.4406 389.3726 287.1125 -4.2105 420.1486 424.3590 389.2718 287.9055 -4.2199 420.0566 424.2764 389.2002 288.7273 -4.2308 419.9772 424.2080 389.1454 289.5193 -4.2206 419.9512 424.1718 388.9996 290.3415 -4.1985 419.9076 424.1061 388.7829 291.1340 -4.2189 419.7231 423.9419 388.8131 291.9255 -4.2192 419.7347 423.9540 388.6249 292.7470 -4.2005 419.6026 423.8031 388.6203 293.5353 -4.2072 419.5791 423.7863 388.4742 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