DTA measure 1ón Date: 2024102:958 Lower limit = 100.0 C Upper limit = 340.0 C Rate = 10.00 C/min Mtime = 1439.22 s Mass = 950.700 mg data_number = 1781 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1745 -0.9298 149.4742 150.4040 137.7838 2.0270 -0.9033 149.4446 150.3478 137.7195 2.7888 -0.8632 149.4076 150.2708 137.6772 3.6115 -0.8686 149.3781 150.2468 137.6346 4.4343 -0.8510 149.3514 150.2024 137.6043 5.1965 -0.8595 149.3071 150.1667 137.5731 6.0490 -0.8645 149.2744 150.1389 137.4964 6.8093 -0.8585 149.2349 150.0934 137.4515 7.6293 -0.8550 149.2117 150.0667 137.4018 8.4458 -0.8266 149.1634 149.9900 137.3695 9.2050 -0.7933 149.1495 149.9427 137.3258 10.0533 -0.7747 149.1099 149.8846 137.2881 10.8113 -0.7142 149.0625 149.7766 137.2331 11.6300 -0.6725 149.0208 149.6933 137.1907 12.4483 -0.6641 148.9893 149.6534 137.1425 13.2070 -0.6636 148.9532 149.6168 137.0904 14.0560 -0.6561 148.9086 149.5647 137.0390 14.8440 -0.6465 148.8862 149.5327 137.0026 15.6338 -0.6375 148.8652 149.5026 136.9631 16.4523 -0.6268 148.8243 149.4510 136.9078 17.2403 -0.6248 148.7814 149.4062 136.8686 18.0588 -0.6158 148.7611 149.3769 136.8095 18.8470 -0.6073 148.7098 149.3171 136.7682 19.6360 -0.6033 148.6891 149.2924 136.7163 20.4545 -0.5984 148.6581 149.2565 136.6806 21.2495 -0.5838 148.5986 149.1824 136.6327 22.0695 -0.5643 148.5605 149.1249 136.5781 22.8583 -0.5504 148.5228 149.0732 136.5323 23.6470 -0.5674 148.4890 149.0563 136.5042 24.4975 -0.5768 148.4737 149.0505 136.4486 25.2583 -0.5736 148.4299 149.0035 136.3898 26.0795 -0.5683 148.4044 148.9727 136.3503 26.8720 -0.5621 148.3742 148.9363 136.3016 27.6635 -0.5566 148.3310 148.8875 136.2679 28.5158 -0.5487 148.2889 148.8375 136.2192 29.2775 -0.5440 148.2713 148.8153 136.1777 30.0998 -0.5386 148.2296 148.7682 136.1177 30.8928 -0.5328 148.1881 148.7209 136.0652 31.6898 -0.5278 148.1412 148.6690 136.0521 32.5118 -0.5210 148.0932 148.6142 136.0143 33.3035 -0.5168 148.0596 148.5763 135.9468 34.1255 -0.5122 148.0310 148.5432 135.9092 34.9175 -0.5061 147.9975 148.5035 135.8636 35.7095 -0.4991 147.9481 148.4472 135.8172 36.5315 -0.4922 147.8981 148.3903 135.7696 37.3235 -0.4869 147.8760 148.3629 135.7393 38.1455 -0.4807 147.8296 148.3103 135.6777 38.9375 -0.4450 147.7995 148.2444 135.6212 39.7295 -0.4268 147.7758 148.2026 135.5776 40.5515 -0.4300 147.7339 148.1639 135.5315 41.3435 -0.4313 147.6814 148.1126 135.5067 42.1683 -0.4383 147.6562 148.0945 135.4712 42.9603 -0.4390 147.6275 148.0665 135.4144 43.7518 -0.4275 147.5762 148.0037 135.3553 44.5743 -0.4132 147.5420 147.9551 135.3130 45.3660 -0.4095 147.5030 147.9125 135.2612 46.1880 -0.4048 147.4651 147.8699 135.2269 46.9805 -0.4060 147.4522 147.8582 135.1908 47.7715 -0.3932 147.4151 147.8083 135.1579 48.5940 -0.3868 147.3653 147.7521 135.1060 49.3858 -0.3740 147.3068 147.6808 135.0474 50.2078 -0.3727 147.2697 147.6424 134.9994 51.0010 -0.3725 147.2188 147.5913 134.9682 51.7935 -0.3726 147.2155 147.5881 134.9263 52.6160 -0.3744 147.1817 147.5561 134.8719 53.4078 -0.3741 147.1356 147.5096 134.8157 54.2298 -0.3689 147.0945 147.4635 134.7690 55.0220 -0.3692 147.0503 147.4195 134.7177 55.8135 -0.3636 147.0111 147.3747 134.7019 56.6660 -0.3608 146.9896 147.3504 134.6359 57.4278 -0.3584 146.9417 147.3001 134.5756 58.2498 -0.3493 146.8924 147.2416 134.5478 59.0418 -0.3463 146.8646 147.2109 134.4970 59.8335 -0.3338 146.8072 147.1410 134.4502 60.6858 -0.3186 146.7629 147.0814 134.4120 61.4475 -0.2910 146.7329 147.0239 134.3869 62.2695 -0.3111 146.6934 147.0045 134.3395 63.0615 -0.3040 146.6608 146.9648 134.2897 63.8535 -0.2900 146.6146 146.9045 134.2365 64.7055 -0.3126 146.5671 146.8797 134.1956 65.4675 -0.3153 146.5412 146.8565 134.1493 66.2895 -0.3103 146.5236 146.8339 134.0995 67.0815 -0.3072 146.4779 146.7851 134.0611 67.8735 -0.2869 146.4356 146.7224 134.0395 68.7260 -0.3017 146.3889 146.6906 133.9864 69.4885 -0.3034 146.3535 146.6569 133.9285 70.3105 -0.3012 146.3107 146.6119 133.8541 71.1028 -0.2949 146.2873 146.5822 133.8239 71.8925 -0.2918 146.2513 146.5431 133.8068 72.7125 -0.2859 146.2073 146.4932 133.7366 73.5003 -0.2829 146.1656 146.4485 133.7012 74.3185 -0.2789 146.1092 146.3881 133.6452 75.1065 -0.2780 146.0953 146.3733 133.6088 75.8948 -0.2743 146.0620 146.3363 133.5630 76.7135 -0.2690 146.0054 146.2744 133.5241 77.5020 -0.2660 145.9707 146.2368 133.4946 78.3200 -0.2638 145.9364 146.2001 133.4239 79.1080 -0.2590 145.8827 146.1417 133.4213 79.8970 -0.2525 145.8261 146.0786 133.3791 80.7153 -0.2508 145.7941 146.0449 133.3367 81.5050 -0.2504 145.7536 146.0041 133.2866 82.3243 -0.2471 145.7218 145.9689 133.2324 83.1130 -0.2425 145.6842 145.9266 133.1876 83.9020 -0.2384 145.6456 145.8840 133.1431 84.7215 -0.2387 145.6031 145.8418 133.0819 85.5110 -0.2359 145.5820 145.8179 133.0497 86.3298 -0.2327 145.5412 145.7739 133.0187 87.1185 -0.2311 145.4856 145.7167 132.9777 87.9083 -0.2284 145.4568 145.6851 132.9327 88.7295 -0.2269 145.4087 145.6356 132.8801 89.5208 -0.2212 145.3746 145.5957 132.8123 90.3420 -0.2161 145.3193 145.5354 132.7898 91.1323 -0.2169 145.2939 145.5108 132.7380 91.9238 -0.2172 145.2584 145.4756 132.6876 92.7465 -0.2120 145.2047 145.4166 132.6532 93.5078 -0.2076 145.1862 145.3939 132.6100 94.3603 -0.2041 145.1167 145.3209 132.5772 95.1520 -0.2010 145.1011 145.3021 132.5295 95.9435 -0.1944 145.0560 145.2503 132.4957 96.7660 -0.1942 145.0078 145.2019 132.4453 97.5275 -0.1916 144.9813 145.1729 132.4094 98.3800 -0.1871 144.9393 145.1264 132.3467 99.1418 -0.1825 144.9013 145.0839 132.2977 99.9638 -0.1816 144.8546 145.0362 132.2478 100.7865 -0.1803 144.8383 145.0186 132.2124 101.5485 -0.1802 144.7689 144.9491 132.1885 102.4010 -0.1764 144.7313 144.9077 132.1219 103.1628 -0.1738 144.6825 144.8562 132.0854 103.9848 -0.1696 144.6386 144.8082 132.0570 104.7770 -0.1677 144.6056 144.7734 131.9974 105.5685 -0.1632 144.5762 144.7394 131.9663 106.4215 -0.1585 144.5243 144.6827 131.9236 107.1835 -0.1623 144.4779 144.6401 131.8862 108.0058 -0.1592 144.4299 144.5891 131.8316 108.7978 -0.1579 144.4040 144.5619 131.7949 109.5895 -0.1558 144.3565 144.5122 131.7304 110.4115 -0.1501 144.3377 144.4878 131.7021 111.2035 -0.1479 144.2949 144.4428 131.6528 112.0255 -0.1479 144.2516 144.3995 131.6126 112.8175 -0.1469 144.2132 144.3601 131.5673 113.6095 -0.1364 144.1649 144.3013 131.5179 114.4315 -0.1372 144.1121 144.2493 131.4873 115.2235 -0.1361 144.0857 144.2218 131.4360 116.0455 -0.1334 144.0379 144.1713 131.3889 116.8375 -0.1288 144.0040 144.1327 131.3680 117.6295 -0.1260 143.9667 144.0927 131.3196 118.4515 -0.1241 143.9210 144.0450 131.2770 119.2435 -0.1231 143.8848 144.0079 131.2246 120.0655 -0.1201 143.8432 143.9633 131.1855 120.8575 -0.1204 143.8044 143.9248 131.1351 121.6495 -0.1157 143.7484 143.8640 131.0851 122.4715 -0.1117 143.6990 143.8107 131.0509 123.2635 -0.1090 143.6833 143.7923 131.0067 124.0855 -0.1105 143.6464 143.7569 130.9588 124.8775 -0.1107 143.6102 143.7209 130.9320 125.6693 -0.1097 143.5587 143.6685 130.8818 126.4930 -0.1064 143.5046 143.6110 130.8563 127.2848 -0.1048 143.4690 143.5738 130.8099 128.1068 -0.1005 143.4260 143.5264 130.7599 128.8990 -0.0983 143.3922 143.4905 130.7214 129.6905 -0.0952 143.3446 143.4398 130.7014 130.5130 -0.0951 143.3065 143.4016 130.6306 131.3048 -0.0945 143.2651 143.3597 130.5766 132.1275 -0.0940 143.2365 143.3305 130.5351 132.9200 -0.0915 143.1812 143.2727 130.4942 133.7125 -0.0866 143.1391 143.2257 130.4477 134.5655 -0.0829 143.0953 143.1783 130.4139 135.3233 -0.0863 143.0724 143.1587 130.3608 136.1430 -0.0853 143.0287 143.1140 130.3296 136.9310 -0.0804 142.9792 143.0597 130.2931 137.7190 -0.0799 142.9307 143.0106 130.2464 138.5370 -0.0776 142.8921 142.9697 130.2111 139.3250 -0.0735 142.8481 142.9216 130.1602 140.1430 -0.0693 142.8193 142.8886 130.1069 140.9310 -0.0675 142.7864 142.8538 130.0711 141.7200 -0.0683 142.7452 142.8135 130.0199 142.5688 -0.0648 142.6978 142.7626 129.9988 143.3270 -0.0667 142.6646 142.7313 129.9516 144.1460 -0.0644 142.6502 142.7146 129.9032 144.9350 -0.0615 142.5813 142.6428 129.8878 145.7250 -0.0601 142.5244 142.5845 129.8423 146.5738 -0.0596 142.4886 142.5481 129.7935 147.3323 -0.0591 142.4525 142.5116 129.7392 148.1510 -0.0578 142.4016 142.4594 129.6821 148.9695 -0.0532 142.3679 142.4211 129.6486 149.7290 -0.0505 142.3298 142.3802 129.6249 150.5788 -0.0502 142.2963 142.3466 129.5643 151.3383 -0.0466 142.2473 142.2940 129.5435 152.1583 -0.0423 142.2079 142.2502 129.4939 152.9785 -0.0415 142.1697 142.2112 129.4797 153.7400 -0.0419 142.1227 142.1647 129.4247 154.5673 -0.0398 142.0822 142.1220 129.3818 155.3595 -0.0397 142.0433 142.0829 129.3327 156.1825 -0.0352 142.0155 142.0507 129.2836 156.9745 -0.0359 141.9632 141.9991 129.2502 157.7965 -0.0345 141.9174 141.9519 129.2023 158.5885 -0.0322 141.8741 141.9063 129.1449 159.3805 -0.0308 141.8273 141.8581 129.1184 160.2025 -0.0303 141.7858 141.8160 129.0864 160.9650 -0.0263 141.7567 141.7829 129.0330 161.8175 -0.0247 141.7183 141.7430 129.0033 162.6095 -0.0234 141.6621 141.6855 128.9471 163.4015 -0.0228 141.6340 141.6568 128.9006 164.2235 -0.0204 141.5975 141.6178 128.8579 164.9855 -0.0178 141.5446 141.5624 128.8209 165.8375 -0.0135 141.5049 141.5184 128.7776 166.6295 -0.0142 141.4774 141.4916 128.7520 167.4215 -0.0138 141.4134 141.4271 128.6815 168.2435 -0.0116 141.3749 141.3866 128.6523 169.0055 -0.0121 141.3669 141.3790 128.6126 169.8575 -0.0122 141.3052 141.3174 128.5735 170.6495 -0.0115 141.2670 141.2785 128.5538 171.4413 -0.0070 141.2166 141.2236 128.4990 172.2635 -0.0026 141.1687 141.1712 128.4716 173.0553 0.0011 141.1202 141.1191 128.4166 173.8770 0.0027 141.0857 141.0829 128.3792 174.6693 0.0006 141.0417 141.0412 128.3451 175.4608 0.0039 141.0040 141.0001 128.2922 176.2833 0.0056 140.9588 140.9532 128.2303 177.0748 0.0048 140.9334 140.9286 128.1911 177.8968 0.0089 140.8861 140.8772 128.1497 178.6890 0.0117 140.8383 140.8266 128.1254 179.4805 0.0095 140.8157 140.8062 128.0913 180.3030 0.0109 140.7841 140.7732 128.0389 181.0645 0.0150 140.7320 140.7170 128.0046 181.9170 0.0157 140.6901 140.6744 127.9734 182.7090 0.0181 140.6458 140.6277 127.9353 183.5005 0.0197 140.5962 140.5765 127.8739 184.3230 0.0175 140.5499 140.5324 127.8325 185.1148 0.0199 140.5145 140.4946 127.7840 185.9368 0.0227 140.4770 140.4543 127.7685 186.7288 0.0223 140.4442 140.4219 127.7239 187.5215 0.0237 140.3959 140.3722 127.6683 188.3438 0.0251 140.3422 140.3170 127.6392 189.1055 0.0283 140.3084 140.2801 127.5865 189.9580 0.0251 140.2607 140.2356 127.5396 190.7495 0.0287 140.2125 140.1837 127.5155 191.5415 0.0302 140.1873 140.1571 127.4786 192.3635 0.0328 140.1448 140.1120 127.4220 193.1255 0.0314 140.1035 140.0722 127.3862 193.9775 0.0352 140.0764 140.0412 127.3506 194.7695 0.0361 140.0206 139.9845 127.3247 195.5615 0.0401 139.9708 139.9307 127.2732 196.3835 0.0398 139.9253 139.8855 127.2211 197.1455 0.0385 139.9010 139.8625 127.1842 197.9975 0.0412 139.8402 139.7991 127.1537 198.7895 0.0443 139.8172 139.7729 127.0959 199.5823 0.0477 139.7758 139.7281 127.0619 200.4028 0.0541 139.7332 139.6791 127.0357 201.1608 0.0828 139.6827 139.5999 127.0064 202.0095 0.0677 139.6445 139.5768 126.9628 202.7980 0.0878 139.6137 139.5259 126.9201 203.5860 0.1170 139.5764 139.4594 126.8619 204.4043 0.1063 139.5258 139.4196 126.8210 205.1758 0.1000 139.4738 139.3738 126.7746 206.0080 0.1257 139.4357 139.3100 126.7337 206.7660 0.1279 139.3965 139.2686 126.6860 207.6153 0.1060 139.3602 139.2542 126.6729 208.4040 0.1055 139.3159 139.2104 126.6239 209.1930 0.1091 139.2907 139.1816 126.5713 210.0118 0.1006 139.2464 139.1458 126.5328 210.7710 0.1082 139.1956 139.0874 126.4889 211.6195 0.1153 139.1774 139.0621 126.4411 212.4080 0.1016 139.1193 139.0177 126.4058 213.1978 0.1129 139.0776 138.9647 126.3668 214.0168 0.0832 139.0333 138.9502 126.3182 214.8070 0.0699 138.9952 138.9253 126.2886 215.6275 0.0698 138.9407 138.8709 126.2447 216.4193 0.0684 138.9120 138.8435 126.2227 217.2105 0.0701 138.8631 138.7930 126.1749 218.0325 0.0704 138.8327 138.7623 126.1175 218.7943 0.0719 138.7859 138.7141 126.0903 219.6460 0.0725 138.7399 138.6674 126.0476 220.4385 0.0728 138.7082 138.6354 126.0090 221.2298 0.0733 138.6683 138.5950 125.9706 222.0523 0.0769 138.6235 138.5466 125.9279 222.8140 0.0784 138.5903 138.5119 125.8833 223.6660 0.0812 138.5228 138.4416 125.8220 224.4278 0.0801 138.4947 138.4145 125.7998 225.2498 0.0805 138.4541 138.3736 125.7662 226.0443 0.0835 138.4012 138.3177 125.7322 226.8378 0.0840 138.3764 138.2925 125.6924 227.6900 0.0844 138.3249 138.2405 125.6399 228.4518 0.0861 138.2919 138.2059 125.6029 229.2738 0.0873 138.2485 138.1612 125.5781 230.0660 0.0886 138.2078 138.1192 125.5133 230.8575 0.0905 138.1714 138.0809 125.4805 231.7100 0.0895 138.1174 138.0279 125.4334 232.4718 0.0905 138.0612 137.9708 125.3940 233.2938 0.0901 138.0317 137.9416 125.3694 234.0860 0.0922 137.9983 137.9061 125.3275 234.8775 0.0939 137.9447 137.8508 125.2902 235.7338 0.0968 137.8907 137.7939 125.2386 236.4775 0.0963 137.8761 137.7797 125.2081 237.3298 0.0978 137.8446 137.7468 125.1497 238.0915 0.0996 137.7908 137.6912 125.1231 238.9138 0.1004 137.7507 137.6503 125.0706 239.7358 0.1016 137.7121 137.6104 125.0377 240.4975 0.1047 137.6708 137.5661 125.0216 241.3495 0.1047 137.6275 137.5228 124.9567 242.1415 0.1059 137.5804 137.4745 124.9220 242.9335 0.1058 137.5500 137.4442 124.8929 243.7555 0.1072 137.5108 137.4036 124.8409 244.5175 0.1076 137.4576 137.3500 124.8105 245.3695 0.1098 137.4330 137.3232 124.7603 246.1615 0.1119 137.3960 137.2842 124.7421 246.9535 0.1120 137.3344 137.2224 124.6960 247.7755 0.1150 137.2915 137.1765 124.6361 248.5675 0.1203 137.2629 137.1426 124.6048 249.3895 0.1188 137.2169 137.0981 124.5524 250.1815 0.1178 137.1820 137.0643 124.5204 250.9743 0.1187 137.1306 137.0118 124.4819 251.7963 0.1163 137.0733 136.9570 124.4283 252.5885 0.1166 137.0305 136.9139 124.4010 253.4113 0.1156 137.0134 136.8978 124.3650 254.2030 0.1167 136.9813 136.8645 124.3255 254.9955 0.1174 136.9363 136.8188 124.2899 255.8180 0.1202 136.8844 136.7642 124.2559 256.5978 0.1206 136.8334 136.7128 124.2065 257.4260 0.1207 136.8018 136.6811 124.1683 258.2178 0.1229 136.7757 136.6528 124.1434 259.0405 0.1243 136.7260 136.6016 124.0945 259.8333 0.1221 136.6886 136.5666 124.0576 260.6245 0.1269 136.6455 136.5186 124.0202 261.4470 0.1299 136.5994 136.4695 123.9823 262.2385 0.1200 136.5592 136.4392 123.9375 263.0608 0.1000 136.5134 136.4134 123.8910 263.8525 0.0693 136.4861 136.4168 123.8748 264.6710 0.0631 136.4494 136.3864 123.8370 265.4900 0.0774 136.4034 136.3260 123.7850 266.2785 0.1041 136.3482 136.2441 123.7324 267.0670 0.1188 136.3158 136.1969 123.6923 267.8858 0.1224 136.2640 136.1416 123.6558 268.6740 0.1188 136.2248 136.1060 123.6133 269.4930 0.1190 136.1719 136.0530 123.5739 270.2815 0.1313 136.1300 135.9987 123.5517 271.0700 0.1449 136.1017 135.9568 123.5098 271.8888 0.1488 136.0587 135.9099 123.4704 272.6773 0.1471 136.0268 135.8797 123.4321 273.4950 0.1468 135.9847 135.8379 123.3929 274.2838 0.1477 135.9290 135.7813 123.3465 275.0730 0.1459 135.8893 135.7433 123.3058 275.9220 0.1466 135.8571 135.7105 123.2729 276.6823 0.1475 135.8087 135.6612 123.2392 277.5008 0.1517 135.7745 135.6227 123.1958 278.3195 0.1522 135.7355 135.5833 123.1610 279.0783 0.1544 135.7007 135.5463 123.1360 279.9278 0.1562 135.6604 135.5042 123.1027 280.6878 0.1566 135.6092 135.4527 123.0530 281.5088 0.1572 135.5852 135.4280 123.0258 282.3285 0.1606 135.5194 135.3588 123.0117 283.0905 0.1584 135.4837 135.3253 122.9913 283.9428 0.1584 135.4498 135.2914 122.9441 284.7048 0.1611 135.4032 135.2420 122.9280 285.5265 0.1645 135.3622 135.1977 122.9032 286.3488 0.1668 135.3236 135.1568 122.8569 287.1105 0.1706 135.2754 135.1048 122.8587 287.9625 0.1659 135.2348 135.0689 122.8541 288.7245 0.1605 135.2027 135.0422 122.8124 289.5465 0.1635 135.1649 135.0014 122.8002 290.3685 0.1617 135.1328 134.9711 122.7945 291.1305 0.1537 135.0785 134.9247 122.7634 291.9825 0.1454 135.0259 134.8805 122.7365 292.7445 0.1445 134.9831 134.8386 122.7384 293.5665 0.1481 134.9432 134.7951 122.7192 294.3885 0.1496 134.9026 134.7530 122.7205 295.1505 0.1643 134.8691 134.7048 122.7317 296.0025 0.1735 134.8357 134.6622 122.7295 296.7645 0.1733 134.8044 134.6311 122.7397 297.5865 0.1748 134.7500 134.5753 122.7544 298.4085 0.1739 134.7012 134.5273 122.7540 299.1705 0.1741 134.6646 134.4905 122.7693 300.0225 0.1741 134.6183 134.4442 122.7788 300.7853 0.1755 134.5774 134.4019 122.7807 301.6078 0.1801 134.5406 134.3605 122.8162 302.4003 0.1791 134.5038 134.3247 122.8367 303.1915 0.1813 134.4547 134.2734 122.8485 304.0445 0.1773 134.4254 134.2480 122.8886 304.8060 0.1789 134.3812 134.2022 122.9004 305.6278 0.1804 134.3509 134.1705 122.9610 306.4500 0.1806 134.3126 134.1320 122.9823 307.2115 0.1769 134.2692 134.0923 123.0220 308.0640 0.1817 134.2318 134.0501 123.0817 308.8258 0.1811 134.1752 133.9941 123.1298 309.6478 0.1769 134.1417 133.9648 123.1827 310.4700 0.1769 134.1131 133.9363 123.2319 311.2315 0.1796 134.0535 133.8739 123.2950 312.0840 0.1769 134.0117 133.8348 123.3521 312.8758 0.1758 133.9897 133.8139 123.4233 313.6675 0.1777 133.9324 133.7547 123.4879 314.4900 0.1834 133.8953 133.7120 123.5744 315.2515 0.1803 133.8550 133.6747 123.6620 316.1040 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