DTA measure 1olom1 Date: 2024102:115 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.17 s Mass = 950.700 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1565 -0.7060 253.2883 253.9943 253.1308 1.9485 -0.7110 253.2923 254.0033 253.1330 2.7405 -0.7071 253.3061 254.0132 253.1085 3.5625 -0.7188 253.2937 254.0125 253.1100 4.3245 -0.6826 253.2995 253.9820 253.1089 5.1765 -0.6599 253.3055 253.9655 253.1146 5.9685 -0.6575 253.3010 253.9585 253.1210 6.7603 -0.6738 253.3187 253.9924 253.1300 7.5825 -0.7496 253.3067 254.0563 253.1174 8.3740 -0.7639 253.3120 254.0759 253.1213 9.1963 -0.7378 253.3197 254.0575 253.1489 9.9883 -0.7628 253.3241 254.0869 253.1585 10.7795 -0.7552 253.3021 254.0573 253.1859 11.6020 -0.7309 253.3287 254.0596 253.1895 12.3938 -0.6994 253.3345 254.0339 253.2025 13.2160 -0.7187 253.3403 254.0590 253.2491 14.0080 -0.7338 253.3247 254.0584 253.2666 14.7995 -0.7621 253.3349 254.0969 253.3083 15.6223 -0.7806 253.3429 254.1234 253.3457 16.4138 -0.7525 253.3240 254.0764 253.3974 17.2358 -0.7040 253.3363 254.0403 253.4494 18.0280 -0.7039 253.3438 254.0476 253.4805 18.8205 -0.7623 253.3314 254.0938 253.5228 19.6430 -0.7788 253.3275 254.1062 253.5985 20.4045 -0.7675 253.3372 254.1047 253.6626 21.2568 -0.7153 253.3462 254.0615 253.7313 22.0488 -0.6591 253.3576 254.0167 253.8116 22.8405 -0.6398 253.3700 254.0098 253.8914 23.6630 -0.6376 253.3568 253.9944 253.9672 24.4255 -0.6354 253.3595 253.9948 254.0563 25.2775 -0.6365 253.3474 253.9838 254.1537 26.0698 -0.6388 253.3679 254.0067 254.2406 26.8615 -0.6403 253.3717 254.0119 254.3584 27.6835 -0.6444 253.3755 254.0199 254.4657 28.4455 -0.6439 253.3853 254.0292 254.5730 29.2975 -0.6400 253.4058 254.0458 254.6968 30.0895 -0.6406 253.3828 254.0234 254.7864 30.8815 -0.6411 253.3635 254.0046 254.9154 31.7038 -0.6440 253.3800 254.0240 255.0426 32.4665 -0.6479 253.4046 254.0525 255.1579 33.3178 -0.6466 253.4060 254.0526 255.3105 34.1040 -0.6511 253.4097 254.0608 255.4358 34.8938 -0.6529 253.4017 254.0546 255.5645 35.6773 -0.6535 253.4244 254.0779 255.7035 36.4960 -0.6561 253.4370 254.0930 255.8374 37.3138 -0.6592 253.4278 254.0870 255.9772 38.0718 -0.6644 253.4269 254.0913 256.1113 38.9198 -0.6673 253.4385 254.1058 256.3074 39.6780 -0.6673 253.4360 254.1033 256.4475 40.5023 -0.6673 253.4438 254.1112 256.5906 41.2915 -0.6688 253.4452 254.1140 256.7616 42.0808 -0.6704 253.4572 254.1276 256.9163 42.9290 -0.6718 253.4750 254.1468 257.0737 43.6870 -0.6731 253.4643 254.1374 257.2158 44.5058 -0.6765 253.4785 254.1551 257.3784 45.2975 -0.6812 253.4956 254.1768 257.5339 46.0908 -0.6812 253.4941 254.1753 257.7076 46.9098 -0.6834 253.5025 254.1859 257.8798 47.6990 -0.6839 253.5143 254.1982 258.0473 48.5175 -0.6887 253.5411 254.2298 258.2068 49.3058 -0.6879 253.5519 254.2398 258.3586 50.0958 -0.6932 253.5517 254.2449 258.4997 50.9448 -0.6939 253.5611 254.2550 258.6562 51.7040 -0.6985 253.5707 254.2692 258.8238 52.5248 -0.7010 253.5911 254.2921 258.9962 53.3165 -0.7072 253.5973 254.3045 259.1440 54.1080 -0.7114 253.6123 254.3237 259.2998 54.9603 -0.7130 253.6336 254.3466 259.4579 55.7223 -0.7173 253.6445 254.3618 259.6021 56.5438 -0.7205 253.6477 254.3682 259.7750 57.3360 -0.7259 253.6553 254.3811 259.9188 58.1275 -0.7273 253.6595 254.3868 260.0631 58.9500 -0.7297 253.6910 254.4206 260.2241 59.7418 -0.7296 253.6901 254.4197 260.3620 60.5648 -0.7354 253.7191 254.4545 260.5220 61.3570 -0.7376 253.7443 254.4819 260.6785 62.1485 -0.7420 253.7465 254.4884 260.8217 62.9710 -0.7453 253.7803 254.5256 260.9649 63.7325 -0.7479 253.7856 254.5335 261.1138 64.5850 -0.7530 253.8042 254.5571 261.2457 65.3770 -0.7576 253.8080 254.5656 261.3696 66.1685 -0.7641 253.8327 254.5968 261.5027 66.9910 -0.7680 253.8516 254.6196 261.6238 67.7525 -0.7704 253.8767 254.6470 261.7410 68.6050 -0.7766 253.9053 254.6819 261.8885 69.3968 -0.7754 253.9159 254.6912 262.0142 70.1885 -0.7742 253.9312 254.7054 262.1371 71.0110 -0.7801 253.9397 254.7198 262.2659 71.7725 -0.7819 253.9636 254.7455 262.3834 72.6245 -0.7833 253.9951 254.7784 262.5283 73.4165 -0.7828 254.0172 254.8000 262.6305 74.2085 -0.7859 254.0418 254.8277 262.7527 75.0305 -0.7858 254.0513 254.8371 262.8723 75.8225 -0.7934 254.0499 254.8433 263.0061 76.6445 -0.7975 254.0888 254.8864 263.1439 77.4365 -0.7980 254.1274 254.9254 263.2659 78.2285 -0.8024 254.1597 254.9622 263.3547 79.0505 -0.8068 254.1674 254.9742 263.4648 79.8425 -0.8098 254.1738 254.9836 263.5857 80.6645 -0.8123 254.2114 255.0237 263.6969 81.4565 -0.8175 254.2548 255.0722 263.7971 82.2485 -0.8205 254.2692 255.0897 263.9282 83.0705 -0.8217 254.2920 255.1137 264.0235 83.8625 -0.8239 254.3130 255.1369 264.1154 84.6848 -0.8248 254.3461 255.1709 264.2269 85.4775 -0.8310 254.3673 255.1983 264.3503 86.2693 -0.8343 254.3846 255.2189 264.4432 87.0963 -0.8404 254.4058 255.2462 264.5382 87.8888 -0.8429 254.4488 255.2917 264.6484 88.7108 -0.8428 254.4661 255.3088 264.7779 89.5030 -0.8458 254.5043 255.3500 264.8806 90.2955 -0.8499 254.5206 255.3705 264.9870 91.1180 -0.8536 254.5457 255.3992 265.1041 91.9098 -0.8570 254.5860 255.4430 265.1998 92.7318 -0.8577 254.6041 255.4618 265.3032 93.5240 -0.8605 254.6385 255.4990 265.4389 94.3155 -0.8590 254.6579 255.5169 265.5372 95.1680 -0.8619 254.6787 255.5406 265.6446 95.9298 -0.8674 254.7397 255.6071 265.7547 96.7518 -0.8705 254.7648 255.6353 265.8784 97.5438 -0.8748 254.7993 255.6740 265.9815 98.3348 -0.8790 254.8262 255.7052 266.1100 99.1830 -0.8732 254.8507 255.7239 266.2304 99.9410 -0.8710 254.8838 255.7548 266.3465 100.7590 -0.8591 254.9251 255.7841 266.4530 101.5473 -0.8358 254.9660 255.8018 266.5776 102.3350 -0.7979 254.9971 255.7950 266.6915 103.1530 -0.8220 255.0133 255.8354 266.8149 103.9410 -0.8565 255.0626 255.9191 266.9434 104.7590 -0.8723 255.0799 255.9522 267.0749 105.5470 -0.8827 255.0977 255.9804 267.1927 106.3355 -0.8920 255.1352 256.0271 267.3104 107.1545 -0.8927 255.1824 256.0751 267.4266 107.9430 -0.8971 255.2155 256.1126 267.5563 108.7618 -0.9040 255.2447 256.1488 267.6788 109.5505 -0.9065 255.2865 256.1931 267.8090 110.3400 -0.9050 255.3318 256.2368 267.9231 111.1885 -0.9071 255.3463 256.2534 268.0525 111.9473 -0.9120 255.3878 256.2998 268.1867 112.7673 -0.9189 255.4216 256.3405 268.3105 113.5575 -0.9229 255.4640 256.3870 268.4272 114.3475 -0.9253 255.4828 256.4081 268.5788 115.1978 -0.9222 255.5438 256.4660 268.7121 115.9598 -0.9274 255.5939 256.5214 268.8381 116.7818 -0.9267 255.6242 256.5509 268.9710 117.5733 -0.9353 255.6790 256.6144 269.0899 118.3645 -0.9418 255.7096 256.6514 269.1971 119.2165 -0.9403 255.7438 256.6840 269.3194 119.9785 -0.9449 255.7761 256.7209 269.4392 120.8008 -0.9499 255.8178 256.7677 269.5673 121.5928 -0.9555 255.8556 256.8111 269.6811 122.3845 -0.9589 255.9077 256.8666 269.8331 123.2065 -0.9662 255.9451 256.9113 269.9528 123.9985 -0.9707 255.9842 256.9549 270.0655 124.8205 -0.9660 256.0424 257.0084 270.2159 125.6125 -0.9654 256.0771 257.0424 270.3308 126.4045 -0.9699 256.1102 257.0802 270.4813 127.2265 -0.9714 256.1542 257.1257 270.6069 127.9885 -0.9734 256.2059 257.1794 270.7381 128.8405 -0.9795 256.2474 257.2269 270.8799 129.6325 -0.9870 256.2837 257.2707 271.0131 130.4245 -0.9919 256.3355 257.3273 271.1208 131.2465 -0.9988 256.3712 257.3701 271.2663 132.0085 -0.9995 256.4064 257.4059 271.3893 132.8605 -1.0022 256.4530 257.4552 271.5220 133.6225 -1.0062 256.5017 257.5079 271.6735 134.4445 -1.0125 256.5508 257.5633 271.8236 135.2665 -1.0130 256.6002 257.6132 271.9502 136.0283 -1.0186 256.6571 257.6757 272.0882 136.8803 -1.0192 256.7002 257.7194 272.2411 137.6423 -1.0218 256.7427 257.7645 272.3809 138.4640 -1.0228 256.7970 257.8198 272.5013 139.2860 -1.0241 256.8489 257.8730 272.6388 140.0475 -1.0297 256.8837 257.9135 272.7629 140.9000 -1.0355 256.9429 257.9784 272.9116 141.6618 -1.0399 256.9821 258.0220 273.0341 142.4838 -1.0417 257.0388 258.0805 273.1749 143.2760 -1.0413 257.0811 258.1225 273.3198 144.0675 -1.0440 257.1390 258.1830 273.4635 144.9200 -1.0518 257.1944 258.2462 273.5947 145.6818 -1.0534 257.2293 258.2828 273.7249 146.5038 -1.0587 257.2777 258.3365 273.8886 147.2960 -1.0608 257.3384 258.3992 273.9928 148.0880 -1.0616 257.4006 258.4622 274.1227 148.9408 -1.0577 257.4461 258.5038 274.2663 149.7025 -1.0490 257.4922 258.5412 274.3970 150.5248 -1.0485 257.5450 258.5935 274.5404 151.3168 -1.0545 257.5852 258.6397 274.6501 152.1085 -1.0564 257.6565 258.7128 274.8052 152.9613 -1.0620 257.7157 258.7777 274.9416 153.7235 -1.0630 257.7667 258.8297 275.0626 154.5455 -1.0646 257.8234 258.8880 275.2076 155.3378 -1.0685 257.8846 258.9531 275.3315 156.1295 -1.0698 257.9109 258.9808 275.4610 156.9815 -1.0759 257.9988 259.0746 275.6155 157.7435 -1.0771 258.0404 259.1175 275.7357 158.5655 -1.0784 258.0934 259.1719 275.8645 159.3575 -1.0829 258.1553 259.2382 275.9923 160.1495 -1.0906 258.1916 259.2821 276.1153 161.0015 -1.0878 258.2803 259.3681 276.2694 161.7635 -1.0896 258.3371 259.4267 276.3753 162.5835 -1.0914 258.3964 259.4878 276.5234 163.3700 -1.0958 258.4521 259.5479 276.6360 164.1600 -1.1031 258.5171 259.6202 276.7784 164.9773 -1.1020 258.5640 259.6661 276.9018 165.7660 -1.1046 258.6166 259.7212 277.0150 166.5835 -1.1050 258.6818 259.7868 277.1533 167.3720 -1.1076 258.7497 259.8573 277.2830 168.1593 -1.1080 258.8298 259.9378 277.4186 169.0080 -1.1109 258.8841 259.9950 277.5398 169.7660 -1.1162 258.9199 260.0361 277.6587 170.5843 -1.1204 258.9861 260.1065 277.7647 171.3730 -1.1249 259.0380 260.1630 277.9041 172.1603 -1.1323 259.1204 260.2527 278.0381 173.0098 -1.1374 259.1730 260.3103 278.1636 173.7690 -1.1388 259.2211 260.3599 278.2681 174.5875 -1.1396 259.2762 260.4158 278.3979 175.4063 -1.1381 259.3483 260.4864 278.5289 176.1645 -1.1429 259.4245 260.5674 278.6445 177.0130 -1.1446 259.4965 260.6410 278.7625 177.8023 -1.1473 259.5470 260.6943 278.8904 178.5923 -1.1495 259.5978 260.7474 279.0373 179.4118 -1.1526 259.6823 260.8349 279.1292 180.2020 -1.1545 259.7575 260.9120 279.2425 181.0230 -1.1560 259.8250 260.9810 279.3771 181.8150 -1.1595 259.8681 261.0275 279.4791 182.6063 -1.1614 259.9133 261.0747 279.6190 183.4283 -1.1644 260.0088 261.1732 279.7328 184.1898 -1.1646 260.0694 261.2340 279.8409 185.0418 -1.1666 260.1521 261.3187 279.9416 185.8330 -1.1690 260.2022 261.3711 280.0635 186.6245 -1.1750 260.3010 261.4759 280.1768 187.4470 -1.1758 260.3503 261.5261 280.3191 188.2085 -1.1769 260.3874 261.5642 280.4434 189.0610 -1.1786 260.4635 261.6421 280.5514 189.8530 -1.1792 260.5398 261.7191 280.6703 190.6445 -1.1854 260.6002 261.7856 280.8006 191.4670 -1.1849 260.6803 261.8652 280.9247 192.2285 -1.1878 260.7533 261.9411 281.0650 193.0810 -1.1897 260.8174 262.0070 281.1765 193.8730 -1.1919 260.8858 262.0778 281.2882 194.6645 -1.1963 260.9490 262.1453 281.3941 195.4868 -1.1982 261.0380 262.2362 281.5240 196.2485 -1.1998 261.0852 262.2850 281.6664 197.1010 -1.2025 261.1789 262.3814 281.7911 197.8928 -1.2027 261.2574 262.4601 281.8957 198.6845 -1.2047 261.3075 262.5121 282.0330 199.5068 -1.2090 261.3813 262.5903 282.1743 200.2985 -1.2104 261.4568 262.6672 282.3015 201.1205 -1.2085 261.5107 262.7192 282.4207 201.9125 -1.2112 261.6119 262.8230 282.5393 202.7045 -1.2170 261.6654 262.8825 282.6704 203.5265 -1.2168 261.7453 262.9621 282.7961 204.3185 -1.2203 261.8255 263.0457 282.9248 205.1405 -1.2237 261.9012 263.1250 283.0552 205.9325 -1.2255 261.9646 263.1901 283.1790 206.7245 -1.2311 262.0462 263.2773 283.3099 207.5765 -1.2335 262.1091 263.3426 283.4510 208.3385 -1.2369 262.1863 263.4232 283.5536 209.1605 -1.2376 262.2593 263.4969 283.6857 209.9525 -1.2368 262.3522 263.5889 283.8198 210.7445 -1.2397 262.4267 263.6664 283.9361 211.5965 -1.2382 262.4850 263.7232 284.0567 212.3585 -1.2430 262.5590 263.8021 284.2044 213.1800 -1.2444 262.6265 263.8709 284.3217 213.9725 -1.2510 262.7168 263.9677 284.4518 214.7645 -1.2519 262.7586 264.0105 284.5842 215.6160 -1.2537 262.8574 264.1111 284.7030 216.3778 -1.2566 262.9322 264.1888 284.8194 217.1998 -1.2586 263.0206 264.2792 284.9584 218.0223 -1.2584 263.1032 264.3616 285.0828 218.7845 -1.2617 263.1923 264.4540 285.2036 219.6370 -1.2684 263.2669 264.5352 285.3473 220.3988 -1.2697 263.3270 264.5967 285.4664 221.2208 -1.2771 263.4090 264.6861 285.5776 222.0430 -1.2782 263.4931 264.7713 285.7167 222.8045 -1.2801 263.5549 264.8349 285.8201 223.6570 -1.2820 263.6322 264.9142 285.9389 224.4185 -1.2846 263.7234 265.0080 286.0744 225.2445 -1.2847 263.8154 265.1001 286.2169 226.0675 -1.2853 263.8788 265.1641 286.3561 226.8260 -1.2906 263.9502 265.2408 286.4871 227.6740 -1.2943 264.0399 265.3342 286.6257 228.4320 -1.2965 264.1244 265.4209 286.7422 229.2500 -1.3021 264.2000 265.5021 286.8782 230.0380 -1.3012 264.2931 265.5943 287.0094 230.8260 -1.3012 264.3795 265.6807 287.1401 231.6448 -1.3087 264.4448 265.7535 287.2663 232.4330 -1.3078 264.5359 265.8437 287.4006 233.2510 -1.3082 264.6247 265.9329 287.5431 234.0398 -1.3143 264.7115 266.0259 287.6698 234.8290 -1.3185 264.7811 266.0997 287.8052 235.6478 -1.3179 264.8635 266.1814 287.9465 236.4360 -1.3172 264.9366 266.2538 288.1015 237.2548 -1.3237 265.0098 266.3334 288.2513 238.0435 -1.3247 265.1027 266.4274 288.3724 238.8333 -1.3271 265.1823 266.5094 288.5064 239.6530 -1.3311 265.3000 266.6312 288.6596 240.4423 -1.3313 265.3754 266.7068 288.7933 241.2623 -1.3337 265.4475 266.7812 288.9426 242.0523 -1.3380 265.5345 266.8724 289.0647 242.8435 -1.3419 265.6161 266.9580 289.1790 243.6658 -1.3443 265.7006 267.0449 289.3385 244.4275 -1.3468 265.7829 267.1297 289.4696 245.2795 -1.3505 265.8755 267.2260 289.6062 246.0708 -1.3559 265.9571 267.3130 289.7560 246.8625 -1.3579 266.0403 267.3982 289.8983 247.6845 -1.3574 266.1351 267.4925 290.0386 248.4465 -1.3613 266.2210 267.5823 290.1697 249.2985 -1.3622 266.2959 267.6582 290.3152 250.0605 -1.3604 266.3801 267.7405 290.4417 250.8825 -1.3572 266.4683 267.8255 290.5674 251.6748 -1.3602 266.5697 267.9299 290.7007 252.4665 -1.3676 266.6490 268.0166 290.8311 253.3185 -1.3703 266.7430 268.1133 290.9569 254.0805 -1.3748 266.8217 268.1965 291.0960 254.9035 -1.3720 266.9067 268.2787 291.2342 255.6955 -1.3733 266.9978 268.3711 291.3650 256.4875 -1.3762 267.1215 268.4976 291.5197 257.3095 -1.3782 267.1918 268.5700 291.6575 258.1015 -1.3842 267.2538 268.6379 291.7817 258.9235 -1.3863 267.3658 268.7521 291.9203 259.7155 -1.3860 267.4549 268.8409 292.0443 260.5075 -1.3841 267.5445 268.9286 292.1763 261.3295 -1.3923 267.6257 269.0179 292.3164 262.1215 -1.4000 267.7353 269.1353 292.4700 262.9430 -1.4019 267.8270 269.2289 292.5897 263.7353 -1.4042 267.9027 269.3069 292.7328 264.5268 -1.4056 267.9998 269.4054 292.8555 265.3493 -1.4089 268.1056 269.5145 292.9951 266.1408 -1.4101 268.1963 269.6064 293.1421 266.9628 -1.4128 268.2878 269.7005 293.2596 267.7550 -1.4174 268.3872 269.8046 293.4005 268.5465 -1.4183 268.4737 269.8920 293.5182 269.3690 -1.4218 268.5693 269.9912 293.6489 270.1608 -1.4245 268.6430 270.0675 293.7744 270.9828 -1.4277 268.7635 270.1912 293.9139 271.7750 -1.4289 268.8570 270.2859 294.0300 272.5665 -1.4313 268.9196 270.3509 294.1557 273.3890 -1.4365 269.0277 270.4642 294.3034 274.1808 -1.4363 269.1070 270.5433 294.4300 275.0028 -1.4370 269.2225 270.6595 294.5764 275.7948 -1.4414 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