DTA measure 3olom1 Date: 2024102:1135 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.13 s Mass = 950.700 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3495 -3.5651 406.9155 410.4806 409.4662 3.9635 -3.5638 406.9760 410.5398 409.4953 5.5625 -3.5612 407.0487 410.6099 409.5045 7.1915 -3.5600 407.0955 410.6556 409.4797 8.7905 -3.5593 407.1713 410.7307 409.4597 10.3894 -3.5585 407.2237 410.7822 409.3993 12.0039 -3.5603 407.2922 410.8525 409.3518 13.6030 -3.5586 407.3476 410.9062 409.2559 15.2320 -3.5543 407.3961 410.9505 409.1354 16.8318 -3.5542 407.4616 411.0158 409.0143 18.4308 -3.5518 407.5241 411.0759 408.8757 20.0426 -3.5445 407.5860 411.1305 408.6987 21.6340 -3.5397 407.6194 411.1592 408.5347 23.2545 -3.5398 407.6724 411.2122 408.3363 24.8461 -3.5341 407.7177 411.2518 408.1424 26.4371 -3.5297 407.7552 411.2849 407.9566 28.0280 -3.5259 407.7988 411.3247 407.7464 29.6341 -3.5214 407.8584 411.3798 407.4995 31.2563 -3.5131 407.9009 411.4139 407.2558 32.8491 -3.5086 407.9236 411.4322 407.0269 34.4565 -3.5001 407.9634 411.4635 406.7699 36.0488 -3.4958 407.9965 411.4924 406.5100 37.6598 -3.4884 408.0319 411.5202 406.2583 39.2734 -3.4759 408.0634 411.5394 406.0172 40.8716 -3.4709 408.0765 411.5474 405.7780 42.4708 -3.4600 408.0970 411.5571 405.5176 44.0696 -3.4557 408.1201 411.5758 405.2707 45.6686 -3.4497 408.1489 411.5986 405.0590 47.2975 -3.4396 408.1719 411.6115 404.8111 48.8966 -3.4302 408.1855 411.6157 404.5776 50.4955 -3.4255 408.1842 411.6098 404.3671 52.1095 -3.4161 408.1949 411.6109 404.1365 53.7085 -3.4081 408.2055 411.6136 403.9151 55.3225 -3.4012 408.1971 411.5983 403.7038 56.9365 -3.3919 408.1986 411.5904 403.4674 58.5355 -3.3843 408.2205 411.6048 403.2608 60.1495 -3.3736 408.2348 411.6083 403.0415 61.7484 -3.3622 408.2262 411.5884 402.8722 63.3620 -3.3531 408.2118 411.5649 402.6633 64.9759 -3.3427 408.2016 411.5444 402.4666 66.5748 -3.3389 408.2058 411.5447 402.2634 68.1888 -3.3321 408.1738 411.5059 402.0824 69.7878 -3.3228 408.1851 411.5080 401.9191 71.4019 -3.3144 408.1671 411.4815 401.7277 73.0159 -3.3074 408.1485 411.4559 401.5320 74.6296 -3.3014 408.1187 411.4201 401.3496 76.2286 -3.2950 408.1006 411.3956 401.1567 77.8276 -3.2867 408.0860 411.3727 401.0071 79.4574 -3.2797 408.0596 411.3392 400.8202 81.0565 -3.2729 408.0344 411.3073 400.6618 82.7130 -3.2750 407.9999 411.2749 400.4981 84.4073 -3.2574 407.9869 411.2443 400.3188 85.9976 -3.2392 407.9519 411.1911 400.1343 87.5890 -3.2447 407.9191 411.1638 399.9584 89.1965 -3.2388 407.8871 411.1259 399.7848 90.8031 -3.2336 407.8540 411.0876 399.6142 92.4100 -3.2241 407.8049 411.0290 399.4323 94.0079 -3.2205 407.7706 410.9911 399.2661 95.6020 -3.2159 407.7116 410.9276 399.0846 97.1959 -3.2113 407.6723 410.8836 398.8996 98.8209 -3.2040 407.6428 410.8468 398.7289 100.4170 -3.1963 407.6009 410.7972 398.5152 102.0141 -3.1888 407.5501 410.7388 398.3121 103.6269 -3.1949 407.5093 410.7042 398.1212 105.2245 -3.1866 407.4471 410.6337 397.9325 106.8235 -3.2185 407.3854 410.6039 397.7389 108.4684 -3.2294 407.3399 410.5694 397.5322 110.2071 -3.2182 407.2746 410.4928 397.3189 111.8059 -3.2127 407.2174 410.4300 397.1162 113.4050 -3.1680 407.1571 410.3252 396.9094 115.0340 -3.1378 407.1049 410.2427 396.7040 116.6328 -3.1339 407.0396 410.1735 396.5258 118.2318 -3.1266 406.9626 410.0892 396.3337 119.8458 -3.1190 406.9074 410.0264 396.1335 121.4454 -3.1127 406.8407 409.9533 395.9304 123.0599 -3.1072 406.7795 409.8867 395.7411 124.6738 -3.1003 406.7007 409.8010 395.5693 126.2729 -3.0935 406.6234 409.7169 395.3667 127.8726 -3.0897 406.5601 409.6498 395.1655 129.4866 -3.0996 406.4879 409.5875 394.9789 131.1005 -3.1358 406.4162 409.5520 394.7924 132.7145 -3.1206 406.3364 409.4569 394.5855 134.3135 -3.0822 406.2806 409.3628 394.4086 135.9125 -3.0554 406.1986 409.2540 394.2143 137.5265 -3.0452 406.1119 409.1572 394.0089 139.1405 -3.0428 406.0322 409.0750 393.7993 140.7394 -3.0374 405.9408 408.9781 393.6043 142.3528 -3.0299 405.8548 408.8847 393.3970 143.9518 -3.0219 405.7633 408.7852 393.2301 145.5508 -3.0197 405.6674 408.6871 393.0221 147.1798 -3.0169 405.5667 408.5836 392.8140 148.7730 -3.0056 405.4802 408.4858 392.6234 150.3791 -2.9975 405.4085 408.4060 392.4323 151.9701 -2.9929 405.3211 408.3140 392.2409 153.5611 -2.9865 405.2121 408.1986 392.0422 155.1823 -2.9782 405.1150 408.0932 391.8411 156.7743 -2.9735 405.0328 408.0063 391.6401 158.3815 -2.9692 404.9422 407.9114 391.4594 159.9736 -2.9603 404.8363 407.7966 391.2519 161.5813 -2.9565 404.7424 407.6989 391.0539 163.2056 -2.9519 404.6617 407.6135 390.8576 164.8011 -2.9444 404.5380 407.4824 390.6550 166.3989 -2.9385 404.4535 407.3920 390.4493 167.9978 -2.9338 404.3395 407.2734 390.2453 169.6115 -2.9300 404.2272 407.1572 390.0386 171.2256 -2.9240 404.1090 407.0330 389.8334 172.8398 -2.9197 404.0196 406.9393 389.6220 174.4385 -2.9158 403.9140 406.8298 389.4157 176.0378 -2.9115 403.8061 406.7176 389.2066 177.6515 -2.8982 403.6870 406.5852 389.0008 179.2655 -2.8926 403.5859 406.4785 388.7974 180.8795 -2.8863 403.4716 406.3579 388.5983 182.4785 -2.8796 403.3517 406.2314 388.3941 184.0925 -2.8746 403.2391 406.1137 388.1972 185.6915 -2.8682 403.1156 405.9838 388.0094 187.3205 -2.8615 402.9909 405.8524 387.8070 188.9195 -2.8578 402.8895 405.7473 387.6060 190.5190 -2.8713 402.7672 405.6384 387.3965 192.1330 -2.8695 402.6572 405.5267 387.2162 193.7469 -2.8629 402.5293 405.3922 387.0191 195.3611 -2.8540 402.4058 405.2599 386.8042 196.9608 -2.8672 402.2760 405.1432 386.6258 198.5748 -2.9519 402.1498 405.1017 386.4420 200.1738 -2.9883 402.0477 405.0359 386.2517 201.7884 -2.8597 401.9106 404.7703 386.0538 203.4028 -2.8200 401.8002 404.6202 385.8725 205.0166 -2.8220 401.6593 404.4813 385.6786 206.6191 -2.7983 401.5387 404.3370 385.4687 208.2195 -2.7962 401.3967 404.1929 385.2581 209.8335 -2.7784 401.2707 404.0491 385.0669 211.4484 -2.7686 401.1306 403.8992 384.8653 213.0443 -2.7545 401.0080 403.7625 384.6563 214.6515 -2.7459 400.8804 403.6263 384.4682 216.2428 -2.7396 400.7447 403.4842 384.2554 217.8346 -2.7361 400.6212 403.3573 384.0398 219.4578 -2.7306 400.4908 403.2214 383.8427 221.0490 -2.7200 400.3560 403.0760 383.6484 222.6404 -2.7188 400.2263 402.9450 383.4449 224.2483 -2.7157 400.0880 402.8037 383.2485 225.8414 -2.7056 399.9405 402.6461 383.0516 227.4640 -2.6867 399.7961 402.4828 382.8420 229.0594 -2.6926 399.6689 402.3615 382.6526 230.6541 -2.6874 399.5244 402.2118 382.4609 232.2675 -2.6833 399.3889 402.0722 382.2780 233.8658 -2.6767 399.2506 401.9273 382.0739 235.4795 -2.6729 399.0966 401.7695 381.8634 237.0934 -2.6684 398.9579 401.6262 381.6670 238.6920 -2.6591 398.8181 401.4772 381.4634 240.2909 -2.6574 398.6815 401.3389 381.2524 241.8898 -2.6537 398.5435 401.1972 381.0660 243.5189 -2.6484 398.4105 401.0588 380.8601 245.1180 -2.6402 398.2528 400.8930 380.6463 246.7168 -2.6358 398.0949 400.7308 380.4383 248.3308 -2.6311 397.9573 400.5884 380.2363 249.9296 -2.6277 397.8336 400.4613 380.0471 251.5436 -2.6218 397.6696 400.2914 379.8336 253.1578 -2.6169 397.5205 400.1374 379.6456 254.7566 -2.6081 397.3834 399.9916 379.4262 256.3555 -2.6027 397.2272 399.8300 379.2158 257.9695 -2.5990 397.0624 399.6615 379.0084 259.5685 -2.5932 396.9186 399.5118 378.8099 261.1975 -2.5883 396.7644 399.3528 378.5865 262.7965 -2.5864 396.6139 399.2004 378.3877 264.3955 -2.5814 396.4509 399.0323 378.1813 266.0095 -2.5757 396.3015 398.8771 377.9915 267.6234 -2.5714 396.1516 398.7230 377.7876 269.2373 -2.5697 395.9976 398.5672 377.5842 270.8358 -2.5620 395.8491 398.4111 377.3789 272.4498 -2.5533 395.6993 398.2526 377.1769 274.0493 -2.5502 395.5254 398.0756 376.9828 275.6639 -2.5452 395.3677 397.9129 376.7723 277.2743 -2.5369 395.1994 397.7363 376.5945 278.8800 -2.5337 395.0614 397.5951 376.3847 280.4711 -2.5287 394.9106 397.4393 376.1942 282.0621 -2.5234 394.7395 397.2629 376.0167 283.6831 -2.5205 394.5889 397.1094 375.7991 285.2914 -2.5154 394.4170 396.9324 375.6050 286.8835 -2.5101 394.2716 396.7818 375.4043 288.4910 -2.5036 394.1115 396.6151 375.2102 290.0844 -2.4975 393.9541 396.4516 375.0135 291.7099 -2.4924 393.7877 396.2801 374.8150 293.3061 -2.4876 393.6210 396.1085 374.5961 294.9183 -2.4830 393.4657 395.9487 374.3786 296.5156 -2.4797 393.3073 395.7869 374.1821 298.1295 -2.4720 393.1411 395.6130 373.9862 299.7436 -2.4640 392.9774 395.4414 373.7861 301.3425 -2.4605 392.8175 395.2780 373.5807 302.9421 -2.4592 392.6346 395.0938 373.3630 304.5565 -2.4530 392.4843 394.9372 373.1797 306.1555 -2.4469 392.3188 394.7657 372.9508 307.7845 -2.4429 392.1526 394.5955 372.7509 309.3835 -2.4365 391.9801 394.4166 372.5569 310.9825 -2.4335 391.8266 394.2601 372.3495 312.5965 -2.4269 391.6589 394.0858 372.1541 314.1955 -2.4237 391.4859 393.9096 371.9414 315.8245 -2.4197 391.3124 393.7321 371.7434 317.4233 -2.4165 391.1587 393.5752 371.5445 319.0370 -2.4085 390.9696 393.3781 371.3646 320.6360 -2.4055 390.7970 393.2025 371.1521 322.2354 -2.3977 390.6336 393.0313 370.9635 323.8650 -2.3939 390.4636 392.8575 370.7442 325.4638 -2.3934 390.3082 392.7016 370.5699 327.0628 -2.3861 390.1322 392.5183 370.3583 328.6768 -2.3799 389.9734 392.3533 370.1824 330.2775 -2.3781 389.7999 392.1780 369.9924 331.8916 -2.3742 389.6210 391.9951 369.8089 333.5059 -2.3690 389.4408 391.8098 369.6093 335.1059 -2.3666 389.2613 391.6279 369.4008 336.7055 -2.3608 389.1089 391.4697 369.2012 338.3195 -2.3564 388.9292 391.2856 369.0043 339.9385 -2.3499 388.7596 391.1095 368.8071 341.5326 -2.3461 388.5945 390.9406 368.5973 343.1233 -2.3408 388.4303 390.7711 368.3919 344.7300 -2.3318 388.2512 390.5830 368.1980 346.3210 -2.3316 388.0976 390.4292 367.9802 347.9269 -2.3271 387.9115 390.2386 367.7671 349.5338 -2.3193 387.7201 390.0394 367.5667 351.1413 -2.3181 387.5745 389.8926 367.3681 352.7341 -2.3175 387.3877 389.7052 367.1658 354.3275 -2.3121 387.2222 389.5343 366.9512 355.9519 -2.3039 387.0524 389.3563 366.7552 357.5495 -2.3012 386.8707 389.1719 366.5549 359.1499 -2.2980 386.6825 388.9805 366.3500 360.7535 -2.2927 386.5143 388.8070 366.1443 362.3525 -2.2896 386.3399 388.6295 365.9417 363.9666 -2.2845 386.1562 388.4407 365.7359 365.5814 -2.2804 385.9872 388.2676 365.5362 367.1800 -2.2745 385.8027 388.0772 365.3232 368.7938 -2.2703 385.6283 387.8986 365.1434 370.3928 -2.2681 385.4456 387.7136 364.9344 371.9918 -2.2599 385.2862 387.5461 364.7449 373.6209 -2.2557 385.0956 387.3513 364.5277 375.2199 -2.2515 384.9263 387.1777 364.3461 376.8338 -2.2493 384.7311 386.9804 364.1446 378.4326 -2.2424 384.5625 386.8049 363.9365 380.0316 -2.2380 384.3971 386.6351 363.7573 381.6609 -2.2320 384.2041 386.4361 363.5582 383.2596 -2.2277 384.0262 386.2539 363.3411 384.8735 -2.2230 383.8635 386.0865 363.1258 386.4725 -2.2197 383.6671 385.8868 362.9253 388.0865 -2.2171 383.4795 385.6966 362.7214 389.7014 -2.2105 383.3023 385.5128 362.5052 391.3164 -2.2070 383.1226 385.3296 362.3017 392.9155 -2.2037 382.9605 385.1643 362.0942 394.5144 -2.1958 382.7690 384.9648 361.8933 396.1285 -2.1919 382.5881 384.7800 361.6803 397.7570 -2.1892 382.4150 384.6043 361.4569 399.3558 -2.1833 382.2266 384.4100 361.2432 400.9558 -2.1781 382.0517 384.2297 361.0339 402.5708 -2.1752 381.8730 384.0482 360.8374 404.1696 -2.1745 381.6780 383.8525 360.6133 405.7918 -2.1680 381.4872 383.6552 360.3906 407.3831 -2.1632 381.3175 383.4807 360.1899 408.9740 -2.1602 381.1394 383.2996 359.9789 410.5808 -2.1538 380.9589 383.1127 359.7869 412.1873 -2.1533 380.7641 382.9173 359.5720 413.7950 -2.1484 380.5722 382.7206 359.3670 415.3873 -2.1425 380.3887 382.5312 359.1661 416.9948 -2.1374 380.2231 382.3606 358.9455 418.5890 -2.1320 380.0254 382.1574 358.7615 420.2164 -2.1272 379.8415 381.9687 358.5506 421.8124 -2.1237 379.6735 381.7972 358.3421 423.4116 -2.1173 379.4808 381.5980 358.1470 425.0139 -2.1152 379.3033 381.4185 357.9462 426.6288 -2.1108 379.1095 381.2202 357.7451 428.2276 -2.1061 378.9312 381.0373 357.5356 429.8566 -2.0990 378.7487 380.8477 357.3334 431.4555 -2.0957 378.5470 380.6427 357.1410 433.0546 -2.0938 378.3796 380.4735 356.9510 434.6686 -2.0894 378.1771 380.2666 356.7581 436.2675 -2.0866 377.9987 380.0853 356.5554 437.8815 -2.0815 377.7917 379.8732 356.3650 439.4955 -2.0762 377.6287 379.7049 356.1706 441.0969 -2.0733 377.4449 379.5181 355.9615 442.7025 -2.0683 377.2371 379.3054 355.7551 444.3015 -2.0676 377.0555 379.1231 355.5672 445.9300 -2.0635 376.8665 378.9300 355.3516 447.5294 -2.0595 376.6887 378.7482 355.1607 449.1428 -2.0516 376.5023 378.5540 354.9403 450.7418 -2.0470 376.3082 378.3552 354.7463 452.3408 -2.0428 376.1256 378.1683 354.5252 453.9706 -2.0398 375.9410 377.9808 354.3217 455.5699 -2.0361 375.7412 377.7773 354.1131 457.1838 -2.0329 375.5583 377.5912 353.9235 458.7830 -2.0275 375.3802 377.4077 353.6956 460.3983 -2.0235 375.1854 377.2089 353.4703 462.0125 -2.0197 374.9841 377.0038 353.2810 463.6268 -2.0149 374.7949 376.8098 353.0759 465.2268 -2.0106 374.6247 376.6353 352.8680 466.8269 -2.0054 374.4513 376.4567 352.6574 468.4421 -1.9983 374.2422 376.2405 352.4689 470.0529 -1.9933 374.0526 376.0459 352.2412 471.6598 -1.9905 373.8704 375.8610 352.0535 473.2511 -1.9838 373.6861 375.6699 351.8469 474.8430 -1.9785 373.4836 375.4621 351.6460 476.4490 -1.9778 373.2926 375.2704 351.4291 478.0550 -1.9686 373.1134 375.0820 351.2343 479.6610 -1.9682 372.9327 374.9009 351.0320 481.2546 -1.9670 372.7528 374.7198 350.8338 482.8643 -1.9606 372.5514 374.5120 350.6325 484.4600 -1.9595 372.3635 374.3230 350.4406 486.0863 -1.9545 372.1632 374.1177 350.2250 487.6808 -1.9494 371.9825 373.9319 350.0280 489.2784 -1.9438 371.7965 373.7404 349.8249 490.8911 -1.9431 371.5946 373.5377 349.6523 492.4900 -1.9408 371.4116 373.3524 349.4457 494.1039 -1.9366 371.2108 373.1474 349.2483 495.7179 -1.9294 371.0390 372.9684 349.0420 497.3168 -1.9239 370.8474 372.7713 348.8423 498.9158 -1.9230 370.6560 372.5790 348.6507 500.5298 -1.9161 370.4460 372.3622 348.4511 502.1439 -1.9131 370.2621 372.1752 348.2568 503.7480 -1.9098 370.0816 371.9915 348.0673 505.3618 -1.9064 369.8781 371.7846 347.8426 506.9608 -1.9028 369.6870 371.5897 347.6489 508.5598 -1.8990 369.4951 371.3942 347.4324 510.1886 -1.8923 369.3154 371.2077 347.2407 511.8026 -1.8891 369.1221 371.0112 347.0304 513.4015 -1.8875 368.9345 370.8220 346.8148 515.0005 -1.8836 368.7339 370.6175 346.6151 516.6145 -1.8817 368.5402 370.4219 346.3991 518.2435 -1.8762 368.3430 370.2192 346.1883 519.8450 -1.8707 368.1518 370.0224 345.9727 521.4445 -1.8702 367.9744 369.8446 345.7821 523.0584 -1.8619 367.7783 369.6402 345.5706 524.6576 -1.8560 367.5862 369.4423 345.3585 526.2870 -1.8562 367.3870 369.2432 345.1517 527.8858 -1.8509 367.2126 369.0635 344.9644 529.4998 -1.8429 367.0293 368.8722 344.7613 531.0988 -1.8411 366.8287 368.6698 344.5535 532.7129 -1.8381 366.6351 368.4731 344.3479 534.3221 -1.8337 366.4356 368.2692 344.1482 535.9283 -1.8304 366.2535 368.0839 343.9418 537.5203 -1.8253 366.0649 367.8902 343.7372 539.1133 -1.8188 365.8826 367.7013 343.5359 540.7353 -1.8146 365.6823 367.4969 343.3390 542.3421 -1.8151 365.4806 367.2956 343.1460 543.9369 -1.8093 365.3005 367.1098 342.9376 545.5336 -1.8044 365.0873 366.8917 342.7401 547.1418 -1.8001 364.9192 366.7193 342.5287 548.7649 -1.7977 364.7017 366.4994 342.3262 550.3599 -1.7954 364.5136 366.3089 342.1242 551.9566 -1.7902 364.3239 366.1141 341.9136 553.5700 -1.7881 364.1399 365.9281 341.7133 555.1676 -1.7836 363.9349 365.7185 341.4978 556.7818 -1.7836 363.7644 365.5481 341.2920 558.3958 -1.7756 363.5619 365.3375 341.0776 559.9946 -1.7726 363.3574 365.1300 340.8711 561.5935 -1.7666 363.1592 364.9257 340.6555 563.2075 -1.7621 362.9746 364.7366 340.4473 564.8215 -1.7583 362.7830 364.5413 340.2234 566.4355 -1.7563 362.5885 364.3448 340.0237 568.0345 -1.7533 362.3792 364.1326 339.8078 569.6485 -1.7484 362.1864 363.9348 339.5978 571.2475 -1.7459 362.0110 363.7570 339.3863 572.8761 -1.7412 361.8197 363.5609 339.1672 574.4750 -1.7335 361.6038 363.3373 338.9597 576.0889 -1.7334 361.4140 363.1474 338.7534 577.6878 -1.7291 361.2222 362.9513 338.5371 579.3169 -1.7187 361.0285 362.7472 338.3538 580.9159 -1.7162 360.8432 362.5593 338.1372 582.5298 -1.7153 360.6429 362.3582 337.9258 584.1288 -1.7122 360.4540 362.1662 337.7203 585.7433 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