DTA measure 1fazis_lassu Date: 2025225:1149 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1310.97 s Mass = 957.300 mg data_number = 1631 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1278 1.3782 233.1287 231.7506 221.8353 1.9193 1.3793 233.0907 231.7114 221.7102 2.7410 1.3784 233.0274 231.6491 221.5686 3.5025 1.3732 232.9973 231.6241 221.4508 4.3545 1.3730 232.9627 231.5897 221.3240 5.1165 1.3708 232.9196 231.5488 221.2059 5.9388 1.3620 232.8766 231.5146 221.0832 6.7605 1.3540 232.8188 231.4648 220.9759 7.5225 1.3535 232.7788 231.4253 220.8606 8.3745 1.3554 232.7447 231.3892 220.7544 9.1365 1.3553 232.7021 231.3468 220.6488 9.9585 1.3532 232.6665 231.3132 220.5387 10.7805 1.3527 232.6361 231.2834 220.3964 11.5425 1.3516 232.6102 231.2586 220.2956 12.3945 1.3546 232.5611 231.2065 220.1960 13.1565 1.3574 232.5068 231.1494 220.0834 13.9785 1.3582 232.4636 231.1054 219.9816 14.8005 1.3553 232.4371 231.0819 219.8953 15.5625 1.3524 232.3964 231.0441 219.8082 16.4145 1.3556 232.3413 230.9856 219.6977 17.2065 1.3552 232.2877 230.9325 219.5975 17.9985 1.3532 232.2580 230.9047 219.5177 18.8205 1.3549 232.2044 230.8495 219.4215 19.5825 1.3597 232.1707 230.8110 219.3386 20.4345 1.3623 232.1116 230.7492 219.2490 21.2263 1.3595 232.0791 230.7196 219.1805 22.0178 1.3581 232.0350 230.6769 219.1077 22.8405 1.3573 231.9783 230.6209 219.0662 23.6018 1.3605 231.9494 230.5889 218.9955 24.4540 1.3644 231.8977 230.5334 218.9172 25.2460 1.3604 231.8576 230.4973 218.8650 26.0375 1.3587 231.8183 230.4596 218.8168 26.8600 1.3546 231.7752 230.4206 218.7573 27.6518 1.3509 231.7537 230.4028 218.7303 28.4738 1.3528 231.6972 230.3443 218.6934 29.2660 1.3511 231.6441 230.2930 218.6481 30.0575 1.3554 231.5938 230.2383 218.6246 30.8800 1.3561 231.5368 230.1807 218.6040 31.6718 1.3584 231.5061 230.1477 218.5987 32.4938 1.3573 231.4762 230.1190 218.5959 33.2860 1.3572 231.4471 230.0899 218.5856 34.0775 1.3580 231.3893 230.0312 218.6004 34.8905 1.3612 231.3406 229.9793 218.6088 35.6815 1.3626 231.2987 229.9361 218.6188 36.5338 1.3622 231.2556 229.8934 218.6590 37.2955 1.3651 231.2268 229.8617 218.6823 38.1178 1.3653 231.1796 229.8143 218.6974 38.9095 1.3656 231.1404 229.7747 218.7314 39.7015 1.3633 231.0799 229.7167 218.7689 40.5543 1.3637 231.0244 229.6607 218.8051 41.3168 1.3666 230.9957 229.6291 218.8527 42.1385 1.3699 230.9591 229.5892 218.9074 42.9305 1.3816 230.9106 229.5291 218.9654 43.7235 1.3883 230.8717 229.4834 219.0378 44.5755 1.3824 230.8482 229.4658 219.1072 45.3375 1.3795 230.7938 229.4143 219.1858 46.1593 1.3800 230.7616 229.3816 219.2571 46.9478 1.3802 230.7192 229.3389 219.3381 47.7348 1.3801 230.6784 229.2983 219.4410 48.5528 1.3770 230.6383 229.2612 219.5326 49.3103 1.3769 230.5760 229.1991 219.6167 50.1590 1.3724 230.5175 229.1451 219.7220 50.9208 1.3805 230.5068 229.1263 219.8315 51.7423 1.3808 230.4930 229.1122 219.9369 52.5608 1.3777 230.4242 229.0466 220.0531 53.3188 1.3781 230.3832 229.0051 220.1595 54.1670 1.3778 230.3436 228.9659 220.2551 54.9055 1.3802 230.3328 228.9526 220.3605 55.7673 1.3771 230.2782 228.9011 220.4975 56.5260 1.3701 230.2262 228.8562 220.6074 57.3445 1.3716 230.2017 228.8301 220.7240 58.1640 1.3643 230.1604 228.7960 220.8592 58.9220 1.3573 230.1203 228.7630 220.9715 59.7705 1.3562 230.0645 228.7082 221.1076 60.5590 1.3533 230.0204 228.6670 221.2412 61.3775 1.3557 229.9949 228.6392 221.3519 62.1980 1.3576 229.9686 228.6110 221.4915 62.9870 1.3486 229.9318 228.5832 221.6345 63.7760 1.3414 229.8909 228.5496 221.7691 64.6275 1.3203 229.8469 228.5267 221.8843 65.3895 1.3070 229.8242 228.5172 222.0122 66.2115 1.2950 229.7737 228.4787 222.1502 67.0035 1.2892 229.7476 228.4585 222.2697 67.7943 1.2970 229.7167 228.4197 222.4019 68.6163 1.2976 229.7008 228.4031 222.5485 69.3775 1.2937 229.6506 228.3568 222.6843 70.2300 1.2863 229.6026 228.3163 222.8262 71.0220 1.2846 229.5668 228.2823 222.9408 71.8135 1.2788 229.5565 228.2777 223.0848 72.6360 1.2736 229.5167 228.2432 223.2253 73.3975 1.2729 229.4870 228.2141 223.3395 74.2500 1.2627 229.4447 228.1820 223.4729 75.0420 1.2512 229.4253 228.1740 223.5960 75.8335 1.2552 229.3825 228.1273 223.7422 76.6560 1.2528 229.3556 228.1028 223.8805 77.4175 1.2525 229.3153 228.0628 223.9907 78.2700 1.2484 229.2770 228.0287 224.0999 79.0318 1.2425 229.2404 227.9979 224.2316 79.8538 1.2382 229.2088 227.9705 224.3490 80.6760 1.2337 229.1726 227.9389 224.4752 81.4375 1.2259 229.1413 227.9154 224.5713 82.2900 1.2190 229.1255 227.9066 224.7134 83.0518 1.2122 229.0902 227.8780 224.8246 83.8738 1.2088 229.0523 227.8435 224.9358 84.6960 1.2010 229.0398 227.8388 225.0786 85.4575 1.1967 229.0199 227.8232 225.1887 86.3098 1.1938 228.9799 227.7861 225.2950 87.1018 1.1868 228.9602 227.7734 225.4169 87.8935 1.1744 228.9375 227.7631 225.5136 88.7158 1.1591 228.9119 227.7529 225.6316 89.4775 1.1493 228.8782 227.7288 225.7245 90.3295 1.1405 228.8477 227.7072 225.8392 91.1215 1.1375 228.8148 227.6773 225.9462 91.9135 1.1445 228.7976 227.6531 226.0559 92.7355 1.1492 228.7647 227.6155 226.1791 93.4975 1.1428 228.7521 227.6093 226.2815 94.3495 1.1348 228.7312 227.5964 226.3918 95.1415 1.1222 228.7014 227.5792 226.4971 95.9345 1.1138 228.6687 227.5549 226.6013 96.7565 1.1138 228.6430 227.5292 226.7017 97.5185 1.0997 228.6196 227.5199 226.7818 98.3705 1.0921 228.6053 227.5132 226.8729 99.1625 1.0844 228.5924 227.5081 226.9844 99.9538 1.0767 228.5760 227.4994 227.0866 100.7765 1.0714 228.5536 227.4822 227.2029 101.5680 1.0656 228.5294 227.4638 227.2721 102.3898 1.0534 228.5147 227.4613 227.3623 103.1820 1.0485 228.4685 227.4200 227.4490 103.9735 1.0395 228.4561 227.4166 227.5321 104.8265 1.0336 228.4244 227.3908 227.6267 105.5888 1.0232 228.3943 227.3711 227.7227 106.4115 1.0112 228.3816 227.3704 227.8089 107.2040 1.0075 228.3583 227.3508 227.9018 107.9955 1.0027 228.3288 227.3261 227.9746 108.8485 0.9949 228.3338 227.3390 228.0554 109.6108 0.9870 228.3064 227.3193 228.1310 110.4315 0.9784 228.2915 227.3130 228.2198 111.2193 0.9683 228.2800 227.3117 228.2958 112.0070 0.9550 228.2474 227.2925 228.3791 112.8553 0.9507 228.2476 227.2969 228.4713 113.6133 0.9451 228.2071 227.2620 228.5458 114.4320 0.9365 228.2219 227.2854 228.6399 115.2200 0.9265 228.2142 227.2877 228.6986 116.0080 0.9202 228.1881 227.2679 228.7801 116.8560 0.9150 228.1632 227.2482 228.8604 117.6143 0.9051 228.1545 227.2494 228.9417 118.4320 0.8990 228.1376 227.2386 229.0270 119.2500 0.8874 228.1054 227.2179 229.1308 120.0080 0.8806 228.0963 227.2157 229.1830 120.8568 0.8709 228.0702 227.1993 229.2882 121.6150 0.8616 228.0661 227.2045 229.3719 122.4338 0.8520 228.0597 227.2078 229.4482 123.2523 0.8439 228.0489 227.2050 229.5373 124.0120 0.8361 228.0202 227.1841 229.6408 124.8605 0.8280 228.0148 227.1869 229.7165 125.6495 0.8169 227.9890 227.1720 229.8035 126.4398 0.8094 227.9857 227.1763 229.8826 127.2593 0.8020 227.9795 227.1775 229.9845 128.0200 0.7895 227.9662 227.1767 230.0658 128.8718 0.7794 227.9461 227.1668 230.1436 129.6338 0.7715 227.9409 227.1694 230.2405 130.4553 0.7646 227.9229 227.1582 230.3339 131.2765 0.7554 227.9426 227.1872 230.4163 132.0385 0.7463 227.9277 227.1814 230.4826 132.8908 0.7363 227.9055 227.1692 230.5908 133.6525 0.7297 227.8923 227.1626 230.6749 134.4745 0.7189 227.8995 227.1806 230.7762 135.2668 0.7114 227.8830 227.1715 230.8805 136.0585 0.7024 227.8784 227.1760 230.9567 136.9105 0.6963 227.8602 227.1639 231.0526 137.6725 0.6866 227.8537 227.1670 231.1467 138.4945 0.6742 227.8511 227.1769 231.2535 139.2865 0.6641 227.8402 227.1762 231.3642 140.0785 0.6535 227.8386 227.1851 231.4607 140.9005 0.6446 227.8338 227.1892 231.5492 141.6925 0.6357 227.8147 227.1790 231.6298 142.5145 0.6270 227.8109 227.1839 231.7432 143.3065 0.6197 227.8144 227.1947 231.8429 144.0985 0.6093 227.8013 227.1920 231.9370 144.9205 0.5978 227.7955 227.1977 232.0403 145.6825 0.5917 227.7806 227.1889 232.1452 146.5345 0.5824 227.7849 227.2025 232.2641 147.3113 0.5739 227.7817 227.2078 232.3502 148.1335 0.5623 227.7712 227.2090 232.4489 148.9255 0.5553 227.7693 227.2140 232.5504 149.7170 0.5430 227.7631 227.2201 232.6348 150.5693 0.5288 227.7786 227.2498 232.7348 151.3310 0.5228 227.7792 227.2564 232.8289 152.1528 0.5108 227.7433 227.2326 232.9133 152.9450 0.4986 227.7535 227.2549 233.0153 153.7365 0.4875 227.7564 227.2690 233.1295 154.5890 0.4821 227.7637 227.2816 233.2168 155.3508 0.4691 227.7713 227.3022 233.3199 156.1728 0.4595 227.7650 227.3055 233.4280 156.9670 0.4492 227.7579 227.3086 233.5244 157.7605 0.4312 227.7658 227.3346 233.6204 158.6130 0.4151 227.7737 227.3586 233.7501 159.3748 0.4092 227.7830 227.3738 233.8445 160.1968 0.4097 227.7812 227.3715 233.9535 161.0190 0.3988 227.7723 227.3735 234.0488 161.7805 0.3899 227.7867 227.3968 234.1459 162.6333 0.3804 227.7831 227.4027 234.2714 163.3955 0.3696 227.7787 227.4091 234.3397 164.2178 0.3613 227.7861 227.4248 234.4681 165.0398 0.3529 227.7853 227.4324 234.5800 165.8015 0.3420 227.7828 227.4408 234.6862 166.6535 0.3321 227.7941 227.4620 234.7993 167.4178 0.3238 227.7996 227.4758 234.8913 168.2418 0.3117 227.7962 227.4845 234.9985 169.0635 0.3020 227.7992 227.4972 235.1157 169.8255 0.2912 227.7988 227.5076 235.2248 170.6775 0.2838 227.8024 227.5187 235.3392 171.4395 0.2728 227.8168 227.5439 235.4414 172.2615 0.2611 227.8129 227.5518 235.5488 173.0835 0.2525 227.8558 227.6033 235.6541 173.8455 0.2419 227.8403 227.5984 235.7705 174.6958 0.2303 227.8468 227.6166 235.8894 175.4835 0.2204 227.8615 227.6412 236.0001 176.2715 0.2095 227.8632 227.6537 236.0966 177.0900 0.2009 227.8591 227.6582 236.1975 177.8478 0.1919 227.8596 227.6678 236.3019 178.6958 0.1790 227.8699 227.6909 236.4189 179.4840 0.1690 227.8906 227.7216 236.5447 180.2718 0.1601 227.9069 227.7468 236.6323 181.0903 0.1512 227.9324 227.7812 236.7360 181.8490 0.1393 227.9298 227.7905 236.8546 182.6978 0.1233 227.9448 227.8215 236.9794 183.4560 0.1058 227.9550 227.8491 237.0755 184.2750 0.0911 227.9607 227.8696 237.1882 185.0933 0.0912 227.9797 227.8885 237.2861 185.8528 0.0822 227.9906 227.9084 237.3699 186.7023 0.0733 228.0048 227.9315 237.5087 187.4910 0.0623 228.0279 227.9655 237.6036 188.2808 0.0557 228.0365 227.9808 237.6999 189.0998 0.0415 228.0380 227.9965 237.8027 189.8600 0.0296 228.0499 228.0203 237.9062 190.7088 0.0211 228.0544 228.0333 238.0175 191.4988 0.0104 228.0807 228.0703 238.1171 192.2903 0.0001 228.1079 228.1078 238.2262 193.1115 -0.0139 228.1209 228.1347 238.3417 193.8735 -0.0231 228.1130 228.1361 238.4272 194.7255 -0.0335 228.1353 228.1688 238.5475 195.5173 -0.0412 228.1719 228.2130 238.6490 196.3088 -0.0506 228.1828 228.2334 238.7434 197.1315 -0.0641 228.2075 228.2716 238.8579 197.8928 -0.0751 228.2163 228.2914 238.9437 198.7450 -0.0844 228.2358 228.3202 239.0535 199.5070 -0.0960 228.2532 228.3492 239.1463 200.3288 -0.1052 228.2734 228.3786 239.2442 201.1210 -0.1195 228.2945 228.4140 239.3471 201.9125 -0.1306 228.3006 228.4311 239.4524 202.7650 -0.1411 228.3042 228.4452 239.5514 203.5268 -0.1497 228.3323 228.4820 239.6528 204.3488 -0.1597 228.3444 228.5041 239.7308 205.1410 -0.1716 228.3580 228.5296 239.8631 205.9325 -0.1848 228.3979 228.5827 239.9620 206.7558 -0.1953 228.4314 228.6267 240.0455 207.5478 -0.2041 228.4540 228.6580 240.1399 208.3698 -0.2040 228.4602 228.6642 240.2337 209.1620 -0.1986 228.4839 228.6824 240.3400 209.9535 -0.2004 228.5111 228.7116 240.4295 210.7775 -0.2164 228.5369 228.7533 240.5219 211.5708 -0.2336 228.5558 228.7893 240.6201 212.3928 -0.2429 228.5891 228.8320 240.7218 213.1848 -0.2497 228.5976 228.8474 240.8128 213.9765 -0.2659 228.6149 228.8808 240.9049 214.7988 -0.2779 228.6475 228.9254 241.0117 215.5905 -0.2917 228.6616 228.9533 241.1064 216.4125 -0.3029 228.6930 228.9959 241.2039 217.2045 -0.3115 228.7222 229.0337 241.2799 217.9965 -0.3242 228.7462 229.0704 241.3732 218.8185 -0.3343 228.7563 229.0906 241.4683 219.6105 -0.3436 228.7931 229.1367 241.5614 220.4325 -0.3536 228.8284 229.1820 241.6596 221.2245 -0.3622 228.8456 229.2079 241.7455 222.0165 -0.3707 228.8787 229.2494 241.8121 222.8685 -0.3843 228.8916 229.2758 241.9201 223.6305 -0.3948 228.9150 229.3097 242.0151 224.4525 -0.4300 228.9479 229.3780 242.1326 225.2445 -0.4583 228.9594 229.4177 242.2205 226.0365 -0.4745 229.0076 229.4821 242.3042 226.8883 -0.4697 229.0340 229.5037 242.4079 227.6505 -0.4918 229.0590 229.5509 242.5005 228.4720 -0.5047 229.0932 229.5978 242.5838 229.2660 -0.5131 229.1150 229.6281 242.7050 230.0878 -0.5213 229.1525 229.6739 242.7938 230.8800 -0.5331 229.1910 229.7241 242.8982 231.6715 -0.5378 229.1989 229.7367 242.9876 232.5240 -0.5460 229.2345 229.7805 243.0998 233.2858 -0.5550 229.2683 229.8233 243.2026 234.1078 -0.5446 229.2921 229.8367 243.2992 234.9000 -0.5502 229.3247 229.8749 243.4008 235.6915 -0.5615 229.3516 229.9131 243.5207 236.5440 -0.5725 229.3946 229.9671 243.6088 237.3058 -0.5798 229.4273 230.0071 243.6900 238.1275 -0.5837 229.4843 230.0681 243.7865 238.9460 -0.6037 229.4986 230.1023 243.9238 239.7040 -0.6126 229.5309 230.1435 244.0135 240.5523 -0.6259 229.5645 230.1904 244.1173 241.3103 -0.6328 229.5901 230.2229 244.2353 242.1290 -0.6401 229.6346 230.2747 244.3035 242.9170 -0.6614 229.6642 230.3256 244.3980 243.7050 -0.6917 229.7161 230.4078 244.4934 244.5540 -0.7047 229.7446 230.4493 244.6125 245.3120 -0.7182 229.7615 230.4797 244.7224 246.1310 -0.7052 229.8045 230.5097 244.8356 246.9495 -0.7041 229.8488 230.5528 244.9141 247.7080 -0.7055 229.8862 230.5917 244.9996 248.5570 -0.7111 229.9173 230.6284 245.1197 249.3450 -0.7188 229.9506 230.6694 245.2202 250.1340 -0.7277 229.9673 230.6951 245.3293 250.9520 -0.7395 230.0158 230.7553 245.4291 251.7403 -0.7483 230.0525 230.8008 245.5208 252.5593 -0.7618 230.0767 230.8385 245.6515 253.3488 -0.7723 230.1208 230.8931 245.7458 254.1383 -0.7810 230.1573 230.9382 245.8224 254.9590 -0.7856 230.2007 230.9863 245.9280 255.7480 -0.7923 230.2385 231.0308 246.0381 256.5670 -0.8048 230.2811 231.0860 246.1345 257.3558 -0.8197 230.3086 231.1283 246.2372 258.1470 -0.8289 230.3334 231.1623 246.3342 258.9685 -0.8337 230.3789 231.2126 246.4346 259.7300 -0.8437 230.4344 231.2781 246.5173 260.5818 -0.8488 230.4833 231.3321 246.6297 261.3735 -0.8842 230.5087 231.3929 246.7433 262.1655 -0.8916 230.5567 231.4483 246.8363 262.9875 -0.8894 230.5977 231.4871 246.8891 263.7495 -0.9016 230.6201 231.5217 246.9967 264.6015 -0.9116 230.6915 231.6032 247.1336 265.3635 -0.9307 230.7156 231.6464 247.2320 266.1855 -0.9409 230.7534 231.6943 247.3166 266.9775 -0.9529 230.8036 231.7565 247.4073 267.7695 -0.9735 230.8309 231.8044 247.5160 268.6215 -0.9779 230.8853 231.8632 247.6192 269.3835 -0.9851 230.9245 231.9096 247.7243 270.2055 -0.9912 230.9524 231.9437 247.8089 270.9975 -0.9988 231.0102 232.0090 247.9397 271.7895 -1.0105 231.0309 232.0415 248.0622 272.6415 -1.0139 231.1064 232.1203 248.1613 273.4035 -1.0240 231.1432 232.1673 248.2502 274.2255 -1.0328 231.1983 232.2311 248.3617 275.0175 -1.0378 231.2502 232.2880 248.4646 275.8095 -1.0434 231.2854 232.3288 248.5730 276.6315 -1.0598 231.3359 232.3957 248.6872 277.4235 -1.0682 231.3721 232.4403 248.7752 278.2450 -1.0798 231.4113 232.4910 248.8872 279.0373 -1.0901 231.4719 232.5620 249.0366 279.8285 -1.0986 231.5085 232.6071 249.1240 280.6813 -1.1039 231.5505 232.6545 249.2321 281.4428 -1.1147 231.5921 232.7068 249.3260 282.2648 -1.1210 231.6425 232.7634 249.4628 283.0573 -1.1269 231.6848 232.8117 249.5639 283.8495 -1.1402 231.7311 232.8713 249.6681 284.6720 -1.1474 231.7873 232.9347 249.7804 285.4638 -1.1542 231.8210 232.9752 249.8902 286.2875 -1.1611 231.8804 233.0415 250.0002 287.0800 -1.1771 231.9218 233.0989 250.1039 287.8738 -1.1806 231.9691 233.1497 250.2004 288.7010 -1.1928 232.0181 233.2109 250.3141 289.4635 -1.2068 232.0631 233.2699 250.4490 290.3158 -1.2143 232.1138 233.3282 250.5472 291.0798 -1.2206 232.1558 233.3763 250.6581 291.9055 -1.2290 232.2118 233.4408 250.7515 292.7275 -1.2557 232.2737 233.5294 250.8904 293.4895 -1.2677 232.3309 233.5986 251.0072 294.3415 -1.2803 232.3629 233.6432 251.1056 295.1035 -1.2907 232.4224 233.7131 251.1851 295.9255 -1.2949 232.4789 233.7738 251.2964 296.7480 -1.3021 232.5334 233.8355 251.4283 297.5105 -1.3151 232.5968 233.9119 251.5341 298.3625 -1.3206 232.6629 233.9836 251.6514 299.1245 -1.3238 232.6769 234.0007 251.7508 299.9465 -1.3331 232.7324 234.0654 251.8771 300.7685 -1.3496 232.7792 234.1288 251.9765 301.5305 -1.3608 232.8358 234.1966 252.0667 302.3825 -1.3720 232.8958 234.2677 252.1839 303.1743 -1.3750 232.9343 234.3093 252.2930 303.9638 -1.3896 232.9897 234.3793 252.3869 304.7818 -1.4011 233.0484 234.4495 252.4894 305.5395 -1.4081 233.1051 234.5131 252.5832 306.3878 -1.4154 233.1564 234.5718 252.7090 307.1758 -1.4217 233.2089 234.6306 252.8219 307.9638 -1.4340 233.2677 234.7017 252.9261 308.7813 -1.4337 233.3234 234.7571 253.0289 309.5390 -1.4449 233.3657 234.8105 253.1225 310.3873 -1.4442 233.4291 234.8734 253.2399 311.1758 -1.4531 233.4895 234.9427 253.3420 311.9630 -1.4667 233.5289 234.9956 253.4552 312.7818 -1.4691 233.6025 235.0716 253.5322 313.5395 -1.4728 233.6578 235.1306 253.6449 314.3875 -1.4939 233.7087 235.2026 253.7706 315.1788 -1.4928 233.7624 235.2552 253.8725 315.9690 -1.5058 233.8253 235.3311 253.9826 316.7878 -1.5172 233.8907 235.4079 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