DTA measure 1pb2_down Date: 2026428:1749 Lower limit = 220.0 C Upper limit = 440.0 C Rate = 8.00 C/min Mtime = 1648.32 s Mass = 100.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3969 -3.7769 392.4697 396.2466 403.1243 3.9914 -3.7753 392.7962 396.5715 403.1463 5.5961 -3.7737 393.1223 396.8960 403.1641 7.2018 -3.7731 393.4429 397.2160 403.1920 8.8066 -3.7727 393.7672 397.5398 403.2048 10.4114 -3.7727 394.0887 397.8614 403.2107 12.0368 -3.7724 394.3917 398.1641 403.2036 13.6424 -3.7713 394.7025 398.4738 403.1759 15.2523 -3.7693 395.0172 398.7865 403.1357 16.8570 -3.7684 395.3175 399.0859 403.0785 18.4474 -3.7682 395.6123 399.3804 403.0116 20.0573 -3.7675 395.9151 399.6826 402.9358 21.6620 -3.7681 396.2247 399.9928 402.8523 23.2729 -3.7672 396.5309 400.2981 402.7516 24.8930 -3.7662 396.8235 400.5897 402.6473 26.5031 -3.7663 397.1158 400.8821 402.5254 28.1086 -3.7673 397.4028 401.1701 402.3995 29.7134 -3.7671 397.6909 401.4580 402.2715 31.3239 -3.7668 397.9823 401.7491 402.1421 32.9290 -3.7655 398.2595 402.0250 401.9976 34.5389 -3.7660 398.5446 402.3106 401.8409 36.1599 -3.7649 398.8280 402.5929 401.6854 37.7699 -3.7649 399.0973 402.8622 401.5311 39.3746 -3.7645 399.3562 403.1207 401.3723 40.9800 -3.7657 399.6054 403.3711 401.2124 42.5903 -3.7653 399.8680 403.6333 401.0529 44.1950 -3.7656 400.1270 403.8926 400.8946 45.8110 -3.7647 400.3860 404.1507 400.7189 47.4311 -3.7652 400.6364 404.4015 400.5296 49.0308 -3.7658 400.8728 404.6387 400.3547 50.6313 -3.7657 401.1097 404.8754 400.1792 52.2259 -3.7657 401.3415 405.1072 399.9975 53.8258 -3.7660 401.5796 405.3456 399.8225 55.4159 -3.7672 401.8032 405.5704 399.6386 57.0206 -3.7682 402.0200 405.7882 399.4678 58.6203 -3.7691 402.2378 406.0070 399.3241 60.2310 -3.7701 402.4440 406.2141 399.1583 61.8359 -3.7705 402.6550 406.4255 398.9937 63.4355 -3.7722 402.8649 406.6372 398.8366 65.0458 -3.7740 403.0687 406.8427 398.6746 66.6511 -3.7743 403.2689 407.0432 398.5197 68.2508 -3.7750 403.4636 407.2386 398.3560 69.8458 -3.7774 403.6420 407.4193 398.1897 71.4510 -3.7795 403.8401 407.6196 398.0243 73.0609 -3.7801 404.0259 407.8060 397.8551 74.6656 -3.7823 404.2035 407.9857 397.6878 76.2761 -3.7822 404.3791 408.1614 397.5259 77.8813 -3.7828 404.5532 408.3360 397.3635 79.4860 -3.7847 404.7286 408.5133 397.2067 81.1010 -3.7875 404.8908 408.6783 397.0388 82.6913 -3.7884 405.0473 408.8357 396.8826 84.3013 -3.7911 405.2050 408.9961 396.7261 85.9060 -3.7944 405.3520 409.1464 396.5611 87.5168 -3.7976 405.4982 409.2958 396.4036 89.1216 -3.8002 405.6586 409.4588 396.2327 90.7315 -3.8036 405.8136 409.6172 396.0635 92.3365 -3.8067 405.9487 409.7554 395.8981 93.9420 -3.8107 406.0716 409.8822 395.7302 95.5519 -3.8137 406.1979 410.0116 395.5640 97.1573 -3.8159 406.3318 410.1477 395.3900 98.7675 -3.8195 406.4411 410.2606 395.2104 100.3723 -3.8216 406.5621 410.3837 395.0371 101.9981 -3.8240 406.6772 410.5012 394.8510 103.6033 -3.8270 406.7928 410.6198 394.6854 105.2080 -3.8302 406.9048 410.7350 394.5206 106.8184 -3.8333 407.0045 410.8379 394.3588 108.4236 -3.8382 407.1118 410.9500 394.1888 110.0335 -3.8424 407.2064 411.0488 394.0092 111.6386 -3.8454 407.2918 411.1372 393.8412 113.2338 -3.8476 407.3820 411.2296 393.6721 114.8488 -3.8511 407.4671 411.3181 393.4944 116.4493 -3.8550 407.5531 411.4081 393.3184 118.0490 -3.8584 407.6490 411.5074 393.1453 119.6539 -3.8626 407.7381 411.6007 392.9802 121.2595 -3.8651 407.8145 411.6796 392.8110 122.8643 -3.8689 407.8928 411.7618 392.6511 124.4690 -3.8720 407.9625 411.8346 392.4830 126.0850 -3.8762 408.0201 411.8963 392.3049 127.6795 -3.8807 408.0834 411.9641 392.1399 129.2843 -3.8839 408.1446 412.0285 391.9812 130.8849 -3.8877 408.1978 412.0855 391.8163 132.4948 -3.8909 408.2562 412.1471 391.6590 134.0995 -3.8930 408.2979 412.1909 391.4965 135.7104 -3.8972 408.3431 412.2403 391.3323 137.3151 -3.9032 408.3806 412.2838 391.1639 138.9354 -3.9061 408.4174 412.3235 390.9877 140.5461 -3.9104 408.4566 412.3670 390.8091 142.1509 -3.9145 408.4818 412.3963 390.6391 143.7565 -3.9186 408.5235 412.4421 390.4564 145.3614 -3.9222 408.5699 412.4921 390.2748 146.9713 -3.9263 408.5938 412.5201 390.1053 148.5769 -3.9306 408.6176 412.5481 389.9286 150.1869 -3.9352 408.6381 412.5734 389.7655 151.8071 -3.9383 408.6494 412.5877 389.5837 153.4179 -3.9411 408.6666 412.6077 389.4063 155.0226 -3.9447 408.6820 412.6267 389.2283 156.6171 -3.9472 408.6964 412.6436 389.0529 158.2380 -3.9526 408.7008 412.6534 388.8757 159.8430 -3.9586 408.7073 412.6659 388.7000 161.4533 -3.9626 408.7084 412.6710 388.5259 163.0689 -3.9668 408.7120 412.6788 388.3446 164.6685 -3.9701 408.7103 412.6804 388.1622 166.2945 -3.9752 408.7102 412.6854 387.9833 167.8995 -3.9796 408.7116 412.6912 387.8028 169.5098 -3.9826 408.7221 412.7046 387.6249 171.1151 -3.9833 408.7091 412.6924 387.4420 172.7250 -3.9858 408.6844 412.6702 387.2465 174.3304 -3.9900 408.6649 412.6549 387.0606 175.9355 -3.9932 408.6448 412.6380 386.8799 177.5556 -3.9976 408.6258 412.6234 386.6942 179.1504 -4.0007 408.6113 412.6120 386.5053 180.7405 -4.0048 408.5956 412.6003 386.3203 182.3401 -4.0065 408.5846 412.5912 386.1434 183.9403 -4.0108 408.5714 412.5822 385.9660 185.5455 -4.0127 408.5523 412.5650 385.7879 187.1503 -4.0171 408.5226 412.5397 385.6178 188.7551 -4.0187 408.4712 412.4899 385.4533 190.3403 -4.0210 408.4297 412.4507 385.2820 191.9655 -4.0253 408.3896 412.4149 385.1015 193.5656 -4.0295 408.3475 412.3770 384.9301 195.1709 -4.0323 408.3091 412.3414 384.7469 196.7808 -4.0353 408.2651 412.3004 384.5632 198.3861 -4.0387 408.2171 412.2558 384.3806 199.9759 -4.0415 408.1778 412.2193 384.1949 201.5806 -4.0432 408.1309 412.1741 384.0036 203.1863 -4.0444 408.0904 412.1348 383.8201 204.8116 -4.0462 408.0428 412.0891 383.6287 206.4164 -4.0482 407.9956 412.0438 383.4427 208.0220 -4.0495 407.9414 411.9909 383.2656 209.6269 -4.0514 407.8914 411.9428 383.0834 211.2319 -4.0532 407.8396 411.8928 382.9019 212.8425 -4.0568 407.7733 411.8301 382.7192 214.4473 -4.0579 407.7070 411.7649 382.5351 216.0578 -4.0603 407.6370 411.6974 382.3528 217.6629 -4.0616 407.5670 411.6286 382.1709 219.2676 -4.0632 407.5000 411.5633 381.9929 220.8785 -4.0653 407.4255 411.4908 381.8063 222.4833 -4.0667 407.3533 411.4200 381.6185 224.0931 -4.0674 407.2791 411.3464 381.4166 225.7190 -4.0695 407.2035 411.2730 381.2099 227.3241 -4.0692 407.1313 411.2006 381.0084 228.9340 -4.0707 407.0614 411.1321 380.8182 230.5238 -4.0721 406.9877 411.0598 380.6237 232.1650 -4.0725 406.9111 410.9836 380.4155 233.7698 -4.0734 406.8292 410.9026 380.2068 235.3700 -4.0723 406.7505 410.8228 380.0046 236.9905 -4.0721 406.6669 410.7391 379.8022 238.5953 -4.0727 406.5838 410.6565 379.5953 240.2059 -4.0725 406.5004 410.5730 379.3909 241.7955 -4.0737 406.4079 410.4815 379.1899 243.3900 -4.0764 406.3266 410.4030 378.9923 244.9955 -4.0765 406.2372 410.3137 378.7965 246.6108 -4.0761 406.1455 410.2216 378.5991 248.2155 -4.0765 406.0578 410.1343 378.4096 249.8206 -4.0770 405.9669 410.0439 378.2144 251.4055 -4.0775 405.8744 409.9519 378.0269 253.0103 -4.0777 405.7724 409.8501 377.8499 254.6201 -4.0781 405.6637 409.7418 377.6547 256.2255 -4.0797 405.5551 409.6349 377.4645 257.8255 -4.0800 405.4566 409.5367 377.2846 259.4354 -4.0794 405.3592 409.4386 377.1022 261.0403 -4.0773 405.2539 409.3312 376.9085 262.6459 -4.0765 405.1432 409.2196 376.7198 264.2506 -4.0760 405.0469 409.1229 376.5393 265.8560 -4.0747 404.9456 409.0202 376.3634 267.4611 -4.0745 404.8351 408.9096 376.1866 269.0556 -4.0729 404.7325 408.8054 376.0091 270.6663 -4.0725 404.6104 408.6829 375.8393 272.2713 -4.0726 404.4930 408.5655 375.6651 273.8811 -4.0730 404.3777 408.4506 375.4851 275.4869 -4.0725 404.2675 408.3400 375.2921 277.0916 -4.0731 404.1610 408.2341 375.1104 278.7016 -4.0727 404.0563 408.1291 374.9107 280.3073 -4.0718 403.9423 408.0141 374.7046 281.9171 -4.0708 403.8175 407.8883 374.5070 283.5065 -4.0674 403.6938 407.7612 374.3087 285.1174 -4.0639 403.5792 407.6431 374.1067 286.7273 -4.0612 403.4519 407.5131 373.9008 288.3525 -4.0608 403.3361 407.3969 373.6937 289.9425 -4.0601 403.2100 407.2701 373.5040 291.5476 -4.0606 403.0836 407.1442 373.3119 293.1575 -4.0592 402.9602 407.0193 373.1152 294.7628 -4.0576 402.8491 406.9067 372.9248 296.3731 -4.0560 402.7266 406.7826 372.7402 297.9779 -4.0553 402.6036 406.6589 372.5549 299.5884 -4.0551 402.4746 406.5296 372.3714 301.2089 -4.0529 402.3439 406.3968 372.1797 302.8136 -4.0494 402.2148 406.2642 371.9920 304.4235 -4.0483 402.0889 406.1371 371.8091 306.0236 -4.0479 401.9654 406.0133 371.6207 307.6186 -4.0450 401.8423 405.8872 371.4431 309.2285 -4.0438 401.7032 405.7470 371.2740 310.8133 -4.0414 401.5715 405.6129 371.0990 312.4134 -4.0393 401.4286 405.4678 370.9180 314.0335 -4.0368 401.2818 405.3187 370.7345 315.6339 -4.0364 401.1430 405.1793 370.5524 317.2389 -4.0357 401.0140 405.0497 370.3763 318.8488 -4.0343 400.8846 404.9189 370.1880 320.4541 -4.0324 400.7493 404.7817 369.9900 322.0593 -4.0297 400.6095 404.6392 369.7923 323.6640 -4.0287 400.4754 404.5040 369.5923 325.2851 -4.0269 400.3294 404.3562 369.3931 326.8899 -4.0248 400.1930 404.2179 369.2001 328.4946 -4.0228 400.0511 404.0738 369.0051 330.1001 -4.0210 399.9054 403.9264 368.8020 331.7103 -4.0188 399.7717 403.7906 368.5992 333.3153 -4.0149 399.6255 403.6404 368.4086 334.9105 -4.0127 399.4825 403.4952 368.2215 336.5306 -4.0109 399.3412 403.3521 368.0203 338.1413 -4.0085 399.2170 403.2255 367.8238 339.7463 -4.0070 399.0835 403.0905 367.6256 341.3510 -4.0056 398.9240 402.9296 367.4409 342.9619 -4.0039 398.7675 402.7714 367.2574 344.5666 -3.9999 398.6282 402.6281 367.0646 346.1769 -3.9962 398.4852 402.4814 366.8695 347.7823 -3.9942 398.3412 402.3354 366.6805 349.4075 -3.9927 398.1766 402.1692 366.5039 351.0128 -3.9902 398.0149 402.0051 366.3238 352.6180 -3.9870 397.8713 401.8583 366.1444 354.2279 -3.9857 397.7288 401.7145 365.9474 355.8333 -3.9842 397.5701 401.5543 365.7578 357.4435 -3.9826 397.4147 401.3973 365.5768 359.0585 -3.9799 397.2606 401.2406 365.3989 360.6641 -3.9778 397.1108 401.0886 365.2028 362.2895 -3.9749 396.9616 400.9365 365.0026 363.8790 -3.9727 396.8014 400.7740 364.7958 365.4846 -3.9705 396.6422 400.6127 364.5939 367.0945 -3.9666 396.4928 400.4595 364.3874 368.7044 -3.9641 396.3464 400.3105 364.1776 370.3098 -3.9618 396.1848 400.1465 363.9752 371.9046 -3.9590 396.0380 399.9971 363.7841 373.4889 -3.9550 395.8877 399.8427 363.5747 375.0941 -3.9505 395.7303 399.6808 363.3634 376.7148 -3.9482 395.5720 399.5202 363.1589 378.2990 -3.9443 395.4097 399.3540 362.9694 379.9046 -3.9396 395.2493 399.1889 362.7705 381.5095 -3.9377 395.0892 399.0269 362.5608 383.1143 -3.9363 394.9327 398.8690 362.3527 384.7198 -3.9324 394.7721 398.7045 362.1524 386.3196 -3.9288 394.6168 398.5456 361.9484 387.9090 -3.9253 394.4716 398.3969 361.7472 389.5198 -3.9232 394.3141 398.2373 361.5422 391.1400 -3.9198 394.1472 398.0670 361.3371 392.7448 -3.9169 393.9826 397.8995 361.1405 394.3503 -3.9140 393.8256 397.7396 360.9387 395.9399 -3.9107 393.6573 397.5680 360.7569 397.5498 -3.9082 393.4873 397.3954 360.5625 399.1551 -3.9047 393.3289 397.2336 360.3702 400.7654 -3.9017 393.1589 397.0606 360.1888 402.3701 -3.8973 393.0042 396.9015 359.9950 403.9913 -3.8926 392.8326 396.7252 359.7997 405.6011 -3.8913 392.6775 396.5688 359.6072 407.2060 -3.8903 392.5159 396.4063 359.4196 408.8168 -3.8881 392.3489 396.2369 359.2513 410.4215 -3.8871 392.1830 396.0701 359.0642 412.0315 -3.8841 392.0089 395.8931 358.8802 413.6371 -3.8797 391.8398 395.7194 358.6885 415.2624 -3.8769 391.6645 395.5414 358.4925 416.8725 -3.8722 391.4951 395.3673 358.2993 418.4780 -3.8675 391.3347 395.2023 358.1014 420.0725 -3.8631 391.1629 395.0259 357.9068 421.6778 -3.8613 390.9943 394.8556 357.7082 423.2881 -3.8584 390.8249 394.6833 357.4978 424.8933 -3.8555 390.6494 394.5049 357.2880 426.5038 -3.8517 390.4833 394.3350 357.0886 428.1239 -3.8473 390.3078 394.1551 356.8853 429.7293 -3.8431 390.1404 393.9835 356.6889 431.3395 -3.8402 389.9817 393.8219 356.4892 432.9443 -3.8360 389.8092 393.6452 356.2828 434.5550 -3.8324 389.6395 393.4719 356.0785 436.1496 -3.8288 389.4705 393.2993 355.8742 437.7496 -3.8270 389.2957 393.1227 355.6723 439.3396 -3.8235 389.1140 392.9374 355.4685 440.9598 -3.8196 388.9315 392.7511 355.2693 442.5596 -3.8162 388.7599 392.5761 355.0703 444.1549 -3.8135 388.5949 392.4084 354.8724 445.7648 -3.8102 388.4205 392.2307 354.6711 447.3701 -3.8070 388.2438 392.0508 354.4740 448.9804 -3.8033 388.0637 391.8671 354.2776 450.5851 -3.8008 387.8938 391.6946 354.0655 452.1905 -3.7974 387.7226 391.5200 353.8671 453.8110 -3.7930 387.5459 391.3389 353.6790 455.4004 -3.7889 387.3785 391.1674 353.4805 457.0109 -3.7834 387.1996 390.9830 353.2830 458.6160 -3.7799 387.0208 390.8007 353.0878 460.2156 -3.7771 386.8494 390.6265 352.8982 461.8263 -3.7744 386.6705 390.4448 352.7178 463.4313 -3.7677 386.4906 390.2583 352.5372 465.0566 -3.7619 386.3064 390.0682 352.3404 466.6623 -3.7580 386.1328 389.8908 352.1548 468.2670 -3.7554 385.9566 389.7120 351.9677 469.8774 -3.7514 385.7768 389.5282 351.7837 471.4826 -3.7470 385.6046 389.3517 351.5891 473.0925 -3.7429 385.4329 389.1758 351.4043 474.6975 -3.7403 385.2463 388.9865 351.2097 476.3235 -3.7370 385.0585 388.7956 351.0103 477.9283 -3.7328 384.8724 388.6052 350.8156 479.5334 -3.7286 384.6837 388.4123 350.6181 481.1439 -3.7241 384.5010 388.2251 350.4106 482.7486 -3.7194 384.3284 388.0479 350.1989 484.3588 -3.7152 384.1411 387.8563 350.0027 485.9643 -3.7101 383.9664 387.6765 349.7986 487.5895 -3.7060 383.7802 387.4862 349.5792 489.1943 -3.7022 383.5904 387.2926 349.3686 490.7999 -3.6976 383.4153 387.1129 349.1648 492.4099 -3.6915 383.2413 386.9327 348.9534 494.0146 -3.6862 383.0698 386.7560 348.7415 495.6255 -3.6814 382.8908 386.5721 348.5356 497.2303 -3.6784 382.7073 386.3857 348.3232 498.8453 -3.6744 382.5275 386.2019 348.1143 500.4500 -3.6696 382.3382 386.0078 347.9126 502.0453 -3.6649 382.1615 385.8264 347.7094 503.6503 -3.6582 381.9782 385.6364 347.5048 505.2499 -3.6538 381.8141 385.4679 347.2905 506.8555 -3.6490 381.6344 385.2835 347.0825 508.4553 -3.6446 381.4457 385.0903 346.8717 510.0754 -3.6396 381.2648 384.9044 346.6572 511.6811 -3.6345 381.0813 384.7158 346.4579 513.2859 -3.6303 380.8896 384.5199 346.2456 514.8958 -3.6273 380.6985 384.3258 346.0362 516.5011 -3.6229 380.5065 384.1294 345.8343 518.1114 -3.6175 380.3207 383.9382 345.6265 519.7161 -3.6123 380.1397 383.7520 345.4327 521.3313 -3.6063 379.9605 383.5668 345.2428 522.9420 -3.5999 379.7812 383.3811 345.0374 524.5468 -3.5946 379.5985 383.1931 344.8335 526.1566 -3.5893 379.4143 383.0035 344.6390 527.7623 -3.5855 379.2118 382.7973 344.4474 529.3671 -3.5815 379.0307 382.6122 344.2508 530.9770 -3.5767 378.8531 382.4298 344.0553 532.5981 -3.5720 378.6861 382.2581 343.8680 534.2080 -3.5667 378.5039 382.0705 343.6751 535.8134 -3.5612 378.3115 381.8727 343.4858 537.4236 -3.5582 378.1132 381.6715 343.2921 539.0286 -3.5533 377.9298 381.4831 343.0897 540.6341 -3.5500 377.7482 381.2982 342.9157 542.2440 -3.5462 377.5618 381.1080 342.7393 543.8644 -3.5436 377.3710 380.9146 342.5389 545.4750 -3.5396 377.1728 380.7125 342.3563 547.0798 -3.5346 376.9912 380.5259 342.1645 548.6899 -3.5303 376.8066 380.3369 341.9756 550.2954 -3.5259 376.6144 380.1403 341.7831 551.9001 -3.5206 376.4246 379.9451 341.5845 553.5104 -3.5170 376.2300 379.7470 341.3927 555.1311 -3.5121 376.0422 379.5543 341.1987 556.7410 -3.5085 375.8532 379.3617 340.9994 558.3463 -3.5031 375.6563 379.1594 340.7999 559.9618 -3.4986 375.4709 378.9695 340.6003 561.5668 -3.4936 375.2904 378.7839 340.3947 563.1569 -3.4893 375.1037 378.5929 340.1940 564.7565 -3.4856 374.9154 378.4010 339.9837 566.3569 -3.4831 374.7286 378.2117 339.7894 567.9721 -3.4805 374.5358 378.0163 339.5667 569.5720 -3.4760 374.3555 377.8315 339.3566 571.1775 -3.4724 374.1552 377.6276 339.1609 572.7823 -3.4683 373.9652 377.4335 338.9558 574.3876 -3.4634 373.7837 377.2471 338.7459 575.9774 -3.4596 373.5989 377.0585 338.5407 577.5770 -3.4569 373.4094 376.8663 338.3433 579.1828 -3.4538 373.2241 376.6779 338.1438 580.8029 -3.4477 373.0330 376.4807 337.9326 582.4079 -3.4444 372.8453 376.2897 337.7244 584.0185 -3.4421 372.6442 376.0863 337.5234 585.6233 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