DTA measure 1pb_3_updown_1 Date: 2026428:1712 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 952.56 s Mass = 100.000 mg data_number = 1185 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1600 -1.3736 244.3433 245.7169 251.0385 1.8855 -1.3708 244.4019 245.7727 251.0295 2.7545 -1.3665 244.4818 245.8483 251.0096 3.5313 -1.3628 244.5464 245.9092 250.9965 4.3490 -1.3593 244.6031 245.9623 250.9917 5.1780 -1.3557 244.6707 246.0264 250.9828 5.9445 -1.3516 244.7276 246.0791 250.9814 6.8033 -1.3479 244.7954 246.1433 250.9713 7.5700 -1.3452 244.8580 246.2032 250.9683 8.3885 -1.3425 244.9274 246.2700 250.9636 9.1960 -1.3399 244.9992 246.3391 250.9622 9.9830 -1.3368 245.0761 246.4129 250.9664 10.8110 -1.3338 245.1519 246.4857 250.9807 11.5775 -1.3313 245.2171 246.5485 250.9925 12.4373 -1.3293 245.2916 246.6209 250.9992 13.2038 -1.3263 245.3643 246.6905 251.0203 14.0215 -1.3221 245.4398 246.7619 251.0442 14.8290 -1.3188 245.5207 246.8395 251.0775 15.6160 -1.3146 245.5873 246.9019 251.1075 16.4448 -1.3108 245.6524 246.9632 251.1470 17.2115 -1.3063 245.7213 247.0276 251.1819 18.0498 -1.3019 245.7915 247.0934 251.2295 18.8060 -1.2970 245.8550 247.1521 251.2752 19.6648 -1.2922 245.9316 247.2238 251.3295 20.4320 -1.2895 245.9980 247.2875 251.3825 21.2705 -1.2859 246.0684 247.3543 251.4553 22.0575 -1.2805 246.1392 247.4197 251.5183 22.8548 -1.2756 246.2086 247.4842 251.5884 23.6828 -1.2721 246.2797 247.5518 251.6738 24.4500 -1.2701 246.3485 247.6186 251.7496 25.2783 -1.2664 246.4225 247.6889 251.8355 26.0345 -1.2627 246.4831 247.7458 251.9234 26.8933 -1.2590 246.5464 247.8054 252.0173 27.6495 -1.2574 246.6076 247.8650 252.1037 28.4785 -1.2555 246.6770 247.9325 252.2008 29.2655 -1.2520 246.7452 247.9973 252.3008 30.0628 -1.2489 246.8282 248.0771 252.4040 30.8908 -1.2464 246.8980 248.1444 252.5177 31.6473 -1.2438 246.9564 248.2002 252.6214 32.4760 -1.2415 247.0290 248.2705 252.7381 33.2425 -1.2389 247.0990 248.3379 252.8451 34.0910 -1.2361 247.1712 248.4073 252.9635 34.8575 -1.2329 247.2340 248.4669 253.0696 35.6855 -1.2301 247.2997 248.5298 253.1891 36.4735 -1.2266 247.3630 248.5896 253.3075 37.2708 -1.2245 247.4327 248.6572 253.4332 38.0988 -1.2222 247.5061 248.7283 253.5681 38.8550 -1.2198 247.5722 248.7920 253.6910 39.6838 -1.2179 247.6472 248.8651 253.8231 40.4505 -1.2152 247.7115 248.9267 253.9491 41.2990 -1.2128 247.7856 248.9984 254.0868 42.0758 -1.2112 247.8524 249.0635 254.2254 42.8935 -1.2090 247.9246 249.1336 254.3597 43.7010 -1.2066 247.9924 249.1990 254.4969 44.4888 -1.2039 248.0574 249.2614 254.6257 45.3785 -1.1995 248.1347 249.3342 254.7725 46.3193 -1.1964 248.2110 249.4074 254.9228 47.0755 -1.1950 248.2742 249.4692 255.0341 47.9445 -1.1914 248.3567 249.5481 255.1765 48.7018 -1.1903 248.4211 249.6114 255.2980 49.5195 -1.1898 248.4862 249.6760 255.4255 50.3270 -1.1892 248.5706 249.7598 255.5509 51.1140 -1.1872 248.6506 249.8378 255.6850 51.9420 -1.1869 248.7199 249.9068 255.8171 52.7090 -1.1860 248.7911 249.9771 255.9395 53.5683 -1.1853 248.8706 250.0559 256.0898 54.3040 -1.1853 248.9332 250.1185 256.2114 55.1525 -1.1841 249.0096 250.1937 256.3473 55.9600 -1.1822 249.0848 250.2669 256.4778 56.7685 -1.1808 249.1655 250.3463 256.6077 57.5658 -1.1796 249.2442 250.4238 256.7316 58.3630 -1.1786 249.3094 250.4881 256.8611 59.1808 -1.1778 249.3898 250.5676 256.9961 59.9575 -1.1773 249.4605 250.6378 257.1214 60.8070 -1.1765 249.5356 250.7121 257.2660 61.5735 -1.1755 249.6025 250.7780 257.3833 62.4015 -1.1757 249.6767 250.8524 257.5165 63.1988 -1.1746 249.7493 250.9239 257.6343 63.9960 -1.1746 249.8233 250.9979 257.7534 64.8145 -1.1747 249.8949 251.0696 257.8787 65.5915 -1.1737 249.9642 251.1379 258.0023 66.4400 -1.1722 250.0429 251.2151 258.1362 67.1758 -1.1714 250.1196 251.2911 258.2529 68.0345 -1.1692 250.1954 251.3646 258.3904 68.8013 -1.1687 250.2592 251.4279 258.5059 69.6300 -1.1680 250.3297 251.4977 258.6349 70.4170 -1.1666 250.4034 251.5700 258.7699 71.2245 -1.1648 250.4818 251.6466 258.8937 72.0423 -1.1641 250.5577 251.7218 259.0144 72.8088 -1.1631 250.6334 251.7965 259.1315 73.6685 -1.1621 250.7250 251.8871 259.2634 74.4350 -1.1620 250.8053 251.9673 259.3825 75.2630 -1.1606 250.8864 252.0471 259.5180 76.0500 -1.1597 250.9599 252.1196 259.6424 76.8580 -1.1595 251.0375 252.1970 259.7773 77.6763 -1.1578 251.1191 252.2769 259.9016 78.4428 -1.1572 251.1918 252.3490 260.0217 79.3015 -1.1569 251.2714 252.4283 260.1557 80.0683 -1.1560 251.3405 252.4965 260.2792 80.8970 -1.1557 251.4207 252.5764 260.4195 81.6840 -1.1555 251.5008 252.6563 260.5626 82.4915 -1.1559 251.5789 252.7348 260.7063 83.3093 -1.1564 251.6625 252.8190 260.8457 84.0758 -1.1554 251.7383 252.8937 260.9796 84.9355 -1.1543 251.8266 252.9809 261.1296 85.7020 -1.1548 251.9036 253.0584 261.2574 86.5300 -1.1548 251.9947 253.1495 261.3949 87.3273 -1.1541 252.0786 253.2327 261.5373 88.1250 -1.1534 252.1551 253.3085 261.6701 88.9535 -1.1539 252.2411 253.3950 261.8185 89.7200 -1.1544 252.3138 253.4681 261.9553 90.5685 -1.1548 252.3895 253.5444 262.1026 91.3350 -1.1555 252.4708 253.6264 262.2348 92.1538 -1.1557 252.5661 253.7218 262.3730 92.9510 -1.1562 252.6518 253.8080 262.5069 93.7380 -1.1570 252.7299 253.8869 262.6557 94.5353 -1.1572 252.8147 253.9718 262.8002 95.3333 -1.1574 252.8898 254.0473 262.9359 96.1513 -1.1569 252.9681 254.1250 263.0713 96.9075 -1.1572 253.0478 254.2050 263.2015 97.7663 -1.1553 253.1364 254.2917 263.3462 98.5328 -1.1552 253.2149 254.3701 263.4785 99.3515 -1.1562 253.3041 254.4603 263.6132 100.1488 -1.1558 253.3857 254.5415 263.7470 100.9460 -1.1549 253.4643 254.6193 263.8814 101.7638 -1.1554 253.5519 254.7073 264.0240 102.5303 -1.1562 253.6332 254.7894 264.1525 103.3893 -1.1557 253.7237 254.8795 264.3067 104.1155 -1.1569 253.8094 254.9663 264.4267 104.9845 -1.1565 253.9102 255.0668 264.5724 105.7408 -1.1573 253.9938 255.1511 264.6988 106.5585 -1.1581 254.0739 255.2319 264.8303 107.3660 -1.1590 254.1598 255.3187 264.9704 108.1533 -1.1606 254.2476 255.4082 265.0970 108.9718 -1.1618 254.3440 255.5058 265.2311 109.7485 -1.1620 254.4343 255.5963 265.3641 110.5970 -1.1620 254.5304 255.6924 265.5014 111.3635 -1.1633 254.6142 255.7775 265.6315 112.1920 -1.1638 254.7023 255.8661 265.7679 112.9898 -1.1653 254.7845 255.9499 265.8949 113.7870 -1.1656 254.8722 256.0378 266.0302 114.6048 -1.1670 254.9639 256.1309 266.1641 115.3815 -1.1683 255.0530 256.2212 266.2835 116.2303 -1.1692 255.1441 256.3133 266.4192 116.9665 -1.1691 255.2270 256.3961 266.5433 117.8255 -1.1698 255.3219 256.4916 266.6884 118.5920 -1.1697 255.4006 256.5702 266.8107 119.4098 -1.1694 255.4927 256.6622 266.9458 120.2070 -1.1692 255.5828 256.7519 267.0764 121.0043 -1.1689 255.6733 256.8422 267.1981 121.8330 -1.1701 255.7620 256.9321 267.3306 122.5895 -1.1719 255.8505 257.0224 267.4552 123.4585 -1.1734 255.9457 257.1191 267.5921 124.2150 -1.1737 256.0254 257.1991 267.7120 125.0438 -1.1745 256.1195 257.2939 267.8455 125.8410 -1.1728 256.2112 257.3840 267.9748 126.6383 -1.1733 256.3053 257.4787 268.1063 127.4355 -1.1737 256.3993 257.5730 268.2265 128.2430 -1.1759 256.4917 257.6676 268.3486 129.0615 -1.1767 256.5818 257.7585 268.4819 129.8385 -1.1783 256.6674 257.8457 268.6034 130.6870 -1.1786 256.7679 257.9465 268.7344 131.4535 -1.1791 256.8564 258.0355 268.8495 132.2815 -1.1816 256.9594 258.1411 268.9807 133.0490 -1.1827 257.0455 258.2282 269.1019 133.8770 -1.1843 257.1382 258.3225 269.2297 134.6640 -1.1861 257.2396 258.4258 269.3435 135.4715 -1.1871 257.3421 258.5293 269.4774 136.2895 -1.1883 257.4388 258.6271 269.6031 137.0568 -1.1894 257.5243 258.7137 269.7192 137.9155 -1.1905 257.6248 258.8153 269.8584 138.6820 -1.1909 257.7127 258.9036 269.9738 139.5100 -1.1918 257.8217 259.0135 270.0897 140.2973 -1.1930 257.9190 259.1120 270.2082 141.1055 -1.1932 258.0094 259.2027 270.3326 141.9233 -1.1937 258.1083 259.3020 270.4438 142.6898 -1.1936 258.1961 259.3897 270.5609 143.5485 -1.1935 258.2927 259.4862 270.6952 144.2848 -1.1930 258.3838 259.5768 270.8084 145.1440 -1.1936 258.4903 259.6840 270.9358 145.9003 -1.1945 258.5809 259.7753 271.0419 146.7385 -1.1962 258.6785 259.8747 271.1696 147.5260 -1.1961 258.7725 259.9687 271.2951 148.3238 -1.1965 258.8661 260.0626 271.4138 149.1518 -1.1973 258.9678 260.1651 271.5363 149.9183 -1.1990 259.0714 260.2704 271.6433 150.7770 -1.1995 259.1789 260.3784 271.7615 151.5335 -1.1997 259.2756 260.4753 271.8737 152.3725 -1.1995 259.3744 260.5740 271.9916 153.1595 -1.1994 259.4705 260.6699 272.1073 153.9568 -1.2005 259.5721 260.7726 272.2310 154.7848 -1.2006 259.6775 260.8782 272.3490 155.5513 -1.2000 259.7739 260.9739 272.4618 156.4008 -1.2006 259.8725 261.0731 272.5764 157.1673 -1.2014 259.9686 261.1699 272.6861 157.9850 -1.2021 260.0627 261.2648 272.8054 158.7413 -1.2028 260.1474 261.3502 272.9105 159.5795 -1.2040 260.2502 261.4542 273.0395 160.3668 -1.2051 260.3473 261.5523 273.1512 161.1545 -1.2061 260.4489 261.6550 273.2659 161.9825 -1.2058 260.5532 261.7591 273.3871 162.7490 -1.2054 260.6484 261.8538 273.4845 163.5975 -1.2055 260.7496 261.9551 273.6038 164.3640 -1.2063 260.8467 262.0530 273.7101 165.1818 -1.2078 260.9514 262.1592 273.8264 165.9790 -1.2088 261.0555 262.2643 273.9442 166.7773 -1.2103 261.1562 262.3665 274.0621 167.5950 -1.2104 261.2594 262.4698 274.1887 168.3615 -1.2103 261.3523 262.5626 274.3019 169.2203 -1.2112 261.4634 262.6747 274.4303 169.9765 -1.2103 261.5603 262.7706 274.5399 170.8045 -1.2109 261.6792 262.8902 274.6692 171.6023 -1.2124 261.7859 262.9983 274.7958 172.4000 -1.2133 261.8873 263.1006 274.9237 173.1973 -1.2126 262.0008 263.2135 275.0542 173.9945 -1.2136 262.1042 263.3178 275.1825 174.8123 -1.2145 262.2101 263.4246 275.3187 175.5685 -1.2146 262.3088 263.5234 275.4411 176.4378 -1.2173 262.4229 263.6402 275.5881 177.1948 -1.2199 262.5184 263.7382 275.7198 178.0228 -1.2226 262.6216 263.8442 275.8542 178.8200 -1.2257 262.7329 263.9587 275.9846 179.6173 -1.2284 262.8309 264.0593 276.1164 180.4453 -1.2293 262.9309 264.1602 276.2468 181.2015 -1.2312 263.0253 264.2565 276.3714 182.0705 -1.2309 263.1393 264.3702 276.5193 182.8275 -1.2318 263.2427 264.4745 276.6498 183.6558 -1.2329 263.3470 264.5799 276.7822 184.4530 -1.2348 263.4605 264.6953 276.9170 185.2503 -1.2373 263.5710 264.8083 277.0562 186.0783 -1.2390 263.6810 264.9201 277.2013 186.8345 -1.2403 263.7847 265.0249 277.3343 187.7045 -1.2410 263.9005 265.1415 277.4847 188.4608 -1.2421 263.9960 265.2382 277.6072 189.2888 -1.2432 264.1038 265.3470 277.7448 190.0860 -1.2438 264.2047 265.4486 277.8757 190.8833 -1.2449 264.3129 265.5577 278.0083 191.7120 -1.2461 264.4239 265.6700 278.1560 192.4685 -1.2459 264.5343 265.7802 278.2845 193.3375 -1.2458 264.6584 265.9042 278.4262 194.0938 -1.2466 264.7541 266.0007 278.5461 194.9218 -1.2476 264.8538 266.1013 278.6891 195.7190 -1.2492 264.9567 266.2058 278.8218 196.5173 -1.2503 265.0684 266.3187 278.9575 197.3453 -1.2522 265.1742 266.4265 279.1060 198.1015 -1.2539 265.2754 266.5293 279.2345 198.9705 -1.2529 265.3897 266.6426 279.3716 199.7268 -1.2540 265.4848 266.7387 279.4983 200.5555 -1.2547 265.5941 266.8487 279.6359 201.3530 -1.2545 265.7055 266.9601 279.7616 202.1503 -1.2550 265.8124 267.0674 279.8888 202.9783 -1.2555 265.9232 267.1787 280.0323 203.7345 -1.2564 266.0254 267.2818 280.1521 204.6040 -1.2577 266.1468 267.4045 280.2898 205.3608 -1.2579 266.2545 267.5124 280.4084 206.1888 -1.2574 266.3702 267.6276 280.5411 206.9860 -1.2574 266.4757 267.7331 280.6641 207.7833 -1.2577 266.5809 267.8386 280.7895 208.6113 -1.2598 266.6969 267.9567 280.9205 209.3675 -1.2614 266.8057 268.0671 281.0387 210.2368 -1.2607 266.9272 268.1878 281.1855 210.9938 -1.2602 267.0298 268.2900 281.3104 211.8218 -1.2611 267.1415 268.4025 281.4448 212.6190 -1.2617 267.2462 268.5079 281.5774 213.4163 -1.2628 267.3568 268.6195 281.7064 214.2445 -1.2632 267.4821 268.7453 281.8432 215.0015 -1.2655 267.5847 268.8502 281.9633 215.8705 -1.2659 267.6997 268.9656 282.1000 216.6268 -1.2663 267.8076 269.0739 282.2304 217.4548 -1.2676 267.9209 269.1884 282.3638 218.2525 -1.2694 268.0326 269.3020 282.4919 219.0503 -1.2715 268.1429 269.4144 282.6131 219.8373 -1.2720 268.2520 269.5240 282.7434 220.6345 -1.2740 268.3599 269.6339 282.8843 221.4625 -1.2751 268.4772 269.7523 283.0152 222.2188 -1.2756 268.5893 269.8649 283.1398 223.0785 -1.2771 268.7029 269.9801 283.2742 223.8348 -1.2782 268.7964 270.0745 283.3863 224.6628 -1.2793 268.9098 270.1891 283.5071 225.4293 -1.2803 269.0202 270.3006 283.6213 226.2470 -1.2813 269.1427 270.4241 283.7419 227.0448 -1.2832 269.2598 270.5431 283.8601 227.8425 -1.2844 269.3802 270.6646 283.9858 228.6603 -1.2853 269.4941 270.7794 284.1219 229.4268 -1.2852 269.6048 270.8900 284.2502 230.2548 -1.2860 269.7303 271.0163 284.3811 231.0215 -1.2876 269.8441 271.1317 284.4925 231.8708 -1.2878 269.9652 271.2530 284.6239 232.6373 -1.2889 270.0747 271.3637 284.7374 233.4653 -1.2901 270.1882 271.4783 284.8568 234.2625 -1.2894 270.2981 271.5875 284.9750 235.0495 -1.2874 270.4131 271.7005 285.0889 235.8878 -1.2857 270.5383 271.8240 285.2154 236.6445 -1.2855 270.6446 271.9301 285.3239 237.4730 -1.2857 270.7536 272.0394 285.4459 238.2395 -1.2842 270.8658 272.1499 285.5657 239.0983 -1.2843 270.9820 272.2663 285.6950 239.8648 -1.2851 271.0900 272.3751 285.8077 240.6825 -1.2884 271.2216 272.5100 285.9250 241.4905 -1.2891 271.3389 272.6280 286.0425 242.2780 -1.2912 271.4481 272.7393 286.1558 243.1060 -1.2946 271.5637 272.8583 286.2762 243.8725 -1.2981 271.6754 272.9735 286.3878 244.7005 -1.3010 271.7963 273.0974 286.5122 245.4670 -1.3027 271.9020 273.2047 286.6253 246.3155 -1.3056 272.0258 273.3314 286.7446 247.0933 -1.3079 272.1432 273.4512 286.8583 247.9110 -1.3097 272.2649 273.5746 286.9762 248.7083 -1.3109 272.3844 273.6954 287.0914 249.5055 -1.3131 272.5079 273.8210 287.2052 250.3335 -1.3139 272.6248 273.9387 287.3300 251.0898 -1.3163 272.7368 274.0531 287.4492 251.9493 -1.3162 272.8629 274.1791 287.5776 252.7160 -1.3181 272.9711 274.2892 287.6891 253.5440 -1.3191 273.0927 274.4118 287.8191 254.3310 -1.3215 273.2136 274.5351 287.9369 255.1385 -1.3238 273.3297 274.6535 288.0678 255.9570 -1.3256 273.4521 274.7777 288.2072 256.7238 -1.3272 273.5616 274.8888 288.3268 257.5825 -1.3282 273.6930 275.0212 288.4579 258.3490 -1.3289 273.8055 275.1345 288.5935 259.1770 -1.3305 273.9233 275.2538 288.7399 259.9640 -1.3308 274.0376 275.3684 288.8725 260.7725 -1.3321 274.1574 275.4895 289.0091 261.5903 -1.3342 274.2816 275.6158 289.1395 262.3568 -1.3358 274.3898 275.7256 289.2676 263.2155 -1.3363 274.5220 275.8583 289.4109 263.9823 -1.3384 274.6357 275.9741 289.5387 264.8110 -1.3396 274.7573 276.0969 289.6735 265.5980 -1.3411 274.8853 276.2263 289.8077 266.4055 -1.3432 275.0058 276.3490 289.9511 267.2028 -1.3461 275.1222 276.4683 290.0929 268.0000 -1.3456 275.2468 276.5925 290.2382 268.8180 -1.3465 275.3636 276.7102 290.3768 269.5955 -1.3487 275.4741 276.8229 290.5028 270.4440 -1.3497 275.5956 276.9453 290.6527 271.2105 -1.3513 275.7130 277.0643 290.7924 272.0385 -1.3533 275.8304 277.1838 290.9382 272.8363 -1.3552 275.9497 277.3049 291.0671 273.6340 -1.3575 276.0720 277.4294 291.1999 274.4518 -1.3599 276.1870 277.5469 291.3463 275.2285 -1.3635 276.2983 277.6618 291.4752 276.0878 -1.3658 276.4317 277.7975 291.6147 276.8548 -1.3677 276.5519 277.9196 291.7406 277.6725 -1.3699 276.6817 278.0516 291.8789 278.4800 -1.3718 276.8025 278.1743 292.0139 279.2670 -1.3733 276.9284 278.3017 292.1418 280.0953 -1.3741 277.0549 278.4290 292.2734 280.8625 -1.3753 277.1693 278.5446 292.4099 281.7213 -1.3755 277.2980 278.6735 292.5578 282.4775 -1.3759 277.4123 278.7882 292.6807 283.3055 -1.3759 277.5321 278.9080 292.8228 284.0928 -1.3768 277.6471 279.0239 292.9611 284.8805 -1.3791 277.7692 279.1483 293.0967 285.7085 -1.3827 277.8981 279.2808 293.2343 286.4750 -1.3851 278.0181 279.4032 293.3519 287.2928 -1.3876 278.1382 279.5257 293.4870 288.0598 -1.3885 278.2546 279.6430 293.6217 288.9190 -1.3884 278.3932 279.7816 293.7623 289.6753 -1.3897 278.5049 279.8946 293.8889 290.5033 -1.3904 278.6299 280.0203 294.0161 291.2903 -1.3909 278.7481 280.1390 294.1450 292.0883 -1.3924 278.8671 280.2595 294.2677 292.9165 -1.3948 278.9964 280.3912 294.3959 293.6728 -1.3949 279.1017 280.4967 294.5195 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