DTA measure 1pb_3_updown_meres Date: 2026428:159 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 902.70 s Mass = 1148.100 mg data_number = 1123 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1590 -0.3409 197.9580 198.2988 247.9310 1.9460 -0.3378 198.2190 198.5568 247.9409 2.7740 -0.3344 198.4894 198.8239 247.9532 3.5410 -0.3311 198.7346 199.0657 247.9726 4.4003 -0.3285 199.0137 199.3422 247.9848 5.1360 -0.3264 199.2498 199.5763 248.0006 5.9845 -0.3241 199.5175 199.8416 248.0155 6.7613 -0.3220 199.7828 200.1048 248.0377 7.5798 -0.3206 200.0424 200.3630 248.0589 8.3773 -0.3195 200.2975 200.6170 248.0743 9.1745 -0.3182 200.5654 200.8836 248.1005 10.0025 -0.3154 200.8353 201.1506 248.1312 10.7695 -0.3129 201.0907 201.4035 248.1669 11.6185 -0.3109 201.3744 201.6853 248.2002 12.3953 -0.3096 201.6210 201.9305 248.2285 13.2130 -0.3075 201.8802 202.1877 248.2674 14.0103 -0.3031 202.1261 202.4293 248.3110 14.8085 -0.3008 202.3801 202.6809 248.3689 15.6365 -0.2990 202.6458 202.9448 248.4275 16.4030 -0.2956 202.8873 203.1829 248.4822 17.2515 -0.2937 203.1554 203.4491 248.5446 18.0288 -0.2906 203.4122 203.7027 248.6048 18.8470 -0.2883 203.6619 203.9502 248.6752 19.6443 -0.2867 203.9018 204.1885 248.7471 20.4415 -0.2847 204.1462 204.4310 248.8230 21.2695 -0.2834 204.4034 204.6869 248.9148 22.0368 -0.2808 204.6361 204.9169 249.0034 22.8855 -0.2781 204.9057 205.1838 249.0987 23.6623 -0.2741 205.1468 205.4210 249.1925 24.4800 -0.2731 205.3962 205.6693 249.3019 25.2570 -0.2706 205.6351 205.9058 249.4018 26.0755 -0.2682 205.8857 206.1539 249.5125 26.8830 -0.2669 206.1246 206.3915 249.6236 27.6700 -0.2660 206.3671 206.6331 249.7357 28.4980 -0.2645 206.6176 206.8822 249.8576 29.2650 -0.2628 206.8474 207.1103 249.9742 30.1243 -0.2612 207.1090 207.3701 250.1104 30.8908 -0.2594 207.3374 207.5968 250.2424 31.7085 -0.2579 207.5906 207.8485 250.3715 32.5160 -0.2562 207.8358 208.0920 250.5118 33.3035 -0.2545 208.0692 208.3237 250.6474 34.1320 -0.2523 208.3167 208.5691 250.7903 34.8985 -0.2507 208.5440 208.7947 250.9269 35.7573 -0.2480 208.7957 209.0437 251.0681 36.5238 -0.2472 209.0194 209.2666 251.2062 37.3420 -0.2458 209.2622 209.5079 251.3529 38.1500 -0.2453 209.4981 209.7434 251.5100 38.9370 -0.2447 209.7300 209.9747 251.6553 39.7548 -0.2427 209.9775 210.2202 251.7995 40.5315 -0.2416 210.2104 210.4520 251.9398 41.3810 -0.2407 210.4499 210.6905 252.1037 42.1373 -0.2403 210.6607 210.9010 252.2400 42.9755 -0.2390 210.8992 211.1382 252.3852 43.7625 -0.2362 211.1275 211.3636 252.5350 44.5495 -0.2362 211.3575 211.5937 252.6825 45.3783 -0.2352 211.6016 211.8368 252.8321 46.1450 -0.2353 211.8228 212.0581 252.9789 46.9935 -0.2343 212.0728 212.3071 253.1311 47.7600 -0.2328 212.2938 212.5266 253.2762 48.5880 -0.2301 212.5331 212.7632 253.4188 49.3450 -0.2298 212.7547 212.9845 253.5548 50.1733 -0.2302 212.9982 213.2284 253.7088 50.9705 -0.2301 213.2223 213.4524 253.8522 51.7575 -0.2302 213.4383 213.6685 253.9950 52.5858 -0.2308 213.6752 213.9060 254.1565 53.3530 -0.2313 213.8873 214.1186 254.3016 54.2015 -0.2326 214.1260 214.3586 254.4612 54.9783 -0.2324 214.3478 214.5802 254.5993 55.7960 -0.2328 214.5741 214.8068 254.7591 56.5835 -0.2333 214.7941 215.0274 254.9041 57.3915 -0.2328 215.0213 215.2541 255.0446 58.2093 -0.2324 215.2600 215.4924 255.1957 58.9758 -0.2331 215.4777 215.7108 255.3346 59.8345 -0.2326 215.7128 215.9454 255.4880 60.5915 -0.2324 215.9246 216.1570 255.6216 61.4198 -0.2334 216.1465 216.3799 255.7699 62.2170 -0.2342 216.3812 216.6154 255.9201 63.0143 -0.2355 216.5992 216.8347 256.0701 63.8423 -0.2374 216.8341 217.0715 256.2269 64.5985 -0.2378 217.0405 217.2783 256.3697 65.4275 -0.2388 217.2634 217.5022 256.5230 66.1940 -0.2394 217.4758 217.7152 256.6674 67.0425 -0.2402 217.7133 217.9536 256.8237 67.8193 -0.2406 217.9241 218.1646 256.9600 68.6378 -0.2418 218.1477 218.3895 257.1070 69.4353 -0.2438 218.3622 218.6060 257.2495 70.2325 -0.2451 218.5699 218.8150 257.3946 71.0605 -0.2453 218.7873 219.0326 257.5411 71.8270 -0.2453 218.9863 219.2316 257.6826 72.6760 -0.2467 219.2171 219.4639 257.8364 73.4533 -0.2478 219.4271 219.6749 257.9669 74.2710 -0.2494 219.6526 219.9021 258.1064 75.0375 -0.2511 219.8593 220.1103 258.2438 75.8660 -0.2522 220.0816 220.3339 258.3848 76.6638 -0.2521 220.3005 220.5526 258.5213 77.4610 -0.2514 220.5222 220.7735 258.6460 78.2788 -0.2532 220.7482 221.0015 258.7761 79.0555 -0.2555 220.9613 221.2168 258.8956 79.9050 -0.2591 221.1999 221.4589 259.0229 80.6715 -0.2624 221.4060 221.6684 259.1401 81.4995 -0.2652 221.6190 221.8841 259.2638 82.2968 -0.2659 221.8345 222.1004 259.3857 83.0945 -0.2668 222.0578 222.3245 259.5132 83.8820 -0.2697 222.2677 222.5374 259.6338 84.6895 -0.2721 222.4758 222.7479 259.7514 85.5073 -0.2746 222.6828 222.9574 259.8698 86.2738 -0.2763 222.8757 223.1520 259.9776 87.1335 -0.2788 223.1013 223.3801 260.1078 87.9000 -0.2817 223.3009 223.5826 260.2265 88.7280 -0.2850 223.5143 223.7993 260.3583 89.5155 -0.2869 223.7167 224.0036 260.4813 90.3235 -0.2889 223.9320 224.2209 260.5988 91.1413 -0.2908 224.1527 224.4435 260.7201 91.9078 -0.2922 224.3543 224.6465 260.8304 92.7665 -0.2946 224.5740 224.8686 260.9498 93.5338 -0.2979 224.7773 225.0752 261.0572 94.3620 -0.3007 224.9975 225.2982 261.1704 95.1490 -0.3035 225.2027 225.5062 261.2839 95.9565 -0.3043 225.4148 225.7190 261.4149 96.7745 -0.3048 225.6255 225.9302 261.5421 97.5418 -0.3067 225.8249 226.1316 261.6594 98.3698 -0.3089 226.0413 226.3502 261.7924 99.1363 -0.3112 226.2482 226.5595 261.9050 99.9950 -0.3131 226.4729 226.7860 262.0321 100.7518 -0.3163 226.6751 226.9914 262.1450 101.5905 -0.3195 226.8894 227.2090 262.2617 102.3775 -0.3216 227.0938 227.4154 262.3934 103.1748 -0.3239 227.2968 227.6207 262.5060 104.0033 -0.3253 227.5176 227.8429 262.6386 104.7600 -0.3257 227.7164 228.0421 262.7503 105.6085 -0.3278 227.9283 228.2561 262.8781 106.3853 -0.3301 228.1359 228.4660 263.0095 107.2030 -0.3330 228.3465 228.6795 263.1440 107.9900 -0.3343 228.5446 228.8789 263.2764 108.7883 -0.3366 228.7495 229.0862 263.4118 109.6060 -0.3398 228.9611 229.3009 263.5532 110.3725 -0.3433 229.1496 229.4930 263.6811 111.2210 -0.3455 229.3483 229.6938 263.8397 111.9568 -0.3485 229.5298 229.8783 263.9761 112.8165 -0.3513 229.7492 230.1005 264.1265 113.6035 -0.3546 229.9456 230.3002 264.2870 114.4008 -0.3565 230.1443 230.5008 264.4332 115.1980 -0.3590 230.3472 230.7062 264.5746 115.9953 -0.3612 230.5428 230.9040 264.7157 116.8138 -0.3627 230.7518 231.1145 264.8604 117.5805 -0.3631 230.9590 231.3221 264.9992 118.4393 -0.3668 231.1763 231.5432 265.1535 119.2058 -0.3696 231.3611 231.7306 265.2904 120.0235 -0.3723 231.5667 231.9390 265.4345 120.8318 -0.3742 231.7638 232.1380 265.5757 121.6190 -0.3760 231.9588 232.3347 265.7252 122.4470 -0.3787 232.1689 232.5476 265.8690 123.2135 -0.3811 232.3638 232.7449 266.0007 124.0625 -0.3847 232.5655 232.9502 266.1452 124.8295 -0.3880 232.7497 233.1377 266.2773 125.6575 -0.3913 232.9595 233.3508 266.4221 126.4548 -0.3948 233.1589 233.5537 266.5647 127.2520 -0.3973 233.3542 233.7514 266.7067 128.0705 -0.4003 233.5521 233.9524 266.8483 128.8475 -0.4023 233.7377 234.1401 266.9854 129.6653 -0.4048 233.9372 234.3419 267.1250 130.4318 -0.4064 234.1208 234.5272 267.2599 131.2905 -0.4078 234.3369 234.7447 267.4106 132.0578 -0.4101 234.5183 234.9284 267.5466 132.8860 -0.4132 234.7234 235.1366 267.6948 133.6730 -0.4157 234.9244 235.3401 267.8298 134.4805 -0.4190 235.1306 235.5496 267.9758 135.2985 -0.4221 235.3258 235.7479 268.1252 136.0658 -0.4235 235.5029 235.9264 268.2578 136.9245 -0.4268 235.7070 236.1338 268.4086 137.6910 -0.4290 235.8927 236.3216 268.5410 138.5190 -0.4327 236.0931 236.5258 268.6878 139.3065 -0.4358 236.2737 236.7095 268.8143 140.1145 -0.4383 236.4564 236.8947 268.9499 140.9323 -0.4423 236.6527 237.0950 269.0945 141.6988 -0.4455 236.8426 237.2881 269.2292 142.5575 -0.4486 237.0428 237.4914 269.3680 143.3240 -0.4521 237.2185 237.6706 269.4875 144.1530 -0.4553 237.4164 237.8717 269.6270 144.9400 -0.4583 237.5983 238.0566 269.7535 145.7475 -0.4615 237.7988 238.2604 269.8789 146.5653 -0.4648 237.9978 238.4626 270.0030 147.3318 -0.4672 238.1834 238.6507 270.1224 148.1915 -0.4702 238.3811 238.8513 270.2656 148.9580 -0.4740 238.5626 239.0366 270.3802 149.7860 -0.4759 238.7657 239.2416 270.5047 150.5730 -0.4786 238.9498 239.4284 270.6202 151.3810 -0.4819 239.1387 239.6206 270.7282 152.1993 -0.4856 239.3417 239.8273 270.8393 152.9658 -0.4873 239.5299 240.0172 270.9458 153.8245 -0.4893 239.7387 240.2280 271.0689 154.5920 -0.4913 239.9158 240.4071 271.1701 155.4200 -0.4929 240.1123 240.6052 271.2874 156.2070 -0.4955 240.3036 240.7991 271.3988 157.0145 -0.4984 240.4895 240.9879 271.5185 157.8330 -0.5020 240.6808 241.1829 271.6362 158.5998 -0.5047 240.8665 241.3711 271.7503 159.4585 -0.5064 241.0671 241.5735 271.8706 160.2250 -0.5086 241.2459 241.7545 271.9749 161.0530 -0.5104 241.4414 241.9518 272.1016 161.8405 -0.5118 241.6317 242.1435 272.2199 162.6485 -0.5149 241.8276 242.3425 272.3367 163.4663 -0.5180 242.0078 242.5258 272.4580 164.2328 -0.5207 242.1806 242.7013 272.5802 165.0915 -0.5250 242.3836 242.9086 272.7227 165.8583 -0.5276 242.5614 243.0889 272.8359 166.6868 -0.5301 242.7496 243.2797 272.9583 167.4740 -0.5317 242.9433 243.4750 273.0913 168.2713 -0.5348 243.1264 243.6611 273.2185 169.0890 -0.5382 243.3068 243.8450 273.3526 169.8555 -0.5401 243.4808 244.0208 273.4810 170.7040 -0.5408 243.6750 244.2158 273.6163 171.4705 -0.5424 243.8535 244.3959 273.7341 172.2985 -0.5465 244.0477 244.5942 273.8671 173.0555 -0.5497 244.2176 244.7673 273.9897 173.8735 -0.5533 244.3961 244.9494 274.1233 174.6810 -0.5569 244.5772 245.1341 274.2569 175.4680 -0.5589 244.7578 245.3167 274.3802 176.2858 -0.5602 244.9397 245.4998 274.5128 177.0628 -0.5614 245.1229 245.6844 274.6507 177.9120 -0.5646 245.3154 245.8800 274.7853 178.6478 -0.5678 245.4846 246.0524 274.9065 179.5065 -0.5721 245.6730 246.2450 275.0468 180.2628 -0.5752 245.8489 246.4241 275.1702 181.0908 -0.5777 246.0368 246.6144 275.3019 181.8880 -0.5797 246.2207 246.8004 275.4398 182.6863 -0.5825 246.3999 246.9824 275.5708 183.5040 -0.5848 246.5768 247.1615 275.7105 184.2705 -0.5876 246.7494 247.3370 275.8441 185.1293 -0.5895 246.9407 247.5301 275.9932 185.8650 -0.5925 247.1150 247.7075 276.1226 186.7135 -0.5936 247.3090 247.9026 276.2663 187.4908 -0.5951 247.4805 248.0756 276.3866 188.3090 -0.5973 247.6592 248.2565 276.5200 189.1063 -0.5993 247.8388 248.4381 276.6509 189.9035 -0.6024 248.0221 248.6245 276.7840 190.7315 -0.6058 248.2041 248.8099 276.9251 191.4878 -0.6090 248.3714 248.9804 277.0501 192.3475 -0.6124 248.5638 249.1762 277.1877 193.1140 -0.6147 248.7335 249.3482 277.3149 193.9420 -0.6182 248.9153 249.5335 277.4538 194.6983 -0.6214 249.0950 249.7164 277.5800 195.5365 -0.6251 249.2825 249.9076 277.7132 196.3235 -0.6270 249.4546 250.0817 277.8480 197.1208 -0.6300 249.6328 250.2628 277.9872 197.9498 -0.6327 249.8118 250.4445 278.1281 198.7163 -0.6346 249.9730 250.6076 278.2543 199.5750 -0.6359 250.1631 250.7990 278.3931 200.3313 -0.6371 250.3286 250.9658 278.5182 201.1695 -0.6391 250.5093 251.1484 278.6511 201.9565 -0.6405 250.6799 251.3204 278.7823 202.7645 -0.6433 250.8640 251.5073 278.9095 203.5520 -0.6459 251.0412 251.6871 279.0338 204.3595 -0.6485 251.2296 251.8781 279.1605 205.1773 -0.6506 251.4054 252.0560 279.2967 205.9438 -0.6526 251.5674 252.2200 279.4222 206.8025 -0.6550 251.7522 252.4072 279.5649 207.5693 -0.6586 251.9241 252.5827 279.6887 208.3980 -0.6613 252.1072 252.7685 279.8218 209.1850 -0.6625 252.2684 252.9309 279.9522 209.9925 -0.6651 252.4437 253.1089 280.0877 210.8103 -0.6681 252.6259 253.2941 280.2191 211.5768 -0.6709 252.7920 253.4630 280.3435 212.4360 -0.6747 252.9763 253.6510 280.4800 213.2030 -0.6766 253.1388 253.8154 280.6025 214.0310 -0.6790 253.3262 254.0052 280.7347 214.8078 -0.6817 253.5005 254.1822 280.8610 215.6358 -0.6838 253.6812 254.3650 280.9912 216.4023 -0.6858 253.8449 254.5307 281.1139 217.2305 -0.6880 254.0246 254.7126 281.2462 218.0285 -0.6915 254.2010 254.8925 281.3706 218.8155 -0.6947 254.3670 255.0617 281.5058 219.6538 -0.6972 254.5462 255.2434 281.6435 220.4100 -0.6992 254.7086 255.4078 281.7571 221.2688 -0.7006 254.8948 255.5954 281.8925 222.0353 -0.7015 255.0628 255.7643 282.0171 222.8643 -0.7038 255.2440 255.9477 282.1498 223.6615 -0.7049 255.4223 256.1272 282.2699 224.4485 -0.7061 255.6046 256.3106 282.3971 225.2868 -0.7091 255.7868 256.4959 282.5280 226.0430 -0.7111 255.9565 256.6676 282.6520 226.9023 -0.7136 256.1421 256.8557 282.7910 227.6693 -0.7153 256.3113 257.0266 282.9040 228.4973 -0.7164 256.4810 257.1974 283.0351 229.2945 -0.7183 256.6432 257.3615 283.1694 230.0815 -0.7197 256.8181 257.5378 283.2965 230.9198 -0.7203 257.0009 257.7212 283.4322 231.6763 -0.7214 257.1582 257.8796 283.5462 232.5255 -0.7233 257.3332 258.0565 283.6839 233.3023 -0.7268 257.5073 258.2341 283.8043 234.1200 -0.7294 257.6837 258.4131 283.9317 234.9070 -0.7308 257.8497 258.5805 284.0550 235.7043 -0.7320 258.0282 258.7601 284.1770 236.5220 -0.7331 258.1951 258.9282 284.3035 237.2895 -0.7336 258.3624 259.0960 284.4171 238.1483 -0.7335 258.5513 259.2847 284.5498 238.9045 -0.7332 258.7055 259.4387 284.6658 239.7325 -0.7334 258.8795 259.6129 284.7883 240.5298 -0.7331 259.0522 259.7853 284.9055 241.3168 -0.7334 259.2143 259.9477 285.0240 242.1455 -0.7329 259.3900 260.1229 285.1481 242.9123 -0.7330 259.5554 260.2884 285.2602 243.7608 -0.7334 259.7447 260.4781 285.3847 244.5273 -0.7333 259.9023 260.6355 285.5076 245.3553 -0.7328 260.0753 260.8081 285.6350 246.1115 -0.7336 260.2340 260.9676 285.7502 246.9405 -0.7347 260.4056 261.1403 285.8756 247.7378 -0.7337 260.5786 261.3124 285.9925 248.5350 -0.7340 260.7569 261.4908 286.1134 249.3528 -0.7335 260.9359 261.6695 286.2295 250.1295 -0.7339 261.1099 261.8437 286.3501 250.9785 -0.7428 261.2836 262.0265 286.4751 251.7455 -0.7595 261.4451 262.2046 286.6063 252.5735 -0.7677 261.6272 262.3949 286.7458 253.3708 -0.7640 261.8048 262.5687 286.8751 254.1578 -0.7600 261.9643 262.7243 287.0028 254.9863 -0.7559 262.1454 262.9013 287.1400 255.7533 -0.7538 262.3173 263.0711 287.2742 256.6120 -0.7503 262.5011 263.2514 287.4181 257.3683 -0.7476 262.6606 263.4083 287.5388 258.2065 -0.7459 262.8357 263.5816 287.6785 258.9938 -0.7439 262.9957 263.7396 287.8229 259.7918 -0.7424 263.1577 263.9001 287.9685 260.6198 -0.7423 263.3239 264.0662 288.1161 261.3863 -0.7423 263.4873 264.2296 288.2510 262.2450 -0.7407 263.6718 264.4125 288.3988 263.0013 -0.7401 263.8303 264.5704 288.5408 263.8403 -0.7408 264.0133 264.7541 288.6911 264.6275 -0.7410 264.1827 264.9237 288.8387 265.4248 -0.7424 264.3474 265.0898 288.9808 266.2528 -0.7419 264.5221 265.2640 289.1255 267.0193 -0.7396 264.6869 265.4265 289.2583 267.8780 -0.7393 264.8628 265.6022 289.4042 268.6353 -0.7407 265.0251 265.7658 289.5426 269.4735 -0.7424 265.2138 265.9561 289.6935 270.2605 -0.7433 265.3836 266.1269 289.8372 271.0578 -0.7449 265.5395 266.2844 289.9810 271.8858 -0.7451 265.6982 266.4433 290.1216 272.6523 -0.7444 265.8482 266.5925 290.2654 273.5113 -0.7454 266.0310 266.7764 290.4273 274.2683 -0.7467 266.1849 266.9316 290.5711 275.1065 -0.7473 266.3559 267.1033 290.7199 275.8935 -0.7493 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