DTA measure 1proba lehules Date: 2026428:1610 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.89 s Mass = 1148.100 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4635 -0.9748 232.1898 233.1646 203.8761 4.0888 -0.9719 232.0748 233.0467 203.7115 5.6938 -0.9665 231.9540 232.9205 203.5586 7.3044 -0.9597 231.8412 232.8009 203.4069 8.9091 -0.9540 231.7148 232.6688 203.2652 10.5036 -0.9504 231.5893 232.5398 203.1268 12.1091 -0.9456 231.4642 232.4098 202.9864 13.7193 -0.9396 231.3469 232.2865 202.8514 15.3291 -0.9352 231.2323 232.1675 202.7315 16.9503 -0.9331 231.1098 232.0429 202.6183 18.5601 -0.9305 230.9793 231.9098 202.5139 20.1598 -0.9294 230.8642 231.7936 202.4210 21.7548 -0.9278 230.7487 231.6766 202.3392 23.3651 -0.9254 230.6179 231.5433 202.2747 24.9545 -0.9236 230.4965 231.4201 202.1954 26.5495 -0.9211 230.3674 231.2885 202.1189 28.1599 -0.9174 230.2506 231.1681 202.0578 29.7800 -0.9163 230.1273 231.0436 202.0025 31.3643 -0.9130 229.9990 230.9120 201.9630 32.9751 -0.9112 229.8704 230.7816 201.9249 34.5799 -0.9085 229.7464 230.6548 201.8924 36.1846 -0.9073 229.6192 230.5265 201.8662 37.7900 -0.9059 229.4919 230.3978 201.8584 39.3900 -0.9060 229.3657 230.2717 201.8602 40.9999 -0.9062 229.2392 230.1453 201.8668 42.6203 -0.9065 229.1084 230.0148 201.8775 44.2309 -0.9067 228.9832 229.8898 201.9095 45.8356 -0.9067 228.8521 229.7588 201.9536 47.4408 -0.9144 228.7233 229.6376 201.9963 49.0513 -0.9193 228.6029 229.5221 202.0467 50.6406 -0.9211 228.4755 229.3966 202.1096 52.2515 -0.9203 228.3488 229.2691 202.1825 53.8563 -0.9190 228.2220 229.1410 202.2482 55.4815 -0.9178 228.0868 229.0046 202.3313 57.0871 -0.9173 227.9571 228.8745 202.4094 58.6920 -0.9173 227.8287 228.7460 202.4979 60.3021 -0.9185 227.6991 228.6176 202.5990 61.9076 -0.9195 227.5787 228.4982 202.7020 63.5021 -0.9207 227.4563 228.3770 202.8021 65.1076 -0.9207 227.3246 228.2454 202.9094 66.7178 -0.9215 227.2070 228.1285 203.0167 68.3379 -0.9232 227.0963 228.0195 203.1417 69.9431 -0.9249 226.9758 227.9006 203.2776 71.5535 -0.9272 226.8453 227.7726 203.3988 73.1583 -0.9289 226.7252 227.6541 203.5272 74.7688 -0.9310 226.5872 227.5182 203.6672 76.3585 -0.9341 226.4718 227.4059 203.8061 77.9735 -0.9382 226.3567 227.2949 203.9487 79.5788 -0.9433 226.2421 227.1854 204.0912 81.2045 -0.9464 226.1425 227.0889 204.2309 82.8041 -0.9495 226.0316 226.9811 204.3872 84.4091 -0.9523 225.9184 226.8706 204.5325 85.9993 -0.9552 225.8073 226.7624 204.6757 87.5989 -0.9568 225.6990 226.6558 204.8386 89.2036 -0.9605 225.5818 226.5423 205.0086 90.8090 -0.9633 225.4721 226.4354 205.1698 92.4090 -0.9644 225.3661 226.3305 205.3214 94.0291 -0.9677 225.2700 226.2377 205.4785 95.6295 -0.9704 225.1689 226.1393 205.6310 97.2345 -0.9744 225.0717 226.0461 205.7893 98.8241 -0.9787 224.9851 225.9637 205.9488 100.4348 -0.9820 224.9007 225.8827 206.1112 102.0395 -0.9853 224.7979 225.7832 206.2842 103.6494 -0.9893 224.6827 225.6721 206.4482 105.2550 -0.9919 224.5774 225.5693 206.6169 106.8701 -0.9950 224.4682 225.4632 206.7920 108.4800 -0.9979 224.3742 225.3721 206.9732 110.0853 -0.9981 224.2851 225.2832 207.1486 111.6956 -1.0016 224.1952 225.1968 207.3218 113.3004 -1.0054 224.1071 225.1125 207.5031 114.8853 -1.0073 224.0167 225.0239 207.6809 116.4955 -1.0109 223.9246 224.9355 207.8539 118.1003 -1.0146 223.8430 224.8576 208.0185 119.7256 -1.0189 223.7540 224.7729 208.1888 121.3313 -1.0208 223.6771 224.6979 208.3602 122.9360 -1.0217 223.6109 224.6326 208.5211 124.5460 -1.0237 223.5385 224.5622 208.7041 126.1516 -1.0268 223.4596 224.4865 208.8720 127.7615 -1.0290 223.3917 224.4207 209.0422 129.3664 -1.0333 223.3228 224.3561 209.2156 130.9925 -1.0343 223.2575 224.2918 209.3978 132.5973 -1.0385 223.1929 224.2314 209.5750 134.2075 -1.0421 223.1174 224.1595 209.7567 135.8129 -1.0476 223.0489 224.0965 209.9343 137.4176 -1.0494 222.9796 224.0290 210.1073 139.0275 -1.0490 222.9080 223.9570 210.2812 140.6331 -1.0531 222.8521 223.9052 210.4486 142.2739 -1.0576 222.8057 223.8632 210.6226 143.8945 -1.0592 222.7550 223.8142 210.7935 145.5049 -1.0601 222.7022 223.7623 210.9625 147.1096 -1.0603 222.6592 223.7195 211.1352 148.6945 -1.0626 222.6122 223.6748 211.3043 150.2945 -1.0656 222.5580 223.6235 211.4777 151.9146 -1.0674 222.5085 223.5759 211.6628 153.5094 -1.0683 222.4560 223.5243 211.8465 155.1149 -1.0705 222.4099 223.4804 212.0193 156.7248 -1.0729 222.3737 223.4466 212.2105 158.3244 -1.0751 222.3333 223.4083 212.3993 159.9249 -1.0743 222.2899 223.3642 212.5761 161.5503 -1.0751 222.2557 223.3308 212.7524 163.1504 -1.0772 222.2124 223.2896 212.9304 164.7556 -1.0798 222.1829 223.2627 213.1200 166.3655 -1.0820 222.1450 223.2269 213.3051 167.9703 -1.0828 222.1134 223.1962 213.4855 169.5811 -1.0823 222.0879 223.1702 213.6631 171.1859 -1.0829 222.0649 223.1478 213.8450 172.7906 -1.0847 222.0345 223.1191 214.0159 174.4115 -1.0850 222.0083 223.0933 214.1926 176.0165 -1.0846 222.0021 223.0867 214.3742 177.6264 -1.0865 221.9774 223.0638 214.5455 179.2166 -1.0877 221.9529 223.0407 214.7185 180.8266 -1.0886 221.9387 223.0273 214.8978 182.4321 -1.0895 221.9319 223.0214 215.0811 184.0371 -1.0924 221.9123 223.0047 215.2758 185.6470 -1.0917 221.8951 222.9868 215.4816 187.2681 -1.0905 221.8783 222.9688 215.6810 188.8626 -1.0904 221.8590 222.9494 215.8754 190.4678 -1.0904 221.8453 222.9357 216.0696 192.0783 -1.0898 221.8406 222.9305 216.2650 193.6831 -1.0903 221.8377 222.9280 216.4729 195.2888 -1.0920 221.8334 222.9254 216.6841 196.8986 -1.0922 221.8259 222.9181 216.8765 198.5034 -1.0906 221.8246 222.9153 217.0693 200.1296 -1.0890 221.8312 222.9202 217.2633 201.7190 -1.0904 221.8398 222.9301 217.4570 203.3290 -1.0918 221.8497 222.9416 217.6556 204.9346 -1.0929 221.8514 222.9443 217.8560 206.5394 -1.0924 221.8613 222.9537 218.0505 208.1493 -1.0907 221.8748 222.9655 218.2423 209.7601 -1.0910 221.8897 222.9807 218.4271 211.3700 -1.0897 221.9035 222.9932 218.6119 212.9543 -1.0895 221.9182 223.0078 218.7984 214.5700 -1.0897 221.9306 223.0203 218.9796 216.1750 -1.0892 221.9552 223.0444 219.1428 217.7695 -1.0882 221.9760 223.0642 219.3203 219.3750 -1.0870 222.0049 223.0920 219.5017 220.9800 -1.0862 222.0294 223.1156 219.6846 222.5644 -1.0862 222.0706 223.1568 219.8817 224.1700 -1.0845 222.0951 223.1796 220.0701 225.7748 -1.0837 222.1162 223.1999 220.2689 227.3955 -1.0821 222.1454 223.2275 220.4584 229.0006 -1.0834 222.1752 223.2585 220.6413 230.6105 -1.0838 222.2024 223.2862 220.8341 232.2153 -1.0824 222.2339 223.3163 221.0323 233.8208 -1.0821 222.2609 223.3430 221.2291 235.4104 -1.0823 222.2822 223.3645 221.4149 237.0255 -1.0795 222.3168 223.3963 221.6051 238.6311 -1.0789 222.3587 223.4376 221.7960 240.2513 -1.0782 222.4134 223.4917 221.9942 241.8611 -1.0781 222.4645 223.5425 222.1912 243.4666 -1.0761 222.5120 223.5880 222.3803 245.0768 -1.0742 222.5481 223.6223 222.5786 246.6816 -1.0726 222.5982 223.6708 222.7865 248.2924 -1.0709 222.6553 223.7262 222.9823 249.8971 -1.0702 222.6988 223.7690 223.1652 251.5176 -1.0699 222.7431 223.8130 223.3472 253.1281 -1.0699 222.8058 223.8756 223.5331 254.7329 -1.0683 222.8653 223.9336 223.7171 256.3428 -1.0676 222.9267 223.9944 223.9039 257.9484 -1.0662 222.9850 224.0512 224.0883 259.5481 -1.0644 223.0359 224.1002 224.2670 261.1531 -1.0628 223.0842 224.1470 224.4458 262.7638 -1.0618 223.1506 224.2124 224.6334 264.3839 -1.0602 223.2299 224.2902 224.8121 265.9895 -1.0590 223.3001 224.3591 225.0040 267.5995 -1.0564 223.3697 224.4260 225.1894 269.2043 -1.0547 223.4491 224.5038 225.3799 270.8151 -1.0529 223.5026 224.5554 225.5849 272.4199 -1.0519 223.5624 224.6143 225.7976 274.0145 -1.0501 223.6471 224.6971 225.9981 275.6201 -1.0483 223.7182 224.7665 226.2023 277.2351 -1.0450 223.7831 224.8281 226.4298 278.8351 -1.0446 223.8584 224.9030 226.6457 280.4405 -1.0430 223.9344 224.9774 226.8629 282.0401 -1.0409 224.0151 225.0559 227.0707 283.6453 -1.0389 224.1059 225.1448 227.2827 285.2301 -1.0372 224.1809 225.2181 227.4970 286.8349 -1.0332 224.2511 225.2844 227.7077 288.4404 -1.0311 224.3313 225.3624 227.9279 290.0454 -1.0305 224.4189 225.4494 228.1518 291.6505 -1.0286 224.5012 225.5298 228.3645 293.2661 -1.0274 224.5800 225.6073 228.5745 294.8763 -1.0266 224.6580 225.6847 228.7836 296.4664 -1.0238 224.7449 225.7687 228.9772 298.0763 -1.0209 224.8345 225.8553 229.1826 299.6810 -1.0204 224.9275 225.9479 229.3945 301.2865 -1.0206 225.0214 226.0420 229.6034 302.8966 -1.0203 225.1179 226.1382 229.8156 304.5019 -1.0191 225.2076 226.2267 230.0203 306.1276 -1.0177 225.3043 226.3220 230.2208 307.7170 -1.0158 225.3872 226.4031 230.4163 309.3278 -1.0140 225.4901 226.5041 230.6053 310.9326 -1.0108 225.5915 226.6023 230.8051 312.5379 -1.0101 225.7009 226.7110 231.0105 314.1483 -1.0091 225.8003 226.8093 231.2099 315.7530 -1.0080 225.8967 226.9047 231.4071 317.3638 -1.0073 226.0096 227.0169 231.5969 318.9840 -1.0045 226.1095 227.1140 231.7915 320.5990 -1.0020 226.2161 227.2180 231.9657 322.2046 -0.9991 226.3078 227.3069 232.1528 323.7993 -0.9974 226.4154 227.4128 232.3395 325.4043 -0.9965 226.5334 227.5299 232.5154 327.0149 -0.9915 226.6367 227.6282 232.6833 328.6248 -0.9902 226.7370 227.7272 232.8493 330.2299 -0.9892 226.8398 227.8289 233.0256 331.8558 -0.9873 226.9525 227.9399 233.2135 333.4605 -0.9847 227.0837 228.0684 233.4067 335.0710 -0.9844 227.2093 228.1938 233.5865 336.6761 -0.9822 227.3207 228.3029 233.7644 338.2860 -0.9793 227.4381 228.4174 233.9455 339.8864 -0.9776 227.5574 228.5350 234.1319 341.4863 -0.9761 227.6840 228.6601 234.3320 343.1014 -0.9745 227.7980 228.7725 234.5343 344.7070 -0.9724 227.9200 228.8924 234.7463 346.3066 -0.9707 228.0482 229.0190 234.9361 347.9014 -0.9683 228.1747 229.1430 235.1303 349.5120 -0.9674 228.2986 229.2660 235.3317 351.1168 -0.9657 228.4194 229.3851 235.5335 352.7220 -0.9647 228.5368 229.5016 235.7483 354.3273 -0.9617 228.6602 229.6219 235.9767 355.9320 -0.9587 228.7834 229.7422 236.1787 357.5224 -0.9569 228.9093 229.8662 236.3810 359.1425 -0.9547 229.0437 229.9985 236.5858 360.7480 -0.9522 229.1648 230.1170 236.7953 362.3530 -0.9509 229.2880 230.2389 236.9940 363.9629 -0.9502 229.4207 230.3709 237.1977 365.5685 -0.9486 229.5565 230.5051 237.4045 367.1631 -0.9468 229.6828 230.6296 237.6124 368.7680 -0.9436 229.8271 230.7708 237.8217 370.3788 -0.9424 229.9542 230.8966 238.0294 371.9989 -0.9409 230.0783 231.0192 238.2256 373.6044 -0.9393 230.2103 231.1497 238.4270 375.1991 -0.9383 230.3478 231.2862 238.6313 376.8039 -0.9347 230.4886 231.4233 238.8187 378.4146 -0.9332 230.6275 231.5607 239.0233 380.0195 -0.9319 230.7688 231.7007 239.2148 381.6301 -0.9315 230.9185 231.8500 239.3998 383.2249 -0.9307 231.0598 231.9905 239.6014 384.8348 -0.9287 231.2008 232.1295 239.7977 386.4559 -0.9282 231.3398 232.2679 239.9916 388.0606 -0.9266 231.4706 232.3971 240.1831 389.6559 -0.9266 231.6116 232.5382 240.3734 391.2609 -0.9255 231.7659 232.6915 240.5679 392.8713 -0.9232 231.9205 232.8437 240.7516 394.4765 -0.9230 232.0769 232.9998 240.9408 396.0864 -0.9230 232.2201 233.1431 241.1290 397.6919 -0.9211 232.3607 233.2818 241.3195 399.3123 -0.9198 232.5119 233.4317 241.5169 400.9221 -0.9193 232.6679 233.5872 241.7219 402.5278 -0.9171 232.8166 233.7337 241.9200 404.1378 -0.9145 232.9614 233.8759 242.1131 405.7374 -0.9137 233.1206 234.0343 242.3245 407.3223 -0.9120 233.2624 234.1744 242.5280 408.9325 -0.9101 233.4135 234.3236 242.7417 410.5321 -0.9101 233.5608 234.4708 242.9625 412.1481 -0.9093 233.7139 234.6231 243.1938 413.7478 -0.9081 233.8725 234.7807 243.4058 415.3530 -0.9080 234.0277 234.9357 243.6219 416.9583 -0.9065 234.1793 235.0858 243.8461 418.5681 -0.9050 234.3369 235.2419 244.0879 420.1630 -0.9056 234.4868 235.3924 244.3220 421.7735 -0.9050 234.6428 235.5478 244.5560 423.3629 -0.9036 234.7809 235.6845 244.7707 424.9734 -0.9027 234.9438 235.8465 244.9932 426.5939 -0.9027 235.1176 236.0203 245.2174 428.1986 -0.9022 235.2779 236.1801 245.4431 429.8140 -0.9014 235.4356 236.3370 245.6714 431.4194 -0.9015 235.5901 236.4916 245.8959 433.0293 -0.9011 235.7501 236.6512 246.1176 434.6348 -0.9015 235.9095 236.8110 246.3421 436.2449 -0.9018 236.0812 236.9830 246.5725 437.8651 -0.9011 236.2485 237.1496 246.8011 439.4759 -0.9006 236.4161 237.3167 247.0241 441.0806 -0.9009 236.5774 237.4783 247.2518 442.6860 -0.9023 236.7397 237.6421 247.4640 444.2963 -0.9027 236.9095 237.8123 247.6787 445.9010 -0.9026 237.0843 237.9869 247.8960 447.5115 -0.9019 237.2480 238.1499 248.1023 449.1320 -0.9046 237.4132 238.3178 248.3069 450.7419 -0.9050 237.5791 238.4841 248.5126 452.3525 -0.9056 237.7558 238.6614 248.7270 453.9626 -0.9061 237.9152 238.8213 248.9340 455.5674 -0.9077 238.0881 238.9958 249.1434 457.1729 -0.9074 238.2640 239.1714 249.3467 458.7830 -0.9062 238.4418 239.3480 249.5449 460.4033 -0.9062 238.6195 239.5257 249.7443 462.0140 -0.9075 238.7936 239.7012 249.9420 463.6188 -0.9078 238.9704 239.8782 250.1542 465.2286 -0.9097 239.1406 240.0503 250.3540 466.8340 -0.9102 239.3080 240.2182 250.5576 468.4391 -0.9116 239.4883 240.3999 250.7463 470.0439 -0.9115 239.6675 240.5790 250.9452 471.6590 -0.9127 239.8371 240.7498 251.1472 473.2595 -0.9142 240.0223 240.9365 251.3450 474.8694 -0.9153 240.1977 241.1130 251.5545 476.4639 -0.9169 240.3682 241.2851 251.7615 478.0539 -0.9180 240.5388 241.4568 251.9611 479.6641 -0.9182 240.7298 241.6480 252.1620 481.2638 -0.9179 240.9184 241.8363 252.3626 482.8685 -0.9179 241.1021 242.0200 252.5687 484.4948 -0.9176 241.2814 242.1989 252.7591 486.0944 -0.9197 241.4626 242.3823 252.9495 487.7044 -0.9204 241.6345 242.5549 253.1447 489.3100 -0.9213 241.8093 242.7306 253.3479 490.9096 -0.9229 241.9884 242.9112 253.5400 492.5195 -0.9232 242.1647 243.0879 253.7257 494.1253 -0.9223 242.3527 243.2750 253.9154 495.7351 -0.9235 242.5485 243.4719 254.1074 497.3401 -0.9231 242.7249 243.6480 254.2998 498.9456 -0.9242 242.9096 243.8338 254.4889 500.5555 -0.9245 243.0973 244.0218 254.6746 502.1608 -0.9263 243.2719 244.1983 254.8503 503.7711 -0.9248 243.4506 244.3754 255.0458 505.3759 -0.9245 243.6540 244.5785 255.2236 506.9864 -0.9246 243.8514 244.7760 255.3999 508.6069 -0.9247 244.0328 244.9576 255.5921 510.2116 -0.9255 244.2195 245.1450 255.7779 511.8225 -0.9270 244.3958 245.3228 255.9555 513.4273 -0.9279 244.5738 245.5017 256.1416 515.0371 -0.9254 244.7581 245.6836 256.3253 516.6429 -0.9245 244.9522 245.8767 256.5060 518.2528 -0.9273 245.1543 246.0816 256.6923 519.8575 -0.9283 245.3505 246.2788 256.8743 521.4633 -0.9314 245.5392 246.4707 257.0663 523.0731 -0.9337 245.7310 246.6647 257.2628 524.6781 -0.9356 245.9153 246.8509 257.4681 526.2888 -0.9370 246.1063 247.0434 257.6618 527.8935 -0.9381 246.2996 247.2377 257.8714 529.5034 -0.9407 246.4848 247.4254 258.0811 531.1090 -0.9428 246.6772 247.6200 258.2986 532.7344 -0.9436 246.8595 247.8031 258.5154 534.3393 -0.9442 247.0657 248.0099 258.7302 535.9398 -0.9459 247.2669 248.2128 258.9569 537.5343 -0.9481 247.4551 248.4032 259.1899 539.1445 -0.9490 247.6446 248.5935 259.4198 540.7294 -0.9498 247.8245 248.7743 259.6424 542.3290 -0.9534 248.0047 248.9581 259.8673 543.9390 -0.9537 248.1845 249.1382 260.0952 545.5549 -0.9565 248.3896 249.3461 260.3121 547.1596 -0.9565 248.5817 249.5383 260.5303 548.7543 -0.9592 248.7783 249.7375 260.7527 550.3599 -0.9607 248.9853 249.9461 260.9708 551.9646 -0.9636 249.1782 250.1418 261.1934 553.5696 -0.9665 249.3716 250.3381 261.4088 555.1751 -0.9684 249.5634 250.5318 261.6219 556.7799 -0.9705 249.7563 250.7268 261.8341 558.4003 -0.9734 249.9704 250.9438 262.0518 560.0109 -0.9753 250.1637 251.1390 262.2610 561.6618 -0.9793 250.3581 251.3373 262.4833 563.2619 -0.9813 250.5545 251.5358 262.6958 564.8876 -0.9838 250.7520 251.7359 262.9202 566.6000 -0.9871 250.9550 251.9421 263.1433 568.2360 -0.9909 251.1583 252.1492 263.3536 569.8413 -0.9909 251.3553 252.3461 263.5686 571.4460 -0.9925 251.5500 252.5425 263.7866 573.0568 -0.9949 251.7581 252.7530 263.9989 574.6770 -0.9966 251.9659 252.9625 264.2161 576.2869 -0.9977 252.1642 253.1619 264.4317 577.8924 -1.0011 252.3750 253.3761 264.6460 579.4974 -1.0027 252.5700 253.5728 264.8514 581.1073 -1.0031 252.7530 253.7560 265.0616 582.7129 -1.0043 252.9553 253.9597 265.2733 584.3229 -1.0080 253.1601 254.1681 265.4880 586.0206 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