DTA measure 1gyors Date: 20241015:159 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.66 s Mass = 951 mg data_number = 1266 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2670 -1.0380 263.1470 264.1850 263.5702 2.0888 -1.0379 263.1495 264.1874 263.5530 2.9113 -1.0347 263.1589 264.1936 263.5632 3.6725 -1.0314 263.1638 264.1952 263.5721 4.5250 -1.0317 263.1356 264.1673 263.5723 5.2868 -1.0331 263.1579 264.1910 263.5743 6.1088 -1.0300 263.1858 264.2158 263.5783 6.9310 -1.0276 263.1614 264.1891 263.5729 7.6925 -1.0282 263.1864 264.2146 263.5797 8.5450 -1.0293 263.1885 264.2177 263.5891 9.3370 -1.0299 263.2006 264.2305 263.5852 10.1285 -1.0328 263.2158 264.2486 263.6053 10.9508 -1.0309 263.1787 264.2097 263.6233 11.7125 -1.0305 263.1870 264.2175 263.6519 12.5648 -1.0273 263.2006 264.2280 263.7139 13.3568 -1.0276 263.2165 264.2441 263.7320 14.1485 -1.0281 263.2247 264.2527 263.7544 14.9708 -1.0244 263.2219 264.2463 263.8007 15.7325 -1.0303 263.2310 264.2613 263.8372 16.5845 -1.0294 263.2212 264.2506 263.8907 17.3770 -1.0293 263.2160 264.2453 263.9582 18.1685 -1.0317 263.2434 264.2751 264.0021 18.9905 -1.0317 263.2354 264.2671 264.0627 19.7825 -1.0343 263.2275 264.2618 264.1108 20.6045 -1.0324 263.2435 264.2759 264.1837 21.3965 -1.0340 263.2526 264.2866 264.2843 22.1885 -1.0339 263.2641 264.2980 264.3585 23.0405 -1.0295 263.2656 264.2951 264.4715 23.8025 -1.0282 263.2660 264.2942 264.5636 24.6253 -1.0308 263.2576 264.2884 264.6587 25.4665 -1.0324 263.2545 264.2869 264.7649 26.4065 -1.0339 263.2666 264.3005 264.8787 27.2585 -1.0311 263.2891 264.3202 265.0123 28.0505 -1.0343 263.2858 264.3201 265.1258 28.8425 -1.0375 263.2914 264.3289 265.2510 29.6653 -1.0368 263.2970 264.3337 265.3583 30.4260 -1.0410 263.2964 264.3375 265.4725 31.2733 -1.0434 263.3038 264.3472 265.6258 32.0323 -1.0445 263.3274 264.3720 265.7588 32.8510 -1.0450 263.3222 264.3672 265.9012 33.6693 -1.0475 263.3299 264.3774 266.0324 34.4273 -1.0495 263.3327 264.3822 266.1733 35.2768 -1.0518 263.3583 264.4102 266.3469 36.0343 -1.0512 263.3550 264.4062 266.4797 36.8523 -1.0527 263.3489 264.4016 266.6245 37.6705 -1.0571 263.3591 264.4162 266.7867 38.4280 -1.0570 263.3762 264.4332 266.9402 39.2773 -1.0621 263.3808 264.4430 267.1081 40.0655 -1.0660 263.3905 264.4565 267.2583 40.8550 -1.0666 263.4124 264.4790 267.4396 41.6745 -1.0676 263.4061 264.4736 267.6125 42.4343 -1.0728 263.4251 264.4980 267.7411 43.2843 -1.0753 263.4131 264.4885 267.9197 44.0743 -1.0791 263.4375 264.5166 268.1014 44.8645 -1.0811 263.4493 264.5304 268.2621 45.6848 -1.0836 263.4563 264.5398 268.4189 46.4440 -1.0858 263.4800 264.5659 268.5839 47.2948 -1.0882 263.4869 264.5751 268.7563 48.0850 -1.0904 263.4914 264.5818 268.9181 48.8753 -1.0961 263.5170 264.6131 269.0735 49.6970 -1.0981 263.5367 264.6349 269.2496 50.4585 -1.1010 263.5574 264.6584 269.4107 51.3110 -1.1042 263.5534 264.6576 269.5690 52.0728 -1.1070 263.5538 264.6608 269.7150 52.8948 -1.1089 263.5628 264.6717 269.8502 53.6870 -1.1151 263.5765 264.6916 270.0016 54.4785 -1.1189 263.6058 264.7247 270.1709 55.3310 -1.1245 263.6309 264.7553 270.3172 56.0928 -1.1267 263.6303 264.7570 270.4510 56.9148 -1.1293 263.6509 264.7802 270.6060 57.7070 -1.1328 263.6662 264.7989 270.7491 58.4985 -1.1375 263.6837 264.8212 270.8904 59.3508 -1.1415 263.7017 264.8431 271.0685 60.1125 -1.1426 263.7168 264.8593 271.1922 60.9348 -1.1484 263.7221 264.8704 271.3375 61.7270 -1.1514 263.7406 264.8921 271.4621 62.5185 -1.1537 263.7706 264.9243 271.5967 63.3408 -1.1578 263.8042 264.9619 271.7328 64.1325 -1.1649 263.8165 264.9813 271.8560 64.9545 -1.1698 263.8389 265.0087 271.9974 65.7468 -1.1718 263.8542 265.0259 272.1302 66.5385 -1.1709 263.8676 265.0386 272.2429 67.3608 -1.1737 263.8931 265.0668 272.3879 68.1525 -1.1720 263.9086 265.0806 272.5101 68.9745 -1.1738 263.9291 265.1030 272.6446 69.7665 -1.1859 263.9529 265.1388 272.7585 70.5585 -1.1923 263.9691 265.1614 272.8865 71.3805 -1.1963 263.9835 265.1798 273.0096 72.1425 -1.2001 264.0153 265.2154 273.1318 72.9945 -1.2036 264.0612 265.2647 273.2321 73.7865 -1.2025 264.0753 265.2778 273.3588 74.5785 -1.2077 264.0867 265.2944 273.4898 75.4005 -1.2108 264.1251 265.3359 273.6130 76.1625 -1.2139 264.1346 265.3485 273.7238 77.1658 -1.2172 264.1761 265.3933 273.8666 78.0085 -1.2218 264.2071 265.4289 274.0125 78.8010 -1.2252 264.2260 265.4512 274.1091 79.6238 -1.2267 264.2473 265.4741 274.2066 80.3858 -1.2302 264.2734 265.5037 274.3130 81.2380 -1.2382 264.2980 265.5362 274.4371 81.9998 -1.2395 264.3129 265.5523 274.5585 82.8218 -1.2422 264.3364 265.5787 274.6569 83.6440 -1.2446 264.3584 265.6030 274.7546 84.4055 -1.2500 264.4020 265.6520 274.8701 85.2580 -1.2539 264.4290 265.6830 274.9804 86.0500 -1.2553 264.4647 265.7200 275.0896 86.8425 -1.2565 264.4922 265.7486 275.2075 87.6650 -1.2601 264.5312 265.7914 275.3100 88.4265 -1.2657 264.5708 265.8365 275.4080 89.2790 -1.2684 264.5709 265.8393 275.5515 90.0408 -1.2737 264.6130 265.8867 275.6206 90.8628 -1.2781 264.6415 265.9195 275.7440 91.6848 -1.2850 264.6661 265.9511 275.8456 92.4465 -1.2873 264.6901 265.9774 275.9628 93.2993 -1.2883 264.7433 266.0315 276.0747 94.0615 -1.2910 264.7815 266.0725 276.1935 94.8810 -1.2914 264.8086 266.1000 276.3053 95.6990 -1.2943 264.8318 266.1261 276.4196 96.4570 -1.2986 264.8667 266.1653 276.5115 97.3050 -1.3022 264.8952 266.1974 276.6401 98.0633 -1.3076 264.9288 266.2365 276.7501 98.8820 -1.3092 264.9738 266.2831 276.8753 99.7010 -1.3114 265.0205 266.3319 276.9769 100.4600 -1.3100 265.0321 266.3421 277.0826 101.3080 -1.3147 265.0588 266.3735 277.2076 102.0663 -1.3201 265.0772 266.3973 277.3082 102.8850 -1.3239 265.1071 266.4310 277.4294 103.7035 -1.3248 265.1571 266.4819 277.5548 104.4620 -1.3265 265.1937 266.5202 277.6669 105.3105 -1.3293 265.2162 266.5455 277.7820 106.0990 -1.3306 265.2871 266.6177 277.9132 106.8880 -1.3319 265.3334 266.6653 278.0446 107.7068 -1.3355 265.3542 266.6897 278.1803 108.4968 -1.3374 265.3903 266.7277 278.3073 109.3165 -1.3419 265.4077 266.7496 278.4432 110.1085 -1.3453 265.4351 266.7805 278.5626 110.9003 -1.3479 265.5114 266.8593 278.6900 111.7205 -1.3491 265.5650 266.9141 278.8242 112.5115 -1.3515 265.5846 266.9361 278.9692 113.3335 -1.3540 265.6012 266.9552 279.0905 114.1255 -1.3599 265.6426 267.0025 279.2159 114.9175 -1.3698 265.7042 267.0740 279.3278 115.7395 -1.3692 265.7430 267.1122 279.4666 116.5315 -1.3729 265.7871 267.1601 279.6077 117.3535 -1.3737 265.8193 267.1930 279.7281 118.1240 -1.3794 265.8572 267.2367 279.8607 118.9455 -1.3857 265.9120 267.2977 279.9766 119.7675 -1.3896 265.9397 267.3293 280.1154 120.5295 -1.3923 265.9830 267.3752 280.2328 121.3815 -1.3916 266.0452 267.4368 280.3657 122.1435 -1.3968 266.0968 267.4936 280.5151 122.9675 -1.4030 266.1298 267.5328 280.6509 123.7895 -1.4019 266.1668 267.5687 280.7927 124.5515 -1.4079 266.2076 267.6155 280.9093 125.4035 -1.4093 266.2539 267.6631 281.0615 126.1653 -1.4129 266.3018 267.7147 281.1718 126.9875 -1.4158 266.3384 267.7542 281.2846 127.8575 -1.4180 266.3829 267.8009 281.4524 128.7933 -1.4248 266.4305 267.8553 281.6044 129.6148 -1.4276 266.4696 267.8971 281.7426 130.4073 -1.4312 266.5348 267.9660 281.8760 131.1988 -1.4344 266.5898 268.0243 282.0098 132.0213 -1.4374 266.6534 268.0908 282.1218 132.8128 -1.4392 266.6907 268.1298 282.2127 133.6348 -1.4432 266.7200 268.1632 282.3580 134.4270 -1.4458 266.7714 268.2173 282.4988 135.2185 -1.4493 266.8163 268.2656 282.6424 136.0710 -1.4511 266.8831 268.3342 282.7767 136.8328 -1.4545 266.9232 268.3777 282.8944 137.6548 -1.4574 266.9890 268.4464 283.0151 138.4470 -1.4590 267.0094 268.4684 283.1355 139.2385 -1.4609 267.0673 268.5283 283.2503 140.0910 -1.4631 267.1219 268.5850 283.3895 140.8528 -1.4645 267.1634 268.6279 283.5041 141.6748 -1.4698 267.2046 268.6743 283.6333 142.4668 -1.4743 267.2766 268.7509 283.7631 143.2588 -1.4750 267.3307 268.8057 283.8912 144.1118 -1.4777 267.3736 268.8513 284.0154 144.8735 -1.4838 267.4411 268.9249 284.1408 145.6958 -1.4827 267.4976 268.9803 284.2690 146.5180 -1.4861 267.5392 269.0254 284.4080 147.2805 -1.4928 267.5809 269.0737 284.5341 148.1325 -1.4934 267.6527 269.1461 284.6669 148.8945 -1.4980 267.6994 269.1974 284.8014 149.7165 -1.5016 267.7646 269.2661 284.9165 150.5385 -1.5044 267.8219 269.3264 285.0398 151.3005 -1.5046 267.8659 269.3705 285.1637 152.1525 -1.5057 267.9247 269.4303 285.3221 152.9145 -1.5069 267.9820 269.4889 285.4419 153.7365 -1.5114 268.0358 269.5473 285.5903 154.5285 -1.5167 268.1033 269.6200 285.7300 155.3205 -1.5180 268.1277 269.6456 285.8482 156.1725 -1.5196 268.2002 269.7198 285.9777 156.9345 -1.5227 268.2571 269.7798 286.1080 157.7560 -1.5263 268.3138 269.8401 286.2425 158.5915 -1.5283 268.3742 269.9024 286.3579 159.5220 -1.5362 268.4442 269.9804 286.5134 160.3713 -1.5379 268.5092 270.0472 286.6769 161.1293 -1.5408 268.5563 270.0971 286.8143 161.9473 -1.5434 268.5998 270.1432 286.9367 162.7653 -1.5483 268.6768 270.2251 287.0514 163.5238 -1.5557 268.7363 270.2920 287.1476 164.3700 -1.5562 268.7927 270.3489 287.2852 165.1295 -1.5587 268.8523 270.4110 287.4486 165.9488 -1.5624 268.9054 270.4678 287.5963 166.7670 -1.5670 268.9625 270.5295 287.6914 167.5258 -1.5683 269.0171 270.5854 287.8275 168.3743 -1.5728 269.1128 270.6856 287.9549 169.1328 -1.5750 269.1687 270.7438 288.0896 169.9513 -1.5778 269.2308 270.8086 288.2004 170.7700 -1.5795 269.2979 270.8774 288.3407 171.5285 -1.5823 269.3633 270.9455 288.4487 172.3778 -1.5873 269.4220 271.0093 288.6082 173.1363 -1.5927 269.4666 271.0594 288.7181 173.9560 -1.5991 269.5298 271.1289 288.8537 174.7758 -1.5972 269.5939 271.1910 288.9729 175.5353 -1.5972 269.6791 271.2763 289.1242 176.3850 -1.5965 269.7301 271.3267 289.2536 177.1450 -1.6011 269.7900 271.3910 289.3731 177.9683 -1.6077 269.8714 271.4792 289.4909 178.7878 -1.6121 269.9442 271.5562 289.6253 179.5478 -1.6129 270.0119 271.6248 289.7448 180.4000 -1.6140 270.0814 271.6954 289.8674 181.1618 -1.6181 270.1292 271.7473 289.9881 181.9838 -1.6242 270.1800 271.8043 290.1074 182.7760 -1.6400 270.2514 271.8914 290.2453 183.5675 -1.6478 270.3297 271.9774 290.3626 184.4200 -1.6505 270.3886 272.0390 290.4927 185.1818 -1.6550 270.4673 272.1224 290.6114 186.0038 -1.6564 270.5511 272.2074 290.7379 186.8560 -1.6575 270.6006 272.2580 290.8678 187.6480 -1.6533 270.6652 272.3184 290.9960 188.4395 -1.6493 270.7299 272.3792 291.1027 189.3083 -1.6487 270.8107 272.4594 291.2405 190.0775 -1.6529 270.8762 272.5291 291.3408 190.8698 -1.6587 270.9492 272.6079 291.4651 191.6615 -1.6644 271.0262 272.6906 291.5964 192.4840 -1.6654 271.0927 272.7581 291.7307 193.2758 -1.6663 271.1699 272.8363 291.8559 194.0978 -1.6731 271.2633 272.9364 291.9689 194.8898 -1.6779 271.3025 272.9804 292.1052 195.6815 -1.6816 271.3792 273.0608 292.1957 196.5035 -1.6844 271.4551 273.1395 292.3549 197.2955 -1.6852 271.5211 273.2063 292.4901 198.1183 -1.6885 271.5974 273.2859 292.5960 198.9115 -1.6873 271.6763 273.3636 292.7380 199.7415 -1.6957 271.7452 273.4409 292.8770 200.5125 -1.6997 271.8070 273.5068 293.0133 201.3345 -1.7012 271.8935 273.5947 293.1439 202.0965 -1.7031 271.9528 273.6559 293.2651 202.9485 -1.7080 272.0164 273.7243 293.3994 203.7405 -1.7106 272.1090 273.8196 293.5372 204.5325 -1.7131 272.1792 273.8922 293.6758 205.3545 -1.7154 272.2551 273.9705 293.7887 206.1465 -1.7178 272.3291 274.0469 293.9306 206.9685 -1.7231 272.4297 274.1528 294.0774 207.7605 -1.7253 272.4847 274.2100 294.2074 208.5518 -1.7278 272.5470 274.2747 294.3556 209.3743 -1.7317 272.6250 274.3567 294.4866 210.1973 -1.7332 272.7151 274.4483 294.6237 210.9505 -1.7372 272.7889 274.5261 294.7441 211.8030 -1.7404 272.8760 274.6164 294.8979 212.5950 -1.7401 272.9518 274.6919 295.0218 213.3875 -1.7424 273.0283 274.7706 295.1735 214.2100 -1.7475 273.0895 274.8370 295.3114 214.9715 -1.7541 273.1803 274.9344 295.4274 215.8240 -1.7555 273.2578 275.0134 295.5814 216.6160 -1.7579 273.3366 275.0945 295.7208 217.4075 -1.7575 273.4126 275.1701 295.8515 218.2300 -1.7602 273.4957 275.2560 296.0028 219.0218 -1.7614 273.5771 275.3385 296.1255 219.8438 -1.7668 273.6646 275.4314 296.2651 220.6598 -1.7700 273.7346 275.5046 296.4000 221.4215 -1.7723 273.8316 275.6039 296.5203 222.2438 -1.7741 273.9091 275.6832 296.6445 223.0620 -1.7764 273.9854 275.7618 296.7858 223.8200 -1.7766 274.0450 275.8216 296.9233 224.6680 -1.7799 274.1497 275.9295 297.0735 225.4560 -1.7839 274.2209 276.0048 297.1935 226.2440 -1.7885 274.3118 276.1003 297.3179 227.0620 -1.7927 274.4164 276.2091 297.4602 227.8200 -1.7982 274.4771 276.2752 297.5976 228.6680 -1.7981 274.5484 276.3465 297.7428 229.4560 -1.8035 274.6181 276.4216 297.8453 230.2625 -1.8077 274.7081 276.5158 297.9822 231.0468 -1.8107 274.8080 276.6187 298.1001 231.8655 -1.8125 274.9002 276.7127 298.2501 232.6540 -1.8159 274.9698 276.7857 298.3921 233.4723 -1.8155 275.0462 276.8617 298.5071 234.2618 -1.8205 275.1276 276.9482 298.6355 235.0510 -1.8233 275.2168 277.0401 298.7729 235.8998 -1.8265 275.2923 277.1188 298.9073 236.6593 -1.8318 275.3752 277.2070 299.0202 237.4793 -1.8360 275.4806 277.3166 299.1361 238.2688 -1.8352 275.5860 277.4211 299.2898 239.0590 -1.8380 275.6592 277.4972 299.4077 239.9088 -1.8439 275.7348 277.5788 299.5491 240.6813 -1.8487 275.7936 277.6423 299.6417 241.4545 -1.8535 275.9049 277.7584 299.7731 242.3065 -1.8561 275.9971 277.8532 299.9226 243.0985 -1.8544 276.0966 277.9509 300.0397 243.8905 -1.8542 276.1574 278.0116 300.1518 244.7125 -1.8607 276.2466 278.1073 300.2895 245.4745 -1.8671 276.3338 278.2009 300.4290 246.3265 -1.8678 276.4255 278.2932 300.5395 247.1185 -1.8708 276.5404 278.4112 300.6671 247.9105 -1.8739 276.6161 278.4900 300.8039 248.7325 -1.8744 276.6921 278.5665 300.9288 249.4945 -1.8778 276.7819 278.6597 301.0343 250.3465 -1.8783 276.8599 278.7382 301.1794 251.1305 -1.8830 276.9418 278.8249 301.2946 251.9395 -1.8839 277.0424 278.9263 301.4192 252.7315 -1.8881 277.1394 279.0276 301.5417 253.5535 -1.8895 277.2412 279.1306 301.6638 254.3155 -1.8923 277.3192 279.2115 301.7679 255.1675 -1.8973 277.4277 279.3249 301.9100 255.9293 -1.8959 277.4922 279.3881 302.0214 256.7513 -1.8949 277.5981 279.4930 302.1580 257.5735 -1.8989 277.6867 279.5857 302.2703 258.3345 -1.9032 277.7735 279.6767 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