DTA measure 1lassu Date: 20241015:162 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.47 s Mass = 951 mg data_number = 1583 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2660 -1.3206 246.0539 247.3744 261.9226 2.0843 -1.3162 246.0920 247.4082 261.9126 2.8420 -1.3180 246.1462 247.4642 261.8823 3.6903 -1.3173 246.2126 247.5299 261.8602 4.4780 -1.3162 246.2593 247.5756 261.8573 5.2670 -1.3163 246.3024 247.6187 261.8410 6.0850 -1.3169 246.3401 247.6570 261.8393 6.8730 -1.3146 246.3934 247.7079 261.8320 7.6918 -1.3147 246.4595 247.7743 261.8245 8.4800 -1.3144 246.5086 247.8230 261.8438 9.2683 -1.3128 246.5487 247.8615 261.8582 10.0800 -1.3124 246.6086 247.9210 261.8670 10.8990 -1.3127 246.6706 247.9833 261.9003 11.6593 -1.3116 246.7276 248.0392 261.9199 12.5085 -1.3093 246.7794 248.0887 261.9465 13.2980 -1.3083 246.8332 248.1415 261.9904 14.0885 -1.3106 246.8940 248.2047 262.0461 14.9088 -1.3078 246.9385 248.2463 262.0951 15.6700 -1.3105 246.9961 248.3066 262.1564 16.5208 -1.3092 247.0416 248.3508 262.2082 17.3115 -1.3110 247.0907 248.4018 262.2798 18.1033 -1.3096 247.1388 248.4483 262.3421 18.9245 -1.3069 247.2104 248.5172 262.4218 19.7055 -1.3066 247.2412 248.5478 262.4942 20.4955 -1.3078 247.3025 248.6103 262.5754 21.3475 -1.3074 247.3925 248.6998 262.7103 22.1095 -1.3058 247.4227 248.7285 262.7944 22.9315 -1.3052 247.4871 248.7923 262.9056 23.7235 -1.3052 247.5385 248.8437 263.0160 24.5158 -1.3072 247.5793 248.8864 263.1365 25.3675 -1.3076 247.6338 248.9415 263.2642 26.1295 -1.3116 247.7020 249.0135 263.3573 26.9515 -1.3130 247.7635 249.0765 263.4925 27.7435 -1.3091 247.8192 249.1283 263.6255 28.5355 -1.3105 247.8550 249.1655 263.7502 29.3575 -1.3099 247.9156 249.2255 263.8874 30.1595 -1.3105 247.9663 249.2768 264.0413 30.9313 -1.3135 248.0192 249.3326 264.1765 31.7833 -1.3156 248.0759 249.3915 264.3098 32.5448 -1.3155 248.1446 249.4600 264.4603 33.3668 -1.3135 248.2100 249.5235 264.5988 34.1890 -1.3132 248.2569 249.5701 264.7530 34.9508 -1.3179 248.3166 249.6345 264.8895 35.8030 -1.3226 248.3772 249.6998 265.0606 36.5648 -1.3231 248.4534 249.7765 265.2009 37.3868 -1.3266 248.4988 249.8254 265.3611 38.1790 -1.3245 248.5581 249.8826 265.4985 38.9705 -1.3261 248.6108 249.9369 265.6388 39.8230 -1.3266 248.6586 249.9852 265.8087 40.6090 -1.3260 248.7208 250.0468 265.9449 41.3898 -1.3279 248.7919 250.1199 266.0807 42.2118 -1.3299 248.8453 250.1753 266.2299 43.0040 -1.3328 248.9112 250.2439 266.3939 43.7955 -1.3339 248.9724 250.3063 266.5488 44.6480 -1.3333 249.0397 250.3729 266.7046 45.4098 -1.3376 249.0834 250.4209 266.8398 46.2318 -1.3394 249.1455 250.4849 266.9790 47.0538 -1.3386 249.2017 250.5403 267.1134 47.8155 -1.3429 249.2651 250.6080 267.2581 48.6678 -1.3456 249.3296 250.6753 267.3768 49.4295 -1.3468 249.3811 250.7280 267.5109 50.2515 -1.3483 249.4557 250.8041 267.6534 51.0678 -1.3512 249.5251 250.8763 267.7847 51.8595 -1.3514 249.5787 250.9301 267.9076 52.6515 -1.3550 249.6334 250.9885 268.0226 53.4735 -1.3577 249.7075 251.0653 268.1433 54.2655 -1.3591 249.7759 251.1349 268.2740 55.0883 -1.3588 249.8272 251.1860 268.3916 55.8805 -1.3606 249.8961 251.2567 268.5090 56.6735 -1.3652 249.9742 251.3395 268.6168 57.4955 -1.3666 250.0299 251.3965 268.7281 58.2610 -1.3698 250.0820 251.4518 268.8113 59.1180 -1.3674 250.1453 251.5127 268.9361 59.9105 -1.3712 250.2175 251.5887 269.0600 60.7200 -1.3726 250.2796 251.6523 269.1370 61.5053 -1.3747 250.3523 251.7269 269.2398 62.3220 -1.3762 250.4391 251.8153 269.3516 63.0810 -1.3773 250.4853 251.8626 269.4492 63.9295 -1.3805 250.5486 251.9291 269.5303 64.7175 -1.3827 250.5969 251.9796 269.6282 65.5053 -1.3834 250.6797 252.0630 269.7259 66.3235 -1.3866 250.7339 252.1205 269.8075 67.1118 -1.3875 250.8129 252.2004 269.9078 67.9295 -1.3878 250.8693 252.2571 269.9983 68.7175 -1.3895 250.9268 252.3163 270.0725 69.5068 -1.3924 250.9981 252.3905 270.1683 70.3250 -1.3916 251.0744 252.4660 270.2695 71.1200 -1.3944 251.1458 252.5402 270.3380 71.9158 -1.3961 251.2093 252.6054 270.4203 72.7345 -1.3997 251.2819 252.6816 270.5171 73.5233 -1.4004 251.3425 252.7429 270.5961 74.3133 -1.4035 251.4143 252.8178 270.6680 75.1625 -1.4050 251.4955 252.9005 270.7827 75.9205 -1.4111 251.5740 252.9851 270.8628 76.7398 -1.4119 251.6118 253.0237 270.9319 77.5298 -1.4104 251.6628 253.0731 271.0072 78.3198 -1.4130 251.7663 253.1793 271.1005 79.1710 -1.4123 251.8465 253.2588 271.1752 79.9320 -1.4142 251.8888 253.3029 271.2709 80.7538 -1.4170 251.9601 253.3771 271.3523 81.5465 -1.4187 252.0224 253.4411 271.4380 82.3580 -1.4210 252.1127 253.5337 271.5236 83.1495 -1.4229 252.1507 253.5736 271.6137 83.9720 -1.4224 252.2303 253.6527 271.7089 84.7638 -1.4243 252.3245 253.7488 271.7963 85.5858 -1.4308 252.3904 253.8212 271.8822 86.3780 -1.4309 252.4491 253.8800 271.9825 87.1695 -1.4317 252.5341 253.9658 272.0605 87.9920 -1.4349 252.5733 254.0082 272.1503 88.7535 -1.4346 252.6544 254.0890 272.2403 89.6060 -1.4354 252.7400 254.1754 272.3518 90.3980 -1.4408 252.8162 254.2570 272.4402 91.1970 -1.4471 252.8909 254.3380 272.5271 91.9928 -1.4457 252.9700 254.4157 272.6348 92.8148 -1.4468 253.0266 254.4734 272.7417 93.5765 -1.4504 253.0983 254.5487 272.8368 94.4290 -1.4502 253.1671 254.6173 272.9419 95.1908 -1.4523 253.2262 254.6786 273.0279 96.0128 -1.4534 253.3141 254.7675 273.1364 96.8348 -1.4548 253.3882 254.8430 273.2525 97.5965 -1.4606 253.4411 254.9016 273.3602 98.4488 -1.4582 253.5251 254.9833 273.4733 99.2105 -1.4619 253.5903 255.0522 273.5839 100.0325 -1.4628 253.6762 255.1390 273.6814 100.8545 -1.4636 253.7564 255.2200 273.8070 101.6358 -1.4679 253.8224 255.2903 273.9110 102.4275 -1.4709 253.8878 255.3586 274.0257 103.2795 -1.4707 253.9575 255.4282 274.1409 104.0415 -1.4735 254.0221 255.4956 274.2411 104.8635 -1.4771 254.0999 255.5769 274.3567 105.6555 -1.4751 254.1710 255.6462 274.4828 106.4475 -1.4781 254.2477 255.7258 274.6052 107.2995 -1.4790 254.3268 255.8058 274.7354 108.0615 -1.4808 254.3954 255.8762 274.8134 108.8835 -1.4878 254.4534 255.9411 274.9233 109.6755 -1.4833 254.5403 256.0236 275.0554 110.4670 -1.4802 254.6281 256.1083 275.1597 111.2893 -1.4797 254.6851 256.1648 275.2911 112.0920 -1.4859 254.7455 256.2314 275.3826 112.8650 -1.4897 254.8200 256.3097 275.4952 113.7170 -1.4933 254.9131 256.4064 275.6399 114.5090 -1.4922 254.9963 256.4885 275.7555 115.3005 -1.4958 255.0783 256.5741 275.8582 116.1230 -1.4978 255.1600 256.6578 275.9903 116.8848 -1.5045 255.2187 256.7232 276.0911 117.7370 -1.5075 255.3013 256.8088 276.2142 118.5290 -1.5113 255.3686 256.8799 276.3306 119.3205 -1.5133 255.4555 256.9689 276.4505 120.1430 -1.5110 255.5257 257.0367 276.5736 120.9045 -1.5100 255.5712 257.0811 276.6743 121.7573 -1.5149 255.6610 257.1759 276.7994 122.5098 -1.5134 255.7300 257.2434 276.9158 123.3698 -1.5115 255.8305 257.3420 277.0034 124.1618 -1.5136 255.9142 257.4278 277.1265 124.9533 -1.5193 255.9900 257.5093 277.2317 125.7720 -1.5264 256.0599 257.5863 277.3336 126.5300 -1.5303 256.1221 257.6524 277.4276 127.3780 -1.5318 256.2091 257.7408 277.5429 128.1360 -1.5347 256.3035 257.8383 277.6378 128.9560 -1.5298 256.3621 257.8919 277.7449 129.7728 -1.5301 256.4428 257.9730 277.8267 130.5320 -1.5387 256.5235 258.0623 277.9234 131.3790 -1.5424 256.6052 258.1476 278.0359 132.1380 -1.5441 256.6790 258.2231 278.1214 132.9660 -1.5459 256.7494 258.2952 278.2311 133.7540 -1.5481 256.8374 258.3855 278.3171 134.5420 -1.5490 256.9232 258.4722 278.4107 135.3908 -1.5517 257.0119 258.5636 278.5029 136.1490 -1.5555 257.0765 258.6319 278.5926 136.9670 -1.5536 257.1530 258.7066 278.6914 137.7853 -1.5549 257.2325 258.7874 278.7876 138.5443 -1.5561 257.3094 258.8656 278.8861 139.3940 -1.5577 257.3989 258.9566 278.9814 140.1828 -1.5611 257.4700 259.0311 279.0649 140.9728 -1.5626 257.5592 259.1218 279.1440 141.7930 -1.5666 257.6378 259.2044 279.2450 142.5523 -1.5667 257.7122 259.2789 279.3213 143.4015 -1.5680 257.8203 259.3883 279.4094 144.1908 -1.5678 257.8771 259.4449 279.5277 144.9810 -1.5684 257.9499 259.5183 279.6319 145.8015 -1.5714 258.0284 259.5998 279.7286 146.5928 -1.5774 258.0892 259.6666 279.8119 147.4140 -1.5770 258.1803 259.7572 279.9217 148.2055 -1.5773 258.2667 259.8440 280.0157 148.9975 -1.5702 258.3450 259.9153 280.1191 149.8195 -1.5740 258.4346 260.0086 280.2272 150.5815 -1.5808 258.5203 260.1011 280.3153 151.4335 -1.5827 258.5946 260.1773 280.4077 152.2255 -1.5874 258.6717 260.2591 280.5391 153.0400 -1.5904 258.7365 260.3268 280.6416 153.8245 -1.5898 258.8414 260.4312 280.7292 154.6468 -1.5890 258.9345 260.5235 280.8485 155.4145 -1.5876 259.0036 260.5912 280.9489 156.2395 -1.5897 259.0968 260.6865 281.0297 157.0613 -1.5937 259.1807 260.7744 281.1352 157.8233 -1.5986 259.2540 260.8526 281.2427 158.6753 -1.6017 259.3436 260.9452 281.3452 159.4370 -1.6049 259.4189 261.0237 281.4516 160.2590 -1.6093 259.4946 261.1040 281.5483 161.0813 -1.6080 259.5872 261.1952 281.6769 161.8428 -1.6118 259.6675 261.2793 281.7677 162.6950 -1.6137 259.7357 261.3494 281.8796 163.4823 -1.6143 259.8274 261.4417 281.9833 164.2638 -1.6150 259.9251 261.5401 282.0904 165.0858 -1.6159 260.0254 261.6412 282.1980 165.8783 -1.6085 260.0918 261.7003 282.2931 166.6695 -1.6108 260.1581 261.7689 282.3982 167.5220 -1.6196 260.2627 261.8823 282.5206 168.2843 -1.6181 260.3278 261.9458 282.6241 169.1080 -1.6166 260.4158 262.0324 282.7353 169.9010 -1.6245 260.4986 262.1231 282.8333 170.6925 -1.6279 260.5782 262.2061 282.9406 171.5450 -1.6336 260.6765 262.3101 283.0472 172.3068 -1.6371 260.7628 262.3999 283.1422 173.1288 -1.6404 260.8474 262.4878 283.2420 173.9320 -1.6335 260.9351 262.5686 283.3823 174.7248 -1.6328 260.9967 262.6295 283.4740 175.5165 -1.6318 261.1028 262.7346 283.5735 176.3685 -1.6340 261.1816 262.8156 283.6837 177.1305 -1.6357 261.2637 262.8994 283.7920 177.9525 -1.6416 261.3510 262.9926 283.8958 178.7445 -1.6441 261.4330 263.0771 284.0039 179.5365 -1.6447 261.5176 263.1623 284.0854 180.3885 -1.6471 261.6164 263.2635 284.1922 181.1505 -1.6522 261.6800 263.3321 284.2874 181.9725 -1.6550 261.7832 263.4381 284.3987 182.7645 -1.6552 261.8754 263.5306 284.5124 183.5778 -1.6582 261.9427 263.6009 284.6182 184.3753 -1.6577 262.0247 263.6824 284.7065 185.1975 -1.6604 262.0940 263.7544 284.8061 185.9595 -1.6640 262.1998 263.8638 284.9025 186.8120 -1.6624 262.2920 263.9544 285.0045 187.5745 -1.6617 262.3654 264.0271 285.1218 188.3965 -1.6678 262.4464 264.1142 285.2317 189.2183 -1.6684 262.5514 264.2198 285.3399 189.9778 -1.6696 262.6369 264.3064 285.4221 190.8260 -1.6726 262.7349 264.4074 285.5184 191.5858 -1.6771 262.8256 264.5027 285.6134 192.4043 -1.6794 262.9074 264.5867 285.7148 193.1923 -1.6764 262.9920 264.6683 285.8347 194.0168 -1.6760 263.0741 264.7501 285.9229 194.7815 -1.6795 263.1499 264.8294 286.0203 195.6298 -1.6830 263.2335 264.9166 286.1351 196.3883 -1.6825 263.3235 265.0060 286.2122 197.2065 -1.6816 263.4267 265.1083 286.3165 198.0250 -1.6808 263.5181 265.1989 286.4014 198.7825 -1.6843 263.6027 265.2870 286.5147 199.6305 -1.6829 263.6935 265.3763 286.6377 200.4190 -1.6874 263.7803 265.4677 286.7202 201.2080 -1.6887 263.8777 265.5664 286.8359 202.0273 -1.6909 263.9577 265.6486 286.9347 202.8153 -1.6928 264.0360 265.7289 287.0447 203.6330 -1.6916 264.1298 265.8214 287.1496 204.4213 -1.6932 264.2083 265.9015 287.2443 205.2093 -1.6975 264.3002 265.9977 287.3431 206.0338 -1.6907 264.4019 266.0926 287.4626 206.8243 -1.6904 264.4662 266.1566 287.5751 207.6428 -1.6914 264.5563 266.2477 287.6888 208.4353 -1.6947 264.6521 266.3468 287.8016 209.2360 -1.6934 264.7521 266.4455 287.9109 210.0303 -1.6936 264.8447 266.5383 288.0215 210.8210 -1.6923 264.9229 266.6152 288.1358 211.6728 -1.6957 265.0016 266.6973 288.2388 212.4353 -1.7046 265.1007 266.8052 288.3478 213.2578 -1.7070 265.2165 266.9235 288.4526 214.0510 -1.7049 265.2887 266.9936 288.5791 214.8450 -1.7106 265.3705 267.0811 288.6801 215.6670 -1.7250 265.4655 267.1904 288.7921 216.4285 -1.7336 265.5453 267.2789 288.9054 217.2810 -1.7300 265.6304 267.3603 289.0270 218.0465 -1.7290 265.7375 267.4665 289.1318 218.8698 -1.7312 265.8236 267.5548 289.2411 219.6920 -1.7359 265.9271 267.6630 289.3887 220.4535 -1.7412 266.0055 267.7467 289.4906 221.3058 -1.7460 266.1089 267.8550 289.6238 222.0675 -1.7444 266.1925 267.9369 289.7480 222.8898 -1.7445 266.2887 268.0332 289.8692 223.7115 -1.7473 266.3607 268.1080 289.9573 224.4735 -1.7415 266.4445 268.1860 290.0668 225.3255 -1.7510 266.5599 268.3109 290.1963 226.0875 -1.7537 266.6329 268.3866 290.3098 226.9095 -1.7511 266.7278 268.4790 290.4285 227.7315 -1.7549 266.8151 268.5701 290.5397 228.4935 -1.7626 266.9209 268.6835 290.6450 229.3455 -1.7649 267.0141 268.7790 290.7549 230.1075 -1.7658 267.1033 268.8691 290.8568 230.9295 -1.7594 267.1842 268.9436 290.9751 231.7515 -1.7633 267.2771 269.0404 291.0860 232.5135 -1.7717 267.3802 269.1518 291.1868 233.3655 -1.7761 267.4637 269.2398 291.3210 234.1275 -1.7757 267.5609 269.3366 291.4009 234.9748 -1.7749 267.6618 269.4367 291.4909 235.7325 -1.7783 267.7453 269.5236 291.6075 236.5843 -1.7823 267.8484 269.6306 291.6932 237.3465 -1.7836 267.9498 269.7335 291.7862 238.1685 -1.7860 268.0306 269.8165 291.8959 238.9605 -1.7812 268.1278 269.9090 291.9771 239.7520 -1.7793 268.2061 269.9854 292.0665 240.5800 -1.7861 268.3180 270.1041 292.1688 241.3718 -1.7907 268.4189 270.2095 292.2664 242.1938 -1.7923 268.5062 270.2985 292.3727 242.9860 -1.7872 268.5897 270.3769 292.4556 243.7775 -1.7994 268.6658 270.4651 292.5516 244.6035 -1.8010 268.7711 270.5721 292.6425 245.4230 -1.7996 268.8833 270.6829 292.7291 246.1735 -1.8047 268.9553 270.7599 292.8049 247.0260 -1.8052 269.0601 270.8653 292.8903 247.7878 -1.8130 269.1542 270.9672 292.9860 248.6098 -1.8235 269.2532 271.0766 293.0930 249.4320 -1.8277 269.3485 271.1762 293.1780 250.1935 -1.8285 269.4328 271.2613 293.2516 251.0458 -1.8169 269.5308 271.3477 293.3729 251.8075 -1.8147 269.6313 271.4460 293.4485 252.6298 -1.8175 269.7133 271.5308 293.5320 253.4518 -1.8175 269.8030 271.6205 293.6267 254.2120 -1.8190 269.9018 271.7208 293.7310 255.0590 -1.8187 269.9937 271.8124 293.8217 255.8680 -1.8236 270.0950 271.9186 293.9201 256.6260 -1.8210 270.1769 271.9979 294.0216 257.4440 -1.8231 270.2699 272.0930 294.1266 258.2323 -1.8250 270.3774 272.2024 294.2052 259.0200 -1.8309 270.4652 272.2961 294.2985 259.8680 -1.8327 270.5523 272.3851 294.4000 260.6260 -1.8289 270.6609 272.4898 294.4942 261.4440 -1.8285 270.7618 272.5903 294.6023 262.2620 -1.8330 270.8360 272.6689 294.6826 263.0200 -1.8377 270.9166 272.7543 294.7825 263.8680 -1.8446 271.0279 272.8725 294.8823 264.6263 -1.8450 271.1200 272.9650 294.9890 265.4653 -1.8451 271.2183 273.0634 295.0585 266.2540 -1.8443 271.3236 273.1680 295.1613 267.0723 -1.8462 271.4126 273.2588 295.2767 267.8313 -1.8469 271.5019 273.3488 295.3714 268.6805 -1.8517 271.6067 273.4584 295.4269 269.4390 -1.8527 271.7038 273.5564 295.5534 270.2610 -1.8567 271.7701 273.6268 295.6749 271.0808 -1.8590 271.8795 273.7385 295.7765 271.8403 -1.8625 271.9708 273.8333 295.8841 272.6905 -1.8637 272.0594 273.9231 296.0143 273.4795 -1.8573 272.1593 274.0166 296.0967 274.2698 -1.8549 272.2421 274.0970 296.1969 275.0898 -1.8651 272.3455 274.2106 296.3118 275.8943 -1.8708 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361.5465 365.1822 384.3145 949.1185 -3.6375 361.6516 365.2891 384.4386 949.9415 -3.6386 361.7715 365.4101 384.5532 950.7335 -3.6404 361.8747 365.5151 384.6704 951.5470 -3.6453 361.9914 365.6367 384.8040 952.3395 -3.6470 362.1027 365.7497 384.9331 953.1615 -3.6523 362.2223 365.8745 385.0643 953.9535 -3.6545 362.3469 366.0014 385.1699 954.7775 -3.6551 362.4529 366.1080 385.2906 955.5695 -3.6561 362.5489 366.2051 385.3991 956.3625 -3.6568 362.6593 366.3162 385.5255 957.1845 -3.6597 362.7842 366.4439 385.6469 957.9765 -3.6614 362.8894 366.5508 385.7645 958.7993 -3.6607 363.0144 366.6751 385.8848 959.5915 -3.6630 363.1406 366.8036 385.9848 960.3825 -3.6640 363.2327 366.8967 386.1075 961.2343 -3.6652 363.3520 367.0172 386.2139 962.0008 -3.6666 363.4473 367.1139 386.3278 962.7983 -3.6690 363.5697 367.2387 386.4046 963.6170 -3.6742 363.6813 367.3555 386.5318 964.3818 -3.6773 363.7954 367.4728 386.6329 965.2025 -3.6793 363.8947 367.5740 386.7495 966.0208 -3.6826 364.0212 367.7038 386.8489 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