DTA measure 2gyors Date: 20241015:1537 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1514.98 s Mass = 951 mg data_number = 1882 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1768 -4.2367 417.6049 421.8416 420.1434 1.9705 -4.2328 417.6346 421.8674 420.1418 2.7545 -4.2329 417.6662 421.8990 420.1533 3.5768 -4.2348 417.7123 421.9471 420.1539 4.3685 -4.2320 417.7555 421.9875 420.1522 5.1605 -4.2325 417.7740 422.0065 420.1518 5.9825 -4.2323 417.8107 422.0430 420.1441 6.7745 -4.2314 417.8219 422.0533 420.1321 7.5965 -4.2313 417.8535 422.0848 420.1124 8.3885 -4.2320 417.8930 422.1251 420.0918 9.1805 -4.2313 417.9120 422.1433 420.0628 10.0330 -4.2312 417.9500 422.1813 420.0210 10.7955 -4.2310 417.9918 422.2229 419.9843 11.6175 -4.2301 418.0158 422.2459 419.9359 12.4360 -4.2296 418.0303 422.2599 419.8924 13.2285 -4.2254 418.0573 422.2826 419.8344 14.0215 -4.2255 418.0736 422.2991 419.7888 14.8435 -4.2258 418.1123 422.3381 419.6955 15.6338 -4.2241 418.1417 422.3658 419.6287 16.4513 -4.2199 418.1657 422.3856 419.5600 17.2380 -4.2175 418.1940 422.4115 419.4865 18.0273 -4.2183 418.2222 422.4404 419.4104 18.8458 -4.2121 418.2397 422.4517 419.3252 19.6035 -4.2098 418.2646 422.4744 419.2508 20.4520 -4.2077 418.2672 422.4749 419.1418 21.2400 -4.2066 418.3003 422.5069 419.0541 22.0480 -4.2092 418.3250 422.5342 418.9405 22.8268 -4.2048 418.3714 422.5762 418.8530 23.6448 -4.1997 418.3882 422.5879 418.7458 24.4328 -4.1967 418.4113 422.6079 418.6521 25.2515 -4.1928 418.4583 422.6511 418.5393 26.0398 -4.1906 418.4566 422.6471 418.4460 26.8288 -4.1896 418.4705 422.6601 418.3318 27.6775 -4.1859 418.4761 422.6620 418.2065 28.4360 -4.1823 418.5217 422.7039 418.0863 29.2558 -4.1761 418.5405 422.7165 417.9674 30.0750 -4.1732 418.5424 422.7156 417.8804 30.8343 -4.1694 418.5615 422.7310 417.7667 31.6840 -4.1640 418.5863 422.7503 417.6246 32.4568 -4.1616 418.6028 422.7645 417.5203 33.2298 -4.1599 418.6051 422.7650 417.4118 34.0823 -4.1573 418.6304 422.7877 417.2927 34.8743 -4.1515 418.6451 422.7967 417.1724 35.6658 -4.1482 418.6503 422.7985 417.0455 36.4880 -4.1419 418.6621 422.8040 416.9013 37.2495 -4.1393 418.6713 422.8106 416.7930 38.1030 -4.1360 418.6861 422.8221 416.6659 38.8648 -4.1332 418.6875 422.8207 416.5653 39.6868 -4.1307 418.6886 422.8192 416.4312 40.4790 -4.1221 418.7060 422.8282 416.3417 41.2705 -4.1189 418.7242 422.8431 416.2084 42.1230 -4.1152 418.7301 422.8453 416.0625 42.9085 -4.1079 418.7469 422.8548 415.9559 43.6828 -4.1071 418.7514 422.8586 415.8458 44.5048 -4.1034 418.7690 422.8724 415.7228 45.2970 -4.0982 418.7817 422.8799 415.5894 46.0885 -4.0938 418.7896 422.8834 415.4877 46.9410 -4.0871 418.7875 422.8746 415.3750 47.7025 -4.0819 418.8046 422.8865 415.2633 48.5248 -4.0796 418.8066 422.8862 415.1303 49.3170 -4.0756 418.7895 422.8651 415.0045 50.1085 -4.0700 418.7907 422.8607 414.8952 50.9308 -4.0639 418.7934 422.8573 414.7835 51.7225 -4.0630 418.8063 422.8693 414.6535 52.5448 -4.0579 418.8174 422.8752 414.5533 53.3530 -4.0519 418.8127 422.8645 414.4376 54.1458 -4.0457 418.8119 422.8576 414.3015 54.9375 -4.0411 418.8295 422.8707 414.2005 55.7595 -4.0381 418.8021 422.8402 414.0842 56.5215 -4.0334 418.7990 422.8325 413.9881 57.3735 -4.0290 418.8067 422.8357 413.8932 58.1655 -4.0202 418.7901 422.8103 413.7696 58.9575 -4.0158 418.7887 422.8044 413.6725 59.7795 -4.0153 418.8086 422.8238 413.6097 60.5415 -4.0149 418.8185 422.8334 413.4998 61.3935 -4.0098 418.8074 422.8172 413.3843 62.1855 -4.0035 418.7843 422.7878 413.2789 62.9978 -3.9988 418.7660 422.7648 413.1741 63.7905 -3.9928 418.7808 422.7737 413.0803 64.6125 -3.9879 418.7455 422.7334 412.9955 65.3743 -3.9826 418.7481 422.7307 412.9110 66.2263 -3.9801 418.7507 422.7308 412.8253 66.9885 -3.9787 418.7517 422.7304 412.7407 67.8098 -3.9708 418.7446 422.7154 412.6469 68.6323 -3.9669 418.7519 422.7188 412.5503 69.3945 -3.9636 418.7486 422.7122 412.4628 70.2475 -3.9616 418.7224 422.6840 412.3705 71.0098 -3.9564 418.7090 422.6654 412.2769 71.8318 -3.9548 418.6891 422.6438 412.2027 72.6240 -3.9488 418.6790 422.6278 412.1195 73.4573 -3.9394 418.6686 422.6080 412.0280 74.2305 -3.9369 418.6600 422.5969 411.9584 75.0530 -3.9326 418.6350 422.5676 411.8595 75.8448 -3.9310 418.6376 422.5686 411.7674 76.6675 -3.9272 418.6243 422.5516 411.6688 77.4600 -3.9221 418.5983 422.5204 411.6153 78.2515 -3.9194 418.5784 422.4978 411.5372 79.0738 -3.9154 418.5733 422.4887 411.4344 79.8618 -3.9144 418.5626 422.4770 411.3437 80.6803 -3.9117 418.5536 422.4653 411.2654 81.4670 -3.9056 418.5463 422.4519 411.1707 82.2560 -3.8998 418.5160 422.4158 411.0816 83.0743 -3.8966 418.5060 422.4026 411.0056 83.8893 -3.8946 418.4897 422.3842 410.9204 84.6670 -3.8904 418.4844 422.3749 410.8371 85.4858 -3.8841 418.4420 422.3261 410.7476 86.3055 -3.8787 418.4219 422.3005 410.6564 87.0690 -3.8794 418.4130 422.2923 410.5834 87.9175 -3.8725 418.3934 422.2659 410.4587 88.6763 -3.8701 418.3898 422.2599 410.3745 89.4950 -3.8707 418.3622 422.2329 410.2821 90.3130 -3.8655 418.3425 422.2080 410.2005 91.0710 -3.8630 418.3128 422.1758 410.1037 91.9205 -3.8603 418.3014 422.1617 410.0018 92.7093 -3.8564 418.2758 422.1322 409.9119 93.4980 -3.8541 418.2527 422.1067 409.8364 94.3033 -3.8474 418.2330 422.0804 409.7351 95.1235 -3.8435 418.2095 422.0530 409.6237 95.8838 -3.8383 418.1889 422.0272 409.5430 96.7345 -3.8286 418.1613 421.9900 409.4445 97.5238 -3.8186 418.1207 421.9393 409.3482 98.3135 -3.8201 418.0905 421.9106 409.2499 99.1345 -3.8244 418.0860 421.9104 409.1721 99.8965 -3.8208 418.0693 421.8901 409.0846 100.7483 -3.8151 418.0351 421.8502 409.0070 101.5395 -3.8112 418.0079 421.8191 408.9159 102.3315 -3.8038 417.9655 421.7693 408.7986 103.1535 -3.8016 417.9613 421.7629 408.6956 103.9360 -3.7917 417.9339 421.7256 408.6044 104.7275 -3.7810 417.9027 421.6836 408.5254 105.5798 -3.7820 417.8683 421.6503 408.4154 106.3455 -3.7837 417.8386 421.6222 408.3237 107.1675 -3.7763 417.8091 421.5854 408.2460 107.9595 -3.7726 417.7842 421.5568 408.1293 108.7515 -3.7721 417.7718 421.5439 408.0425 109.5735 -3.7660 417.7272 421.4932 407.9435 110.3655 -3.7645 417.7108 421.4753 407.8418 111.1875 -3.7625 417.6722 421.4347 407.7439 111.9795 -3.7723 417.6202 421.3926 407.6281 112.7715 -3.7633 417.5796 421.3429 407.5192 113.5935 -3.7528 417.5467 421.2995 407.4179 114.3883 -3.7459 417.5337 421.2796 407.3073 115.1843 -3.7416 417.5024 421.2440 407.2295 116.0065 -3.7412 417.4636 421.2047 407.1289 116.7983 -3.7382 417.4510 421.1891 407.0245 117.5898 -3.7315 417.4238 421.1552 406.9180 118.4125 -3.7276 417.3876 421.1152 406.8228 119.2043 -3.7202 417.3299 421.0501 406.7211 120.0258 -3.7168 417.3012 421.0179 406.6211 120.8183 -3.7176 417.2715 420.9891 406.5214 121.6098 -3.7208 417.2321 420.9529 406.4327 122.4320 -3.7206 417.1881 420.9087 406.3218 123.2243 -3.7183 417.1777 420.8960 406.2215 124.0470 -3.7143 417.1309 420.8452 406.1248 124.8385 -3.7097 417.1076 420.8173 406.0091 125.6500 -3.7046 417.0607 420.7654 405.9325 126.4415 -3.7025 417.0054 420.7079 405.8302 127.2640 -3.6985 416.9650 420.6636 405.7306 128.0255 -3.6996 416.9247 420.6243 405.6123 128.8778 -3.6954 416.9016 420.5971 405.5128 129.6698 -3.6905 416.8819 420.5724 405.4269 130.4615 -3.6852 416.8290 420.5142 405.3271 131.2838 -3.6695 416.7893 420.4587 405.2312 132.0455 -3.6599 416.7356 420.3955 405.1269 132.8975 -3.6527 416.6846 420.3373 405.0233 133.6895 -3.6504 416.6413 420.2917 404.9328 134.4815 -3.6467 416.6124 420.2590 404.8436 135.2978 -3.6399 416.5679 420.2078 404.7339 136.0895 -3.6376 416.5322 420.1698 404.6497 136.8815 -3.6385 416.4978 420.1363 404.5442 137.7350 -3.6367 416.4370 420.0737 404.4151 138.4978 -3.6254 416.3882 420.0136 404.3354 139.3228 -3.6170 416.3520 419.9690 404.2300 140.1165 -3.6108 416.3070 419.9178 404.1156 140.9095 -3.6158 416.2711 419.8869 404.0192 141.7315 -3.6155 416.2325 419.8480 403.9101 142.5235 -3.6130 416.2039 419.8169 403.8152 143.3485 -3.6062 416.1537 419.7600 403.6960 144.1428 -3.5942 416.1004 419.6946 403.6022 144.9328 -3.5910 416.0425 419.6335 403.5033 145.7288 -3.5889 416.0070 419.5959 403.4032 146.5180 -3.5946 415.9614 419.5560 403.2924 147.3670 -3.6048 415.9201 419.5249 403.1980 148.1245 -3.5966 415.8597 419.4563 403.0824 148.9425 -3.5901 415.8242 419.4143 402.9758 149.7313 -3.5881 415.7632 419.3513 402.8689 150.5205 -3.5828 415.7236 419.3064 402.7600 151.3695 -3.5782 415.6799 419.2581 402.6575 152.1280 -3.5721 415.6305 419.2026 402.5541 152.9475 -3.5697 415.5895 419.1593 402.4521 153.7365 -3.5704 415.5344 419.1048 402.3399 154.5260 -3.5767 415.4877 419.0644 402.2608 155.3800 -3.5782 415.4351 419.0133 402.1431 156.1448 -3.5808 415.3738 418.9546 402.0318 156.9653 -3.5755 415.3267 418.9022 401.9298 157.7555 -3.5656 415.2568 418.8224 401.8241 158.5473 -3.5582 415.2154 418.7736 401.7157 159.3685 -3.5540 415.1835 418.7375 401.6130 160.1600 -3.5457 415.1272 418.6729 401.5145 160.9798 -3.5213 415.0476 418.5689 401.4002 161.7695 -3.5158 414.9958 418.5116 401.3054 162.5600 -3.5167 414.9506 418.4674 401.2029 163.3798 -3.5135 414.9091 418.4225 401.1026 164.1685 -3.5145 414.8603 418.3748 400.9957 164.9898 -3.5145 414.8032 418.3177 400.8838 165.7820 -3.5104 414.7567 418.2671 400.8071 166.5943 -3.5082 414.6885 418.1967 400.6962 167.3855 -3.5074 414.6401 418.1476 400.5983 168.2083 -3.4935 414.5966 418.0900 400.4748 169.0603 -3.4860 414.5376 418.0235 400.3878 169.8215 -3.4899 414.4782 417.9681 400.2878 170.6740 -3.4849 414.4151 417.9000 400.1978 171.4358 -3.4785 414.3800 417.8585 400.0946 172.2578 -3.4734 414.3058 417.7792 399.9987 173.0800 -3.4708 414.2465 417.7173 399.9159 173.9318 -3.4613 414.2019 417.6631 399.8259 174.6935 -3.4626 414.1379 417.6005 399.7220 175.5483 -3.4613 414.0693 417.5307 399.6245 176.3138 -3.4618 414.0158 417.4776 399.5238 177.1358 -3.4620 413.9663 417.4283 399.4211 177.9608 -3.4599 413.9219 417.3817 399.3247 178.7225 -3.4572 413.8687 417.3259 399.2203 179.5748 -3.4546 413.8002 417.2548 399.1336 180.3365 -3.4533 413.7417 417.1949 399.0491 181.1585 -3.4475 413.6791 417.1267 398.9401 181.9808 -3.4395 413.5902 417.0297 398.8527 182.7425 -3.4400 413.5464 416.9864 398.7529 183.5945 -3.4394 413.4813 416.9206 398.6633 184.3565 -3.4315 413.4120 416.8435 398.5877 185.1793 -3.4328 413.3669 416.7997 398.4600 185.9715 -3.4232 413.3061 416.7292 398.3828 186.7653 -3.4219 413.2513 416.6733 398.2934 187.6175 -3.4197 413.1801 416.5998 398.1681 188.3795 -3.4139 413.1539 416.5678 398.0851 189.2015 -3.4153 413.0849 416.5002 397.9724 189.9935 -3.4163 413.0286 416.4449 397.8878 190.7855 -3.4108 412.9678 416.3785 397.7730 191.6393 -3.3988 412.8800 416.2788 397.6597 192.4023 -3.3980 412.8283 416.2264 397.5556 193.2253 -3.3988 412.7794 416.1782 397.4803 194.0178 -3.3906 412.7064 416.0970 397.3581 194.8103 -3.3938 412.6312 416.0250 397.2608 195.6325 -3.3933 412.5723 415.9656 397.1546 196.4240 -3.3870 412.4968 415.8838 397.0515 197.2460 -3.3834 412.4412 415.8245 396.9442 198.0380 -3.3768 412.3789 415.7556 396.8582 198.8295 -3.3737 412.3260 415.6997 396.7680 199.6520 -3.3753 412.2511 415.6264 396.6723 200.4438 -3.3740 412.1756 415.5496 396.5516 201.3263 -3.3635 412.1098 415.4733 396.4299 202.1175 -3.3594 412.0730 415.4324 396.3476 202.9410 -3.3546 412.0006 415.3552 396.2385 203.7063 -3.3584 411.9344 415.2928 396.1244 204.5610 -3.3618 411.8555 415.2172 396.0383 205.3530 -3.3592 411.7872 415.1465 395.9359 206.1445 -3.3546 411.7339 415.0886 395.8219 206.9668 -3.3510 411.6682 415.0192 395.7230 207.7285 -3.3470 411.6131 414.9601 395.6444 208.5798 -3.3423 411.5299 414.8722 395.5421 209.3688 -3.3398 411.4792 414.8190 395.4213 210.1570 -3.3371 411.4177 414.7548 395.3183 210.9763 -3.3314 411.3240 414.6553 395.2121 211.7350 -3.3294 411.2564 414.5858 395.1227 212.5840 -3.3256 411.1998 414.5254 395.0246 213.3728 -3.3229 411.1279 414.4508 394.9224 214.1620 -3.3192 411.0744 414.3936 394.8155 214.9808 -3.3154 411.0138 414.3292 394.7132 215.7693 -3.3127 410.9488 414.2615 394.6204 216.6030 -3.3138 410.8714 414.1852 394.5097 217.3748 -3.3072 410.8210 414.1282 394.4129 218.1943 -3.3053 410.7290 414.0343 394.3080 218.9543 -3.3033 410.6761 413.9794 394.2072 219.8048 -3.2997 410.5864 413.8862 394.1032 220.5648 -3.2956 410.5035 413.7991 394.0025 221.3855 -3.2930 410.4451 413.7381 393.9147 222.2078 -3.2898 410.3781 413.6679 393.8083 222.9693 -3.2881 410.3159 413.6041 393.7099 223.8200 -3.2816 410.2454 413.5271 393.6151 224.5818 -3.2794 410.1858 413.4652 393.5030 225.4038 -3.2769 410.0924 413.3694 393.4122 226.1950 -3.2776 410.0124 413.2900 393.3119 227.0180 -3.2737 409.9657 413.2394 393.2143 227.7825 -3.2700 409.9008 413.1708 393.1191 228.6348 -3.2694 409.7975 413.0670 393.0309 229.3965 -3.2693 409.7237 412.9930 392.9307 230.2185 -3.2638 409.6794 412.9432 392.8305 231.0408 -3.2579 409.6063 412.8642 392.7359 231.8025 -3.2509 409.5275 412.7785 392.6378 232.6545 -3.2500 409.4592 412.7091 392.5167 233.4165 -3.2490 409.3807 412.6297 392.4321 234.2388 -3.2454 409.3023 412.5477 392.3176 235.0605 -3.2471 409.2334 412.4804 392.1983 235.8225 -3.2433 409.1739 412.4171 392.1098 236.6745 -3.2377 409.0809 412.3186 392.0060 237.4585 -3.2336 409.0219 412.2555 391.8965 238.2665 -3.2303 408.9543 412.1846 391.7931 239.0585 -3.2274 408.8821 412.1096 391.7013 239.8805 -3.2252 408.8050 412.0302 391.6118 240.6425 -3.2243 408.7313 411.9556 391.4975 241.4945 -3.2188 408.6637 411.8825 391.3859 242.2865 -3.2157 408.5799 411.7956 391.2716 243.0785 -3.2117 408.5055 411.7172 391.1741 243.9005 -3.2069 408.4254 411.6323 391.0697 244.6925 -3.2056 408.3666 411.5722 390.9787 245.5143 -3.2022 408.2668 411.4690 390.8702 246.3063 -3.1981 408.1899 411.3881 390.7608 247.0980 -3.1951 408.1360 411.3311 390.6620 247.9078 -3.1926 408.0487 411.2413 390.5577 248.7300 -3.1889 407.9843 411.1732 390.4652 249.4915 -3.1853 407.9066 411.0920 390.3537 250.3440 -3.1808 407.8293 411.0101 390.2327 251.1370 -3.1764 407.7611 410.9376 390.1211 251.9285 -3.1771 407.6947 410.8718 390.0257 252.7510 -3.1737 407.6094 410.7832 389.9228 253.5125 -3.1715 407.5384 410.7099 389.8298 254.3650 -3.1658 407.4301 410.5959 389.6966 255.1570 -3.1618 407.3625 410.5243 389.6033 255.9485 -3.1584 407.2816 410.4399 389.5176 256.7710 -3.1559 407.2196 410.3756 389.4005 257.5525 -3.1533 407.1433 410.2966 389.3040 258.3455 -3.1513 407.0659 410.2172 389.1965 259.1983 -3.1465 406.9690 410.1155 389.1019 259.9605 -3.1448 406.9017 410.0465 388.9990 260.7835 -3.1413 406.8253 409.9665 388.9053 261.6060 -3.1383 406.7508 409.8891 388.7854 262.3685 -3.1365 406.6681 409.8046 388.6839 263.2205 -3.1302 406.5857 409.7159 388.5739 263.9825 -3.1305 406.5025 409.6330 388.4792 264.8045 -3.1277 406.4438 409.5715 388.3748 265.6268 -3.1237 406.3713 409.4950 388.2721 266.3895 -3.1208 406.2978 409.4185 388.1848 267.2415 -3.1163 406.2063 409.3225 388.0859 268.0140 -3.1141 406.1218 409.2359 387.9703 268.8165 -3.1102 406.0432 409.1534 387.8640 269.6393 -3.1100 405.9662 409.0762 387.7764 270.4315 -3.1090 405.8839 408.9928 387.6692 271.2235 -3.1080 405.7986 408.9065 387.5908 272.0455 -3.1006 405.7233 408.8239 387.4736 272.8338 -3.0942 405.6513 408.7455 387.3819 273.6808 -3.0824 405.5463 408.6287 387.2791 274.4993 -3.0852 405.4866 408.5718 387.1787 275.2873 -3.0862 405.3969 408.4831 387.0885 276.0755 -3.0838 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