DTA measure 1gyors_h Date: 2026310:1120 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.31 s Mass = 1173.400 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2000 -4.3352 186.6041 190.9393 247.5998 2.0175 -4.3323 186.8618 191.1941 247.5472 2.7935 -4.3246 187.1013 191.4259 247.4803 3.6215 -4.3130 187.3620 191.6750 247.4304 4.3875 -4.3009 187.6205 191.9214 247.3575 5.2355 -4.2888 187.9156 192.2044 247.3071 6.0123 -4.2747 188.1588 192.4335 247.2251 6.8293 -4.2613 188.4005 192.6618 247.1303 7.6263 -4.2519 188.6190 192.8709 247.0490 8.4235 -4.2402 188.8399 193.0802 246.9491 9.2513 -4.2282 189.0718 193.3000 246.8734 10.0170 -4.2164 189.2914 193.5078 246.8063 10.8655 -4.1997 189.5969 193.7966 246.7231 11.6423 -4.1920 189.8258 194.0178 246.6710 12.4590 -4.1811 190.0866 194.2676 246.6024 13.2563 -4.1617 190.3464 194.5081 246.5406 14.0535 -4.1556 190.5825 194.7381 246.5192 14.8910 -4.1479 190.8168 194.9647 246.4759 15.6470 -4.1399 191.0382 195.1782 246.4397 16.5058 -4.1151 191.2942 195.4092 246.3973 17.2715 -4.1009 191.5401 195.6410 246.3919 18.0993 -4.0883 191.8203 195.9086 246.3706 18.8658 -4.0800 192.0667 196.1467 246.3513 19.6828 -4.0690 192.3279 196.3969 246.2995 20.4900 -4.0527 192.5579 196.6106 246.3033 21.2873 -4.0377 192.7746 196.8123 246.2854 22.1148 -4.0225 192.9985 197.0209 246.2725 22.8705 -4.0111 193.2276 197.2387 246.2397 23.7395 -3.9936 193.4807 197.4744 246.2266 24.4953 -3.9794 193.7237 197.7031 246.2183 25.3228 -3.9704 193.9270 197.8974 246.2274 26.1200 -3.9586 194.1547 198.1133 246.2227 26.9268 -3.9459 194.3385 198.2844 246.2522 27.7443 -3.9316 194.5821 198.5137 246.2714 28.5108 -3.9171 194.8195 198.7366 246.3125 29.3693 -3.8962 195.0756 198.9718 246.3839 30.1350 -3.8812 195.2968 199.1781 246.4227 30.9630 -3.8674 195.5249 199.3923 246.4798 31.7500 -3.8524 195.7868 199.6392 246.5024 32.5565 -3.8416 196.0292 199.8708 246.5916 33.3743 -3.8293 196.2630 200.0923 246.6711 34.1408 -3.8174 196.5037 200.3211 246.7461 34.9993 -3.8073 196.7546 200.5619 246.8573 35.7650 -3.7917 196.9788 200.7705 246.9663 36.5930 -3.7766 197.2077 200.9844 247.0852 37.3795 -3.7614 197.4008 201.1622 247.1635 38.1865 -3.7488 197.6507 201.3995 247.2632 39.0145 -3.7379 197.8670 201.6049 247.3774 39.7703 -3.7277 198.0602 201.7879 247.5068 40.6285 -3.7172 198.2942 202.0114 247.6273 41.3848 -3.7072 198.4925 202.1997 247.7524 42.2025 -3.6992 198.7005 202.3997 247.8711 42.9988 -3.6907 198.9346 202.6253 248.0037 43.7960 -3.6827 199.1513 202.8340 248.1535 44.6135 -3.6679 199.3904 203.0583 248.2921 45.3793 -3.6570 199.6051 203.2621 248.3984 46.2278 -3.6442 199.8227 203.4669 248.5316 46.9940 -3.6308 200.0264 203.6572 248.6902 47.8110 -3.6122 200.2323 203.8445 248.8309 48.6083 -3.6012 200.4336 204.0348 249.0373 49.4055 -3.5905 200.6246 204.2152 249.1931 50.2325 -3.5793 200.8291 204.4083 249.3789 50.9888 -3.5685 201.0147 204.5831 249.5417 51.8475 -3.5596 201.2568 204.8164 249.7363 52.6033 -3.5524 201.4679 205.0203 249.8935 53.4308 -3.5412 201.6896 205.2308 250.0751 54.2280 -3.5259 201.9150 205.4409 250.2343 55.0245 -3.5129 202.1238 205.6367 250.4236 55.8523 -3.5006 202.3580 205.8586 250.6228 56.6085 -3.4918 202.5652 206.0570 250.8289 57.4463 -3.4780 202.7824 206.2604 251.0475 58.2020 -3.4691 202.9512 206.4204 251.2074 59.0608 -3.4655 203.1572 206.6227 251.3838 59.8265 -3.4537 203.3625 206.8161 251.5695 60.6543 -3.4464 203.5783 207.0247 251.7872 61.4515 -3.4377 203.7538 207.1915 251.9658 62.2378 -3.4285 203.9818 207.4102 252.1311 63.0758 -3.4241 204.1844 207.6084 252.3275 63.8320 -3.4200 204.3671 207.7870 252.5680 64.6900 -3.4028 204.6158 208.0186 252.7903 65.4563 -3.3998 204.8390 208.2388 252.9534 66.2843 -3.3901 205.0622 208.4524 253.1500 67.0808 -3.3792 205.2425 208.6217 253.3227 67.8675 -3.3709 205.4341 208.8051 253.5177 68.7058 -3.3701 205.6538 209.0239 253.7093 69.4615 -3.3623 205.8373 209.1996 253.8986 70.2890 -3.3503 206.0298 209.3802 254.0555 71.0555 -3.3435 206.2130 209.5565 254.2153 71.9138 -3.3307 206.4307 209.7614 254.3918 72.6798 -3.3238 206.6419 209.9657 254.6088 73.4975 -3.3199 206.8657 210.1856 254.8250 74.3043 -3.3101 207.0952 210.4052 255.0039 75.0910 -3.3009 207.3239 210.6248 255.1671 75.9190 -3.2921 207.5427 210.8349 255.3569 76.6850 -3.2876 207.7533 211.0409 255.5171 77.5433 -3.2806 207.9491 211.2297 255.6703 78.3098 -3.2781 208.1483 211.4263 255.8500 79.1268 -3.2737 208.3441 211.6178 256.0382 79.9340 -3.2662 208.5457 211.8120 256.1969 80.7210 -3.2590 208.7205 211.9795 256.3413 81.5485 -3.2539 208.9178 212.1717 256.5129 82.3145 -3.2457 209.0816 212.3273 256.6908 83.1733 -3.2432 209.2771 212.5204 256.9194 83.9398 -3.2367 209.4767 212.7134 257.0781 84.7565 -3.2305 209.6936 212.9242 257.2976 85.5333 -3.2245 209.8921 213.1166 257.4479 86.3510 -3.2223 210.0829 213.3053 257.6204 87.1473 -3.2177 210.2692 213.4869 257.7754 87.9445 -3.2104 210.4748 213.6852 257.9474 88.7725 -3.2018 210.6926 213.8944 258.0864 89.5385 -3.1927 210.8458 214.0385 258.1947 90.3865 -3.1895 211.0606 214.2501 258.3685 91.1633 -3.1821 211.2593 214.4414 258.4978 91.9805 -3.1741 211.4438 214.6180 258.6540 92.7773 -3.1711 211.6128 214.7839 258.7847 93.5745 -3.1668 211.7819 214.9487 258.9059 94.4020 -3.1608 211.9676 215.1284 259.0386 95.1680 -3.1561 212.1539 215.3100 259.1590 96.0165 -3.1530 212.3552 215.5082 259.2795 96.7928 -3.1470 212.5409 215.6879 259.3962 97.6100 -3.1403 212.7041 215.8443 259.5538 98.3868 -3.1372 212.8776 216.0147 259.6986 99.2143 -3.1314 213.0866 216.2181 259.8556 99.9905 -3.1265 213.3071 216.4335 259.9772 100.8390 -3.1191 213.5364 216.6555 260.0944 101.6050 -3.1131 213.7183 216.8314 260.2249 102.4325 -3.1113 213.9305 217.0418 260.3507 103.2298 -3.1073 214.1046 217.2119 260.4758 104.0268 -3.0989 214.3016 217.4006 260.6008 104.8438 -3.0950 214.4766 217.5717 260.7319 105.6103 -3.0952 214.6661 217.7614 260.8535 106.4280 -3.0912 214.8415 217.9327 260.9559 107.1935 -3.0866 215.0381 218.1248 261.0750 108.0420 -3.0783 215.2643 218.3426 261.2118 108.8185 -3.0736 215.4084 218.4820 261.3234 109.6355 -3.0625 215.6134 218.6760 261.4462 110.4328 -3.0518 215.8200 218.8718 261.5685 111.2295 -3.0471 216.0602 219.1073 261.6542 112.0468 -3.0438 216.2947 219.3384 261.7796 112.8133 -3.0349 216.4853 219.5202 261.8777 113.6720 -3.0256 216.6916 219.7172 261.9710 114.3965 -3.0239 216.8610 219.8849 262.0540 115.2553 -3.0202 217.0380 220.0581 262.1917 116.0218 -3.0187 217.2086 220.2274 262.2768 116.8385 -3.0178 217.3681 220.3859 262.3676 117.6358 -3.0098 217.5138 220.5236 262.4780 118.4328 -3.0034 217.7093 220.7126 262.5430 119.2600 -2.9935 217.9529 220.9464 262.6238 120.0470 -2.9902 218.1414 221.1316 262.7155 120.8648 -2.9870 218.3426 221.3296 262.7884 121.6405 -2.9829 218.5076 221.4906 262.8983 122.4890 -2.9800 218.6933 221.6733 263.0330 123.2550 -2.9732 218.8609 221.8341 263.1550 124.0825 -2.9752 219.0583 222.0335 263.2674 124.8798 -2.9721 219.2488 222.2209 263.3530 125.6765 -2.9681 219.4020 222.3701 263.4493 126.4938 -2.9598 219.5770 222.5368 263.5764 127.2705 -2.9550 219.7284 222.6835 263.6990 128.0880 -2.9511 219.8913 222.8424 263.8182 128.8538 -2.9444 220.0715 223.0159 263.9461 129.7125 -2.9397 220.2003 223.1400 264.1449 130.4788 -2.9344 220.3686 223.3031 264.2616 131.3060 -2.9278 220.5987 223.5265 264.3927 132.0930 -2.9234 220.7991 223.7225 264.5192 132.9003 -2.9197 220.9782 223.8979 264.6334 133.7173 -2.9161 221.1898 224.1059 264.7496 134.4940 -2.9141 221.3655 224.2796 264.8625 135.3423 -2.9121 221.5445 224.4566 264.9813 136.1183 -2.9066 221.7276 224.6342 265.1030 136.9360 -2.8997 221.9432 224.8429 265.2341 137.7333 -2.8930 222.1371 225.0301 265.3517 138.5295 -2.8887 222.3104 225.1991 265.4717 139.3575 -2.8857 222.5106 225.3963 265.5909 140.1240 -2.8802 222.6735 225.5538 265.7075 140.9718 -2.8730 222.8367 225.7097 265.8686 141.7483 -2.8692 222.9807 225.8499 265.9648 142.5660 -2.8645 223.1580 226.0226 266.0762 143.3628 -2.8617 223.3178 226.1795 266.1874 144.1595 -2.8598 223.4944 226.3543 266.3002 144.9875 -2.8580 223.7028 226.5607 266.4332 145.7533 -2.8565 223.8700 226.7265 266.5632 146.6118 -2.8473 224.0752 226.9225 266.7086 147.3783 -2.8437 224.3074 227.1511 266.8185 148.2055 -2.8390 224.4884 227.3274 266.9369 149.0025 -2.8360 224.6484 227.4844 267.0175 149.7895 -2.8349 224.8161 227.6511 267.1332 150.6270 -2.8310 225.0110 227.8420 267.2828 151.3830 -2.8296 225.1936 228.0232 267.4258 152.2520 -2.8282 225.3407 228.1689 267.5448 153.0073 -2.8230 225.5001 228.3231 267.6727 153.8455 -2.8186 225.7024 228.5210 267.8307 154.6325 -2.8113 225.8476 228.6590 267.9862 155.4293 -2.8087 226.0083 228.8170 268.1493 156.2568 -2.8053 226.1661 228.9714 268.2913 157.0233 -2.7980 226.3196 229.1176 268.4341 157.8815 -2.7944 226.4996 229.2940 268.5833 158.6475 -2.7918 226.6802 229.4720 268.7108 159.4755 -2.7877 226.8679 229.6555 268.8456 160.2720 -2.7823 227.0500 229.8323 268.9716 161.0690 -2.7779 227.2217 229.9996 269.1171 161.8868 -2.7764 227.4050 230.1814 269.2326 162.6628 -2.7745 227.5643 230.3388 269.4049 163.5110 -2.7683 227.7026 230.4709 269.5198 164.2878 -2.7617 227.8611 230.6229 269.6241 165.1048 -2.7580 228.0791 230.8371 269.7654 165.9120 -2.7557 228.2524 231.0080 269.9306 166.6990 -2.7537 228.3938 231.1475 270.0863 167.5260 -2.7513 228.5534 231.3047 270.2558 168.2925 -2.7468 228.6964 231.4432 270.3936 169.1410 -2.7464 228.8654 231.6119 270.5485 169.9065 -2.7465 229.0212 231.7677 270.6925 170.7345 -2.7449 229.1832 231.9281 270.8293 171.5215 -2.7406 229.3113 232.0519 270.9823 172.3078 -2.7367 229.4710 232.2077 271.1733 173.1355 -2.7319 229.6709 232.4028 271.3370 173.9020 -2.7317 229.8669 232.5986 271.4948 174.7188 -2.7287 230.0490 232.7777 271.6383 175.4955 -2.7230 230.1958 232.9188 271.7917 176.3440 -2.7181 230.4075 233.1255 271.9160 177.0993 -2.7186 230.5915 233.3101 272.0556 177.9273 -2.7210 230.7840 233.5049 272.2203 178.7245 -2.7126 230.9393 233.6520 272.3786 179.5105 -2.7137 231.0615 233.7752 272.5301 180.3385 -2.7148 231.2388 233.9536 272.7069 181.1050 -2.7123 231.3991 234.1114 272.8271 181.9525 -2.7115 231.6259 234.3374 272.9735 182.6985 -2.7069 231.8055 234.5124 273.1056 183.5470 -2.7016 231.9830 234.6845 273.2473 184.3128 -2.7019 232.1508 234.8527 273.3640 185.1405 -2.7013 232.3502 235.0515 273.4996 185.9375 -2.6977 232.5989 235.2966 273.6426 186.7340 -2.6900 232.7477 235.4377 273.7967 187.5518 -2.6846 232.8759 235.5605 273.9150 188.3178 -2.6840 233.0173 235.7012 273.9990 189.1760 -2.6826 233.1913 235.8739 274.1435 189.9015 -2.6782 233.3290 236.0072 274.2866 190.7703 -2.6713 233.5349 236.2062 274.3862 191.5258 -2.6713 233.6454 236.3167 274.5160 192.3538 -2.6667 233.8199 236.4866 274.6472 193.1508 -2.6571 233.9795 236.6367 274.7943 193.9473 -2.6504 234.1110 236.7614 274.9401 194.7753 -2.6504 234.2596 236.9100 275.0688 195.5313 -2.6496 234.4185 237.0681 275.1754 196.3995 -2.6526 234.5724 237.2251 275.3090 197.1250 -2.6514 234.7322 237.3836 275.4081 197.9835 -2.6537 234.8599 237.5137 275.5193 198.7493 -2.6559 235.0422 237.6980 275.6456 199.5773 -2.6547 235.2418 237.8965 275.7750 200.3745 -2.6554 235.4587 238.1141 275.8763 201.1605 -2.6562 235.6528 238.3090 276.0033 201.9988 -2.6573 235.8304 238.4877 276.1656 202.7548 -2.6583 235.9611 238.6194 276.3169 203.6128 -2.6537 236.1351 238.7888 276.4254 204.3793 -2.6554 236.2978 238.9532 276.5531 205.2073 -2.6536 236.4605 239.1141 276.6715 206.0035 -2.6496 236.6454 239.2950 276.7946 206.7905 -2.6493 236.7876 239.4369 276.9412 207.6288 -2.6479 236.9930 239.6409 277.0518 208.3843 -2.6451 237.1600 239.8050 277.1650 209.2428 -2.6405 237.3261 239.9667 277.3163 210.0093 -2.6338 237.4989 240.1327 277.4397 210.8368 -2.6319 237.6714 240.3033 277.5509 211.6028 -2.6271 237.8067 240.4338 277.6325 212.4308 -2.6281 237.9664 240.5945 277.7647 213.2278 -2.6265 238.1026 240.7291 277.9071 214.0243 -2.6224 238.2539 240.8762 278.0077 214.8523 -2.6227 238.3797 241.0023 278.0921 215.6078 -2.6205 238.5290 241.1494 278.2127 216.4765 -2.6174 238.7326 241.3500 278.3453 217.2328 -2.6136 238.8853 241.4989 278.4759 218.0603 -2.6097 239.0403 241.6500 278.6232 218.8570 -2.6061 239.2070 241.8131 278.7504 219.6543 -2.6050 239.3330 241.9380 278.8863 220.4820 -2.6066 239.4991 242.1058 278.9774 221.2580 -2.6081 239.6805 242.2886 279.0867 222.0758 -2.6038 239.8429 242.4467 279.1997 222.8523 -2.6003 239.9896 242.5898 279.3264 223.7000 -2.6036 240.1503 242.7539 279.4326 224.4665 -2.6050 240.3260 242.9310 279.5506 225.2945 -2.6029 240.4860 243.0888 279.6845 226.1013 -2.5978 240.6051 243.2029 279.8076 226.8880 -2.5936 240.7662 243.3598 279.9304 227.7160 -2.5936 240.9569 243.5505 280.0361 228.4818 -2.5918 241.1083 243.7000 280.1420 229.3403 -2.5916 241.2934 243.8850 280.2713 230.1068 -2.5843 241.4239 244.0082 280.4102 230.9238 -2.5813 241.5719 244.1532 280.5297 231.7310 -2.5807 241.7472 244.3279 280.6897 232.5180 -2.5801 241.9037 244.4838 280.8383 233.3353 -2.5799 242.0693 244.6492 280.9536 234.1115 -2.5761 242.2390 244.8151 281.1412 234.9600 -2.5748 242.4545 245.0293 281.2609 235.7155 -2.5762 242.6063 245.1825 281.3666 236.5433 -2.5709 242.7709 245.3418 281.5216 237.3303 -2.5695 242.9323 245.5019 281.6624 238.1270 -2.5692 243.1041 245.6733 281.7907 238.9545 -2.5700 243.2526 245.8226 281.9103 239.7108 -2.5712 243.3876 245.9587 282.0394 240.5690 -2.5738 243.5795 246.1532 282.2083 241.3350 -2.5739 243.7264 246.3003 282.3113 242.1528 -2.5703 243.8786 246.4489 282.4443 242.9185 -2.5690 244.0203 246.5893 282.5714 243.7463 -2.5650 244.1620 246.7269 282.6989 244.5333 -2.5638 244.3010 246.8648 282.8408 245.3300 -2.5609 244.4570 247.0179 282.9680 246.1575 -2.5617 244.5759 247.1375 283.0870 246.9240 -2.5660 244.7029 247.2689 283.2009 247.7723 -2.5686 244.8680 247.4366 283.3553 248.5483 -2.5638 245.0118 247.5756 283.5134 249.3660 -2.5604 245.1724 247.7328 283.6647 250.1528 -2.5572 245.3046 247.8618 283.8069 250.9595 -2.5627 245.4834 248.0461 283.9430 251.7773 -2.5637 245.6558 248.2194 284.0596 252.5433 -2.5621 245.8104 248.3725 284.1848 253.4015 -2.5594 246.0085 248.5679 284.3298 254.1680 -2.5567 246.1464 248.7031 284.4957 254.9955 -2.5542 246.2717 248.8259 284.6371 255.7820 -2.5519 246.4534 249.0052 284.7457 256.5793 -2.5485 246.6137 249.1622 284.8761 257.4070 -2.5459 246.7571 249.3030 285.0521 258.1625 -2.5441 246.8927 249.4368 285.1742 259.0315 -2.5427 247.0558 249.5984 285.3216 259.7878 -2.5453 247.2434 249.7887 285.4355 260.6148 -2.5430 247.4148 249.9578 285.5652 261.4120 -2.5413 247.5808 250.1221 285.7053 262.2090 -2.5421 247.7379 250.2800 285.8157 263.0363 -2.5417 247.9240 250.4657 285.9684 263.7925 -2.5422 248.0744 250.6166 286.1061 264.6613 -2.5449 248.2395 250.7844 286.2259 265.4168 -2.5443 248.3513 250.8957 286.3392 266.2448 -2.5426 248.5113 251.0539 286.4831 267.0418 -2.5420 248.6508 251.1928 286.6276 267.8383 -2.5427 248.8022 251.3449 286.7295 268.6663 -2.5452 248.9541 251.4993 286.8604 269.4533 -2.5509 249.1050 251.6559 287.0053 270.2908 -2.5463 249.2671 251.8133 287.1711 271.0775 -2.5457 249.4206 251.9663 287.3214 271.8748 -2.5466 249.6028 252.1494 287.4464 272.7018 -2.5429 249.7461 252.2890 287.5693 273.4683 -2.5395 249.8934 252.4329 287.6925 274.3270 -2.5369 250.0680 252.6049 287.8483 275.0833 -2.5372 250.2193 252.7565 287.9983 275.9205 -2.5362 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