DTA measure 1lassu Date: 2026310:1237 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1273.94 s Mass = 1173.400 mg data_number = 1582 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1693 0.0411 235.8617 235.8207 250.4408 1.9965 0.0380 235.8546 235.8166 250.4117 2.7525 0.0295 235.8756 235.8461 250.3758 3.6215 0.0213 235.9287 235.9074 250.3267 4.3870 0.0156 235.9703 235.9547 250.3029 5.2048 0.0082 235.9684 235.9602 250.2631 6.0020 -0.0011 235.9814 235.9826 250.2625 6.8085 -0.0094 235.9892 235.9985 250.2343 7.6263 -0.0136 236.0360 236.0497 250.1818 8.3925 -0.0174 236.0827 236.1001 250.1812 9.2505 -0.0234 236.1460 236.1693 250.1734 10.0170 -0.0285 236.1912 236.2197 250.1384 10.8448 -0.0424 236.2391 236.2815 250.0614 11.6310 -0.0496 236.2748 236.3243 250.0247 12.4385 -0.0551 236.3201 236.3752 249.9881 13.2563 -0.0560 236.4235 236.4794 249.9690 14.0220 -0.0628 236.4630 236.5258 249.9340 14.8805 -0.0677 236.4986 236.5663 249.9573 15.6265 -0.0685 236.5064 236.5749 249.9525 16.4743 -0.0698 236.5516 236.6214 249.9466 17.2405 -0.0793 236.5930 236.6723 249.9237 18.0685 -0.0825 236.6023 236.6848 249.8887 18.8750 -0.0859 236.6327 236.7185 249.9290 19.6620 -0.0866 236.6755 236.7621 249.9184 20.4900 -0.0892 236.6925 236.7817 249.8716 21.2558 -0.0986 236.7365 236.8351 249.8645 22.1450 -0.1040 236.7797 236.8837 249.8443 22.9730 -0.1047 236.8226 236.9273 249.8605 23.7695 -0.1068 236.8942 237.0010 249.8796 24.5665 -0.1085 236.9541 237.0626 249.8483 25.3843 -0.1097 236.9606 237.0703 249.8222 26.1605 -0.1145 236.9765 237.0910 249.8408 27.0085 -0.1210 236.9960 237.1170 249.8723 27.7853 -0.1227 237.0258 237.1485 249.8858 28.6025 -0.1239 237.0961 237.2200 249.8739 29.3685 -0.1281 237.1218 237.2499 249.9060 30.1965 -0.1330 237.1603 237.2933 249.9708 30.9930 -0.1357 237.2193 237.3550 249.9897 31.7900 -0.1389 237.2635 237.4024 250.0435 32.6078 -0.1432 237.2692 237.4124 250.1081 33.3838 -0.1488 237.3077 237.4565 250.1436 34.2320 -0.1480 237.3456 237.4936 250.2008 34.9985 -0.1552 237.3535 237.5087 250.2485 35.8263 -0.1634 237.4043 237.5677 250.3281 36.6433 -0.1633 237.4494 237.6127 250.3757 37.3995 -0.1666 237.4683 237.6349 250.4193 38.2275 -0.1691 237.5114 237.6805 250.4690 38.9930 -0.1693 237.5405 237.7098 250.5228 39.8415 -0.1802 237.5835 237.7638 250.5723 40.6078 -0.1863 237.6238 237.8101 250.6240 41.4248 -0.1882 237.6459 237.8341 250.7066 42.2220 -0.1874 237.6753 237.8627 250.7748 43.0193 -0.1860 237.7311 237.9171 250.8310 43.8360 -0.1835 237.7755 237.9589 250.9046 44.6025 -0.1812 237.8411 238.0224 250.9511 45.4510 -0.1801 237.9080 238.0881 251.0395 46.2165 -0.1821 237.9454 238.1275 251.1101 47.0445 -0.1905 237.9514 238.1419 251.2055 47.8315 -0.1924 237.9548 238.1471 251.3245 48.6278 -0.1953 237.9829 238.1782 251.4390 49.4558 -0.2007 238.0143 238.2150 251.5374 50.2120 -0.2122 238.0619 238.2741 251.6176 51.0698 -0.2145 238.1085 238.3230 251.7067 51.8055 -0.2149 238.1546 238.3694 251.7910 52.6643 -0.2239 238.1955 238.4194 251.8682 53.4300 -0.2280 238.2497 238.4777 251.9794 54.2578 -0.2301 238.3115 238.5416 252.0958 55.0550 -0.2288 238.3638 238.5926 252.2106 55.8515 -0.2311 238.4012 238.6323 252.3018 56.6690 -0.2331 238.4347 238.6678 252.4273 57.4355 -0.2319 238.4601 238.6920 252.5539 58.2933 -0.2356 238.5244 238.7600 252.6673 59.1213 -0.2344 238.5743 238.8086 252.7675 59.8980 -0.2387 238.6029 238.8416 252.9059 60.7148 -0.2419 238.6410 238.8829 253.0431 61.4915 -0.2488 238.6674 238.9162 253.1388 62.3400 -0.2556 238.7027 238.9582 253.2851 63.1055 -0.2623 238.7423 239.0046 253.3935 63.9335 -0.2693 238.8026 239.0719 253.5259 64.7308 -0.2710 238.8575 239.1284 253.6517 65.7735 -0.2710 238.9114 239.1825 253.8343 66.7650 -0.2743 238.9975 239.2718 254.0184 67.5110 -0.2772 239.0464 239.3237 254.1255 68.3488 -0.2762 239.0881 239.3643 254.2573 69.1045 -0.2802 239.1413 239.4214 254.3698 69.9735 -0.2866 239.1613 239.4480 254.4723 70.7495 -0.2910 239.2013 239.4923 254.5860 71.5670 -0.2959 239.2449 239.5407 254.7084 72.3438 -0.2994 239.2712 239.5707 254.8391 73.1608 -0.3010 239.3231 239.6240 254.9796 74.0910 -0.3084 239.3780 239.6865 255.1290 75.0010 -0.3179 239.4244 239.7422 255.2985 75.7363 -0.3217 239.4817 239.8034 255.3755 76.5945 -0.3275 239.5361 239.8636 255.5140 77.3610 -0.3323 239.5826 239.9149 255.6486 78.1885 -0.3370 239.6069 239.9439 255.7907 78.9750 -0.3369 239.6656 240.0025 255.9023 79.7825 -0.3400 239.7381 240.0782 255.9904 80.6200 -0.3444 239.8018 240.1462 256.1334 81.3760 -0.3480 239.8473 240.1953 256.2806 82.2450 -0.3496 239.9216 240.2712 256.4225 82.9698 -0.3549 239.9547 240.3096 256.5053 83.8385 -0.3598 240.0093 240.3691 256.6516 84.6050 -0.3633 240.0763 240.4396 256.7486 85.4320 -0.3728 240.1398 240.5126 256.8831 86.2190 -0.3807 240.1966 240.5773 257.0151 87.0265 -0.3896 240.2344 240.6240 257.1628 87.8438 -0.3943 240.2974 240.6917 257.3213 88.6405 -0.3997 240.3180 240.7177 257.4232 89.4685 -0.4026 240.3467 240.7493 257.5203 90.2345 -0.4086 240.4177 240.8262 257.6355 91.0825 -0.4139 240.5087 240.9226 257.7612 91.8593 -0.4200 240.5691 240.9891 257.8650 92.6765 -0.4260 240.6613 241.0873 257.9715 93.4733 -0.4334 240.7181 241.1516 258.1153 94.2705 -0.4439 240.7565 241.2005 258.2614 95.0978 -0.4518 240.8163 241.2681 258.4160 95.8640 -0.4566 240.8388 241.2954 258.5291 96.7125 -0.4644 240.8889 241.3533 258.6553 97.4578 -0.4691 240.9544 241.4235 258.7524 98.3163 -0.4717 241.0516 241.5233 258.8884 99.0828 -0.4760 241.0594 241.5354 258.9913 99.8998 -0.4791 241.1065 241.5856 259.0920 100.6968 -0.4806 241.1903 241.6708 259.1797 101.4838 -0.4844 241.2194 241.7038 259.2922 102.3108 -0.4879 241.2473 241.7352 259.4326 103.0773 -0.4897 241.2996 241.7892 259.5521 103.9258 -0.4932 241.3161 241.8093 259.6560 104.6608 -0.4992 241.3280 241.8272 259.7583 105.5090 -0.5105 241.3742 241.8848 259.8623 106.2755 -0.5160 241.4418 241.9577 259.9735 107.1030 -0.5180 241.5090 242.0270 260.0696 107.8895 -0.5149 241.5660 242.0808 260.1556 108.6868 -0.5176 241.6214 242.1390 260.2533 109.5145 -0.5213 241.6552 242.1765 260.3545 110.2803 -0.5250 241.7189 242.2439 260.4459 111.0980 -0.5297 241.8001 242.3298 260.5443 111.8640 -0.5327 241.8871 242.4198 260.6567 112.7223 -0.5384 241.9509 242.4894 260.7635 113.4785 -0.5420 241.9955 242.5375 260.8675 114.3063 -0.5436 242.0598 242.6034 261.0199 115.1028 -0.5465 242.1102 242.6567 261.1532 115.9000 -0.5487 242.1522 242.7009 261.2486 116.7173 -0.5537 242.2187 242.7724 261.3428 117.4935 -0.5581 242.2899 242.8480 261.4379 118.3420 -0.5638 242.3600 242.9239 261.5422 119.0875 -0.5705 242.4226 242.9930 261.6530 119.9458 -0.5752 242.4888 243.0640 261.7708 120.7123 -0.5822 242.5382 243.1204 261.8688 121.5398 -0.5883 242.6271 243.2154 261.9519 122.3058 -0.5924 242.6604 243.2528 262.0408 123.1235 -0.5953 242.7337 243.3290 262.1547 123.9308 -0.6011 242.7952 243.3963 262.2544 124.7170 -0.6070 242.8476 243.4545 262.3637 125.6270 -0.6093 242.9332 243.5425 262.4265 126.4960 -0.6156 242.9852 243.6008 262.4682 127.3025 -0.6230 243.0629 243.6860 262.5307 128.1203 -0.6251 243.1776 243.8026 262.6300 128.8868 -0.6272 243.2281 243.8552 262.7340 129.7445 -0.6301 243.2909 243.9210 262.8077 130.4905 -0.6323 243.3135 243.9458 262.8910 131.3493 -0.6367 243.3877 244.0245 263.0004 132.1148 -0.6394 243.4487 244.0881 263.1316 132.9325 -0.6474 243.5325 244.1798 263.2150 133.7090 -0.6535 243.5770 244.2305 263.3161 134.5260 -0.6553 243.6320 244.2873 263.4411 135.3335 -0.6571 243.6980 244.3551 263.5323 136.1308 -0.6602 243.7798 244.4401 263.5444 136.9578 -0.6635 243.8425 244.5060 263.5897 137.7243 -0.6676 243.8851 244.5528 263.6745 138.5830 -0.6735 243.9530 244.6265 263.7565 139.3693 -0.6798 244.0168 244.6966 263.8356 140.2995 -0.6810 244.0981 244.7792 263.9795 141.0968 -0.6898 244.1675 244.8573 264.0685 141.8930 -0.6958 244.2027 244.8985 264.1592 142.7108 -0.6857 244.2750 244.9607 264.2654 143.4875 -0.6687 244.3558 245.0245 264.3593 144.3353 -0.6663 244.4222 245.0886 264.4800 145.0810 -0.6652 244.4648 245.1300 264.5690 145.9295 -0.6631 244.5132 245.1764 264.6589 146.7053 -0.6643 244.5870 245.2513 264.7504 147.5230 -0.6620 244.6768 245.3389 264.8285 148.3203 -0.6555 244.7431 245.3985 264.9135 149.1783 -0.6571 244.8000 245.4571 264.9844 150.1085 -0.6681 244.8873 245.5553 265.0920 150.8955 -0.6781 244.9431 245.6212 265.1821 151.6923 -0.6891 245.0625 245.7516 265.2945 152.5198 -0.6958 245.1470 245.8429 265.3965 153.2863 -0.7020 245.2291 245.9311 265.4782 154.1440 -0.7030 245.3186 246.0215 265.5827 154.9003 -0.7068 245.3774 246.0843 265.6920 155.7385 -0.7149 245.4404 246.1552 265.8188 156.5040 -0.7242 245.5063 246.2305 265.8903 157.3320 -0.7316 245.5965 246.3281 265.9679 158.1188 -0.7335 245.6173 246.3507 266.0173 158.9255 -0.7306 245.6602 246.3908 266.0792 159.7433 -0.7337 245.7230 246.4568 266.1962 160.5098 -0.7396 245.8074 246.5470 266.3056 161.3680 -0.7444 245.8434 246.5878 266.4249 162.1340 -0.7477 245.9120 246.6597 266.5192 162.9620 -0.7520 246.0047 246.7567 266.6244 163.7590 -0.7555 246.0709 246.8265 266.7241 164.5555 -0.7630 246.1081 246.8711 266.8256 165.3835 -0.7724 246.1541 246.9266 266.9195 166.1498 -0.7763 246.2380 247.0143 267.0061 166.9668 -0.7808 246.2998 247.0806 267.1247 167.7640 -0.7905 246.3864 247.1769 267.2300 168.5813 -0.7973 246.4666 247.2639 267.3417 169.3473 -0.7981 246.5743 247.3724 267.4316 170.1958 -0.7966 246.6807 247.4773 267.5461 170.9623 -0.7960 246.7657 247.5617 267.6512 171.7893 -0.8020 246.8056 247.6076 267.7786 172.5455 -0.8025 246.8889 247.6914 267.8528 173.3733 -0.8069 246.9669 247.7738 267.9627 174.1698 -0.8076 247.0563 247.8639 268.0715 174.9670 -0.8084 247.1424 247.9507 268.1511 175.7843 -0.8166 247.2126 248.0292 268.2574 176.5605 -0.8211 247.2675 248.0886 268.3372 177.4090 -0.8267 247.3347 248.1614 268.4318 178.1645 -0.8319 247.4147 248.2466 268.5245 179.0025 -0.8358 247.4914 248.3272 268.6410 179.7690 -0.8431 247.5327 248.3757 268.7381 180.5965 -0.8549 247.5979 248.4528 268.8259 181.3933 -0.8611 247.6952 248.5563 268.9429 182.1905 -0.8650 247.7712 248.6362 269.0643 183.0183 -0.8704 247.8230 248.6934 269.1888 183.7840 -0.8748 247.9041 248.7789 269.2743 184.6018 -0.8780 247.9991 248.8771 269.3602 185.4090 -0.8776 248.0955 248.9731 269.4548 186.3285 -0.8811 248.1769 249.0580 269.5381 187.0950 -0.8840 248.2463 249.1303 269.6157 187.9433 -0.8869 248.3127 249.1996 269.6842 188.7193 -0.8897 248.3512 249.2409 269.7789 189.5370 -0.8896 248.4285 249.3182 269.8477 190.3443 -0.8873 248.5018 249.3891 269.9833 191.1408 -0.8868 248.5712 249.4580 270.1147 191.9380 -0.8812 248.6134 249.4945 270.2622 192.7350 -0.8844 248.6787 249.5631 270.3673 193.5623 -0.8908 248.7943 249.6852 270.4698 194.3185 -0.8968 248.8716 249.7684 270.5435 195.1873 -0.8973 248.9245 249.8218 270.6694 195.9120 -0.8950 248.9713 249.8663 270.7577 196.8938 -0.8939 249.0622 249.9560 270.8859 197.7523 -0.8950 249.1340 250.0290 270.9749 198.5180 -0.8957 249.2009 250.0966 271.0732 199.3460 -0.8887 249.2786 250.1673 271.1650 200.1433 -0.8841 249.3249 250.2090 271.2656 200.9395 -0.8811 249.4066 250.2877 271.3783 201.7880 -0.8836 249.4882 250.3718 271.4702 202.5545 -0.8908 249.5789 250.4697 271.5385 203.3820 -0.8992 249.6463 250.5455 271.6093 204.1788 -0.9058 249.6935 250.5993 271.7187 204.9760 -0.9125 249.7893 250.7018 271.8115 205.7935 -0.9077 249.9161 250.8239 271.8954 206.5695 -0.9023 250.0022 250.9045 272.0064 207.4180 -0.9051 250.0749 250.9801 272.1072 208.1948 -0.9131 250.1229 251.0359 272.2096 209.0115 -0.9145 250.1869 251.1014 272.2986 209.7883 -0.9157 250.2631 251.1788 272.4130 210.6265 -0.9288 250.3177 251.2465 272.5298 211.4125 -0.9392 250.4071 251.3463 272.6122 212.2098 -0.9407 250.5039 251.4446 272.7133 213.0378 -0.9469 250.5797 251.5266 272.8284 213.8138 -0.9482 250.6645 251.6127 272.9264 214.6620 -0.9508 250.8017 251.7525 273.0279 215.4285 -0.9557 250.8632 251.8189 273.0687 216.2555 -0.9612 250.9286 251.8898 273.1737 217.0528 -0.9618 251.0053 251.9671 273.2693 217.8500 -0.9655 251.0836 252.0491 273.3701 218.6468 -0.9676 251.1659 252.1335 273.5085 219.4435 -0.9732 251.2585 252.2317 273.6088 220.2715 -0.9758 251.3506 252.3264 273.6872 221.0375 -0.9761 251.4218 252.3980 273.7508 221.9060 -0.9802 251.5198 252.5000 273.8721 222.6623 -0.9858 251.6082 252.5940 273.9643 223.4998 -0.9871 251.6905 252.6776 274.0830 224.2865 -0.9863 251.7686 252.7550 274.1876 225.0940 -0.9861 251.8279 252.8140 274.2920 225.9108 -0.9945 251.8655 252.8600 274.4231 226.6875 -0.9990 251.9971 252.9961 274.5271 227.5358 -1.0045 252.0742 253.0787 274.6284 228.3938 -1.0085 252.1473 253.1558 274.7555 229.2525 -1.0154 252.2155 253.2309 274.8856 230.0088 -1.0223 252.2872 253.3095 275.0053 230.8258 -1.0247 252.3684 253.3932 275.1015 231.6023 -1.0268 252.4738 253.5007 275.1804 232.4405 -1.0300 252.5269 253.5569 275.2899 233.2370 -1.0340 252.5977 253.6317 275.4037 234.0238 -1.0368 252.7116 253.7484 275.5068 234.8518 -1.0432 252.8088 253.8520 275.6228 235.6073 -1.0466 252.9004 253.9470 275.7452 236.4555 -1.0518 252.9910 254.0428 275.8664 237.2323 -1.0557 253.0837 254.1393 275.9874 238.0495 -1.0594 253.1896 254.2490 276.0998 238.8360 -1.0640 253.2729 254.3369 276.2202 239.6435 -1.0620 253.3527 254.4147 276.3244 240.4298 -1.0628 253.4237 254.4865 276.4009 241.4113 -1.0676 253.5132 254.5808 276.5402 242.2085 -1.0677 253.5817 254.6494 276.6776 243.0770 -1.0673 253.6875 254.7548 276.8126 243.8328 -1.0722 253.7644 254.8366 276.9185 244.6608 -1.0697 253.8754 254.9450 277.0208 245.4580 -1.0675 253.9557 255.0232 277.1406 246.2543 -1.0706 254.0417 255.1123 277.2566 247.0823 -1.0760 254.0983 255.1743 277.3479 247.8385 -1.0808 254.1664 255.2472 277.4616 248.6968 -1.0861 254.2769 255.3631 277.5545 249.4628 -1.0910 254.3709 255.4619 277.6545 250.2805 -1.0973 254.4535 255.5508 277.7810 251.0778 -1.0995 254.5376 255.6371 277.9136 251.8843 -1.1014 254.6154 255.7168 278.0272 252.6713 -1.1038 254.7168 255.8206 278.1190 253.4890 -1.1100 254.7859 255.8960 278.2080 254.2750 -1.1162 254.8343 255.9505 278.3123 255.0825 -1.1203 254.9374 256.0577 278.4423 255.9105 -1.1233 255.0202 256.1434 278.5157 256.6658 -1.1250 255.1141 256.2391 278.5817 257.5245 -1.1252 255.1648 256.2900 278.7005 258.2910 -1.1290 255.2495 256.3784 278.7855 259.1180 -1.1322 255.3285 256.4607 278.8916 259.9050 -1.1332 255.4112 256.5444 279.0079 260.7125 -1.1376 255.4922 256.6298 279.0729 261.5395 -1.1357 255.6220 256.7577 279.2194 262.3163 -1.1383 255.7262 256.8646 279.3058 263.1340 -1.1400 255.7740 256.9141 279.4290 263.9203 -1.1471 255.8510 256.9981 279.5381 264.7480 -1.1574 255.9289 257.0863 279.6561 265.5145 -1.1627 256.0146 257.1773 279.7571 266.3728 -1.1622 256.1223 257.2844 279.8549 267.1388 -1.1616 256.2050 257.3666 279.9656 267.9565 -1.1636 256.3090 257.4726 280.0724 268.7638 -1.1623 256.4115 257.5737 280.1697 269.5603 -1.1655 256.4840 257.6495 280.2872 270.3883 -1.1608 256.5697 257.7305 280.3681 271.1443 -1.1586 256.6408 257.7994 280.4376 272.0125 -1.1619 256.8034 257.9653 280.5567 272.7688 -1.1652 256.8994 258.0647 280.6498 273.5965 -1.1656 256.9834 258.1491 280.7470 274.3930 -1.1676 257.0657 258.2333 280.8180 275.2005 -1.1686 257.1487 258.3172 280.9292 276.0180 -1.1701 257.2243 258.3944 281.0068 276.7940 -1.1738 257.3338 258.5075 281.1200 277.6220 -1.1773 257.4157 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374.3582 377.2387 397.6783 1183.0263 -2.8829 374.4904 377.3733 397.7523 1183.8943 -2.8869 374.6111 377.4980 397.8405 1184.6505 -2.8916 374.6768 377.5684 397.9453 1185.4683 -2.8939 374.8096 377.7035 398.0551 1186.2338 -2.8985 374.9150 377.8135 398.1458 1187.0925 -2.9028 375.0505 377.9533 398.2491 1187.8590 -2.9069 375.1627 378.0696 398.3411 1188.6863 -2.9126 375.3151 378.2277 398.4018 1189.5038 -2.9156 375.4450 378.3606 398.4771 1190.2805 -2.9183 375.5349 378.4531 398.6139 1191.0978 -2.9234 375.6493 378.5728 398.7095 1191.8945 -2.9269 375.7378 378.6648 398.8216 1192.7225 -2.9164 375.8471 378.7635 398.9176 1193.5193 -2.9159 375.9599 378.8758 398.9918 1194.3160 -2.9179 376.0660 378.9839 399.0506 1195.0825 -2.9163 376.1414 379.0577 399.1384 1195.9100 -2.9143 376.2519 379.1662 399.1847 1196.6965 -2.9060 376.3703 379.2762 399.2040 1197.4835 -2.8999 376.5004 379.4003 399.2840 1198.3110 -2.9001 376.6115 379.5117 399.3989 1199.0770 -2.9025 376.7097 379.6122 399.4806 1199.9255 -2.9027 376.8102 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