DTA measure 1pb3 Date: 2025107:157 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.67 s Mass = 1355.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1785 0.8791 236.2735 235.3944 274.4596 1.9853 0.8825 236.5251 235.6426 274.7120 2.7718 0.8869 236.7485 235.8615 274.9420 3.6093 0.8860 237.0118 236.1259 275.1516 4.3648 0.8890 237.2467 236.3577 275.3744 5.2333 0.8851 237.5162 236.6311 275.5730 5.9580 0.8841 237.7221 236.8381 275.7292 6.8265 0.8846 237.9749 237.0903 275.8831 7.5820 0.8874 238.2025 237.3151 276.0336 8.4195 0.8913 238.4562 237.5649 276.1346 9.2058 0.8960 238.7053 237.8093 276.2142 10.0130 0.8988 238.9724 238.0736 276.2536 10.8298 0.9005 239.2554 238.3549 276.2799 11.6060 0.9016 239.4665 238.5649 276.3226 12.4540 0.9061 239.7428 238.8367 276.3554 13.2195 0.9042 239.9341 239.0299 276.3670 14.0470 0.9034 240.1830 239.2796 276.3583 14.8540 0.9046 240.4649 239.5603 276.3699 15.6400 0.9027 240.7356 239.8328 276.3737 16.4778 0.9061 240.9681 240.0619 276.3709 17.2335 0.9058 241.1892 240.2834 276.3363 18.0708 0.9066 241.4101 240.5035 276.3104 18.8265 0.9078 241.6233 240.7155 276.2787 19.6848 0.9085 241.8860 240.9775 276.2462 20.4503 0.9076 242.1295 241.2219 276.2532 21.2778 0.9073 242.3684 241.4611 276.2348 22.0745 0.9099 242.6075 241.6976 276.2522 22.8608 0.9103 242.8409 241.9306 276.2845 23.7293 0.9120 243.0734 242.1613 276.3337 24.4643 0.9151 243.2797 242.3647 276.3937 25.3223 0.9178 243.5299 242.6121 276.5108 26.0780 0.9199 243.7375 242.8176 276.6111 26.9155 0.9208 244.0103 243.0896 276.7196 27.7020 0.9220 244.2638 243.3418 276.8607 28.4885 0.9229 244.4793 243.5564 277.0252 29.3155 0.9207 244.7128 243.7921 277.2023 30.0818 0.9218 244.9333 244.0116 277.4157 30.9295 0.9211 245.1773 244.2562 277.6440 31.7055 0.9225 245.4044 244.4819 277.8673 32.5228 0.9226 245.6432 244.7205 278.1544 33.3090 0.9236 245.8557 244.9321 278.4848 34.1158 0.9275 246.0747 245.1472 278.7908 34.9023 0.9292 246.3004 245.3713 279.0870 35.6988 0.9344 246.5183 245.5839 279.3792 36.5260 0.9328 246.7372 245.8043 279.7063 37.2820 0.9312 246.9594 246.0282 279.9863 38.1398 0.9326 247.2032 246.2705 280.2929 38.9058 0.9310 247.4274 246.4964 280.5660 39.7230 0.9260 247.6541 246.7280 280.8920 40.5195 0.9228 247.8550 246.9323 281.1753 41.3163 0.9218 248.0717 247.1499 281.4397 42.1435 0.9189 248.3107 247.3918 281.6750 42.9093 0.9144 248.5425 247.6281 281.8884 43.7573 0.9057 248.7969 247.8912 282.0956 44.5333 0.9039 249.0091 248.1052 282.2527 45.3503 0.9009 249.2122 248.3113 282.4092 46.1470 0.9005 249.4164 248.5159 282.5294 46.9435 0.9008 249.6437 248.7429 282.6307 47.7710 0.8972 249.8785 248.9814 282.7160 48.5370 0.8977 250.1247 249.2269 282.7786 49.3948 0.8929 250.3853 249.4923 282.8505 50.1608 0.8905 250.5956 249.7051 282.8712 50.9883 0.8864 250.7800 249.8937 282.8897 51.7845 0.8813 250.9852 250.1040 282.8932 52.5713 0.8792 251.2001 250.3209 282.8814 53.4088 0.8756 251.4255 250.5500 282.8507 54.1643 0.8727 251.6481 250.7754 282.7984 55.0225 0.8728 251.9147 251.0419 282.7196 55.7883 0.8724 252.1095 251.2371 282.6899 56.6155 0.8699 252.3453 251.4754 282.6393 57.4125 0.8676 252.5563 251.6887 282.6028 58.2088 0.8665 252.7788 251.9123 282.5812 59.0363 0.8636 253.0279 252.1642 282.5641 59.8023 0.8563 253.2361 252.3798 282.5491 60.6600 0.8537 253.4696 252.6159 282.5545 61.4158 0.8563 253.6671 252.8107 282.5661 62.2535 0.8526 253.8900 253.0374 282.6347 63.0398 0.8539 254.0999 253.2459 282.7278 63.8368 0.8506 254.2702 253.4196 282.8044 64.6638 0.8435 254.4655 253.6220 282.9269 65.4300 0.8428 254.6507 253.8079 283.0537 66.2880 0.8431 254.8293 253.9862 283.2233 67.0538 0.8406 255.0559 254.2153 283.4077 67.8813 0.8413 255.2738 254.4325 283.5852 68.6778 0.8416 255.4964 254.6548 283.8001 69.4745 0.8406 255.6889 254.8483 284.0867 70.2918 0.8403 255.9386 255.0983 284.3736 71.0675 0.8406 256.1574 255.3168 284.6667 71.9258 0.8418 256.3594 255.5176 285.0006 72.6918 0.8415 256.5552 255.7136 285.3382 73.5085 0.8359 256.7698 255.9339 285.6773 74.3158 0.8347 256.9724 256.1377 286.0111 75.1123 0.8342 257.1597 256.3255 286.2629 75.9395 0.8332 257.3782 256.5450 286.5646 76.6953 0.8304 257.5707 256.7404 286.8512 77.5635 0.8253 257.7934 256.9680 287.2011 78.3293 0.8199 258.0006 257.1807 287.4980 79.1568 0.8158 258.2095 257.3936 287.8155 79.9430 0.8089 258.3770 257.5681 288.0777 80.7498 0.8094 258.5884 257.7790 288.3229 81.5775 0.8023 258.7870 257.9847 288.5592 82.3430 0.8004 258.9799 258.1794 288.7311 83.1603 0.8029 259.1829 258.3800 288.8789 83.9365 0.7998 259.3974 258.5976 289.0397 84.7840 0.7971 259.6058 258.8087 289.1610 85.5603 0.7930 259.8321 259.0392 289.2483 86.3775 0.7905 260.0534 259.2629 289.3023 87.1840 0.7842 260.2431 259.4589 289.3428 87.9705 0.7796 260.4407 259.6611 289.3825 88.7980 0.7735 260.6534 259.8800 289.3973 89.5635 0.7714 260.8015 260.0301 289.3556 90.4218 0.7676 261.0042 260.2366 289.3247 91.1878 0.7647 261.2416 260.4769 289.2683 92.0048 0.7596 261.4716 260.7121 289.2245 92.7705 0.7537 261.6914 260.9377 289.1582 93.5878 0.7527 261.8976 261.1449 289.0539 94.4150 0.7506 262.0948 261.3443 289.0061 95.1810 0.7483 262.2893 261.5410 288.9784 95.9980 0.7396 262.4985 261.7589 288.9316 96.7638 0.7355 262.6556 261.9201 288.8888 97.6220 0.7346 262.8568 262.1222 288.8145 98.3775 0.7335 263.0426 262.3091 288.8176 99.2048 0.7295 263.2516 262.5221 288.8209 100.0015 0.7261 263.4599 262.7338 288.8481 100.7980 0.7230 263.6485 262.9255 288.8640 101.6150 0.7205 263.8701 263.1497 288.8885 102.3915 0.7184 264.0647 263.3463 288.9843 103.2083 0.7173 264.2850 263.5677 289.1045 103.9743 0.7164 264.4640 263.7477 289.2556 104.8325 0.7143 264.6511 263.9368 289.4917 105.5983 0.7139 264.8407 264.1268 289.6929 106.4258 0.7098 265.0673 264.3575 289.9073 107.2120 0.7066 265.2704 264.5638 290.1657 108.0188 0.7063 265.4348 264.7285 290.4615 108.8360 0.7000 265.6371 264.9372 290.7850 109.6018 0.6980 265.8432 265.1452 291.0871 110.4293 0.7005 266.0544 265.3539 291.4531 111.1953 0.6996 266.2402 265.5406 291.7989 112.0530 0.6962 266.4321 265.7359 292.1843 112.8090 0.6912 266.6071 265.9159 292.5189 113.6465 0.6846 266.8266 266.1420 292.8910 114.4328 0.6790 267.0165 266.3375 293.2372 115.2298 0.6735 267.2024 266.5289 293.5681 116.0568 0.6701 267.4223 266.7521 293.8515 116.8330 0.6682 267.6287 266.9605 294.1382 117.6810 0.6627 267.8518 267.1891 294.4238 118.4465 0.6598 268.0081 267.3483 294.6688 119.2738 0.6532 268.2154 267.5622 294.8975 120.0705 0.6480 268.4090 267.7611 295.1142 120.8670 0.6418 268.5750 267.9332 295.2843 121.6843 0.6402 268.7733 268.1331 295.4333 122.4605 0.6389 268.9560 268.3171 295.5428 123.2875 0.6361 269.1531 268.5170 295.6625 124.0535 0.6316 269.3441 268.7125 295.7571 124.9015 0.6307 269.5419 268.9112 295.7994 125.6773 0.6289 269.7314 269.1025 295.7980 126.4945 0.6255 269.9143 269.2888 295.8093 127.2913 0.6231 270.1008 269.4777 295.7910 128.0875 0.6208 270.2712 269.6504 295.7411 128.9153 0.6174 270.4691 269.8516 295.6568 129.6810 0.6155 270.6495 270.0339 295.6136 130.5390 0.6135 270.8296 270.2161 295.5401 131.3050 0.6122 271.0041 270.3919 295.4847 132.1425 0.6071 271.1819 270.5748 295.4181 132.9288 0.6029 271.4043 270.8014 295.3555 133.7255 0.6005 271.5564 270.9559 295.2621 134.5528 0.6001 271.7776 271.1775 295.1761 135.3188 0.5946 272.0041 271.4095 295.1228 136.1770 0.5852 272.2353 271.6501 295.1090 136.9425 0.5799 272.4287 271.8488 295.0667 137.7700 0.5796 272.5974 272.0177 295.0642 138.5360 0.5776 272.7740 272.1963 295.0761 139.3630 0.5732 273.0058 272.4326 295.1263 140.1805 0.5711 273.2002 272.6291 295.2119 140.9565 0.5692 273.3854 272.8162 295.3280 141.7840 0.5678 273.6028 273.0349 295.4620 142.5500 0.5648 273.7130 273.1482 295.5967 143.3975 0.5643 273.9069 273.3426 295.8192 144.1738 0.5636 274.0824 273.5188 296.0462 145.0013 0.5623 274.2537 273.6914 296.3086 145.7975 0.5572 274.4340 273.8768 296.5572 146.5943 0.5539 274.6093 274.0554 296.8648 147.4218 0.5472 274.7827 274.2355 297.2017 148.1875 0.5423 274.9300 274.3878 297.5244 149.0458 0.5389 275.1213 274.5824 297.9294 149.8115 0.5317 275.3181 274.7864 298.3061 150.6388 0.5270 275.4777 274.9507 298.6862 151.4358 0.5273 275.6984 275.1712 299.0361 152.2320 0.5268 275.8841 275.3572 299.3828 153.0493 0.5249 276.0985 275.5736 299.7092 153.8255 0.5201 276.2816 275.7615 300.0251 154.6833 0.5142 276.4633 275.9491 300.2899 155.4493 0.5078 276.6263 276.1185 300.5631 156.2665 0.5061 276.8172 276.3111 300.8555 157.0628 0.5041 276.9959 276.4918 301.1234 157.8598 0.5002 277.1982 276.6981 301.3611 158.6768 0.4956 277.3604 276.8647 301.5538 159.4528 0.4927 277.5292 277.0366 301.7167 160.2700 0.4901 277.7069 277.2169 301.8926 161.0255 0.4898 277.8724 277.3826 301.9891 161.8938 0.4847 278.0627 277.5780 302.0203 162.6495 0.4802 278.2311 277.7509 302.1032 163.4665 0.4768 278.4289 277.9522 302.1545 164.2733 0.4732 278.6396 278.1664 302.1777 165.0598 0.4664 278.8465 278.3802 302.1919 165.8870 0.4650 279.0117 278.5467 302.1737 166.6528 0.4603 279.1973 278.7370 302.1177 167.5008 0.4537 279.4029 278.9492 302.0595 168.2665 0.4494 279.5875 279.1382 301.9695 169.0938 0.4485 279.7634 279.3149 301.9125 169.8905 0.4440 279.9557 279.5117 301.8588 170.6870 0.4416 280.1255 279.6838 301.7764 171.5040 0.4398 280.3322 279.8924 301.7205 172.2803 0.4333 280.5257 280.0924 301.6688 173.0973 0.4306 280.6790 280.2484 301.6128 173.8630 0.4331 280.8435 280.4104 301.5716 174.7213 0.4316 281.0467 280.6151 301.5730 175.4870 0.4285 281.2162 280.7876 301.5669 176.3143 0.4257 281.3870 280.9613 301.5859 177.1008 0.4237 281.5685 281.1447 301.6039 177.9075 0.4194 281.7324 281.3130 301.6437 178.7245 0.4168 281.8996 281.4829 301.7218 179.4908 0.4183 282.0572 281.6389 301.8265 180.3485 0.4178 282.2859 281.8681 301.9306 181.1145 0.4154 282.4509 282.0355 302.0991 181.9420 0.4117 282.6338 282.2221 302.3028 182.7280 0.4057 282.8129 282.4072 302.4911 183.5350 0.3978 282.9431 282.5453 302.7304 184.3523 0.4017 283.0906 282.6890 303.0048 185.1178 0.4021 283.2666 282.8645 303.2739 185.9760 0.4026 283.4671 283.0645 303.6053 186.7420 0.4001 283.5963 283.1962 303.9040 187.5693 0.3970 283.7625 283.3656 304.2648 188.3558 0.3934 283.9452 283.5518 304.6178 189.1625 0.3929 284.1311 283.7382 304.9457 189.9895 0.3894 284.3130 283.9236 305.3125 190.7558 0.3882 284.4720 284.0838 305.6439 191.6035 0.3866 284.6521 284.2655 306.0046 192.3793 0.3797 284.8400 284.4604 306.3433 193.1968 0.3763 285.0302 284.6539 306.6680 193.9625 0.3707 285.2133 284.8426 306.9651 194.7898 0.3639 285.4100 285.0461 307.2709 195.5968 0.3600 285.5982 285.2382 307.5608 196.3830 0.3582 285.7646 285.4064 307.8140 197.2100 0.3587 285.8960 285.5373 308.0088 197.9760 0.3585 286.0536 285.6951 308.1644 198.8343 0.3534 286.2402 285.8868 308.3267 199.6000 0.3522 286.4107 286.0585 308.4683 200.4278 0.3455 286.6154 286.2699 308.5671 201.2240 0.3370 286.8168 286.4798 308.6192 202.0208 0.3359 286.9937 286.6578 308.6260 202.8483 0.3313 287.1724 286.8411 308.6693 203.6138 0.3301 287.3243 286.9943 308.6587 204.4415 0.3281 287.5191 287.1910 308.6124 205.2073 0.3250 287.6790 287.3540 308.5969 206.0653 0.3205 287.8941 287.5736 308.5398 206.8213 0.3132 288.0730 287.7598 308.4684 207.6585 0.3057 288.2779 287.9723 308.3415 208.4450 0.3015 288.4345 288.1330 308.2462 209.2520 0.3001 288.6101 288.3100 308.1832 210.0688 0.2987 288.7866 288.4880 308.1153 210.8453 0.2945 288.9543 288.6598 308.0502 211.6930 0.2928 289.1438 288.8510 307.9793 212.4588 0.2939 289.2826 288.9887 307.9154 213.2865 0.2947 289.4458 289.1512 307.9027 214.0828 0.2950 289.6214 289.3263 307.8568 214.8795 0.2908 289.7949 289.5041 307.8162 215.6763 0.2875 289.9869 289.6994 307.8634 216.4728 0.2872 290.1613 289.8741 307.8989 217.3003 0.2863 290.3660 290.0797 307.9915 218.0660 0.2848 290.5284 290.2436 308.0845 218.9240 0.2801 290.6860 290.4059 308.2150 219.6900 0.2766 290.8404 290.5638 308.3915 220.5173 0.2689 290.9944 290.7255 308.5923 221.3035 0.2689 291.1727 290.9038 308.8144 222.1003 0.2704 291.3369 291.0665 309.0750 222.9173 0.2693 291.4800 291.2108 309.3570 223.6830 0.2684 291.6446 291.3763 309.6488 224.5413 0.2691 291.8480 291.5789 309.9904 225.2968 0.2637 292.0000 291.7363 310.3124 226.1238 0.2578 292.1738 291.9160 310.6914 226.8898 0.2568 292.3403 292.0835 311.0205 227.7070 0.2561 292.4723 292.2162 311.3950 228.5035 0.2518 292.6053 292.3535 311.7843 229.3003 0.2471 292.7708 292.5237 312.1362 230.1275 0.2456 292.9602 292.7146 312.5450 230.8933 0.2439 293.1178 292.8739 312.8744 231.7413 0.2398 293.3365 293.0968 313.2388 232.5173 0.2379 293.4919 293.2539 313.5222 233.3343 0.2349 293.6537 293.4189 313.8060 234.1310 0.2327 293.7971 293.5644 314.0754 234.9275 0.2274 293.9873 293.7599 314.3323 235.7240 0.2227 294.1708 293.9481 314.5484 236.5208 0.2182 294.3427 294.1245 314.7324 237.3378 0.2128 294.5071 294.2943 314.8853 238.1138 0.2090 294.6576 294.4486 314.9999 238.9620 0.2070 294.8401 294.6331 315.0753 239.7275 0.2016 294.9835 294.7820 315.1170 240.5548 0.1974 295.1741 294.9767 315.1831 241.3515 0.1895 295.3253 295.1358 315.2056 242.1480 0.1894 295.4834 295.2941 315.2272 242.9650 0.1833 295.6611 295.4778 315.1918 243.7415 0.1806 295.8482 295.6676 315.1216 244.5890 0.1813 296.0401 295.8588 315.0386 245.3548 0.1792 296.1842 296.0050 314.9554 246.1825 0.1735 296.3490 296.1755 314.8512 246.9788 0.1698 296.5113 296.3415 314.7510 247.7758 0.1689 296.7029 296.5340 314.6601 248.5928 0.1671 296.8941 296.7270 314.5829 249.3690 0.1666 297.0616 296.8950 314.4826 250.2170 0.1624 297.2462 297.0838 314.3697 250.9825 0.1586 297.4024 297.2438 314.2825 251.8103 0.1578 297.5450 297.3872 314.2224 252.6068 0.1575 297.7259 297.5684 314.1988 253.4033 0.1588 297.9101 297.7512 314.2231 254.2205 0.1561 298.0874 297.9313 314.2226 254.9965 0.1509 298.2550 298.1041 314.2058 255.8445 0.1441 298.3974 298.2533 314.2488 256.6208 0.1414 298.5486 298.4072 314.3647 257.4375 0.1416 298.7318 298.5902 314.5181 258.2448 0.1408 298.8896 298.7488 314.6573 259.0310 0.1375 299.0403 298.9027 314.8255 259.8583 0.1342 299.2343 299.1002 315.0670 260.6243 0.1295 299.3737 299.2442 315.2924 261.4823 0.1319 299.5587 299.4268 315.6075 262.2483 0.1307 299.7270 299.5962 315.9047 263.0655 0.1279 299.8967 299.7687 316.2392 263.8720 0.1277 300.0630 299.9353 316.6112 264.6585 0.1230 300.2072 300.0842 316.9690 265.4860 0.1166 300.4057 300.2890 317.3674 266.2515 0.1106 300.5621 300.4515 317.7533 267.1203 0.1105 300.7534 300.6429 318.1438 267.8758 0.1074 300.9002 300.7928 318.5104 268.7028 0.1035 301.0543 300.9508 318.9543 269.4995 0.1047 301.2500 301.1453 319.3512 270.2963 0.1032 301.4672 301.3640 319.7068 271.1235 0.1006 301.6406 301.5399 320.0291 271.8793 0.0992 301.7989 301.6997 320.3389 272.7475 0.0939 301.9554 301.8616 320.6475 273.5133 0.0848 302.1076 302.0228 320.8695 274.3408 0.0842 302.2614 302.1772 321.0989 275.1270 0.0784 302.4189 302.3405 321.3030 275.9338 0.0712 302.5741 302.5028 321.4780 276.7513 0.0642 302.7346 302.6704 321.6063 277.5270 0.0599 302.9129 302.8529 321.6669 278.3750 0.0572 303.0929 303.0357 321.7223 279.1510 0.0512 303.2538 303.2025 321.7690 279.9680 0.0507 303.4254 303.3746 321.7966 280.7748 0.0503 303.5675 303.5173 321.7664 281.5613 0.0499 303.7413 303.6915 321.7153 282.3988 0.0455 303.8979 303.8524 321.6360 283.1543 0.0453 304.0469 304.0016 321.5564 284.0125 0.0421 304.2301 304.1880 321.4755 284.7783 0.0389 304.4302 304.3913 321.3482 285.5953 0.0330 304.6026 304.5696 321.2190 286.3920 0.0292 304.7996 304.7704 321.0512 287.1885 0.0259 304.9698 304.9439 320.9447 288.0055 0.0243 305.0857 305.0614 320.8571 288.7715 0.0218 305.2434 305.2217 320.7581 289.5988 0.0190 305.4144 305.3953 320.6865 290.3543 0.0144 305.5720 305.5576 320.6193 291.2023 0.0095 305.7413 305.7318 320.5707 291.9783 0.0051 305.8867 305.8816 320.4881 292.7953 0.0031 306.0579 306.0548 320.4407 293.5923 0.0057 306.2158 306.2102 320.4686 294.3885 0.0057 306.3690 306.3633 320.5354 295.2160 0.0051 306.5761 306.5711 320.6552 295.9820 0.0037 306.7144 306.7107 320.7903 296.8295 0.0016 306.8225 306.8209 320.9747 297.5750 -0.0017 306.9696 306.9713 321.1361 298.4230 -0.0016 307.1498 307.1514 321.4188 299.1885 0.0010 307.3008 307.2998 321.6888 300.0160 0.0003 307.4695 307.4693 322.0105 300.8025 -0.0019 307.6461 307.6481 322.3490 301.5988 -0.0053 307.8185 307.8238 322.7049 302.4265 -0.0077 307.9996 308.0073 323.0855 303.1923 -0.0101 308.1302 308.1403 323.4841 304.0503 -0.0133 308.3022 308.3155 323.8954 304.8063 -0.0139 308.4499 308.4638 324.2855 305.6435 -0.0135 308.5932 308.6067 324.7106 306.3993 -0.0185 308.7235 308.7420 325.0735 307.2268 -0.0252 308.9075 308.9327 325.4695 308.0230 -0.0288 309.0567 309.0854 325.8349 308.8200 -0.0303 309.2370 309.2674 326.1493 309.6473 -0.0337 309.4443 309.4781 326.5042 310.4028 -0.0370 309.5929 309.6300 326.7835 311.2713 -0.0400 309.7630 309.8030 327.1052 312.0268 -0.0414 309.9256 309.9670 327.3522 312.8540 -0.0436 310.0888 310.1324 327.5810 313.6510 -0.0489 310.2672 310.3161 327.7546 314.4473 -0.0518 310.4241 310.4759 327.8788 315.2748 -0.0546 310.5687 310.6233 327.9644 316.0305 -0.0567 310.7251 310.7819 328.0187 316.8988 -0.0584 310.9111 310.9695 328.0662 317.6543 -0.0580 311.0785 311.1365 328.0989 318.4818 -0.0646 311.2327 311.2973 328.0723 319.2783 -0.0643 311.4186 311.4829 328.0203 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