DTA measure 2pb3 Date: 2025107:1537 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.41 s Mass = 1355.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4661 -2.6675 460.2903 462.9578 434.5611 4.0748 -2.6737 460.3233 462.9970 434.8941 5.6831 -2.6852 460.3431 463.0282 435.1223 7.2865 -2.6944 460.3958 463.0902 435.2194 8.9001 -2.7047 460.4364 463.1411 435.1792 10.4881 -2.7144 460.5039 463.2184 435.0121 12.1018 -2.7282 460.5744 463.3026 434.7975 13.7050 -2.7317 460.6178 463.3495 434.4794 15.3186 -2.7413 460.6423 463.3836 434.0051 16.9220 -2.7461 460.7096 463.4557 433.5327 18.5099 -2.7487 460.7293 463.4781 433.0322 20.1083 -2.7500 460.7718 463.5218 432.4400 21.7118 -2.7485 460.8306 463.5791 431.8418 23.3151 -2.7462 460.8676 463.6138 431.2518 24.9236 -2.7478 460.8863 463.6341 430.6890 26.5216 -2.7474 460.8706 463.6179 430.1098 28.1405 -2.7497 460.9428 463.6925 429.5582 29.7388 -2.7535 460.9465 463.7000 429.1529 31.3420 -2.7530 460.9574 463.7104 428.8434 32.9505 -2.7510 460.9651 463.7161 428.5562 34.5538 -2.7473 460.9768 463.7242 428.4094 36.1623 -2.7402 460.9837 463.7239 428.3455 37.7503 -2.7437 461.0050 463.7487 428.3286 39.3536 -2.7476 460.9366 463.6842 428.3895 40.9673 -2.7464 460.9199 463.6663 428.5446 42.5859 -2.7467 460.9467 463.6935 428.6406 44.1944 -2.7449 460.9562 463.7011 428.7097 45.7976 -2.7440 460.9134 463.6574 428.8070 47.4063 -2.7554 460.8973 463.6527 428.8212 49.0098 -2.7589 460.8890 463.6479 428.7670 50.6181 -2.7620 460.8312 463.5932 428.6877 52.2215 -2.7570 460.8348 463.5918 428.5324 53.8403 -2.7568 460.8192 463.5760 428.3142 55.4539 -2.7603 460.8122 463.5724 428.0355 57.0574 -2.7610 460.8026 463.5636 427.7097 58.6708 -2.7605 460.7826 463.5431 427.4088 60.2743 -2.7624 460.7759 463.5383 427.0592 61.8876 -2.7630 460.7197 463.4827 426.6771 63.4910 -2.7642 460.6781 463.4424 426.2535 65.1200 -2.7706 460.6523 463.4229 425.7885 66.7233 -2.7680 460.6152 463.3833 425.3828 68.3318 -2.7663 460.5737 463.3399 424.9792 69.9350 -2.7624 460.5587 463.3211 424.5875 71.5488 -2.7608 460.5293 463.2901 424.2586 73.1523 -2.7568 460.4847 463.2415 423.9892 74.7606 -2.7565 460.4257 463.1822 423.7166 76.3845 -2.7532 460.3864 463.1396 423.5033 77.9778 -2.7503 460.3303 463.0806 423.3208 79.5708 -2.7503 460.2247 462.9750 423.2168 81.1743 -2.7480 460.1283 462.8764 423.1644 82.7828 -2.7483 460.0389 462.7872 423.0908 84.3860 -2.7479 460.0037 462.7516 423.0240 85.9741 -2.7430 459.9671 462.7102 422.9694 87.5774 -2.7443 459.8857 462.6301 422.9151 89.1809 -2.7499 459.8136 462.5635 422.9000 90.8049 -2.7484 459.7352 462.4836 422.8393 92.4080 -2.7457 459.6678 462.4134 422.7332 94.0166 -2.7481 459.5952 462.3433 422.6041 95.6044 -2.7510 459.5543 462.3053 422.4079 97.2079 -2.7596 459.5213 462.2809 422.2622 98.8161 -2.7600 459.4972 462.2572 422.0008 100.4195 -2.7588 459.3965 462.1553 421.7276 102.0279 -2.7611 459.3007 462.0618 421.3755 103.6466 -2.7632 459.2546 462.0178 420.9945 105.2604 -2.7629 459.1734 461.9364 420.6867 106.8481 -2.7650 459.0645 461.8295 420.3815 108.4568 -2.7632 458.9298 461.6930 420.0950 110.0651 -2.7582 458.8386 461.5968 419.7794 111.6736 -2.7589 458.7293 461.4883 419.4576 113.2771 -2.7614 458.6368 461.3982 419.1594 114.8909 -2.7582 458.5600 461.3182 418.9529 116.4788 -2.7547 458.4851 461.2398 418.6234 118.0976 -2.7516 458.3818 461.1334 418.3748 119.7059 -2.7487 458.2826 461.0313 418.1616 121.3146 -2.7517 458.1861 460.9378 418.0030 122.9231 -2.7485 458.0761 460.8246 417.8559 124.5314 -2.7453 457.9531 460.6984 417.7358 126.1399 -2.7451 457.8607 460.6058 417.6428 127.7431 -2.7457 457.7642 460.5099 417.5363 129.3721 -2.7526 457.6694 460.4220 417.3908 130.9601 -2.7591 457.5509 460.3101 417.2871 132.5738 -2.7561 457.4076 460.1637 417.1914 134.1773 -2.7522 457.2966 460.0489 417.0688 135.7858 -2.7509 457.2039 459.9548 416.8950 137.3941 -2.7448 457.1059 459.8507 416.6804 139.0028 -2.7427 456.9574 459.7001 416.4580 140.6060 -2.7421 456.8099 459.5521 416.2516 142.2196 -2.7427 456.6847 459.4274 416.0078 143.8233 -2.7446 456.5965 459.3411 415.7629 145.4213 -2.7407 456.5074 459.2482 415.5122 147.0249 -2.7434 456.3924 459.1358 415.2028 148.6283 -2.7414 456.3115 459.0530 414.8778 150.2315 -2.7413 456.1791 458.9204 414.5671 151.8248 -2.7412 456.0178 458.7590 414.2850 153.4279 -2.7396 455.8727 458.6123 414.0025 155.0468 -2.7323 455.7236 458.4558 413.6787 156.6500 -2.7300 455.6127 458.3427 413.4441 158.2534 -2.7216 455.4911 458.2127 413.2733 159.8620 -2.7160 455.3892 458.1052 413.0990 161.4654 -2.7152 455.2583 457.9736 412.9059 163.0688 -2.7153 455.1064 457.8217 412.7285 164.6774 -2.7112 454.9809 457.6921 412.5455 166.2959 -2.7143 454.8437 457.5580 412.3831 167.9045 -2.7123 454.6829 457.3952 412.2144 169.5078 -2.7138 454.5660 457.2798 412.0165 171.1163 -2.7120 454.3903 457.1024 411.8564 172.7248 -2.7096 454.1380 456.8476 411.6306 174.3330 -2.7118 454.0102 456.7220 411.4834 175.9365 -2.7113 453.9039 456.6151 411.3464 177.5551 -2.7132 453.7594 456.4725 411.2282 179.1688 -2.7100 453.6347 456.3446 411.0440 180.7723 -2.7097 453.4971 456.2069 410.8483 182.3805 -2.7053 453.3719 456.0772 410.6368 183.9840 -2.6995 453.1946 455.8941 410.4393 185.5975 -2.7002 453.0616 455.7618 410.1915 187.2009 -2.7067 452.9363 455.6430 409.9557 188.8298 -2.7082 452.7653 455.4734 409.7281 190.4331 -2.7035 452.6419 455.3453 409.4924 192.0468 -2.7042 452.5159 455.2201 409.2376 193.6499 -2.7069 452.3650 455.0718 409.0304 195.2585 -2.7034 452.2161 454.9195 408.7862 196.8619 -2.6957 452.0395 454.7351 408.5156 198.4755 -2.6926 451.8695 454.5621 408.2680 200.0635 -2.6893 451.6920 454.3814 408.0252 201.6875 -2.6876 451.5286 454.2162 407.7509 203.2909 -2.6839 451.3722 454.0562 407.4815 204.8944 -2.6859 451.2129 453.8987 407.2321 206.5029 -2.6816 451.0455 453.7272 406.9780 208.1010 -2.6816 450.8763 453.5579 406.7493 209.6943 -2.6837 450.7304 453.4141 406.5422 211.2924 -2.6801 450.5510 453.2311 406.3557 212.8959 -2.6806 450.4252 453.1058 406.1868 214.5043 -2.6782 450.2757 452.9539 406.0202 216.1025 -2.6763 450.0984 452.7747 405.8833 217.7061 -2.6666 449.9465 452.6131 405.6969 219.3145 -2.6575 449.7734 452.4309 405.5003 220.9179 -2.6502 449.5597 452.2099 405.3511 222.5110 -2.6515 449.3997 452.0512 405.1994 224.1143 -2.6502 449.2931 451.9433 405.0364 225.7228 -2.6504 449.1081 451.7585 404.8861 227.3261 -2.6505 448.9312 451.5817 404.7219 228.9448 -2.6543 448.7622 451.4165 404.5524 230.5534 -2.6506 448.6097 451.2603 404.3737 232.1565 -2.6547 448.4192 451.0739 404.1076 233.7549 -2.6516 448.1935 450.8450 403.8814 235.3583 -2.6345 448.0200 450.6545 403.6201 236.9668 -2.6302 447.8578 450.4881 403.3791 238.5701 -2.6296 447.6862 450.3159 403.1549 240.1785 -2.6310 447.5588 450.1898 402.9193 241.8025 -2.6304 447.4111 450.0415 402.6704 243.4111 -2.6259 447.2131 449.8390 402.4396 245.0144 -2.6218 447.0458 449.6676 402.1903 246.6281 -2.6232 446.8758 449.4990 401.9322 248.2316 -2.6217 446.6916 449.3133 401.6815 249.8400 -2.6198 446.4987 449.1185 401.4830 251.4333 -2.6158 446.2960 448.9118 401.2178 253.0368 -2.6143 446.1489 448.7633 400.9513 254.6656 -2.6105 445.9718 448.5824 400.7654 256.2691 -2.6020 445.7934 448.3954 400.5777 257.8775 -2.5992 445.6164 448.2155 400.3543 259.4809 -2.5966 445.3832 447.9798 400.1727 261.0946 -2.5921 445.1836 447.7758 400.0057 262.6980 -2.5893 445.0108 447.6001 399.8306 264.3115 -2.5793 444.8357 447.4150 399.6060 265.9303 -2.5781 444.6715 447.2496 399.4311 267.5438 -2.5755 444.4872 447.0626 399.2471 269.1473 -2.5656 444.3068 446.8724 399.0767 270.7555 -2.5632 444.0913 446.6545 398.8862 272.3538 -2.5658 443.8921 446.4579 398.6802 273.9520 -2.5634 443.7105 446.2739 398.4868 275.5605 -2.5645 443.5060 446.0705 398.2839 277.1589 -2.5646 443.3431 445.9077 398.0817 278.7623 -2.5652 443.1532 445.7183 397.8586 280.3708 -2.5566 442.9810 445.5375 397.6612 281.9743 -2.5542 442.7966 445.3507 397.4483 283.5825 -2.5500 442.6218 445.1718 397.1867 285.1808 -2.5439 442.4202 444.9641 396.9658 286.7841 -2.5410 442.2327 444.7737 396.7346 288.3926 -2.5404 442.0620 444.6024 396.4834 290.0115 -2.5350 441.8789 444.4139 396.2372 291.6200 -2.5261 441.7329 444.2590 396.0670 293.2234 -2.5194 441.5533 444.0727 395.8116 294.8320 -2.5202 441.3842 443.9044 395.5858 296.4354 -2.5245 441.1579 443.6825 395.3504 298.0234 -2.5258 440.9751 443.5009 395.1598 299.6474 -2.5202 440.7505 443.2707 394.9523 301.2659 -2.5174 440.5649 443.0823 394.7529 302.8745 -2.5119 440.3808 442.8927 394.5063 304.4829 -2.5110 440.1948 442.7058 394.3047 306.0759 -2.5087 439.9990 442.5077 394.1019 307.6794 -2.5032 439.7936 442.2967 393.9267 309.2878 -2.4997 439.6142 442.1139 393.7474 310.8963 -2.4994 439.3958 441.8952 393.5482 312.5099 -2.4965 439.1892 441.6857 393.3673 314.1133 -2.4948 438.9952 441.4900 393.2062 315.7218 -2.4957 438.7860 441.2817 393.0383 317.3303 -2.4897 438.6455 441.1352 392.8737 318.9389 -2.4877 438.4354 440.9231 392.6723 320.5423 -2.4830 438.2102 440.6932 392.4521 322.1558 -2.4794 438.0111 440.4905 392.2907 323.7593 -2.4731 437.8126 440.2857 392.0718 325.3730 -2.4673 437.6358 440.1031 391.8309 326.9763 -2.4667 437.4498 439.9165 391.5659 328.5849 -2.4658 437.2531 439.7190 391.2996 330.1933 -2.4681 437.0610 439.5291 391.0708 331.7966 -2.4665 436.8573 439.3238 390.8183 333.4051 -2.4607 436.6783 439.1390 390.5724 335.0084 -2.4557 436.5105 438.9663 390.3784 336.5965 -2.4483 436.3049 438.7532 390.1261 338.1946 -2.4442 436.0899 438.5341 389.8933 339.7928 -2.4397 435.8666 438.3063 389.6603 341.4065 -2.4376 435.6279 438.0655 389.4528 343.0149 -2.4333 435.4552 437.8886 389.2464 344.6183 -2.4292 435.3163 437.7456 389.0137 346.2265 -2.4299 435.1347 437.5646 388.8079 347.8249 -2.4233 434.9561 437.3794 388.5822 349.4128 -2.4210 434.7463 437.1673 388.3900 351.0213 -2.4231 434.5004 436.9235 388.1593 352.6246 -2.4181 434.3286 436.7467 387.9592 354.2485 -2.4106 434.1508 436.5614 387.7234 355.8519 -2.4081 433.9693 436.3774 387.5453 357.4605 -2.4072 433.7671 436.1743 387.3772 359.0636 -2.3986 433.5398 435.9384 387.1316 360.6671 -2.3858 433.2880 435.6738 386.9639 362.2756 -2.3854 433.0676 435.4530 386.8095 363.8790 -2.3810 432.8737 435.2547 386.5864 365.5081 -2.3739 432.6901 435.0640 386.3989 367.1114 -2.3692 432.5393 434.9085 386.2813 368.7200 -2.3696 432.2821 434.6517 386.1139 370.3284 -2.3690 432.0913 434.4602 385.9310 371.9213 -2.3676 431.9214 434.2889 385.7295 373.5248 -2.3596 431.6973 434.0569 385.4966 375.1331 -2.3597 431.4845 433.8442 385.2560 376.7570 -2.3594 431.2764 433.6358 385.0566 378.3808 -2.3588 431.0867 433.4455 384.8218 379.9740 -2.3543 430.8821 433.2364 384.5749 381.5980 -2.3470 430.7008 433.0478 384.3330 383.2064 -2.3401 430.4820 432.8221 384.0686 384.7995 -2.3320 430.2458 432.5778 383.8268 386.4183 -2.3292 430.0290 432.3582 383.5345 388.0164 -2.3291 429.8342 432.1632 383.2990 389.6353 -2.3318 429.6356 431.9674 383.1009 391.2489 -2.3259 429.4353 431.7612 382.8852 392.8524 -2.3228 429.2511 431.5738 382.6586 394.4660 -2.3139 429.0635 431.3774 382.4916 396.0694 -2.3131 428.8909 431.2040 382.2707 397.6829 -2.3061 428.6364 430.9426 382.0357 399.2813 -2.3065 428.4264 430.7329 381.8425 400.8946 -2.3032 428.2082 430.5114 381.6456 402.4930 -2.3035 427.9875 430.2910 381.4626 404.0963 -2.3015 427.8146 430.1162 381.2809 405.6996 -2.3012 427.6029 429.9041 381.0929 407.2825 -2.2950 427.4154 429.7104 380.9043 408.8909 -2.2894 427.2599 429.5493 380.7008 410.4943 -2.2825 427.0235 429.3060 380.5469 412.1026 -2.2771 426.8131 429.0902 380.3551 413.7215 -2.2708 426.5713 428.8421 380.1574 415.3146 -2.2682 426.3394 428.6076 379.9658 416.9179 -2.2619 426.1705 428.4324 379.7804 418.5214 -2.2542 425.9323 428.1865 379.5844 420.1296 -2.2526 425.7050 427.9576 379.3845 421.7331 -2.2509 425.5092 427.7601 379.1813 423.3418 -2.2484 425.3350 427.5834 378.9535 424.9450 -2.2439 425.1063 427.3501 378.6990 426.5689 -2.2378 424.9591 427.1969 378.4330 428.1774 -2.2296 424.7357 426.9653 378.1348 429.7858 -2.2247 424.4950 426.7197 377.8582 431.3941 -2.2243 424.2703 426.4946 377.6364 433.0025 -2.2240 424.0737 426.2977 377.3994 434.6060 -2.2203 423.8596 426.0799 377.1566 436.2144 -2.2175 423.6585 425.8761 376.9504 437.8384 -2.2157 423.4998 425.7155 376.7113 439.4263 -2.2104 423.3144 425.5247 376.4583 441.0348 -2.2065 423.1148 425.3213 376.2603 442.6383 -2.2003 422.8720 425.0723 376.0631 444.2468 -2.1942 422.5892 424.7834 375.8489 445.8553 -2.1863 422.3652 424.5515 375.6756 447.4639 -2.1837 422.1648 424.3485 375.4789 449.0980 -2.1823 421.9459 424.1281 375.3270 450.7064 -2.1833 421.7300 423.9133 375.1739 452.3098 -2.1795 421.5422 423.7217 375.0132 453.9233 -2.1777 421.3380 423.5157 374.8505 455.5266 -2.1776 421.1410 423.3185 374.6717 457.1400 -2.1782 420.9108 423.0890 374.4815 458.7333 -2.1731 420.7035 422.8766 374.3224 460.3415 -2.1664 420.5108 422.6772 374.1413 461.9604 -2.1578 420.3262 422.4839 373.8749 463.5588 -2.1510 420.1021 422.2531 373.6034 465.1620 -2.1455 419.8998 422.0454 373.3726 466.7655 -2.1362 419.7018 421.8379 373.2012 468.3639 -2.1357 419.5256 421.6613 372.9843 469.9723 -2.1328 419.3033 421.4361 372.7288 471.5603 -2.1286 419.0862 421.2148 372.4947 473.1688 -2.1251 418.8480 420.9731 372.2382 474.7875 -2.1253 418.6018 420.7272 372.0158 476.3858 -2.1273 418.3456 420.4729 371.7758 477.9941 -2.1275 418.1563 420.2838 371.5294 479.5976 -2.1235 417.9470 420.0705 371.3084 481.2061 -2.1178 417.7383 419.8561 371.1039 482.8094 -2.1129 417.5684 419.6813 370.8660 484.4128 -2.1002 417.3735 419.4737 370.6406 486.0364 -2.1001 417.1541 419.2542 370.4353 487.6399 -2.0995 416.9659 419.0654 370.2423 489.2484 -2.0896 416.7446 418.8341 370.0541 490.8569 -2.0757 416.4983 418.5740 369.8931 492.4653 -2.0714 416.3313 418.4027 369.7056 494.0685 -2.0642 416.1355 418.1997 369.4786 495.6771 -2.0645 415.9224 417.9869 369.2587 497.2959 -2.0638 415.6572 417.7209 369.0055 498.8993 -2.0593 415.4719 417.5312 368.7969 500.5130 -2.0587 415.2791 417.3378 368.5990 502.1164 -2.0548 415.0878 417.1426 368.3821 503.7299 -2.0483 414.8469 416.8952 368.1662 505.3334 -2.0429 414.6184 416.6612 367.9389 506.9469 -2.0365 414.3691 416.4057 367.7550 508.5658 -2.0277 414.1608 416.1885 367.5707 510.1741 -2.0203 413.9631 415.9833 367.3926 511.7825 -2.0177 413.7773 415.7950 367.2056 513.3910 -2.0120 413.5708 415.5829 366.9884 514.9994 -2.0056 413.3547 415.3603 366.7841 516.6079 -1.9997 413.1227 415.1224 366.5615 518.2165 -1.9962 412.9015 414.8976 366.3368 519.8300 -1.9907 412.6898 414.6805 366.1462 521.4436 -1.9780 412.4745 414.4525 365.9424 523.0520 -1.9734 412.2577 414.2310 365.7219 524.6606 -1.9714 412.0581 414.0296 365.4844 526.2691 -1.9704 411.8088 413.7792 365.2614 527.8725 -1.9641 411.6159 413.5800 365.1256 529.4708 -1.9652 411.3721 413.3373 364.9240 531.0688 -1.9634 411.1240 413.0874 364.6910 532.6876 -1.9646 410.9224 412.8870 364.4332 534.2908 -1.9643 410.7259 412.6901 364.1867 535.8943 -1.9581 410.5033 412.4614 363.9630 537.4924 -1.9526 410.3249 412.2775 363.7459 539.1008 -1.9468 410.1207 412.0675 363.5406 540.6990 -1.9431 409.9379 411.8810 363.3079 542.3024 -1.9386 409.6844 411.6229 363.1209 543.9109 -1.9308 409.4635 411.3943 362.9122 545.5143 -1.9289 409.2659 411.1947 362.6559 547.1380 -1.9199 409.0520 410.9718 362.3770 548.7416 -1.9156 408.8391 410.7547 362.1601 550.3500 -1.9141 408.6128 410.5270 361.9516 551.9636 -1.9131 408.4066 410.3197 361.7429 553.5723 -1.9086 408.2386 410.1472 361.5760 555.1754 -1.9084 407.9877 409.8961 361.3662 556.7890 -1.9062 407.7671 409.6733 361.1833 558.4078 -1.9002 407.5507 409.4509 360.9367 560.0111 -1.8938 407.3413 409.2351 360.7505 561.6249 -1.8859 407.1348 409.0207 360.5927 563.2128 -1.8822 406.9051 408.7873 360.4311 564.8366 -1.8804 406.7070 408.5874 360.2399 566.4399 -1.8743 406.4755 408.3498 360.0454 568.0484 -1.8666 406.2277 408.0943 359.8423 569.6673 -1.8665 406.0024 407.8689 359.6454 571.2756 -1.8623 405.7351 407.5974 359.3872 572.8843 -1.8587 405.5379 407.3966 359.1550 574.4926 -1.8514 405.3725 407.2239 358.9365 576.0960 -1.8446 405.1505 406.9951 358.7152 577.7045 -1.8412 404.9588 406.8000 358.4969 579.3131 -1.8369 404.7770 406.6139 358.3293 580.9319 -1.8342 404.5427 406.3769 358.0905 582.5456 -1.8244 404.3354 406.1598 357.9054 584.1489 -1.8176 404.1401 405.9577 357.7023 585.7574 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267.5196 267.7163 227.1230 1598.5585 -0.1973 267.2963 267.4935 226.9541 1600.1631 -0.1959 267.0855 267.2814 226.7886 1601.7875 -0.1934 266.9024 267.0958 226.5750 1603.3923 -0.1890 266.6970 266.8859 226.4004 1604.9963 -0.1872 266.4646 266.6518 226.2557 1606.6213 -0.1849 266.2923 266.4772 226.0811 1608.2254 -0.1836 266.1024 266.2860 225.8997 1609.8349 -0.1762 265.8317 266.0079 225.6942 1611.4600 -0.1804 265.5869 265.7673 225.5261 1613.0690 -0.1800 265.4164 265.5965 225.3764 1614.6738 -0.1769 265.2569 265.4338 225.2151 1616.2833 -0.1830 265.0473 265.2303 225.0294 1617.8925 -0.1842 264.8348 265.0190 224.8685 1619.4973 -0.1855 264.6201 264.8057 224.6796 1621.0960 -0.1823 264.4206 264.6030 224.4791 1622.6853 -0.1737 264.2516 264.4253 224.2974 1624.2998 -0.1706 264.0374 264.2080 224.1737 1625.9040 -0.1685 263.8015 263.9700 223.9828 1627.5088 -0.1716 263.5844 263.7560 223.7561 1629.1125 -0.1697 263.3969 263.5666 223.5554 1630.7173 -0.1688 263.1961 263.3648 223.3344 1632.3210 -0.1661 262.9828 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