DTA measure 1gyors Date: 2026324:1057 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.39 s Mass = 934.500 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1580 -3.8488 183.9871 187.8359 246.5579 1.9860 -3.8424 184.2513 188.0937 246.5335 2.7525 -3.8341 184.5226 188.3568 246.5087 3.6208 -3.8262 184.7888 188.6150 246.4861 4.3768 -3.8154 185.0509 188.8662 246.4500 5.1945 -3.8088 185.3273 189.1361 246.4417 5.9908 -3.8034 185.5755 189.3789 246.4103 6.7880 -3.7960 185.8153 189.6112 246.3753 7.6058 -3.7843 186.0838 189.8681 246.3328 8.3715 -3.7695 186.3363 190.1059 246.2970 9.2300 -3.7569 186.5998 190.3567 246.2811 9.9555 -3.7483 186.8448 190.5931 246.2619 10.8138 -3.7333 187.1383 190.8716 246.2066 11.5798 -3.7236 187.3695 191.0931 246.1846 12.3975 -3.7118 187.6491 191.3608 246.1577 13.2045 -3.7013 187.8945 191.5958 246.1233 13.9910 -3.6907 188.1426 191.8333 246.0784 14.8190 -3.6803 188.3601 192.0404 246.0668 15.5853 -3.6660 188.6072 192.2732 246.0821 16.4433 -3.6575 188.8837 192.5412 246.0519 17.2098 -3.6496 189.1187 192.7682 246.0423 18.0375 -3.6399 189.3924 193.0322 246.0203 18.8135 -3.6343 189.5966 193.2309 246.0228 19.6415 -3.6245 189.8514 193.4759 245.9911 20.4175 -3.6123 190.0919 193.7042 245.9862 21.2350 -3.5965 190.3528 193.9493 245.9905 22.0323 -3.5866 190.5918 194.1784 245.9706 22.8288 -3.5745 190.8132 194.3878 245.9773 23.6565 -3.5646 191.0166 194.5812 246.0132 24.4230 -3.5501 191.2572 194.8072 246.0609 25.2708 -3.5351 191.4877 195.0228 246.0701 26.0473 -3.5246 191.7314 195.2560 246.0917 26.8650 -3.5139 191.9850 195.4990 246.1170 27.6613 -3.5028 192.2180 195.7209 246.1480 28.4585 -3.4924 192.4413 195.9337 246.1790 29.2968 -3.4821 192.6837 196.1658 246.2013 30.0520 -3.4745 192.8993 196.3738 246.2273 30.9108 -3.4563 193.1711 196.6274 246.3053 31.6773 -3.4449 193.4153 196.8602 246.3839 32.5043 -3.4260 193.6235 197.0495 246.4187 33.3015 -3.4155 193.8828 197.2984 246.4505 34.0885 -3.4011 194.0916 197.4927 246.5148 34.9258 -3.3898 194.3833 197.7730 246.6137 35.6820 -3.3765 194.5880 197.9644 246.7099 36.5408 -3.3650 194.8240 198.1891 246.8181 37.3063 -3.3530 195.0478 198.4008 246.9163 38.1240 -3.3381 195.2634 198.6015 247.0070 38.9210 -3.3263 195.4206 198.7469 247.0764 39.7175 -3.3148 195.6651 198.9798 247.1490 40.5353 -3.3029 195.8877 199.1906 247.2674 41.2913 -3.2979 196.0991 199.3970 247.3669 42.1595 -3.2847 196.3424 199.6271 247.4412 42.9158 -3.2753 196.5903 199.8656 247.5806 43.7435 -3.2676 196.8497 200.1173 247.7273 44.5400 -3.2590 197.0937 200.3527 247.8815 45.3270 -3.2445 197.2867 200.5311 248.0200 46.1550 -3.2317 197.5118 200.7435 248.1707 46.9208 -3.2249 197.7048 200.9297 248.2984 47.7793 -3.2170 197.9174 201.1343 248.4407 48.5458 -3.2047 198.1355 201.3402 248.5492 49.3625 -3.1935 198.3687 201.5622 248.6555 50.1700 -3.1809 198.5942 201.7752 248.7736 50.9570 -3.1714 198.8167 201.9881 248.9202 51.7840 -3.1594 199.0259 202.1853 249.0838 52.5505 -3.1538 199.2185 202.3724 249.2635 53.4093 -3.1413 199.4579 202.5992 249.4623 54.1748 -3.1312 199.6896 202.8208 249.6035 54.9925 -3.1216 199.8951 203.0167 249.7305 55.8000 -3.1117 200.1176 203.2293 249.9364 56.5863 -3.1029 200.2921 203.3950 250.1165 57.4140 -3.0893 200.4731 203.5624 250.3032 58.1805 -3.0821 200.6540 203.7362 250.4929 59.0385 -3.0729 200.9051 203.9780 250.6471 59.8048 -3.0672 201.1062 204.1734 250.8281 60.6225 -3.0570 201.3471 204.4042 250.9994 61.4295 -3.0453 201.5729 204.6181 251.1861 62.2160 -3.0364 201.7733 204.8097 251.3828 63.0440 -3.0254 201.9963 205.0217 251.5214 63.8098 -3.0190 202.2144 205.2334 251.6508 64.6785 -3.0109 202.4378 205.4487 251.8390 65.4348 -3.0036 202.6523 205.6559 252.0238 66.2623 -2.9965 202.8693 205.8658 252.2034 67.0590 -2.9852 203.0863 206.0716 252.3767 67.8665 -2.9755 203.2835 206.2590 252.5368 68.6838 -2.9705 203.4939 206.4644 252.7013 69.4395 -2.9628 203.6899 206.6527 252.8596 70.2983 -2.9516 203.9229 206.8745 253.0386 71.0333 -2.9472 204.1089 207.0561 253.2021 71.8815 -2.9402 204.3400 207.2802 253.4310 72.6480 -2.9321 204.5292 207.4613 253.5971 73.4755 -2.9252 204.7518 207.6771 253.7777 74.2620 -2.9183 204.9641 207.8824 253.9331 75.0593 -2.9169 205.1421 208.0590 254.0985 75.8870 -2.9136 205.3122 208.2258 254.2739 76.6425 -2.9046 205.4909 208.3955 254.4390 77.5115 -2.9036 205.6939 208.5975 254.6710 78.2678 -2.8987 205.9041 208.8027 254.8675 79.0948 -2.8919 206.1282 209.0200 255.0856 79.8613 -2.8818 206.3321 209.2138 255.2561 80.6890 -2.8722 206.5501 209.4224 255.4336 81.4855 -2.8640 206.7605 209.6245 255.6103 82.2725 -2.8577 206.9593 209.8170 255.7972 83.1108 -2.8484 207.1649 210.0133 255.9962 83.8660 -2.8448 207.3663 210.2111 256.1544 84.7248 -2.8406 207.6105 210.4511 256.3746 85.4913 -2.8370 207.8033 210.6403 256.5460 86.3183 -2.8312 207.9912 210.8223 256.6810 87.1155 -2.8263 208.1867 211.0129 256.8340 87.9025 -2.8170 208.3684 211.1854 257.0016 88.7398 -2.8082 208.5699 211.3781 257.1921 89.4960 -2.8038 208.7627 211.5664 257.3734 90.3648 -2.7966 208.9744 211.7710 257.5597 91.0895 -2.7919 209.1684 211.9603 257.7137 91.9585 -2.7926 209.4197 212.2124 257.8590 92.7145 -2.7904 209.5935 212.3839 258.0007 93.5418 -2.7832 209.8255 212.6087 258.1813 94.3390 -2.7803 210.0407 212.8210 258.3627 95.1358 -2.7744 210.2266 213.0010 258.5130 95.9633 -2.7683 210.3967 213.1650 258.6550 96.7195 -2.7688 210.5919 213.3607 258.7672 97.5883 -2.7590 210.8327 213.5917 258.9320 98.3540 -2.7548 210.9934 213.7481 259.0918 99.1820 -2.7510 211.1900 213.9410 259.2303 99.9688 -2.7417 211.3802 214.1218 259.3147 100.7653 -2.7349 211.5976 214.3325 259.4289 101.5523 -2.7320 211.7870 214.5190 259.5519 102.3493 -2.7322 211.9951 214.7273 259.7101 103.1765 -2.7265 212.1905 214.9170 259.8979 103.9328 -2.7215 212.3558 215.0773 260.0530 104.7915 -2.7131 212.5397 215.2528 260.1658 105.5570 -2.7062 212.7046 215.4108 260.2742 106.3748 -2.7002 212.9061 215.6062 260.4491 107.1720 -2.6955 213.1098 215.8053 260.5710 107.9683 -2.6894 213.3075 215.9969 260.7126 108.7963 -2.6850 213.5257 216.2107 260.8456 109.5523 -2.6810 213.7096 216.3905 260.9773 110.4205 -2.6733 213.9222 216.5955 261.1014 111.1768 -2.6717 214.0762 216.7479 261.2338 111.9943 -2.6673 214.2986 216.9658 261.3373 112.8010 -2.6637 214.4757 217.1394 261.4595 113.5880 -2.6566 214.6425 217.2991 261.6031 114.3853 -2.6506 214.8152 217.4658 261.7582 115.1815 -2.6460 215.0002 217.6461 261.8887 116.0095 -2.6398 215.2202 217.8599 262.0218 116.7760 -2.6337 215.4058 218.0395 262.1428 117.6340 -2.6287 215.5537 218.1823 262.2468 118.4003 -2.6304 215.7600 218.3904 262.3267 119.2283 -2.6271 215.9874 218.6144 262.4590 120.0245 -2.6252 216.1643 218.7895 262.5579 120.8218 -2.6192 216.3504 218.9696 262.6544 121.6190 -2.6111 216.5712 219.1823 262.7427 122.4153 -2.6070 216.7913 219.3984 262.8426 123.2740 -2.6048 217.0187 219.6235 262.9803 123.9995 -2.6018 217.1970 219.7988 263.1298 124.8678 -2.5990 217.4097 220.0087 263.3016 125.6238 -2.5957 217.5786 220.1743 263.4101 126.4620 -2.5920 217.7767 220.3687 263.5097 127.2483 -2.5875 217.9236 220.5111 263.6341 128.0555 -2.5816 218.0842 220.6658 263.7862 128.8733 -2.5747 218.2616 220.8364 263.9018 129.6393 -2.5675 218.4058 220.9733 264.0063 130.4975 -2.5637 218.6089 221.1726 264.1161 131.2640 -2.5590 218.8279 221.3869 264.2148 132.0918 -2.5531 219.0075 221.5605 264.3308 132.8780 -2.5483 219.1906 221.7389 264.4917 133.6753 -2.5459 219.3810 221.9269 264.5939 134.4930 -2.5400 219.5987 222.1387 264.6855 135.2585 -2.5351 219.7974 222.3325 264.7920 136.1173 -2.5316 220.0148 222.5464 264.9339 136.8735 -2.5270 220.1908 222.7178 265.0426 137.7005 -2.5213 220.4034 222.9248 265.1298 138.4978 -2.5157 220.5723 223.0880 265.2165 139.2948 -2.5146 220.7020 223.2165 265.3573 140.1118 -2.5176 220.8436 223.3613 265.4836 140.8885 -2.5151 220.9746 223.4897 265.5570 141.7363 -2.5086 221.1691 223.6777 265.6449 142.5025 -2.5055 221.3555 223.8610 265.7505 143.3305 -2.5009 221.5671 224.0679 265.8919 144.1168 -2.5026 221.7349 224.2375 266.0202 144.9138 -2.4952 221.8817 224.3768 266.1474 145.7418 -2.4898 222.0958 224.5857 266.2486 146.5078 -2.4822 222.2610 224.7431 266.3588 147.3660 -2.4754 222.4457 224.9211 266.4348 148.1223 -2.4743 222.6091 225.0834 266.5660 148.9603 -2.4709 222.8191 225.2900 266.7349 149.7465 -2.4638 223.0119 225.4757 266.8705 150.5438 -2.4585 223.2255 225.6840 266.9490 151.3718 -2.4532 223.4385 225.8917 267.0561 152.1373 -2.4488 223.6400 226.0888 267.1464 152.9960 -2.4425 223.8294 226.2719 267.2801 153.7523 -2.4404 223.9928 226.4332 267.4322 154.5900 -2.4349 224.1637 226.5986 267.5793 155.3765 -2.4326 224.3802 226.8127 267.7038 156.1738 -2.4314 224.5557 226.9871 267.8587 157.0013 -2.4265 224.7697 227.1962 267.9866 157.7673 -2.4217 224.9738 227.3954 268.0974 158.6260 -2.4161 225.1607 227.5768 268.2003 159.3823 -2.4113 225.3085 227.7197 268.3218 160.2195 -2.4077 225.4891 227.8969 268.4764 161.0168 -2.4013 225.6782 228.0795 268.5905 161.8138 -2.3999 225.8445 228.2443 268.7165 162.6308 -2.3957 226.0168 228.4125 268.8484 163.4075 -2.3913 226.1675 228.5588 268.9600 164.2560 -2.3886 226.3791 228.7677 269.0639 165.0215 -2.3843 226.5306 228.9149 269.1805 165.8495 -2.3807 226.6691 229.0498 269.3090 166.6365 -2.3765 226.8622 229.2387 269.4254 167.4225 -2.3761 227.0340 229.4102 269.5545 168.2198 -2.3765 227.1971 229.5736 269.6881 169.0170 -2.3743 227.3580 229.7323 269.8193 169.8340 -2.3724 227.5103 229.8828 269.9916 170.6003 -2.3670 227.6735 230.0405 270.1461 171.4590 -2.3640 227.8664 230.2304 270.2754 172.2150 -2.3620 228.0340 230.3960 270.3829 173.0525 -2.3572 228.2260 230.5832 270.4966 173.8395 -2.3517 228.3677 230.7193 270.5962 174.6263 -2.3450 228.4981 230.8431 270.7297 175.4638 -2.3416 228.7051 231.0468 270.8713 176.2200 -2.3397 228.8703 231.2100 270.9954 177.0785 -2.3344 229.0381 231.3726 271.1436 177.8443 -2.3312 229.2212 231.5525 271.3061 178.6723 -2.3272 229.4054 231.7326 271.4065 179.4688 -2.3223 229.5841 231.9064 271.5220 180.2555 -2.3202 229.7425 232.0627 271.6689 181.0938 -2.3170 229.9308 232.2478 271.7989 181.8498 -2.3138 230.1071 232.4209 271.9282 182.7078 -2.3063 230.2959 232.6022 272.0494 183.4743 -2.3058 230.4683 232.7740 272.1668 184.3018 -2.3050 230.6340 232.9390 272.3021 185.0985 -2.2986 230.8174 233.1160 272.4118 185.8855 -2.2958 230.9988 233.2946 272.5973 186.7235 -2.2952 231.1844 233.4796 272.7585 187.4790 -2.2958 231.3106 233.6064 272.8723 188.3378 -2.2875 231.4643 233.7519 273.0298 189.1043 -2.2828 231.6072 233.8900 273.1783 189.9313 -2.2775 231.8196 234.0971 273.3329 190.7285 -2.2764 231.9994 234.2758 273.5046 191.5155 -2.2727 232.1762 234.4489 273.6582 192.3530 -2.2712 232.3437 234.6148 273.8015 193.1090 -2.2718 232.5145 234.7863 273.9361 193.9370 -2.2687 232.6847 234.9534 274.0975 194.7030 -2.2678 232.8629 235.1307 274.2398 195.5715 -2.2668 233.0518 235.3186 274.4074 196.3278 -2.2668 233.2219 235.4886 274.5415 197.1550 -2.2676 233.3850 235.6526 274.6913 197.9520 -2.2631 233.5480 235.8111 274.8486 198.7390 -2.2660 233.7140 235.9799 275.0137 199.5563 -2.2669 233.8574 236.1243 275.1715 200.3325 -2.2603 234.0565 236.3168 275.3126 201.1810 -2.2547 234.2178 236.4725 275.4567 201.9063 -2.2523 234.3597 236.6119 275.5594 202.7745 -2.2468 234.5367 236.7835 275.6849 203.5308 -2.2433 234.7106 236.9539 275.8201 204.3480 -2.2374 234.8649 237.1023 275.9906 205.1550 -2.2329 234.9968 237.2297 276.1561 205.9420 -2.2299 235.1605 237.3904 276.3247 206.7700 -2.2323 235.3078 237.5401 276.4692 207.5355 -2.2317 235.4796 237.7113 276.5949 208.3943 -2.2310 235.6897 237.9207 276.7311 209.1608 -2.2302 235.8498 238.0800 276.8624 209.9775 -2.2257 236.0043 238.2300 276.9933 210.7543 -2.2244 236.1782 238.4026 277.1115 211.5720 -2.2219 236.3545 238.5764 277.2464 212.3685 -2.2188 236.5279 238.7467 277.3911 213.1655 -2.2197 236.7003 238.9201 277.5543 213.9935 -2.2185 236.8502 239.0687 277.7123 214.7595 -2.2210 237.0031 239.2241 277.8534 215.6178 -2.2158 237.1295 239.3453 277.9794 216.3535 -2.2169 237.2598 239.4767 278.0840 217.2220 -2.2151 237.4549 239.6701 278.2282 217.9778 -2.2168 237.6352 239.8520 278.3246 218.8058 -2.2119 237.8493 240.0611 278.4651 219.6023 -2.2102 238.0135 240.2237 278.5980 220.3993 -2.2075 238.1808 240.3882 278.7592 221.2273 -2.2087 238.3553 240.5640 278.8463 221.9833 -2.2040 238.4902 240.6942 278.9604 222.8515 -2.1967 238.6787 240.8755 279.1301 223.6078 -2.1953 238.8325 241.0279 279.2869 224.4355 -2.1907 238.9879 241.1786 279.4192 225.2320 -2.1895 239.1559 241.3453 279.5735 226.0293 -2.1865 239.3201 241.5066 279.7074 226.8570 -2.1874 239.5107 241.6981 279.8301 227.6228 -2.1849 239.6658 241.8508 279.8953 228.4815 -2.1795 239.8511 242.0305 280.0244 229.2475 -2.1771 239.9985 242.1756 280.1425 230.0648 -2.1749 240.1678 242.3427 280.2666 230.8620 -2.1748 240.3042 242.4790 280.4104 231.6483 -2.1775 240.4631 242.6406 280.5653 232.4658 -2.1738 240.6423 242.8161 280.7281 233.2425 -2.1742 240.7980 242.9722 280.8473 234.0903 -2.1703 240.9600 243.1303 280.9604 234.8258 -2.1662 241.1070 243.2732 281.0683 235.6845 -2.1652 241.2752 243.4404 281.1905 236.4503 -2.1618 241.4392 243.6010 281.3189 237.2678 -2.1603 241.6043 243.7646 281.4564 238.0650 -2.1627 241.7581 243.9208 281.6020 238.8613 -2.1603 241.9189 244.0791 281.7082 239.6893 -2.1582 242.1062 244.2645 281.8249 240.4455 -2.1567 242.2640 244.4207 281.9536 241.3135 -2.1574 242.4712 244.6285 282.0854 242.0698 -2.1535 242.6343 244.7878 282.1826 242.8978 -2.1567 242.7926 244.9493 282.3087 243.6940 -2.1596 242.9297 245.0893 282.4112 244.4913 -2.1612 243.0863 245.2475 282.5635 245.3193 -2.1602 243.2319 245.3920 282.6888 246.0748 -2.1547 243.3744 245.5291 282.8039 246.9435 -2.1502 243.5735 245.7237 282.9696 247.6998 -2.1482 243.7378 245.8860 283.0710 248.5270 -2.1482 243.9047 246.0529 283.1957 249.3240 -2.1474 244.0611 246.2085 283.3054 250.1213 -2.1473 244.2455 246.3928 283.4053 250.9488 -2.1423 244.4188 246.5611 283.5076 251.7148 -2.1390 244.5672 246.7062 283.6445 252.5735 -2.1387 244.7161 246.8549 283.7716 253.3398 -2.1346 244.8595 246.9941 283.8723 254.1670 -2.1321 245.0293 247.1615 283.9592 254.9540 -2.1312 245.1703 247.3014 284.1124 255.7613 -2.1266 245.3686 247.4952 284.2695 256.5783 -2.1287 245.5057 247.6344 284.4024 257.3448 -2.1299 245.6305 247.7605 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