DTA measure 1lassu Date: 2026324:1153 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1273.88 s Mass = 934.500 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1590 -1.0267 220.3748 221.4014 249.1561 1.9768 -1.0271 220.4766 221.5038 249.0906 2.7433 -1.0308 220.5468 221.5775 249.0597 3.5920 -1.0325 220.6456 221.6781 249.0252 4.3593 -1.0358 220.7473 221.7831 248.9754 5.1873 -1.0428 220.8803 221.9230 248.9381 5.9435 -1.0432 220.9643 222.0076 248.9069 6.7715 -1.0447 221.0317 222.0764 248.8876 7.5688 -1.0474 221.1101 222.1576 248.8442 8.3660 -1.0505 221.2200 222.2705 248.8040 9.1838 -1.0511 221.3131 222.3642 248.7533 9.9503 -1.0518 221.4054 222.4572 248.6920 10.8090 -1.0521 221.4418 222.4938 248.6404 11.5653 -1.0535 221.5320 222.5855 248.6032 12.4035 -1.0558 221.6303 222.6861 248.5640 13.1905 -1.0562 221.7056 222.7618 248.5085 13.9885 -1.0593 221.8173 222.8766 248.4951 14.7860 -1.0595 221.9072 222.9667 248.4702 15.5833 -1.0595 221.9815 223.0410 248.4177 16.4010 -1.0619 222.1232 223.1850 248.3852 17.1675 -1.0574 222.2253 223.2828 248.3582 18.0263 -1.0585 222.3300 223.3885 248.3255 18.7928 -1.0542 222.4138 223.4680 248.2572 19.6105 -1.0553 222.4998 223.5551 248.2188 20.4180 -1.0569 222.6061 223.6630 248.1961 21.2050 -1.0580 222.6703 223.7284 248.2074 22.0330 -1.0582 222.7824 223.8406 248.2041 22.7995 -1.0617 222.8946 223.9563 248.1908 23.6583 -1.0611 222.9942 224.0553 248.1798 24.4155 -1.0638 223.0777 224.1415 248.1814 25.2435 -1.0590 223.1546 224.2136 248.1620 26.0408 -1.0544 223.2342 224.2886 248.1752 26.8380 -1.0515 223.3446 224.3961 248.1632 27.6558 -1.0504 223.4727 224.5231 248.1448 28.4325 -1.0527 223.5607 224.6135 248.1836 29.2810 -1.0494 223.6480 224.6975 248.2635 30.0475 -1.0452 223.7443 224.7896 248.3010 30.8755 -1.0425 223.8383 224.8808 248.3115 31.6735 -1.0392 223.9139 224.9531 248.3351 32.4710 -1.0375 224.0185 225.0560 248.3850 33.2888 -1.0420 224.1028 225.1449 248.4008 34.0655 -1.0438 224.1825 225.2263 248.4324 34.8833 -1.0459 224.2874 225.3333 248.5031 35.6600 -1.0421 224.3766 225.4187 248.5538 36.5085 -1.0440 224.4423 225.4863 248.5879 37.2853 -1.0446 224.5268 225.5715 248.5954 38.1030 -1.0410 224.6090 225.6500 248.6663 38.9003 -1.0402 224.7133 225.7536 248.7220 39.6975 -1.0400 224.7892 225.8292 248.7686 40.5255 -1.0390 224.9302 225.9692 248.8523 41.2920 -1.0387 225.0214 226.0601 248.9204 42.1410 -1.0330 225.1304 226.1635 248.9955 42.9183 -1.0297 225.2110 226.2408 249.1129 43.7360 -1.0274 225.2851 226.3126 249.2295 44.5333 -1.0263 225.3698 226.3961 249.3143 45.3305 -1.0253 225.4403 226.4656 249.4219 46.1585 -1.0213 225.5455 226.5669 249.5279 46.9250 -1.0176 225.6169 226.6346 249.6344 47.7735 -1.0112 225.7446 226.7558 249.7384 48.5503 -1.0106 225.8352 226.8458 249.7975 49.3680 -1.0105 225.8995 226.9100 249.8857 50.1655 -1.0113 225.9784 226.9896 249.9908 50.9635 -1.0162 226.0590 227.0752 250.1437 51.7915 -1.0161 226.1753 227.1914 250.2816 52.5580 -1.0153 226.2601 227.2754 250.4138 53.4065 -1.0122 226.3586 227.3708 250.5249 54.1833 -1.0108 226.4356 227.4464 250.6325 55.0010 -1.0119 226.5181 227.5299 250.7660 55.7983 -1.0136 226.5840 227.5976 250.8798 56.5955 -1.0159 226.6846 227.7005 250.9990 57.4235 -1.0138 226.7745 227.7883 251.1050 58.1900 -1.0109 226.8644 227.8753 251.2081 59.0385 -1.0134 226.9881 228.0015 251.3390 59.8050 -1.0143 227.0381 228.0524 251.4814 60.6228 -1.0151 227.1528 228.1679 251.5933 61.4200 -1.0104 227.2363 228.2467 251.7220 62.2078 -1.0120 227.3145 228.3265 251.8496 63.0258 -1.0115 227.3887 228.4002 252.0218 63.8025 -1.0114 227.4211 228.4325 252.1643 64.6203 -1.0136 227.5204 228.5340 252.3198 65.3868 -1.0111 227.6332 228.6443 252.4434 66.2455 -1.0138 227.7356 228.7494 252.5860 67.0018 -1.0156 227.8269 228.8425 252.6830 67.8195 -1.0177 227.9402 228.9579 252.8039 68.6270 -1.0203 227.9900 229.0103 252.9109 69.4140 -1.0172 228.1094 229.1266 253.0447 70.2318 -1.0197 228.2231 229.2428 253.1650 70.9985 -1.0196 228.3311 229.3507 253.2871 71.8580 -1.0217 228.4097 229.4315 253.4247 72.5835 -1.0236 228.4845 229.5081 253.5769 73.4525 -1.0232 228.6093 229.6326 253.7259 74.2088 -1.0234 228.6750 229.6983 253.8670 75.0265 -1.0223 228.7524 229.7747 254.0415 75.8340 -1.0223 228.8528 229.8751 254.2132 76.6210 -1.0215 228.9665 229.9881 254.3643 77.4490 -1.0233 229.0877 230.1109 254.5049 78.2155 -1.0240 229.1959 230.2199 254.6361 79.0750 -1.0273 229.3017 230.3290 254.7896 79.8418 -1.0292 229.3897 230.4189 254.9396 80.6595 -1.0330 229.4748 230.5078 255.0783 81.4363 -1.0337 229.5722 230.6060 255.1993 82.2540 -1.0336 229.6598 230.6935 255.3238 83.0615 -1.0363 229.7114 230.7477 255.4831 83.8485 -1.0384 229.8124 230.8508 255.6123 84.6868 -1.0377 229.9725 231.0102 255.7637 85.4430 -1.0425 230.0652 231.1077 255.8861 86.2813 -1.0446 230.1635 231.2081 255.9955 87.0583 -1.0437 230.2400 231.2836 256.0835 87.8973 -1.0462 230.3568 231.4030 256.2640 88.6535 -1.0432 230.4271 231.4703 256.4029 89.5225 -1.0443 230.4836 231.5280 256.4984 90.2583 -1.0457 230.5738 231.6195 256.6339 91.1273 -1.0419 230.6777 231.7196 256.8132 91.8630 -1.0440 230.7747 231.8188 256.9414 92.7218 -1.0415 230.8671 231.9086 257.0669 93.4883 -1.0405 230.9688 232.0094 257.1994 94.3573 -1.0409 231.0777 232.1186 257.3277 95.1955 -1.0468 231.1446 232.1914 257.4488 95.9825 -1.0524 231.2682 232.3206 257.5821 96.7798 -1.0521 231.3347 232.3868 257.6915 97.6085 -1.0532 231.4165 232.4697 257.8100 98.3753 -1.0549 231.4829 232.5378 257.9413 99.2340 -1.0587 231.5941 232.6528 258.0522 99.9903 -1.0602 231.6730 232.7332 258.1359 100.8285 -1.0635 231.7496 232.8131 258.2381 101.6155 -1.0650 231.8646 232.9296 258.3231 102.4128 -1.0663 231.9840 233.0503 258.4339 103.2100 -1.0710 232.0128 233.0838 258.5464 104.0073 -1.0729 232.1169 233.1897 258.7084 104.8353 -1.0742 232.2350 233.3092 258.8418 105.5925 -1.0741 232.3218 233.3960 258.9247 106.4615 -1.0734 232.4638 233.5372 259.0405 107.2178 -1.0732 232.5448 233.6181 259.1540 108.0458 -1.0773 232.6604 233.7377 259.2417 108.8430 -1.0800 232.7808 233.8608 259.3465 109.6403 -1.0810 232.8749 233.9559 259.4306 110.4683 -1.0853 232.9440 234.0293 259.5297 111.2348 -1.0894 233.0521 234.1416 259.6163 112.0935 -1.0926 233.1629 234.2556 259.7626 112.8600 -1.0979 233.2370 234.3349 259.9048 113.6880 -1.0928 233.3126 234.4054 260.0196 114.4758 -1.0882 233.4358 234.5240 260.1419 115.2835 -1.0907 233.5452 234.6360 260.2538 116.1013 -1.0955 233.6086 234.7041 260.3508 116.8678 -1.0951 233.6527 234.7478 260.4553 117.7265 -1.0999 233.7844 234.8843 260.5709 118.4930 -1.0999 233.8946 234.9945 260.6576 119.3210 -1.1010 233.9696 235.0706 260.7614 120.0978 -1.1031 234.0501 235.1532 260.8058 120.9155 -1.1033 234.1535 235.2568 260.8483 121.7230 -1.1026 234.2489 235.3515 260.9188 122.5208 -1.1032 234.3405 235.4438 260.9991 123.3083 -1.1057 234.4496 235.5554 261.1236 124.1055 -1.1114 234.5420 235.6534 261.2265 124.9335 -1.1129 234.6423 235.7552 261.3040 125.6898 -1.1114 234.7808 235.8923 261.3974 126.5485 -1.1135 234.9147 236.0282 261.4710 127.3048 -1.1130 235.0380 236.1510 261.5563 128.1225 -1.1147 235.1098 236.2245 261.6425 128.9198 -1.1160 235.1943 236.3104 261.7123 129.7170 -1.1187 235.2856 236.4043 261.8508 130.5348 -1.1228 235.3874 236.5102 261.9710 131.3115 -1.1227 235.4739 236.5966 262.0680 132.1293 -1.1267 235.5742 236.7009 262.1436 132.8855 -1.1284 235.6649 236.7934 262.2496 133.7445 -1.1315 235.7600 236.8914 262.3383 134.5118 -1.1302 235.8592 236.9894 262.4273 135.3295 -1.1305 235.9702 237.1007 262.5168 136.1370 -1.1330 236.0507 237.1838 262.6146 136.9240 -1.1346 236.1273 237.2620 262.6821 137.7418 -1.1335 236.2351 237.3686 262.7754 138.5185 -1.1340 236.3261 237.4601 262.8340 139.3670 -1.1329 236.4474 237.5803 262.9444 140.1335 -1.1334 236.5498 237.6832 263.0551 140.9615 -1.1351 236.6407 237.7758 263.1467 141.7595 -1.1351 236.7530 237.8881 263.2489 142.5570 -1.1328 236.8456 237.9784 263.3383 143.3748 -1.1327 236.9505 238.0832 263.3821 144.1413 -1.1329 237.0499 238.1827 263.4537 145.0000 -1.1294 237.1446 238.2740 263.5571 145.7563 -1.1304 237.2499 238.3803 263.6672 146.5945 -1.1358 237.3527 238.4885 263.7815 147.3815 -1.1390 237.4769 238.6159 263.8702 148.1685 -1.1436 237.5716 238.7152 263.9630 149.0068 -1.1451 237.6330 238.7781 264.0800 149.7630 -1.1474 237.7243 238.8717 264.1554 150.6220 -1.1453 237.8399 238.9852 264.2340 151.3893 -1.1486 237.9241 239.0727 264.3219 152.2173 -1.1467 238.0643 239.2109 264.4356 153.0145 -1.1460 238.1631 239.3091 264.5347 153.8015 -1.1457 238.2282 239.3738 264.6023 154.6398 -1.1393 238.3251 239.4644 264.6965 155.3960 -1.1409 238.3747 239.5155 264.7789 156.2240 -1.1415 238.4900 239.6315 264.8797 156.9905 -1.1437 238.5927 239.7364 264.9901 157.8493 -1.1406 238.7266 239.8672 265.0793 158.6158 -1.1439 238.8147 239.9586 265.1747 159.4335 -1.1478 238.9056 240.0534 265.2801 160.2418 -1.1475 239.0225 240.1701 265.3713 161.0290 -1.1511 239.0957 240.2469 265.4687 161.8673 -1.1507 239.2108 240.3615 265.5464 162.6235 -1.1520 239.3240 240.4760 265.6430 163.4925 -1.1552 239.4240 240.5792 265.7771 164.2488 -1.1588 239.5287 240.6875 265.8890 165.0768 -1.1599 239.6373 240.7972 266.0173 165.8740 -1.1615 239.7052 240.8668 266.0977 166.6713 -1.1655 239.7977 240.9633 266.1673 167.5000 -1.1626 239.9208 241.0833 266.2650 168.2565 -1.1623 240.0170 241.1793 266.3563 169.1255 -1.1597 240.1483 241.3080 266.4548 169.8818 -1.1623 240.2144 241.3768 266.5123 170.7098 -1.1627 240.2808 241.4434 266.6186 171.5070 -1.1592 240.3761 241.5353 266.7112 172.3145 -1.1573 240.4867 241.6441 266.8017 173.1015 -1.1589 240.5835 241.7424 266.8836 173.8998 -1.1619 240.6811 241.8429 266.9414 174.7278 -1.1632 240.7991 241.9623 267.0566 175.4943 -1.1612 240.9036 242.0648 267.1733 176.3530 -1.1597 240.9984 242.1582 267.2955 177.1195 -1.1636 241.1046 242.2682 267.4006 177.9475 -1.1701 241.2043 242.3744 267.4890 178.7448 -1.1648 241.3029 242.4677 267.6129 179.5420 -1.1649 241.3853 242.5503 267.7052 180.3598 -1.1693 241.4327 242.6020 267.8193 181.1365 -1.1661 241.5669 242.7330 267.9356 181.9645 -1.1717 241.7082 242.8799 268.0455 182.7310 -1.1712 241.8168 242.9880 268.1452 183.5908 -1.1687 241.9364 243.1050 268.2931 184.3573 -1.1727 242.0072 243.1798 268.4203 185.1853 -1.1782 242.0660 243.2442 268.5008 185.9825 -1.1772 242.1485 243.3257 268.5909 186.7695 -1.1781 242.2490 243.4271 268.7149 187.5975 -1.1807 242.3818 243.5624 268.8182 188.3538 -1.1866 242.5009 243.6875 268.9009 189.1818 -1.1864 242.6156 243.8020 269.0082 189.9380 -1.1830 242.7224 243.9054 269.1218 190.7865 -1.1910 242.8581 244.0491 269.2497 191.5633 -1.1914 242.9455 244.1369 269.3725 192.3810 -1.1908 243.0287 244.2194 269.4921 193.1680 -1.1920 243.0870 244.2790 269.5913 193.9653 -1.1915 243.1554 244.3469 269.7105 194.7838 -1.1895 243.2393 244.4288 269.8461 195.5505 -1.1912 243.2990 244.4902 269.9482 196.3990 -1.1915 243.3527 244.5442 270.1080 197.1655 -1.1934 243.4224 244.6158 270.2080 197.9935 -1.1951 243.5568 244.7519 270.3189 198.7498 -1.1944 243.6853 244.8797 270.4404 199.5778 -1.1940 243.8038 244.9978 270.5658 200.3750 -1.1925 243.9316 245.1240 270.6623 201.1620 -1.1932 244.0445 245.2377 270.7764 201.9900 -1.1978 244.1487 245.3465 270.8822 202.7565 -1.1943 244.2622 245.4566 270.9782 203.6053 -1.1956 244.3662 245.5618 271.0840 204.3725 -1.1967 244.4700 245.6667 271.1855 205.2005 -1.1969 244.5800 245.7769 271.2863 205.9978 -1.2003 244.6732 245.8735 271.3768 206.7950 -1.2006 244.7798 245.9804 271.4951 207.6128 -1.2037 244.8814 246.0852 271.6115 208.3895 -1.2040 244.9586 246.1626 271.7214 209.2380 -1.2032 245.0710 246.2742 271.8828 209.9738 -1.2046 245.1891 246.3937 271.9812 210.8325 -1.2068 245.2772 246.4840 272.1038 211.5990 -1.2065 245.3382 246.5447 272.2013 212.4168 -1.2081 245.4422 246.6503 272.3044 213.2140 -1.2065 245.5312 246.7377 272.4302 214.0113 -1.2065 245.6302 246.8367 272.5223 214.8700 -1.2120 245.7023 246.9143 272.6200 215.6063 -1.2110 245.8163 247.0272 272.7403 216.4655 -1.2108 245.9666 247.1775 272.8698 217.2320 -1.2133 246.0692 247.2826 272.9690 218.0600 -1.2140 246.1821 247.3961 273.1114 218.8470 -1.2148 246.2689 247.4837 273.1695 219.6545 -1.2175 246.3583 247.5758 273.2545 220.4723 -1.2193 246.4460 247.6654 273.3840 221.2388 -1.2224 246.5506 247.7730 273.4731 222.0978 -1.2235 246.6469 247.8704 273.5866 222.8650 -1.2261 246.7412 247.9673 273.6823 223.6930 -1.2296 246.8870 248.1166 273.8301 224.4800 -1.2311 247.0072 248.2383 273.9644 225.2875 -1.2311 247.0835 248.3145 274.1102 226.1053 -1.2309 247.1483 248.3793 274.2461 226.8718 -1.2323 247.2633 248.4956 274.3268 227.7305 -1.2304 247.3896 248.6200 274.4288 228.4973 -1.2304 247.4843 248.7147 274.5437 229.3260 -1.2322 247.6067 248.8389 274.6571 230.1130 -1.2333 247.6855 248.9188 274.7676 230.9205 -1.2337 247.7602 248.9940 274.8529 231.7075 -1.2350 247.8502 249.0852 274.9339 232.5048 -1.2327 247.9390 249.1717 275.0414 233.3328 -1.2350 248.0549 249.2899 275.1334 234.1710 -1.2392 248.1623 249.4015 275.2142 235.0195 -1.2404 248.2540 249.4945 275.3378 235.7963 -1.2393 248.3385 249.5778 275.4504 236.6140 -1.2367 248.4701 249.7068 275.5545 237.4113 -1.2351 248.5780 249.8131 275.6360 238.2093 -1.2356 248.6607 249.8963 275.7557 239.0375 -1.2367 248.8035 250.0402 275.8894 239.8040 -1.2382 248.9275 250.1657 276.0127 240.6525 -1.2440 249.0419 250.2859 276.1372 241.4293 -1.2483 249.1351 250.3834 276.2103 242.2470 -1.2545 249.2528 250.5072 276.3302 243.0443 -1.2600 249.3371 250.5971 276.4667 243.8415 -1.2628 249.4100 250.6728 276.5756 244.6695 -1.2608 249.5557 250.8164 276.6776 245.4360 -1.2627 249.6794 250.9420 276.7716 246.2845 -1.2573 249.7892 251.0464 276.8859 247.0620 -1.2591 249.8744 251.1335 276.9879 247.8800 -1.2620 249.9844 251.2463 277.0784 248.6773 -1.2625 250.0976 251.3601 277.2014 249.4745 -1.2640 250.2157 251.4797 277.3030 250.3128 -1.2655 250.3000 251.5656 277.3808 251.0895 -1.2636 250.3926 251.6562 277.4818 251.9073 -1.2594 250.5112 251.7707 277.5966 252.6635 -1.2553 250.6133 251.8687 277.6518 253.5325 -1.2590 250.7240 251.9830 277.7584 254.2888 -1.2653 250.8361 252.1014 277.8585 255.1065 -1.2712 250.9285 252.1996 277.9794 255.9038 -1.2728 251.0189 252.2917 278.0612 256.7010 -1.2755 251.0720 252.3475 278.1623 257.5195 -1.2758 251.1799 252.4557 278.2746 258.2863 -1.2762 251.3002 252.5764 278.3590 259.1143 -1.2792 251.4242 252.7034 278.4817 259.9013 -1.2774 251.4909 252.7684 278.5725 260.7293 -1.2724 251.6185 252.8909 278.6675 261.4958 -1.2701 251.7192 252.9893 278.7404 262.3135 -1.2722 251.8556 253.1278 278.8655 263.1210 -1.2693 251.9833 253.2526 278.9676 263.9080 -1.2656 252.1024 253.3680 279.0690 264.7360 -1.2705 252.1980 253.4685 279.1867 265.5025 -1.2708 252.3033 253.5741 279.3042 266.3305 -1.2729 252.4026 253.6754 279.4025 267.0970 -1.2737 252.4812 253.7548 279.4972 267.9458 -1.2688 252.5663 253.8351 279.5962 268.7228 -1.2703 252.6536 253.9239 279.7036 269.5410 -1.2768 252.7532 254.0301 279.8417 270.3383 -1.2834 252.8582 254.1416 279.9437 271.1355 -1.2802 252.9236 254.2038 280.0627 271.9530 -1.2819 253.0265 254.3085 280.1845 272.7198 -1.2804 253.1212 254.4016 280.2973 273.5785 -1.2800 253.2261 254.5061 280.3969 274.3450 -1.2811 253.3103 254.5914 280.4388 275.1730 -1.2842 253.4117 254.6959 280.5140 275.9600 -1.2835 253.5076 254.7911 280.6047 276.7675 -1.2857 253.6181 254.9039 280.7200 277.5545 -1.2921 253.7373 255.0294 280.8612 278.3518 -1.2926 253.8539 255.1465 280.9712 279.1800 -1.2904 253.9601 255.2505 281.0675 279.9463 -1.2922 254.0394 255.3316 281.1943 280.8060 -1.3016 254.1602 255.4618 281.2716 281.5615 -1.3012 254.2766 255.5778 281.3110 282.4005 -1.3020 254.3739 255.6759 281.3968 283.1875 -1.2996 254.4663 255.7659 281.4916 283.9848 -1.2984 254.5937 255.8921 281.5942 284.8128 -1.2975 254.6777 255.9752 281.6912 285.5793 -1.2982 254.7919 256.0901 281.7735 286.4380 -1.2994 254.9144 256.2138 281.8844 287.1943 -1.3020 255.0332 256.3352 282.0067 288.0325 -1.3021 255.1438 256.4459 282.1085 288.8195 -1.3043 255.2374 256.5417 282.1937 289.6168 -1.3063 255.3419 256.6482 282.2742 290.4455 -1.3070 255.4902 256.7972 282.4082 291.2115 -1.3073 255.5921 256.8995 282.5269 292.0400 -1.3064 255.7047 257.0112 282.6178 292.7965 -1.3034 255.7924 257.0958 282.6855 293.6655 -1.3033 255.9268 257.2300 282.7887 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