DTA measure 1gyors Date: 202633:1052 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.53 s Mass = 1153.400 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2098 -4.2403 184.3770 188.6172 247.0403 1.9860 -4.2282 184.6200 188.8482 246.9410 2.8038 -4.2161 184.8993 189.1154 246.8627 3.5800 -4.2027 185.1322 189.3349 246.8053 4.4280 -4.1914 185.3676 189.5590 246.6926 5.1945 -4.1763 185.5993 189.7756 246.6185 6.0223 -4.1673 185.8804 190.0477 246.5511 6.8188 -4.1571 186.1463 190.3034 246.4809 7.6160 -4.1437 186.4052 190.5489 246.3993 8.4338 -4.1351 186.6458 190.7809 246.3405 9.2095 -4.1246 186.9089 191.0335 246.2647 10.0580 -4.1119 187.1921 191.3040 246.2090 10.8143 -4.1048 187.4242 191.5290 246.1601 11.6413 -4.0978 187.6821 191.7798 246.0924 12.4283 -4.0866 187.9281 192.0147 246.0346 13.2255 -4.0787 188.1727 192.2514 245.9864 14.0528 -4.0657 188.4358 192.5015 245.9525 14.8088 -4.0513 188.6673 192.7186 245.9350 15.6675 -4.0450 188.9367 192.9817 245.8774 16.4230 -4.0359 189.2134 193.2492 245.8469 17.2405 -4.0203 189.4835 193.5038 245.8064 18.0275 -4.0060 189.7311 193.7372 245.7854 18.8550 -3.9884 189.9452 193.9337 245.7524 19.6518 -3.9713 190.1941 194.1654 245.7165 20.4388 -3.9615 190.4454 194.4068 245.7148 21.2358 -3.9465 190.6519 194.5984 245.6859 22.0323 -3.9309 190.8918 194.8227 245.6884 22.8603 -3.9229 191.1388 195.0617 245.6733 23.6160 -3.9130 191.3373 195.2503 245.6768 24.4743 -3.9011 191.5758 195.4769 245.6496 25.2408 -3.8895 191.7965 195.6860 245.6534 26.0580 -3.8736 192.0535 195.9270 245.6790 26.8650 -3.8610 192.3061 196.1671 245.7086 27.6520 -3.8492 192.5345 196.3837 245.7589 28.4798 -3.8359 192.7547 196.5906 245.8235 29.2660 -3.8232 192.9656 196.7888 245.9034 30.0633 -3.8108 193.2117 197.0225 245.9474 30.8603 -3.7984 193.4707 197.2691 245.9841 31.6875 -3.7827 193.7042 197.4870 246.0569 32.4540 -3.7693 193.9360 197.7054 246.1595 33.3025 -3.7521 194.1981 197.9502 246.2117 34.0785 -3.7351 194.3899 198.1251 246.3026 34.8960 -3.7227 194.6392 198.3619 246.4126 35.6933 -3.7117 194.8852 198.5969 246.5422 36.4898 -3.7030 195.1453 198.8483 246.6170 37.3175 -3.6881 195.3940 199.0821 246.6668 38.0838 -3.6785 195.6274 199.3059 246.7651 38.9315 -3.6623 195.8512 199.5134 246.8504 39.7083 -3.6480 196.0718 199.7199 246.9398 40.5260 -3.6302 196.3219 199.9522 247.0571 41.3225 -3.6186 196.5264 200.1449 247.1870 42.1195 -3.6048 196.7306 200.3355 247.3069 42.9475 -3.5912 196.9794 200.5706 247.4705 43.7135 -3.5781 197.2271 200.8051 247.6183 44.5615 -3.5603 197.4529 201.0132 247.8035 45.3383 -3.5480 197.6745 201.2225 247.9687 46.1658 -3.5396 197.9177 201.4573 248.1207 46.9625 -3.5320 198.1233 201.6552 248.2693 47.7495 -3.5226 198.3194 201.8420 248.3985 48.5870 -3.5116 198.5596 202.0712 248.5345 49.3533 -3.4990 198.7786 202.2777 248.6879 50.2120 -3.4844 198.9945 202.4789 248.8662 50.9675 -3.4723 199.1883 202.6607 249.0131 51.8055 -3.4615 199.3986 202.8601 249.1499 52.5925 -3.4496 199.6186 203.0682 249.3853 53.3893 -3.4367 199.8195 203.2561 249.6014 54.2168 -3.4273 200.0100 203.4373 249.8238 54.9833 -3.4182 200.2172 203.6354 250.0096 55.8418 -3.4082 200.4650 203.8732 250.1921 56.5973 -3.3978 200.6799 204.0777 250.3871 57.4355 -3.3920 200.9108 204.3027 250.5945 58.2328 -3.3846 201.1333 204.5180 250.8281 59.0290 -3.3823 201.3494 204.7318 251.0004 59.8468 -3.3757 201.5851 204.9608 251.1784 60.6233 -3.3654 201.7845 205.1499 251.4155 61.4710 -3.3531 202.0055 205.3586 251.6330 62.2375 -3.3461 202.2161 205.5622 251.8252 63.0655 -3.3417 202.4545 205.7963 252.0335 63.8618 -3.3303 202.6626 205.9929 252.2300 64.6590 -3.3192 202.8427 206.1619 252.4380 65.4768 -3.3096 203.0570 206.3666 252.6475 66.2530 -3.3002 203.2843 206.5845 252.8356 67.1113 -3.2969 203.5081 206.8050 253.0463 67.8778 -3.2892 203.7119 207.0012 253.2290 68.6953 -3.2815 203.9112 207.1927 253.4378 69.5020 -3.2727 204.1352 207.4080 253.6304 70.2890 -3.2641 204.3390 207.6031 253.8520 71.1268 -3.2514 204.5719 207.8233 254.0771 71.8825 -3.2445 204.7963 208.0408 254.2538 72.7515 -3.2396 205.0128 208.2525 254.4507 73.5073 -3.2351 205.1901 208.4252 254.6330 74.3245 -3.2300 205.3986 208.6286 254.7817 75.1218 -3.2223 205.6073 208.8295 254.9224 75.9188 -3.2124 205.8014 209.0139 255.1031 76.7050 -3.2023 206.0006 209.2029 255.2952 77.5023 -3.1943 206.1921 209.3864 255.4612 78.3200 -3.1872 206.3625 209.5497 255.6186 79.0860 -3.1784 206.5472 209.7256 255.7571 79.9238 -3.1718 206.7564 209.9282 255.9478 80.6903 -3.1668 206.9347 210.1015 256.1448 81.5383 -3.1572 207.1594 210.3166 256.3467 82.3043 -3.1523 207.3708 210.5231 256.5287 83.1220 -3.1498 207.5774 210.7272 256.6698 83.9188 -3.1405 207.7796 210.9201 256.8096 84.7155 -3.1312 207.9972 211.1285 256.9869 85.5128 -3.1259 208.1945 211.3203 257.1312 86.3095 -3.1197 208.3977 211.5174 257.2649 87.1268 -3.1149 208.5991 211.7140 257.4616 87.8933 -3.1134 208.7696 211.8830 257.5774 88.7515 -3.1067 208.9491 212.0558 257.7374 89.5073 -3.1049 209.1483 212.2531 257.8537 90.3455 -3.0989 209.3819 212.4808 257.9916 91.1323 -3.0919 209.5442 212.6362 258.1308 91.9288 -3.0873 209.7511 212.8384 258.2758 92.7260 -3.0844 209.9746 213.0590 258.4356 93.5233 -3.0771 210.1704 213.2474 258.5738 94.3503 -3.0634 210.3917 213.4551 258.7108 95.1065 -3.0594 210.6028 213.6622 258.8896 95.9755 -3.0541 210.8744 213.9284 259.0510 96.7315 -3.0518 211.0716 214.1234 259.1261 97.5588 -3.0450 211.2438 214.2888 259.2741 98.3253 -3.0444 211.4065 214.4509 259.4061 99.1528 -3.0386 211.6173 214.6559 259.5341 99.9393 -3.0360 211.8111 214.8471 259.6305 100.7775 -3.0321 211.9562 214.9883 259.7767 101.5333 -3.0288 212.1255 215.1544 259.9064 102.3608 -3.0204 212.3370 215.3574 260.0221 103.1580 -3.0172 212.5510 215.5681 260.1475 103.9548 -3.0126 212.7850 215.7976 260.2557 104.7823 -3.0106 212.9890 215.9996 260.3594 105.5385 -3.0073 213.1917 216.1990 260.4358 106.4070 -2.9978 213.3861 216.3839 260.5937 107.1628 -2.9931 213.5421 216.5353 260.6952 107.9908 -2.9872 213.7665 216.7537 260.8326 108.7878 -2.9813 213.9864 216.9677 260.9432 109.5843 -2.9779 214.1954 217.1733 261.0549 110.3815 -2.9730 214.4017 217.3747 261.1514 111.1788 -2.9675 214.5705 217.5380 261.2742 112.0370 -2.9603 214.7672 217.7275 261.4054 112.7723 -2.9554 214.9496 217.9051 261.4774 113.6310 -2.9500 215.1555 218.1056 261.5912 114.3865 -2.9478 215.3289 218.2767 261.6671 115.2245 -2.9446 215.4807 218.4253 261.7631 116.0115 -2.9438 215.6523 218.5961 261.8848 116.8083 -2.9425 215.8527 218.7952 261.9825 117.6358 -2.9449 216.0493 218.9942 262.0925 118.4023 -2.9405 216.2094 219.1499 262.2010 119.2608 -2.9349 216.4025 219.3374 262.2912 120.0163 -2.9245 216.5801 219.5046 262.4088 120.8545 -2.9150 216.8182 219.7331 262.5185 121.6413 -2.9094 217.0070 219.9164 262.6314 122.4378 -2.9069 217.2006 220.1076 262.7524 123.2658 -2.9066 217.3941 220.3007 262.8804 124.0323 -2.9014 217.5524 220.4537 262.9810 124.8900 -2.8896 217.7420 220.6316 263.1117 125.6463 -2.8856 217.9359 220.8215 263.2228 126.4845 -2.8824 218.1382 221.0206 263.3523 127.2705 -2.8814 218.3287 221.2101 263.4502 128.0678 -2.8728 218.5337 221.4066 263.5517 128.8958 -2.8599 218.6773 221.5372 263.6870 129.6615 -2.8508 218.8619 221.7128 263.7910 130.5200 -2.8464 219.0414 221.8879 263.9023 131.2865 -2.8427 219.2374 222.0802 264.0108 132.1138 -2.8414 219.4449 222.2863 264.1286 132.9108 -2.8391 219.6264 222.4655 264.2494 133.7080 -2.8355 219.7856 222.6212 264.3681 134.5250 -2.8324 219.9608 222.7932 264.4859 135.3015 -2.8284 220.1453 222.9737 264.6112 136.1500 -2.8261 220.3352 223.1613 264.7224 136.9160 -2.8245 220.4897 223.3142 264.8016 137.7435 -2.8239 220.6672 223.4911 264.9508 138.5408 -2.8214 220.8709 223.6923 265.0534 139.3168 -2.8191 221.0314 223.8506 265.1743 140.1445 -2.8131 221.2374 224.0505 265.2821 140.9110 -2.8104 221.4326 224.2431 265.3750 141.7588 -2.8031 221.6351 224.4382 265.4936 142.5250 -2.8004 221.7867 224.5870 265.5796 143.3428 -2.7938 221.9830 224.7768 265.7094 144.1393 -2.7890 222.1385 224.9276 265.8251 144.9260 -2.7923 222.3280 225.1204 265.9589 145.7438 -2.7868 222.5212 225.3079 266.0566 146.5203 -2.7769 222.7029 225.4798 266.1973 147.3680 -2.7664 222.9002 225.6666 266.3464 148.1345 -2.7591 223.0870 225.8461 266.5018 148.9620 -2.7510 223.2925 226.0435 266.6623 149.7485 -2.7440 223.4503 226.1944 266.7963 150.5560 -2.7372 223.6475 226.3847 266.9299 151.3423 -2.7376 223.8295 226.5671 267.0604 152.1495 -2.7326 223.9988 226.7314 267.2062 152.9673 -2.7288 224.1678 226.8966 267.3466 153.7228 -2.7245 224.3384 227.0629 267.4427 154.5915 -2.7196 224.5194 227.2391 267.6016 155.3478 -2.7169 224.6840 227.4009 267.7358 156.1648 -2.7157 224.8782 227.5939 267.8613 156.9720 -2.7202 225.1105 227.8307 268.0004 157.7590 -2.7180 225.2612 227.9792 268.1357 158.5868 -2.7117 225.4493 228.1611 268.3145 159.3525 -2.7103 225.6540 228.3644 268.4739 160.2113 -2.7065 225.8675 228.5740 268.6330 160.9778 -2.7001 225.9934 228.6935 268.7605 161.7945 -2.6908 226.1446 228.8354 268.8768 162.6020 -2.6881 226.2997 228.9879 268.9422 163.3890 -2.6845 226.4937 229.1782 269.0484 164.2160 -2.6818 226.6703 229.3520 269.2289 164.9825 -2.6830 226.8457 229.5287 269.4078 165.8413 -2.6790 227.0876 229.7666 269.5917 166.6068 -2.6713 227.2615 229.9328 269.7454 167.4245 -2.6676 227.4776 230.1452 269.9161 168.2320 -2.6626 227.6521 230.3146 270.0883 169.0183 -2.6583 227.7973 230.4556 270.2177 169.8460 -2.6354 227.9779 230.6133 270.3525 170.6125 -2.6127 228.1685 230.7812 270.4778 171.4705 -2.6116 228.3556 230.9672 270.6389 172.2368 -2.6170 228.5024 231.1195 270.7865 173.0545 -2.6212 228.6357 231.2568 270.9384 173.8615 -2.6236 228.8022 231.4259 271.0973 174.6480 -2.6270 228.9655 231.5925 271.2534 175.4760 -2.6262 229.1339 231.7601 271.4334 176.2420 -2.6255 229.2522 231.8777 271.5646 177.1003 -2.6247 229.4350 232.0596 271.7271 177.8668 -2.6166 229.6296 232.2461 271.8395 178.6845 -2.6110 229.7889 232.3999 271.9965 179.4910 -2.6083 229.9539 232.5622 272.1572 180.2780 -2.6077 230.1110 232.7187 272.2923 181.1060 -2.6105 230.2747 232.8852 272.4625 181.8720 -2.6060 230.4208 233.0268 272.5712 182.7303 -2.6047 230.6193 233.2240 272.7080 183.4660 -2.6052 230.7868 233.3920 272.8527 184.3143 -2.6019 230.9380 233.5399 273.0013 185.0903 -2.5949 231.0743 233.6691 273.1393 185.9183 -2.5910 231.2368 233.8279 273.3104 186.7153 -2.5897 231.4013 233.9909 273.4460 187.5015 -2.5899 231.5469 234.1368 273.5625 188.3398 -2.5935 231.7334 234.3270 273.7227 189.0955 -2.6027 231.8908 234.4935 273.8468 189.9538 -2.6042 232.0706 234.6747 274.0078 190.7203 -2.6021 232.2717 234.8738 274.1210 191.5583 -2.5991 232.4770 235.0761 274.2251 192.3445 -2.6000 232.6208 235.2208 274.3455 193.1418 -2.5990 232.8124 235.4114 274.4747 193.9698 -2.5952 232.9911 235.5863 274.5608 194.7353 -2.5931 233.1584 235.7515 274.6950 195.5633 -2.5893 233.3413 235.9306 274.8386 196.3195 -2.5919 233.5075 236.0994 274.9724 197.1875 -2.5878 233.7186 236.3064 275.1018 197.9540 -2.5854 233.9068 236.4922 275.2102 198.7820 -2.5804 234.1027 236.6831 275.3334 199.5680 -2.5780 234.2906 236.8686 275.4764 200.3755 -2.5742 234.4474 237.0215 275.6036 201.1933 -2.5697 234.6086 237.1783 275.7393 201.9488 -2.5631 234.7646 237.3277 275.8668 202.8073 -2.5606 234.9566 237.5171 276.0433 203.5635 -2.5603 235.0890 237.6493 276.1749 204.3913 -2.5582 235.2933 237.8515 276.3291 205.1878 -2.5597 235.4464 238.0061 276.4289 205.9748 -2.5581 235.6014 238.1594 276.5187 206.8028 -2.5584 235.7596 238.3180 276.6523 207.5685 -2.5654 235.9106 238.4760 276.7694 208.3860 -2.5649 236.1126 238.6775 276.8585 209.1523 -2.5625 236.2500 238.8125 276.9807 210.0103 -2.5531 236.4291 238.9822 277.1248 210.7665 -2.5493 236.5830 239.1323 277.2531 211.5940 -2.5495 236.7416 239.2911 277.3289 212.3908 -2.5511 236.9062 239.4572 277.4389 213.1880 -2.5508 237.0779 239.6287 277.5304 214.0050 -2.5489 237.2811 239.8300 277.6601 214.7815 -2.5513 237.4381 239.9895 277.7625 215.6300 -2.5461 237.5863 240.1323 277.8928 216.3650 -2.5456 237.7225 240.2681 277.9890 217.2235 -2.5375 237.9550 240.4924 278.1028 217.9900 -2.5402 238.1109 240.6511 278.2105 218.8175 -2.5379 238.2551 240.7929 278.3414 219.6040 -2.5365 238.4397 240.9762 278.4802 220.4115 -2.5294 238.6117 241.1411 278.5795 221.2290 -2.5247 238.7728 241.2975 278.7237 221.9948 -2.5226 238.9279 241.4506 278.8195 222.8535 -2.5219 239.1187 241.6406 278.9406 223.6200 -2.5181 239.2827 241.8009 279.0786 224.4470 -2.5133 239.4645 241.9779 279.1301 225.2033 -2.5116 239.6190 242.1306 279.2426 226.0410 -2.5078 239.8117 242.3195 279.4141 226.8275 -2.5023 239.9249 242.4272 279.5300 227.6248 -2.4950 240.0678 242.5628 279.6798 228.4523 -2.4934 240.2152 242.7086 279.7893 229.2183 -2.4879 240.3644 242.8523 279.9217 230.0770 -2.4858 240.5529 243.0387 280.0631 230.8325 -2.4824 240.6846 243.1669 280.2149 231.6705 -2.4827 240.8445 243.3272 280.3317 232.4575 -2.4799 240.9820 243.4619 280.4168 233.2645 -2.4814 241.1497 243.6311 280.5291 234.0818 -2.4811 241.3380 243.8191 280.6479 234.8585 -2.4781 241.5071 243.9852 280.7274 235.7065 -2.4793 241.7058 244.1851 280.8998 236.4725 -2.4737 241.8500 244.3237 281.0561 237.3005 -2.4723 242.0098 244.4821 281.1855 238.0970 -2.4703 242.1908 244.6612 281.3038 238.8940 -2.4731 242.3548 244.8279 281.4215 239.7118 -2.4730 242.5126 244.9856 281.5694 240.4883 -2.4720 242.6796 245.1516 281.6802 241.3155 -2.4716 242.8204 245.2920 281.8125 242.0820 -2.4755 242.9450 245.4205 281.9544 242.9303 -2.4743 243.0842 245.5585 282.1019 243.7063 -2.4725 243.2432 245.7158 282.2326 244.5240 -2.4654 243.4100 245.8754 282.3517 245.3210 -2.4562 243.5750 246.0312 282.4747 246.1175 -2.4556 243.7457 246.2013 282.6105 246.9455 -2.4593 243.9359 246.3951 282.7568 247.7118 -2.4553 244.0897 246.5450 282.8769 248.5595 -2.4558 244.2825 246.7384 283.0095 249.3363 -2.4580 244.4728 246.9308 283.1342 250.1538 -2.4594 244.6577 247.1171 283.2643 250.9605 -2.4603 244.8283 247.2886 283.3720 251.7475 -2.4578 244.9567 247.4145 283.5032 252.5858 -2.4519 245.1268 247.5788 283.6610 253.3413 -2.4440 245.2819 247.7259 283.8030 254.1998 -2.4414 245.4526 247.8940 283.9300 254.9663 -2.4433 245.6090 248.0523 284.0607 255.7933 -2.4404 245.7355 248.1760 284.2635 256.5905 -2.4387 245.8571 248.2958 284.3815 257.3775 -2.4343 246.0085 248.4427 284.4816 258.2148 -2.4293 246.2329 248.6622 284.6225 258.9813 -2.4280 246.3517 248.7797 284.7234 259.8400 -2.4231 246.5124 248.9356 284.8862 260.5955 -2.4220 246.6311 249.0531 285.0248 261.4335 -2.4242 246.7669 249.1911 285.1803 262.2205 -2.4234 246.9121 249.3355 285.3170 263.0275 -2.4219 247.0769 249.4988 285.4804 263.8448 -2.4274 247.2280 249.6553 285.6475 264.6215 -2.4279 247.3654 249.7933 285.7684 265.4698 -2.4226 247.5436 249.9662 285.8979 266.2355 -2.4187 247.7286 250.1473 286.0170 267.0635 -2.4166 247.9064 250.3230 286.1387 267.8603 -2.4156 248.0606 250.4762 286.2770 268.6468 -2.4119 248.2106 250.6225 286.3996 269.4748 -2.4045 248.3828 250.7873 286.5359 270.2305 -2.4054 248.5371 250.9425 286.6399 271.0785 -2.4058 248.7309 251.1366 286.7883 271.8553 -2.4034 248.8602 251.2636 286.9091 272.6725 -2.4037 249.0229 251.4266 287.0325 273.4590 -2.4048 249.1834 251.5883 287.1515 274.2563 -2.4053 249.3151 251.7204 287.2969 275.0535 -2.4044 249.4419 251.8463 287.4679 275.8395 -2.4021 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