DTA measure 1lassu Date: 202633:1149 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.23 s Mass = 1153.400 mg data_number = 1580 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2318 -1.5609 218.6774 220.2383 248.6638 2.0598 -1.5661 218.7917 220.3578 248.6189 2.8263 -1.5718 218.8856 220.4574 248.5606 3.6440 -1.5790 219.0021 220.5812 248.5209 4.4105 -1.5829 219.1243 220.7073 248.4769 5.2590 -1.5778 219.2249 220.8027 248.4237 6.0258 -1.5810 219.2934 220.8745 248.3943 6.8545 -1.5829 219.3937 220.9765 248.3659 7.6415 -1.5827 219.5027 221.0854 248.3269 8.4285 -1.5802 219.6343 221.2144 248.2910 9.2668 -1.5758 219.7130 221.2888 248.2843 10.0230 -1.5798 219.7744 221.3543 248.2736 10.8715 -1.5786 219.8728 221.4514 248.2062 11.6483 -1.5762 219.9592 221.5355 248.1427 12.4660 -1.5787 220.0725 221.6512 248.1104 13.2530 -1.5749 220.1902 221.7652 248.0912 14.0605 -1.5755 220.3071 221.8826 248.0622 14.8475 -1.5774 220.3913 221.9687 248.0282 15.6448 -1.5813 220.4723 222.0536 247.9963 16.4728 -1.5813 220.5543 222.1356 247.9580 17.2290 -1.5790 220.6718 222.2508 247.9477 18.0878 -1.5796 220.7538 222.3333 247.9526 18.8545 -1.5828 220.8780 222.4607 247.9227 19.6730 -1.5836 220.9753 222.5589 247.8582 20.4703 -1.5822 221.0790 222.6612 247.8739 21.2675 -1.5822 221.1489 222.7310 247.8850 22.0955 -1.5843 221.2453 222.8295 247.8635 22.8620 -1.5828 221.3075 222.8903 247.8636 23.7105 -1.5851 221.4106 222.9957 247.8378 24.4873 -1.5849 221.4855 223.0704 247.8834 25.3050 -1.5871 221.5592 223.1464 247.8937 26.0715 -1.5876 221.6612 223.2488 247.8869 26.8995 -1.5841 221.7890 223.3731 247.8674 27.7275 -1.5821 221.9281 223.5103 247.8952 28.4940 -1.5813 222.0407 223.6221 247.9177 29.3425 -1.5851 222.1464 223.7315 247.9535 30.0885 -1.5827 222.2539 223.8365 247.9819 30.9370 -1.5776 222.3293 223.9069 248.0786 31.7038 -1.5749 222.3934 223.9683 248.1325 32.5323 -1.5765 222.4823 224.0587 248.1737 33.3293 -1.5776 222.5292 224.1068 248.2113 34.1265 -1.5756 222.6508 224.2264 248.2764 34.9445 -1.5792 222.7588 224.3380 248.2990 35.7215 -1.5786 222.8620 224.4406 248.3539 36.5700 -1.5771 222.9281 224.5052 248.4285 37.3365 -1.5756 223.0134 224.5890 248.4746 38.1645 -1.5717 223.0906 224.6622 248.5400 38.9618 -1.5702 223.1526 224.7228 248.6069 39.7590 -1.5688 223.3052 224.8741 248.6659 40.5768 -1.5675 223.4087 224.9762 248.7256 41.3535 -1.5676 223.4893 225.0569 248.8180 42.2023 -1.5626 223.5415 225.1041 248.9134 42.9688 -1.5573 223.6502 225.2075 249.0052 43.7975 -1.5577 223.7802 225.3379 249.1131 44.5948 -1.5585 223.8776 225.4361 249.2430 45.3920 -1.5624 223.9846 225.5469 249.3607 46.2098 -1.5623 224.0800 225.6423 249.4809 46.9865 -1.5633 224.1959 225.7593 249.5768 47.8350 -1.5640 224.2867 225.8507 249.6891 48.6018 -1.5668 224.3773 225.9442 249.7807 49.4305 -1.5666 224.4763 226.0430 249.9118 50.2278 -1.5640 224.6007 226.1647 250.0166 51.0248 -1.5656 224.6852 226.2508 250.1535 51.8425 -1.5637 224.7897 226.3534 250.3070 52.6195 -1.5567 224.8495 226.4063 250.4087 53.4680 -1.5623 224.9460 226.5083 250.5308 54.2345 -1.5671 225.0161 226.5832 250.6607 55.0625 -1.5695 225.0939 226.6634 250.7735 55.8598 -1.5690 225.1894 226.7584 250.8786 56.6570 -1.5686 225.2740 226.8426 251.0249 57.4753 -1.5613 225.3931 226.9544 251.1724 58.2618 -1.5600 225.4933 227.0534 251.3419 59.0695 -1.5601 225.6155 227.1756 251.4921 59.8675 -1.5604 225.7122 227.2726 251.5771 60.6955 -1.5588 225.8050 227.3638 251.7131 61.4620 -1.5595 225.8920 227.4515 251.8601 62.3105 -1.5635 225.9721 227.5356 252.0216 63.0873 -1.5630 226.0435 227.6065 252.1600 63.9050 -1.5634 226.1743 227.7377 252.3169 64.7023 -1.5658 226.2939 227.8597 252.4469 65.4998 -1.5616 226.3906 227.9523 252.5859 66.3283 -1.5593 226.4872 228.0466 252.7418 67.0950 -1.5608 226.5827 228.1435 252.8611 67.9435 -1.5630 226.6503 228.2133 253.0344 68.6895 -1.5649 226.6943 228.2592 253.1639 69.5380 -1.5659 226.8145 228.3804 253.2734 70.3045 -1.5698 226.9271 228.4969 253.4097 71.1325 -1.5674 227.0439 228.6113 253.5448 71.9195 -1.5668 227.1349 228.7017 253.6925 72.7065 -1.5718 227.2553 228.8270 253.8442 73.5348 -1.5721 227.3698 228.9419 253.9852 74.3010 -1.5694 227.4682 229.0376 254.1406 75.1505 -1.5704 227.5494 229.1198 254.2673 75.8855 -1.5728 227.6181 229.1910 254.4050 76.7450 -1.5667 227.7458 229.3126 254.5483 77.5013 -1.5698 227.8651 229.4349 254.7186 78.3395 -1.5713 228.0135 229.5848 254.8799 79.1060 -1.5733 228.0923 229.6656 255.0005 79.9340 -1.5749 228.1687 229.7436 255.1377 80.7210 -1.5786 228.2709 229.8495 255.2746 81.5183 -1.5825 228.3493 229.9318 255.3746 82.3463 -1.5816 228.4432 230.0248 255.5282 83.1025 -1.5835 228.5209 230.1044 255.6413 83.9613 -1.5848 228.6102 230.1950 255.7378 84.7280 -1.5864 228.6781 230.2645 255.8732 85.5463 -1.5853 228.8127 230.3980 256.0488 86.3538 -1.5906 228.9393 230.5299 256.1682 87.1410 -1.5899 229.0621 230.6520 256.3075 87.9383 -1.5921 229.1540 230.7461 256.4318 88.7355 -1.5956 229.2485 230.8442 256.5592 89.5635 -1.5957 229.3530 230.9487 256.6992 90.3198 -1.5992 229.4159 231.0152 256.8079 91.1785 -1.6004 229.5229 231.1233 256.9675 91.9450 -1.6001 229.6351 231.2351 257.1092 92.7730 -1.6012 229.7270 231.3282 257.2128 93.5600 -1.6028 229.8122 231.4150 257.3138 94.3675 -1.6052 229.8871 231.4923 257.3904 95.1855 -1.6091 229.9911 231.6003 257.5114 95.9518 -1.6130 230.0728 231.6857 257.6391 96.8115 -1.6120 230.1732 231.7851 257.7612 97.5473 -1.6153 230.2614 231.8767 257.8629 98.4060 -1.6191 230.3807 231.9998 257.9767 99.1623 -1.6182 230.4760 232.0942 258.0652 100.0005 -1.6179 230.5866 232.2045 258.1824 100.7875 -1.6202 230.6963 232.3164 258.2971 101.5848 -1.6201 230.7766 232.3967 258.3925 102.4128 -1.6205 230.8686 232.4891 258.5260 103.1793 -1.6235 230.9675 232.5910 258.6711 104.0380 -1.6266 231.1003 232.7268 258.8029 104.7943 -1.6279 231.1860 232.8138 258.9066 105.6325 -1.6287 231.2663 232.8951 258.9976 106.4203 -1.6353 231.3787 233.0139 259.1103 107.2178 -1.6376 231.4845 233.1221 259.2147 108.0458 -1.6424 231.5892 233.2316 259.3239 108.8123 -1.6408 231.6672 233.3080 259.4052 109.6710 -1.6435 231.7819 233.4254 259.5087 110.3965 -1.6468 231.8848 233.5316 259.5791 111.2655 -1.6493 232.0210 233.6703 259.6892 112.0218 -1.6498 232.0899 233.7396 259.7983 112.8498 -1.6541 232.1735 233.8276 259.8964 113.6470 -1.6512 232.2589 233.9101 260.0138 114.4448 -1.6511 232.3635 234.0146 260.1361 115.2733 -1.6478 232.4699 234.1177 260.2072 116.0295 -1.6429 232.5954 234.2384 260.2696 116.8985 -1.6453 232.7359 234.3812 260.3627 117.6548 -1.6494 232.8281 234.4775 260.4409 118.4828 -1.6475 232.9362 234.5837 260.5207 119.2800 -1.6523 233.0000 234.6523 260.6278 120.0875 -1.6559 233.0569 234.7128 260.7333 120.9053 -1.6569 233.1617 234.8186 260.8070 121.6718 -1.6552 233.2525 234.9077 260.8812 122.5315 -1.6536 233.4052 235.0588 260.9919 123.2980 -1.6550 233.5004 235.1554 261.1102 124.1260 -1.6588 233.6126 235.2714 261.2151 124.9130 -1.6615 233.7115 235.3730 261.2986 125.7205 -1.6680 233.7964 235.4644 261.3800 126.5383 -1.6699 233.8936 235.5634 261.4652 127.3150 -1.6708 233.9890 235.6598 261.5346 128.1328 -1.6716 234.0973 235.7688 261.6613 128.9095 -1.6688 234.2001 235.8688 261.7766 129.7580 -1.6674 234.3121 235.9795 261.8364 130.5248 -1.6698 234.4120 236.0819 261.9113 131.3535 -1.6688 234.4809 236.1497 262.0131 132.1405 -1.6666 234.5860 236.2525 262.1096 132.9275 -1.6687 234.7256 236.3943 262.1860 133.7555 -1.6671 234.8200 236.4872 262.2782 134.5220 -1.6698 234.9157 236.5856 262.3680 135.3705 -1.6671 234.9696 236.6367 262.4688 136.1370 -1.6679 235.0647 236.7327 262.5520 136.9650 -1.6716 235.1518 236.8234 262.6422 137.7520 -1.6708 235.2502 236.9209 262.7465 138.5493 -1.6689 235.3554 237.0243 262.8239 139.3678 -1.6653 235.4759 237.1412 262.9111 140.1345 -1.6659 235.5368 237.2028 262.9615 140.9830 -1.6665 235.6459 237.3124 263.0611 141.7495 -1.6685 235.7186 237.3871 263.1717 142.5775 -1.6677 235.7990 237.4667 263.2498 143.3645 -1.6685 235.9018 237.5703 263.3094 144.1618 -1.6737 236.0191 237.6928 263.3889 144.9898 -1.6715 236.1309 237.8024 263.4891 145.7460 -1.6733 236.2400 237.9134 263.5831 146.6048 -1.6779 236.3597 238.0376 263.6942 147.3713 -1.6781 236.4911 238.1692 263.7998 148.1890 -1.6856 236.6179 238.3035 263.8783 148.9863 -1.6890 236.6953 238.3843 263.9504 149.7835 -1.6866 236.8057 238.4923 264.0314 150.6123 -1.6874 236.9134 238.6008 264.0923 151.3790 -1.6880 236.9996 238.6876 264.1810 152.2275 -1.6893 237.0851 238.7743 264.2955 153.0043 -1.6920 237.1809 238.8729 264.3942 153.8220 -1.6921 237.2544 238.9465 264.4993 154.6193 -1.6911 237.3492 239.0403 264.5824 155.4165 -1.6899 237.4689 239.1588 264.6974 156.2343 -1.6944 237.5470 239.2414 264.8204 157.0008 -1.6963 237.6640 239.3603 264.8889 157.8595 -1.6981 237.8018 239.4999 265.0052 158.6260 -1.7042 237.8886 239.5928 265.1190 159.4438 -1.7013 238.0052 239.7065 265.1884 160.2415 -1.7037 238.1374 239.8411 265.2440 161.0393 -1.7026 238.2347 239.9373 265.3224 161.8673 -1.7033 238.3573 240.0606 265.4322 162.6235 -1.7030 238.4484 240.1514 265.5604 163.4925 -1.7072 238.5593 240.2665 265.6868 164.2488 -1.7077 238.6481 240.3558 265.7931 165.0768 -1.7150 238.7648 240.4797 265.8969 165.8433 -1.7147 238.8268 240.5414 266.0135 166.6713 -1.7131 238.8832 240.5963 266.1343 167.4685 -1.7105 238.9811 240.6916 266.2539 168.2555 -1.7151 239.0997 240.8147 266.3415 169.0938 -1.7119 239.1838 240.8957 266.4542 169.8500 -1.7067 239.2713 240.9780 266.5717 170.7088 -1.7020 239.3845 241.0865 266.6904 171.4753 -1.7021 239.5156 241.2177 266.7726 172.3035 -1.7031 239.6359 241.3390 266.8367 173.1015 -1.7030 239.7576 241.4606 266.9070 173.9090 -1.7068 239.8531 241.5599 266.9954 174.7268 -1.7124 239.9522 241.6647 267.1069 175.5035 -1.7096 240.0545 241.7640 267.2322 176.3213 -1.7102 240.1550 241.8652 267.3617 177.0878 -1.7126 240.2435 241.9561 267.4535 177.9465 -1.7099 240.3316 242.0415 267.5609 178.7130 -1.7090 240.4123 242.1212 267.6757 179.5410 -1.7079 240.5279 242.2358 267.8210 180.3280 -1.7069 240.6400 242.3470 267.9230 181.1355 -1.7084 240.7451 242.4535 268.0264 181.9435 -1.7124 240.8315 242.5438 268.1399 182.7413 -1.7104 240.9246 242.6350 268.2532 183.5693 -1.7112 241.0430 242.7542 268.3671 184.3255 -1.7120 241.1533 242.8653 268.4437 185.1945 -1.7127 241.2693 242.9820 268.5603 185.9508 -1.7137 241.3526 243.0663 268.6555 186.7788 -1.7153 241.4387 243.1540 268.7594 187.5760 -1.7163 241.5604 243.2767 268.8449 188.3733 -1.7192 241.6765 243.3956 268.9197 189.1705 -1.7197 241.7980 243.5177 268.9808 189.9585 -1.7202 241.9082 243.6283 269.0747 190.7968 -1.7223 242.0325 243.7548 269.2029 191.5530 -1.7229 242.1043 243.8272 269.3036 192.4118 -1.7221 242.2052 243.9273 269.4117 193.1783 -1.7269 242.2884 244.0153 269.5406 194.0165 -1.7282 242.3879 244.1161 269.6399 194.8035 -1.7332 242.4674 244.2006 269.7359 195.6008 -1.7341 242.5431 244.2772 269.8354 196.4288 -1.7311 242.6487 244.3798 269.9557 197.1850 -1.7279 242.7679 244.4958 270.0712 198.0035 -1.7271 242.9003 244.6274 270.1762 198.7805 -1.7277 242.9817 244.7093 270.2391 199.6290 -1.7308 243.0906 244.8214 270.3376 200.3853 -1.7328 243.2173 244.9501 270.4037 201.2133 -1.7308 243.3628 245.0936 270.4989 202.0003 -1.7321 243.4332 245.1653 270.5920 202.7975 -1.7358 243.5019 245.2377 270.6975 203.6263 -1.7348 243.6085 245.3433 270.8115 204.3828 -1.7325 243.6661 245.3986 270.9245 205.2415 -1.7384 243.7629 245.5013 271.0402 206.0080 -1.7383 243.8960 245.6343 271.1527 206.8258 -1.7386 243.9975 245.7360 271.2686 207.6230 -1.7353 244.0781 245.8134 271.3790 208.4100 -1.7370 244.1881 245.9250 271.5091 209.2380 -1.7353 244.2926 246.0279 271.6078 210.0045 -1.7384 244.3425 246.0809 271.6916 210.8325 -1.7401 244.4600 246.2000 271.8101 211.5990 -1.7463 244.5381 246.2844 271.9205 212.4475 -1.7443 244.6548 246.3990 272.0061 213.2140 -1.7469 244.7464 246.4933 272.1081 214.0420 -1.7453 244.8745 246.6197 272.2030 214.8295 -1.7466 245.0111 246.7577 272.2990 215.6273 -1.7450 245.1618 246.9067 272.4109 216.4553 -1.7477 245.2581 247.0058 272.5216 217.2115 -1.7491 245.3305 247.0796 272.6104 218.0805 -1.7528 245.4430 247.1958 272.7150 218.8368 -1.7542 245.5372 247.2914 272.7831 219.6648 -1.7590 245.6176 247.3766 272.8770 220.4620 -1.7609 245.7480 247.5089 272.9740 221.2593 -1.7610 245.8836 247.6447 273.0676 222.0570 -1.7600 246.0019 247.7620 273.1449 222.8548 -1.7588 246.1390 247.8978 273.2623 223.6828 -1.7584 246.2568 248.0152 273.3658 224.4493 -1.7633 246.3300 248.0933 273.4470 225.3080 -1.7676 246.4530 248.2207 273.5154 226.0643 -1.7667 246.5406 248.3073 273.5954 226.9025 -1.7624 246.6629 248.4252 273.7114 227.6895 -1.7639 246.7447 248.5086 273.8233 228.4868 -1.7661 246.8632 248.6292 273.9128 229.3153 -1.7683 246.9669 248.7352 274.0111 230.0823 -1.7696 247.0372 248.8069 274.1069 230.9410 -1.7699 247.1622 248.9321 274.2257 231.6973 -1.7719 247.2682 249.0401 274.3286 232.5355 -1.7728 247.3719 249.1447 274.4498 233.3225 -1.7717 247.4895 249.2612 274.5770 234.1198 -1.7668 247.5967 249.3635 274.7075 234.9478 -1.7672 247.6739 249.4411 274.8127 235.7143 -1.7723 247.7559 249.5281 274.9281 236.5735 -1.7734 247.8689 249.6423 275.0458 237.3303 -1.7739 247.9497 249.7237 275.1434 238.1685 -1.7730 248.0615 249.8345 275.2532 238.9555 -1.7741 248.1590 249.9331 275.3678 239.7528 -1.7730 248.2502 250.0231 275.4788 240.5808 -1.7728 248.3580 250.1308 275.6122 241.3473 -1.7729 248.4726 250.2455 275.7292 242.2060 -1.7705 248.5809 250.3514 275.8634 242.9623 -1.7727 248.6531 250.4259 275.9712 243.8010 -1.7724 248.7327 250.5050 276.0889 244.5885 -1.7742 248.8336 250.6078 276.1842 245.3858 -1.7768 248.9425 250.7193 276.2573 246.2138 -1.7810 249.0547 250.8357 276.3583 246.9803 -1.7850 249.1633 250.9483 276.5055 247.8390 -1.7849 249.3075 251.0924 276.6507 248.5953 -1.7918 249.3998 251.1916 276.7782 249.4335 -1.7909 249.5167 251.3077 276.8891 250.2205 -1.7869 249.6170 251.4039 276.9641 251.0280 -1.7907 249.7624 251.5530 277.0232 251.8458 -1.7931 249.8516 251.6446 277.1069 252.6123 -1.7969 249.9336 251.7305 277.2411 253.4710 -1.8019 250.0300 251.8319 277.3723 254.2280 -1.8057 250.1252 251.9309 277.4858 255.0665 -1.8028 250.2496 252.0524 277.6222 255.8535 -1.8027 250.3682 252.1709 277.7491 256.6508 -1.7993 250.5275 252.3268 277.8575 257.4788 -1.7982 250.5960 252.3942 277.9629 258.2453 -1.7964 250.6749 252.4713 278.0813 259.1040 -1.7984 250.7792 252.5776 278.1895 259.8705 -1.7991 250.8746 252.6736 278.2985 260.6985 -1.8014 250.9633 252.7646 278.3914 261.4855 -1.8007 251.0697 252.8705 278.4970 262.2725 -1.8029 251.1502 252.9532 278.6137 263.0703 -1.8060 251.2366 253.0425 278.7369 263.8578 -1.8062 251.3589 253.1652 278.8653 264.6858 -1.8078 251.4731 253.2808 278.9968 265.4420 -1.8063 251.5702 253.3765 279.0701 266.3008 -1.8076 251.6685 253.4761 279.1821 267.0673 -1.8096 251.7874 253.5969 279.2876 267.8850 -1.8120 251.8910 253.7030 279.4124 268.6823 -1.8122 251.9959 253.8080 279.5464 269.4795 -1.8096 252.0869 253.8964 279.6720 270.2973 -1.8108 252.1772 253.9881 279.7890 271.0638 -1.8125 252.2570 254.0695 279.9000 271.9235 -1.8148 252.4109 254.2257 280.0464 272.6490 -1.8125 252.5083 254.3208 280.1508 273.4975 -1.8133 252.5921 254.4055 280.2759 274.2743 -1.8146 252.7321 254.5467 280.3513 275.0920 -1.8187 252.8476 254.6663 280.4740 275.8893 -1.8250 252.9333 254.7583 280.6118 276.6865 -1.8267 253.0061 254.8329 280.7277 277.5145 -1.8303 253.0993 254.9296 280.8569 278.2708 -1.8300 253.1601 254.9902 280.9680 279.1295 -1.8285 253.2792 255.1077 281.0785 279.8968 -1.8256 253.3709 255.1965 281.1943 280.7250 -1.8264 253.4925 255.3189 281.3114 281.5120 -1.8308 253.6151 255.4458 281.4005 282.3093 -1.8295 253.6971 255.5266 281.4862 283.1373 -1.8352 253.8088 255.6440 281.5918 283.8935 -1.8346 253.9209 255.7555 281.6937 284.7318 -1.8355 254.0479 255.8834 281.7839 285.4880 -1.8379 254.1772 256.0151 281.8756 286.3468 -1.8360 254.2789 256.1149 282.0162 287.1140 -1.8369 254.3804 256.2172 282.0914 287.9423 -1.8438 254.4987 256.3425 282.1934 288.7395 -1.8470 254.5668 256.4138 282.2788 289.5265 -1.8498 254.6690 256.5188 282.3982 290.3648 -1.8540 254.8302 256.6841 282.5020 291.1210 -1.8570 254.9509 256.8079 282.5842 291.9798 -1.8578 255.0912 256.9489 282.6671 292.7165 -1.8566 255.1701 257.0267 282.7592 293.5753 -1.8537 255.2667 257.1205 282.8578 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