DTA measure 1olom_fazis.dat Date: 20251112:944 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.45 s Mass = 1163.100 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1580 -4.7032 187.2516 191.9548 247.2926 1.9245 -4.6981 187.4219 192.1200 247.2133 2.7935 -4.6866 187.6552 192.3417 247.1448 3.5180 -4.6769 187.8813 192.5582 247.0881 4.3768 -4.6680 188.1669 192.8348 247.0434 5.1433 -4.6564 188.4236 193.0800 246.9802 5.9703 -4.6416 188.6794 193.3209 246.8803 6.7675 -4.6346 188.8721 193.5067 246.8019 7.5545 -4.6246 189.0936 193.7182 246.7305 8.3918 -4.6156 189.3297 193.9452 246.6568 9.1480 -4.6077 189.5599 194.1676 246.5755 10.0068 -4.5956 189.7957 194.3913 246.5140 10.7723 -4.5879 190.0168 194.6047 246.4552 11.6105 -4.5749 190.3015 194.8764 246.4013 12.3975 -4.5622 190.5127 195.0749 246.3555 13.1938 -4.5510 190.7906 195.3417 246.2640 14.0218 -4.5354 191.0701 195.6055 246.2033 14.7880 -4.5217 191.2778 195.7995 246.1555 15.6358 -4.5088 191.5558 196.0646 246.1121 16.4023 -4.4992 191.7917 196.2909 246.0910 17.2200 -4.4858 192.0186 196.5044 246.0476 18.0163 -4.4707 192.2354 196.7061 246.0174 18.8135 -4.4594 192.4670 196.9264 245.9743 19.6313 -4.4482 192.6912 197.1394 245.9374 20.3970 -4.4386 192.9309 197.3695 245.9315 21.2555 -4.4226 193.1591 197.5817 245.9192 22.0118 -4.4118 193.3800 197.7918 245.8991 22.8393 -4.3972 193.6404 198.0376 245.9002 23.6360 -4.3799 193.8722 198.2522 245.8914 24.4333 -4.3646 194.0981 198.4628 245.8838 25.2608 -4.3493 194.3282 198.6774 245.8870 26.0165 -4.3366 194.5535 198.8901 245.9087 26.8855 -4.3238 194.8148 199.1386 245.9210 27.6408 -4.3085 195.0308 199.3393 245.9595 28.4688 -4.2939 195.2360 199.5299 246.0073 29.2353 -4.2808 195.3997 199.6805 246.0295 30.0623 -4.2651 195.6132 199.8783 246.0711 30.8595 -4.2508 195.8264 200.0772 246.1500 31.6463 -4.2385 196.0518 200.2903 246.1905 32.4838 -4.2246 196.3186 200.5432 246.2375 33.2400 -4.2120 196.5601 200.7721 246.3050 34.0988 -4.1942 196.7683 200.9625 246.3933 34.8643 -4.1801 196.9936 201.1738 246.4486 35.7025 -4.1658 197.1900 201.3558 246.5365 36.4893 -4.1563 197.3783 201.5345 246.6731 37.2858 -4.1456 197.6000 201.7457 246.7767 38.1138 -4.1354 197.8240 201.9594 246.8941 38.8905 -4.1230 198.0307 202.1537 246.9740 39.7380 -4.1107 198.2868 202.3975 247.0929 40.5045 -4.0982 198.4757 202.5740 247.2135 41.3325 -4.0871 198.6887 202.7758 247.3536 42.1288 -4.0802 198.9041 202.9844 247.4698 42.9260 -4.0682 199.1316 203.1998 247.6065 43.7540 -4.0527 199.3467 203.3994 247.7624 44.5195 -4.0385 199.5146 203.5531 247.9296 45.3783 -4.0245 199.7173 203.7418 248.1095 46.1445 -4.0188 199.8889 203.9077 248.2809 46.9615 -4.0062 200.1044 204.1106 248.4187 47.7588 -3.9940 200.3221 204.3161 248.5842 48.5560 -3.9827 200.5331 204.5158 248.7596 49.3728 -3.9750 200.7424 204.7173 248.9383 50.1393 -3.9590 200.9572 204.9161 249.1001 50.9978 -3.9473 201.1775 205.1248 249.2874 51.7533 -3.9338 201.3333 205.2671 249.4510 52.5813 -3.9185 201.5355 205.4540 249.6413 53.3785 -3.9073 201.7624 205.6697 249.7993 54.1645 -3.8993 201.9351 205.8344 249.9663 54.9720 -3.8870 202.1664 206.0534 250.1694 55.7590 -3.8766 202.3551 206.2317 250.3825 56.5860 -3.8689 202.5918 206.4607 250.5384 57.3525 -3.8559 202.7978 206.6537 250.7078 58.2110 -3.8433 203.0206 206.8640 250.8940 58.9768 -3.8345 203.2004 207.0349 251.0764 59.7945 -3.8187 203.4317 207.2504 251.2601 60.6018 -3.8076 203.6503 207.4579 251.4499 61.3880 -3.7978 203.8454 207.6432 251.6380 62.2160 -3.7897 204.0595 207.8491 251.8267 62.9825 -3.7818 204.2531 208.0349 252.0192 63.8403 -3.7716 204.4662 208.2378 252.2275 64.6068 -3.7652 204.6425 208.4078 252.4011 65.4348 -3.7589 204.8374 208.5963 252.5911 66.2313 -3.7513 205.0672 208.8185 252.7896 67.0283 -3.7393 205.2919 209.0312 252.9714 67.8563 -3.7310 205.4508 209.1818 253.1602 68.6120 -3.7219 205.6052 209.3271 253.3182 69.4805 -3.7091 205.8278 209.5368 253.5627 70.2470 -3.7011 206.0103 209.7114 253.7532 71.0745 -3.6899 206.2283 209.9182 253.9552 71.8610 -3.6811 206.4190 210.1001 254.1096 72.6685 -3.6743 206.6111 210.2854 254.2729 73.4863 -3.6646 206.8456 210.5103 254.4270 74.2518 -3.6589 207.0221 210.6810 254.5971 75.0798 -3.6559 207.2331 210.8890 254.7793 75.8458 -3.6518 207.4593 211.1111 254.9600 76.7040 -3.6424 207.6486 211.2910 255.1611 77.4705 -3.6344 207.8235 211.4579 255.3530 78.2985 -3.6212 207.9893 211.6105 255.5348 79.0845 -3.6152 208.1733 211.7885 255.6887 79.8715 -3.6098 208.3617 211.9715 255.8603 80.6995 -3.6005 208.5740 212.1745 256.0036 81.4650 -3.5965 208.7830 212.3796 256.1975 82.3135 -3.5909 209.0007 212.5917 256.4021 83.0903 -3.5844 209.1554 212.7398 256.5511 83.9073 -3.5756 209.3142 212.8899 256.7161 84.6633 -3.5685 209.4801 213.0486 256.8588 85.5015 -3.5643 209.6855 213.2498 257.0301 86.2878 -3.5585 209.8540 213.4125 257.2066 87.0848 -3.5499 210.0257 213.5756 257.3542 87.9128 -3.5413 210.2118 213.7531 257.5245 88.6688 -3.5352 210.3911 213.9263 257.7195 89.5268 -3.5265 210.5876 214.1142 257.8467 90.2933 -3.5234 210.7988 214.3221 257.9919 91.1210 -3.5164 210.9961 214.5125 258.1527 91.8868 -3.5091 211.1638 214.6729 258.2760 92.7045 -3.5034 211.3596 214.8630 258.3997 93.5118 -3.5001 211.5732 215.0733 258.5366 94.2980 -3.4946 211.7623 215.2570 258.6292 95.1260 -3.4913 211.9538 215.4450 258.7648 95.8923 -3.4849 212.1489 215.6338 258.8685 96.7503 -3.4754 212.3499 215.8253 259.0196 97.5168 -3.4702 212.5094 215.9797 259.1416 98.3345 -3.4664 212.6967 216.1631 259.3012 99.1418 -3.4653 212.8903 216.3556 259.4421 99.9383 -3.4568 213.0619 216.5187 259.5649 100.7663 -3.4497 213.2306 216.6804 259.6860 101.5220 -3.4449 213.3964 216.8414 259.8385 102.3598 -3.4350 213.5967 217.0316 260.0062 103.1160 -3.4337 213.7673 217.2010 260.1277 103.9848 -3.4325 213.9460 217.3784 260.2485 104.7403 -3.4288 214.1118 217.5407 260.3697 105.5785 -3.4234 214.3229 217.7463 260.5258 106.3650 -3.4173 214.5134 217.9307 260.6423 107.1720 -3.4054 214.7063 218.1116 260.7987 107.9898 -3.4001 214.9054 218.3055 260.9169 108.7660 -3.3957 215.0964 218.4921 261.0325 109.5833 -3.3892 215.3002 218.6894 261.1613 110.3498 -3.3809 215.4426 218.8236 261.2888 111.2083 -3.3769 215.6330 219.0100 261.3879 111.9638 -3.3713 215.8061 219.1774 261.4981 112.7815 -3.3652 215.9514 219.3167 261.5931 113.5785 -3.3596 216.1353 219.4949 261.6760 114.3750 -3.3551 216.3310 219.6861 261.7819 115.1928 -3.3480 216.5410 219.8890 261.8801 115.9690 -3.3450 216.7304 220.0754 261.9942 116.8170 -3.3370 216.8926 220.2297 262.1336 117.5733 -3.3301 217.0524 220.3825 262.2574 118.4113 -3.3225 217.2151 220.5376 262.3854 119.1975 -3.3179 217.3864 220.7043 262.4315 119.9948 -3.3143 217.5699 220.8842 262.5469 120.8225 -3.3098 217.7629 221.0727 262.6262 121.5883 -3.3023 217.9347 221.2370 262.7509 122.4470 -3.2924 218.1682 221.4606 262.9011 123.2033 -3.2905 218.3435 221.6340 263.0285 124.0405 -3.2812 218.5325 221.8137 263.1419 124.8275 -3.2788 218.7339 222.0128 263.2595 125.6245 -3.2762 218.9260 222.2022 263.4039 126.4518 -3.2697 219.0898 222.3595 263.5598 127.2183 -3.2652 219.2456 222.5107 263.7303 128.0770 -3.2652 219.3514 222.6166 263.8360 128.8325 -3.2637 219.5194 222.7831 263.9239 129.6705 -3.2595 219.7397 222.9992 264.0529 130.4575 -3.2546 219.9293 223.1839 264.1816 131.2543 -3.2493 220.0552 223.3045 264.2761 132.0818 -3.2410 220.2559 223.4968 264.3994 132.8585 -3.2370 220.4717 223.7087 264.5212 133.6755 -3.2324 220.6583 223.8907 264.6388 134.4418 -3.2356 220.8089 224.0444 264.7398 135.3005 -3.2315 221.0127 224.2442 264.8402 136.0765 -3.2258 221.1956 224.4215 264.9481 136.8940 -3.2229 221.3920 224.6150 265.0130 137.6913 -3.2121 221.5528 224.7650 265.1403 138.4878 -3.2009 221.7506 224.9515 265.2311 139.3155 -3.1971 221.9622 225.1592 265.3573 140.0820 -3.1925 222.1333 225.3258 265.4520 140.9298 -3.1849 222.3458 225.5307 265.5559 141.7063 -3.1849 222.5430 225.7279 265.6665 142.5343 -3.1784 222.7082 225.8866 265.8142 143.3203 -3.1758 222.8541 226.0300 265.9322 144.1175 -3.1719 223.0131 226.1850 266.0594 144.9455 -3.1676 223.1831 226.3507 266.1781 145.7008 -3.1656 223.3387 226.5043 266.2938 146.5595 -3.1622 223.4984 226.6605 266.3961 147.3260 -3.1588 223.6881 226.8468 266.4723 148.1430 -3.1520 223.8803 227.0323 266.6019 148.9400 -3.1457 224.0481 227.1938 266.7099 149.7373 -3.1407 224.2112 227.3519 266.7925 150.5645 -3.1347 224.3657 227.5004 266.9259 151.3205 -3.1307 224.5228 227.6536 267.0566 152.1895 -3.1298 224.7218 227.8516 267.2033 152.9453 -3.1302 224.8640 227.9942 267.3405 153.7728 -3.1259 225.0313 228.1572 267.4716 154.5393 -3.1209 225.1759 228.2967 267.5930 155.3668 -3.1174 225.3493 228.4667 267.6967 156.1635 -3.1093 225.5009 228.6102 267.8454 156.9505 -3.1036 225.6552 228.7588 267.9735 157.7880 -3.1013 225.8192 228.9205 268.0735 158.5543 -3.0985 225.9751 229.0736 268.1854 159.4130 -3.0976 226.1609 229.2585 268.3592 160.1685 -3.0969 226.3350 229.4318 268.4981 161.0065 -3.0966 226.5308 229.6274 268.6284 161.7935 -3.0936 226.7219 229.8155 268.7866 162.6005 -3.0901 226.9137 230.0038 268.9217 163.4178 -3.0886 227.1060 230.1946 269.0719 164.1945 -3.0830 227.2796 230.3627 269.1930 165.0423 -3.0776 227.4561 230.5338 269.2861 165.8085 -3.0706 227.6069 230.6776 269.4000 166.6365 -3.0622 227.7598 230.8219 269.5226 167.4330 -3.0522 227.9298 230.9820 269.6365 168.2300 -3.0465 228.0854 231.1319 269.7727 169.0478 -3.0415 228.2431 231.2846 269.9032 169.8240 -3.0401 228.3705 231.4106 270.0364 170.6823 -3.0349 228.5589 231.5937 270.1899 171.4488 -3.0311 228.7399 231.7710 270.3443 172.2658 -3.0287 228.9190 231.9476 270.4888 173.0730 -3.0268 229.0912 232.1180 270.6500 173.8600 -3.0259 229.2727 232.2986 270.7842 174.6978 -3.0272 229.4568 232.4840 270.8944 175.4535 -3.0243 229.5995 232.6239 271.0228 176.3123 -3.0235 229.7684 232.7919 271.1479 177.0678 -3.0237 229.9128 232.9365 271.2531 177.8955 -3.0212 230.0868 233.1080 271.4033 178.6620 -3.0167 230.2458 233.2625 271.5565 179.4788 -3.0179 230.4434 233.4614 271.7036 180.2760 -3.0168 230.6044 233.6212 271.8657 181.0733 -3.0139 230.7547 233.7686 272.0016 181.8900 -3.0133 230.9256 233.9389 272.1493 182.6565 -3.0104 231.1029 234.1133 272.3037 183.5153 -3.0138 231.2751 234.2889 272.4628 184.2810 -3.0121 231.4380 234.4501 272.6081 185.0985 -3.0125 231.6244 234.6369 272.7721 185.8753 -3.0086 231.7587 234.7673 272.9205 186.6925 -3.0057 231.9237 234.9294 273.0414 187.4893 -3.0078 232.0733 235.0811 273.1454 188.2865 -3.0039 232.2490 235.2529 273.2544 189.1143 -2.9973 232.4206 235.4179 273.4070 189.8800 -2.9926 232.5732 235.5658 273.5309 190.7285 -2.9883 232.7362 235.7245 273.6838 191.5048 -2.9855 232.8821 235.8677 273.7919 192.3323 -2.9846 233.0666 236.0511 273.9333 193.0988 -2.9823 233.2051 236.1875 274.0479 193.9160 -2.9789 233.3345 236.3134 274.1815 194.7230 -2.9749 233.4957 236.4707 274.3284 195.5100 -2.9722 233.7175 236.6897 274.4684 196.3378 -2.9682 233.9070 236.8752 274.6009 197.1035 -2.9683 234.0570 237.0253 274.7496 197.9623 -2.9657 234.2497 237.2154 274.8789 198.7283 -2.9593 234.3892 237.3485 275.0256 199.5558 -2.9538 234.5387 237.4925 275.1614 200.3530 -2.9496 234.6921 237.6417 275.2925 201.1498 -2.9430 234.8649 237.8079 275.4156 201.9773 -2.9369 235.0168 237.9538 275.5641 202.7335 -2.9360 235.1525 238.0886 275.6706 203.5713 -2.9331 235.3518 238.2850 275.8009 204.3373 -2.9353 235.5140 238.4493 275.9142 205.1960 -2.9288 235.6889 238.6177 276.0656 205.9513 -2.9279 235.8486 238.7765 276.1967 206.7895 -2.9254 235.9930 238.9184 276.3275 207.5765 -2.9210 236.1714 239.0923 276.4655 208.3628 -2.9170 236.3252 239.2421 276.6110 209.1905 -2.9182 236.5257 239.4438 276.7377 209.9570 -2.9163 236.6788 239.5951 276.8617 210.8053 -2.9091 236.8423 239.7515 277.0564 211.5710 -2.9057 236.9609 239.8666 277.1557 212.3990 -2.9073 237.1270 240.0343 277.2720 213.1860 -2.9105 237.2871 240.1977 277.4100 213.9823 -2.9125 237.4340 240.3466 277.5407 214.8103 -2.9101 237.5858 240.4959 277.6774 215.5665 -2.9110 237.7307 240.6417 277.8088 216.4345 -2.9154 237.9369 240.8523 278.0136 217.1600 -2.9193 238.1050 241.0243 278.1376 218.0185 -2.9193 238.2640 241.1833 278.2399 218.7843 -2.9235 238.4086 241.3321 278.3245 219.6123 -2.9211 238.5726 241.4937 278.4316 220.4095 -2.9195 238.7574 241.6769 278.5418 221.1958 -2.9145 238.9215 241.8360 278.6749 222.0338 -2.9158 239.0848 242.0006 278.8030 222.7900 -2.9146 239.2036 242.1182 278.9531 223.6483 -2.9103 239.3730 242.2833 279.1284 224.4143 -2.9089 239.4551 242.3640 279.2328 225.2423 -2.9077 239.6354 242.5430 279.3356 226.0390 -2.9051 239.8062 242.7113 279.4822 226.8255 -2.9033 239.9521 242.8553 279.6096 227.6638 -2.9041 240.1042 243.0083 279.7430 228.4195 -2.9041 240.2405 243.1446 279.8769 229.2778 -2.8987 240.4116 243.3103 280.0554 230.0443 -2.8950 240.5774 243.4724 280.1771 230.8723 -2.8921 240.7455 243.6376 280.2977 231.6685 -2.8878 240.9069 243.7947 280.4068 232.4555 -2.8851 241.0508 243.9359 280.5117 233.2938 -2.8823 241.2224 244.1047 280.6305 234.0490 -2.8786 241.3588 244.2374 280.7653 234.9078 -2.8769 241.5135 244.3904 280.9011 235.6743 -2.8746 241.6788 244.5535 280.9925 236.5015 -2.8756 241.8399 244.7155 281.1227 237.2985 -2.8725 241.9854 244.8579 281.2476 238.0855 -2.8758 242.1246 245.0004 281.3674 238.9233 -2.8793 242.3065 245.1858 281.5024 239.6790 -2.8781 242.4600 245.3381 281.6294 240.5275 -2.8780 242.7052 245.5832 281.7671 241.3038 -2.8751 242.8136 245.6888 281.8873 242.1210 -2.8702 242.9175 245.7877 281.9961 242.9080 -2.8661 243.0628 245.9290 282.1251 243.7155 -2.8714 243.2077 246.0791 282.2564 244.5328 -2.8720 243.3687 246.2407 282.3843 245.2885 -2.8693 243.5088 246.3781 282.5044 246.1575 -2.8653 243.6812 246.5465 282.6046 246.9130 -2.8629 243.8092 246.6721 282.6992 247.7305 -2.8577 243.9436 246.8012 282.8503 248.5380 -2.8560 244.1373 246.9933 282.9958 249.3243 -2.8545 244.2857 247.1402 283.1492 250.1520 -2.8576 244.4124 247.2700 283.2704 250.9185 -2.8596 244.5509 247.4105 283.3898 251.7768 -2.8603 244.7463 247.6066 283.5448 252.5428 -2.8596 244.8842 247.7438 283.6611 253.3605 -2.8549 245.0639 247.9188 283.7735 254.1675 -2.8487 245.2261 248.0748 283.9145 254.9540 -2.8478 245.3854 248.2332 284.0509 255.7820 -2.8459 245.5891 248.4351 284.1914 256.5480 -2.8456 245.7479 248.5935 284.3097 257.4063 -2.8466 245.8916 248.7382 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