DTA measure 1olom_updown4.dat Date: 20251112:1045 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.83 s Mass = 1163.100 mg data_number = 1068 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4225 2.2742 214.4279 212.1537 196.9394 4.0221 2.2769 214.2168 211.9399 196.8941 5.6269 2.2713 214.0847 211.8134 196.8249 7.2163 2.2652 213.9646 211.6993 196.7562 8.8218 2.2602 213.8357 211.5754 196.7346 10.4370 2.2558 213.6930 211.4373 196.7193 12.0469 2.2559 213.5554 211.2995 196.6298 13.6516 2.2537 213.4003 211.1466 196.5466 15.2564 2.2482 213.2561 211.0079 196.4943 16.8663 2.2447 213.1394 210.8947 196.4947 18.4710 2.2388 212.9562 210.7175 196.5001 20.0663 2.2295 212.7702 210.5406 196.4637 21.6713 2.2202 212.6789 210.4588 196.4284 23.2965 2.2164 212.5357 210.3193 196.4044 24.9013 2.2132 212.3786 210.1653 196.4169 26.5214 2.2030 212.2279 210.0250 196.3965 28.1264 2.1984 212.0369 209.8385 196.3787 29.7370 2.1924 211.9328 209.7404 196.3661 31.3418 2.1850 211.7830 209.5979 196.3624 32.9465 2.1786 211.6658 209.4872 196.4194 34.5666 2.1667 211.5368 209.3700 196.4604 36.1510 2.1580 211.3680 209.2100 196.4173 37.7510 2.1502 211.2214 209.0711 196.5108 39.3613 2.1482 211.0406 208.8924 196.5421 40.9866 2.1520 210.8676 208.7156 196.6091 42.6221 2.1460 210.7660 208.6201 196.6647 44.2318 2.1369 210.6748 208.5379 196.7431 45.8316 2.1297 210.5249 208.3952 196.8233 47.4364 2.1196 210.3495 208.2300 196.8716 49.0463 2.1058 210.2593 208.1535 196.9775 50.6514 2.0952 210.1403 208.0451 197.0816 52.2619 2.0879 210.0345 207.9466 197.2164 53.8820 2.0845 209.8834 207.7989 197.3203 55.4919 2.0705 209.7653 207.6948 197.4312 57.0966 2.0567 209.6323 207.5756 197.5532 58.7015 2.0435 209.4975 207.4539 197.6767 60.2965 2.0319 209.3438 207.3119 197.8359 61.9170 2.0196 209.2183 207.1987 198.0197 63.5269 2.0107 209.0986 207.0880 198.1601 65.1163 1.9997 208.9304 206.9307 198.3064 66.7364 1.9866 208.8339 206.8473 198.4697 68.3363 1.9695 208.7154 206.7459 198.6597 69.9366 1.9493 208.5842 206.6349 198.8496 71.5363 1.9385 208.5200 206.5815 199.0300 73.1461 1.9236 208.3934 206.4698 199.2127 74.7355 1.9043 208.2578 206.3535 199.3369 76.3351 1.8879 208.1425 206.2546 199.5337 77.9450 1.8751 208.0348 206.1598 199.7150 79.5654 1.8658 207.9206 206.0548 199.9138 81.1760 1.8500 207.7929 205.9429 200.1045 82.7808 1.8301 207.6525 205.8224 200.3193 84.3906 1.8074 207.5937 205.7863 200.4832 85.9800 1.7902 207.5376 205.7473 200.6498 87.5899 1.7759 207.4334 205.6576 200.7750 89.2003 1.7563 207.3201 205.5638 200.9781 90.8055 1.7392 207.2074 205.4683 201.1836 92.4154 1.7208 207.0686 205.3478 201.4057 94.0201 1.7057 206.9455 205.2398 201.5488 95.6403 1.6869 206.7962 205.1094 201.7557 97.2406 1.6817 206.6934 205.0118 201.9865 98.8354 1.6728 206.6710 204.9981 202.2020 100.4401 1.6507 206.6504 204.9997 202.3856 102.0449 1.6327 206.5651 204.9324 202.5499 103.6548 1.6265 206.4357 204.8092 202.7331 105.2544 1.6207 206.3390 204.7183 202.9489 106.8438 1.6129 206.2353 204.6224 203.1448 108.4488 1.5987 206.1824 204.5837 203.3020 110.0541 1.5802 206.1028 204.5226 203.4948 111.6795 1.5579 206.0585 204.5006 203.6623 113.2843 1.5419 205.9884 204.4465 203.8658 114.8890 1.5344 205.9501 204.4156 204.0833 116.4994 1.5151 205.8619 204.3468 204.3333 118.1046 1.4897 205.8046 204.3148 204.5437 119.7145 1.4685 205.7351 204.2666 204.7345 121.3193 1.4467 205.6615 204.2149 204.9321 122.9138 1.4253 205.5724 204.1471 205.1110 124.5390 1.4034 205.5225 204.1192 205.3388 126.1489 1.3797 205.4794 204.0997 205.5050 127.7536 1.3589 205.4136 204.0546 205.6185 129.3590 1.3391 205.3245 203.9854 205.8116 130.9641 1.3276 205.2911 203.9635 206.0117 132.5689 1.3148 205.2500 203.9352 206.1799 134.1634 1.3025 205.1837 203.8812 206.3536 135.7835 1.2855 205.1430 203.8575 206.5555 137.3883 1.2729 205.1216 203.8488 206.7203 138.9885 1.2591 205.0841 203.8251 206.9011 140.5988 1.2395 205.0276 203.7881 207.0522 142.2035 1.2230 204.9622 203.7392 207.2223 143.8134 1.2069 204.9473 203.7404 207.4384 145.4181 1.1842 204.8790 203.6948 207.6310 147.0383 1.1658 204.8961 203.7303 207.8812 148.6328 1.1494 204.8792 203.7298 208.0501 150.2385 1.1281 204.8908 203.7627 208.1833 151.8484 1.1047 204.8086 203.7039 208.3518 153.4531 1.0927 204.7467 203.6540 208.5368 155.0786 1.0803 204.6513 203.5710 208.7543 156.7303 1.0579 204.6572 203.5993 208.9641 158.3196 1.0422 204.6511 203.6089 209.1525 159.9346 1.0200 204.5687 203.5487 209.3012 161.5394 1.0055 204.5225 203.5170 209.4508 163.1441 0.9909 204.5206 203.5297 209.6182 164.7489 0.9720 204.5115 203.5394 209.7982 166.3388 0.9578 204.5013 203.5434 209.9895 167.9594 0.9481 204.4741 203.5259 210.1626 169.5641 0.9253 204.4583 203.5330 210.3272 171.1689 0.9044 204.4955 203.5911 210.5086 172.7736 0.8865 204.4987 203.6122 210.6730 174.3636 0.8651 204.4677 203.6026 210.8660 175.9688 0.8458 204.4170 203.5712 211.0601 177.5786 0.8258 204.4396 203.6138 211.2672 179.1834 0.8072 204.4317 203.6246 211.4690 180.8086 0.7873 204.4029 203.6157 211.6181 182.4144 0.7648 204.3900 203.6252 211.8279 184.0089 0.7534 204.4090 203.6556 212.0245 185.6136 0.7386 204.4480 203.7094 212.2582 187.2184 0.7123 204.4270 203.7147 212.4206 188.8283 0.6925 204.3985 203.7060 212.6167 190.4338 0.6739 204.4282 203.7543 212.7849 192.0439 0.6579 204.4546 203.7967 212.9648 193.6640 0.6455 204.4398 203.7943 213.0897 195.2688 0.6349 204.4416 203.8067 213.2244 196.8690 0.6173 204.4497 203.8325 213.4174 198.4639 0.6002 204.4735 203.8733 213.5972 200.0686 0.5867 204.4973 203.9106 213.8021 201.6631 0.5719 204.5303 203.9584 213.9982 203.2679 0.5556 204.5540 203.9984 214.1559 204.8781 0.5305 204.5634 204.0329 214.3032 206.4938 0.5197 204.5424 204.0227 214.5334 208.0985 0.5067 204.5736 204.0669 214.7319 209.7084 0.4941 204.6529 204.1588 214.9321 211.2978 0.4787 204.6275 204.1487 215.1876 212.9081 0.4537 204.6596 204.2059 215.3988 214.5134 0.4365 204.6431 204.2066 215.6069 216.1181 0.4250 204.6983 204.2733 215.7641 217.7280 0.4134 204.7489 204.3355 215.9917 219.3481 0.3968 204.7856 204.3888 216.1971 220.9580 0.3789 204.8259 204.4470 216.4471 222.5628 0.3734 204.8632 204.4898 216.6116 224.1733 0.3663 204.9019 204.5356 216.7993 225.7784 0.3502 204.9311 204.5809 217.0342 227.3780 0.3375 204.9599 204.6224 217.2481 228.9828 0.3195 205.0100 204.6906 217.4168 230.5824 0.3024 205.0803 204.7779 217.6004 232.1871 0.2870 205.1016 204.8146 217.8273 233.7919 0.2741 205.1258 204.8517 218.0221 235.3925 0.2598 205.1482 204.8884 218.1894 236.9973 0.2406 205.1682 204.9276 218.3646 238.6071 0.2212 205.2168 204.9955 218.6019 240.2119 0.2043 205.2658 205.0615 218.8247 241.8218 0.1900 205.2607 205.0707 218.9987 243.4426 0.1772 205.3415 205.1643 219.2077 245.0476 0.1631 205.4191 205.2559 219.4195 246.6575 0.1505 205.4990 205.3484 219.6319 248.2674 0.1354 205.5910 205.4555 219.7962 249.8721 0.1226 205.6269 205.5044 219.9477 251.4769 0.1113 205.6909 205.5797 220.1450 253.0868 0.0966 205.7634 205.6669 220.3537 254.7069 0.0835 205.8179 205.7344 220.5112 256.3175 0.0748 205.8866 205.8118 220.6603 257.9276 0.0637 205.9764 205.9127 220.8539 259.5273 0.0486 206.0404 205.9917 221.0504 261.1166 0.0338 206.0961 206.0623 221.2254 262.7214 0.0205 206.1668 206.1462 221.4273 264.3215 0.0112 206.2389 206.2277 221.6594 265.9370 -0.0006 206.3057 206.3064 221.8305 267.5366 -0.0155 206.3919 206.4074 222.0055 269.1363 -0.0239 206.4739 206.4979 222.2200 270.7461 -0.0392 206.5592 206.5984 222.4379 272.3509 -0.0526 206.6430 206.6956 222.6580 273.9556 -0.0627 206.7110 206.7736 222.8387 275.5710 -0.0721 206.7939 206.8660 223.0266 277.1866 -0.0912 206.8352 206.9264 223.2071 278.7863 -0.1093 206.9112 207.0205 223.3756 280.3859 -0.1260 206.9763 207.1023 223.5671 281.9906 -0.1424 207.0609 207.2033 223.7676 283.6005 -0.1562 207.1244 207.2805 223.9830 285.2104 -0.1636 207.2140 207.3776 224.1872 286.8366 -0.1744 207.3518 207.5262 224.4321 288.4414 -0.1884 207.4525 207.6409 224.5927 290.0359 -0.2020 207.5084 207.7104 224.7666 291.6458 -0.2155 207.5951 207.8105 224.9832 293.2505 -0.2221 207.6875 207.9096 225.1572 294.8501 -0.2320 207.7395 207.9715 225.3698 296.4549 -0.2447 207.8412 208.0858 225.5614 298.0443 -0.2626 207.9475 208.2100 225.7641 299.6490 -0.2816 208.0451 208.3267 226.0077 301.2698 -0.2904 208.1214 208.4118 226.2208 302.8749 -0.3063 208.2329 208.5393 226.4381 304.4796 -0.3199 208.3313 208.6512 226.6237 306.0844 -0.3288 208.4700 208.7989 226.7990 307.6789 -0.3421 208.5514 208.8935 226.9415 309.2893 -0.3516 208.6291 208.9807 227.1149 310.9048 -0.3655 208.7199 209.0853 227.2402 312.6889 -0.3700 208.8395 209.2095 227.4887 314.3295 -0.3749 208.9688 209.3437 227.6555 316.0420 -0.3845 209.0781 209.4626 227.8617 318.9139 -0.4073 209.2677 209.6751 228.1881 321.8056 -0.4230 209.3939 209.8169 228.5509 323.5493 -0.4303 209.5044 209.9347 228.8039 325.5491 -0.4546 209.6507 210.1053 229.0241 327.6254 -0.4674 209.7719 210.2393 229.3197 329.4003 -0.4754 209.8541 210.3295 229.5385 331.1024 -0.4804 209.9976 210.4780 229.7549 332.7071 -0.4862 210.0964 210.5826 229.9842 334.3068 -0.4975 210.2088 210.7064 230.2043 336.0553 -0.5125 210.3765 210.8890 230.4159 337.8453 -0.5200 210.5410 211.0610 230.6713 339.4500 -0.5322 210.6786 211.2109 230.8803 341.0650 -0.5452 210.8287 211.3739 231.1038 342.6851 -0.5607 210.9467 211.5074 231.3616 344.2799 -0.5719 211.0591 211.6310 231.5870 345.8854 -0.5825 211.1344 211.7169 231.7955 347.4953 -0.5978 211.2547 211.8524 231.9862 349.1000 -0.6078 211.3970 212.0048 232.1792 350.7099 -0.6163 211.5197 212.1360 232.3800 352.3208 -0.6248 211.6237 212.2485 232.5593 353.9409 -0.6356 211.7714 212.4070 232.7608 355.6276 -0.6456 211.9080 212.5536 232.9868 357.3964 -0.6520 212.0513 212.7032 233.1901 358.9915 -0.6607 212.1872 212.8479 233.4204 360.5864 -0.6684 212.3237 212.9921 233.6065 362.1911 -0.6723 212.4269 213.0992 233.7903 363.8010 -0.6758 212.5326 213.2083 233.9792 365.4058 -0.6809 212.6205 213.3015 234.1817 367.0003 -0.6926 212.6804 213.3729 234.3781 368.6101 -0.7005 212.8474 213.5479 234.5760 370.2466 -0.7105 213.0341 213.7446 234.8136 371.9283 -0.7186 213.1763 213.8950 235.0023 373.6509 -0.7326 213.2892 214.0218 235.1524 375.2711 -0.7361 213.4294 214.1655 235.3353 376.8819 -0.7479 213.5264 214.2743 235.5420 378.4866 -0.7591 213.6765 214.4356 235.7606 380.0914 -0.7682 213.8224 214.5905 235.9334 381.7013 -0.7736 213.9408 214.7144 236.1257 383.3060 -0.7811 214.0485 214.8296 236.3082 384.9168 -0.7916 214.2173 215.0089 236.4985 386.5370 -0.8010 214.3453 215.1463 236.6965 388.1264 -0.8063 214.5057 215.3120 236.8756 389.7311 -0.8166 214.6188 215.4354 237.0762 391.3313 -0.8242 214.7543 215.5785 237.3492 392.9365 -0.8372 214.8965 215.7337 237.5100 394.5413 -0.8425 215.0071 215.8495 237.6602 396.1306 -0.8513 215.1601 216.0115 237.8700 397.7405 -0.8588 215.3003 216.1591 238.0807 399.3460 -0.8669 215.4426 216.3095 238.2991 400.9715 -0.8711 215.5876 216.4587 238.5225 402.5609 -0.8746 215.7331 216.6077 238.7726 404.1656 -0.8816 215.8917 216.7733 238.9720 405.7755 -0.8856 216.0512 216.9368 239.1847 407.3803 -0.8913 216.2157 217.1069 239.4028 408.9911 -0.8962 216.3681 217.2643 239.5644 410.6010 -0.9008 216.5191 217.4199 239.7711 412.2109 -0.9059 216.6492 217.5551 240.0093 413.8310 -0.9131 216.7990 217.7121 240.2589 415.4460 -0.9207 216.9394 217.8600 240.4583 417.0354 -0.9312 217.0681 217.9993 240.7357 418.6453 -0.9413 217.2477 218.1890 240.9471 420.2505 -0.9486 217.3939 218.3424 241.1291 421.8506 -0.9538 217.5269 218.4807 241.3093 423.4605 -0.9592 217.7262 218.6853 241.5026 425.0601 -0.9716 217.8738 218.8454 241.7301 426.6804 -0.9795 217.9979 218.9774 241.9398 428.2758 -0.9855 218.1127 219.0982 242.1539 429.8805 -0.9917 218.2660 219.2577 242.3665 431.4904 -0.9995 218.4498 219.4493 242.5832 433.0951 -1.0064 218.6117 219.6181 242.8347 434.7050 -1.0117 218.7747 219.7864 243.0353 436.3105 -1.0175 218.9431 219.9606 243.2204 437.9155 -1.0238 219.0536 220.0775 243.4033 439.5408 -1.0327 219.2194 220.2522 243.6036 441.1455 -1.0367 219.3753 220.4120 243.8137 442.7401 -1.0356 219.5502 220.5858 244.0162 444.3454 -1.0423 219.7164 220.7587 244.2396 445.9608 -1.0481 219.8595 220.9076 244.4437 447.5655 -1.0522 220.0198 221.0720 244.6244 449.1754 -1.0560 220.2013 221.2573 244.8208 450.7801 -1.0614 220.3526 221.4139 245.0279 452.4003 -1.0683 220.4876 221.5559 245.2126 454.0104 -1.0753 220.6796 221.7549 245.4111 455.6108 -1.0866 220.8582 221.9448 245.6176 457.2155 -1.0964 221.0535 222.1499 245.8216 458.8203 -1.1038 221.2139 222.3178 246.0031 460.4200 -1.1129 221.3556 222.4685 246.1984 462.0306 -1.1129 221.5474 222.6602 246.4014 463.6509 -1.1136 221.6974 222.8110 246.6385 465.2556 -1.1182 221.8463 222.9645 246.8122 466.8655 -1.1269 221.9801 223.1070 247.0204 468.4703 -1.1380 222.1488 223.2868 247.1912 470.0655 -1.1410 222.3096 223.4506 247.3648 471.6859 -1.1417 222.4704 223.6121 247.5762 473.2804 -1.1466 222.6344 223.7810 247.7760 474.8851 -1.1565 222.7923 223.9488 247.9550 476.5054 -1.1608 222.9375 224.0983 248.0932 478.1160 -1.1688 223.1165 224.2853 248.2981 479.7209 -1.1741 223.2331 224.4072 248.5128 481.3308 -1.1839 223.4036 224.5875 248.6673 482.9510 -1.1898 223.5962 224.7859 248.8533 484.5461 -1.1942 223.8264 225.0205 249.0534 486.1768 -1.1966 224.0495 225.2460 249.2296 487.7661 -1.1954 224.1937 225.3892 249.4317 489.3709 -1.2006 224.3583 225.5588 249.6333 490.9705 -1.2112 224.5743 225.7856 249.8364 492.5756 -1.2156 224.7458 225.9614 250.0744 494.1858 -1.2181 224.9035 226.1216 250.2850 495.7909 -1.2158 225.0674 226.2833 250.4532 497.4008 -1.2200 225.2291 226.4491 250.6291 499.0004 -1.2216 225.4220 226.6436 250.8349 500.6258 -1.2241 225.6198 226.8439 251.0755 502.2314 -1.2279 225.7937 227.0216 251.2975 503.8413 -1.2307 225.9404 227.1711 251.4952 505.4460 -1.2340 226.1004 227.3344 251.7151 507.0508 -1.2406 226.2855 227.5261 251.9442 508.6606 -1.2471 226.4628 227.7099 252.1638 510.2661 -1.2496 226.6315 227.8812 252.4069 511.8916 -1.2584 226.7915 228.0499 252.6443 513.4964 -1.2662 227.0067 228.2728 252.8840 515.1063 -1.2711 227.1640 228.4351 253.0134 516.7110 -1.2775 227.3202 228.5976 253.1754 518.3106 -1.2788 227.4993 228.7781 253.4002 519.9160 -1.2776 227.6678 228.9454 253.6049 521.5211 -1.2877 227.8477 229.1354 253.7932 523.1361 -1.2900 228.0350 229.3250 254.0221 524.7306 -1.2924 228.2128 229.5052 254.1923 526.3354 -1.2979 228.3817 229.6796 254.4017 527.9453 -1.2961 228.6008 229.8969 254.6316 529.5500 -1.2977 228.7710 230.0686 254.8796 531.1548 -1.3001 228.9434 230.2435 255.0540 532.7648 -1.3059 229.1313 230.4371 255.2052 534.3704 -1.3117 229.3167 230.6284 255.3972 535.9956 -1.3167 229.4315 230.7482 255.5978 537.6004 -1.3192 229.6410 230.9603 255.7905 539.2103 -1.3219 229.8577 231.1796 256.0124 540.8150 -1.3281 230.0415 231.3696 256.2485 542.4206 -1.3359 230.2028 231.5387 256.4316 544.0306 -1.3433 230.4233 231.7666 256.6242 545.6354 -1.3423 230.5673 231.9096 256.8554 547.2658 -1.3498 230.7172 232.0670 257.0530 548.8705 -1.3558 230.9061 232.2619 257.2590 550.4701 -1.3571 231.0654 232.4224 257.4639 552.0701 -1.3619 231.2545 232.6164 257.6543 553.6755 -1.3645 231.4491 232.8135 257.8017 555.2700 -1.3625 231.6341 232.9966 257.9515 556.8696 -1.3694 231.8441 233.2135 258.1475 558.4746 -1.3719 232.0396 233.4115 258.3484 560.1006 -1.3737 232.2604 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