DTA measure 1pb2updown Date: 2024109:90 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 883.56 s Mass = 959.100 mg data_number = 1098 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3325 -10.5223 240.5815 251.1038 263.8193 2.1545 -10.3924 240.7561 251.1484 263.8225 2.9465 -10.2701 240.9036 251.1737 263.8296 3.7385 -10.1485 241.1025 251.2510 263.8245 4.5905 -10.0207 241.2717 251.2924 263.8050 5.3525 -9.9061 241.4137 251.3197 263.8272 6.1770 -9.7920 241.5712 251.3632 263.8294 6.9780 -9.6863 241.7348 251.4211 263.8217 7.7705 -9.5748 241.8819 251.4567 263.8325 8.5625 -9.4635 242.0378 251.5013 263.8617 9.4145 -9.3453 242.1970 251.5423 263.8537 10.1765 -9.2303 242.3501 251.5804 263.8586 10.9985 -9.1118 242.5209 251.6327 263.8786 11.7905 -9.0056 242.6694 251.6750 263.9169 12.5825 -8.9003 242.8033 251.7036 263.9392 13.4345 -8.7934 242.9564 251.7498 263.9543 14.1965 -8.6988 243.0973 251.7962 263.9928 15.0183 -8.5943 243.2230 251.8174 264.0335 15.8403 -8.4906 243.3898 251.8805 264.0726 16.6223 -8.3988 243.5294 251.9282 264.1300 17.4158 -8.3040 243.6686 251.9726 264.1844 18.2685 -8.2006 243.8291 252.0297 264.2689 19.0308 -8.1100 243.9636 252.0736 264.3315 19.8535 -8.0138 244.1082 252.1220 264.3824 20.6460 -7.9269 244.2387 252.1656 264.4590 21.4383 -7.8577 244.3645 252.2222 264.5441 22.2873 -7.7735 244.4955 252.2690 264.6175 23.0453 -7.6932 244.6326 252.3257 264.7230 23.8645 -7.6053 244.7830 252.3883 264.8220 24.6525 -7.5135 244.9199 252.4334 264.9189 25.4403 -7.4407 245.0183 252.4590 265.0239 26.2895 -7.3531 245.1779 252.5309 265.1459 27.0550 -7.2771 245.2829 252.5600 265.2571 27.8520 -7.1895 245.4080 252.5975 265.3774 28.6715 -7.0952 245.5381 252.6334 265.5158 29.4925 -7.0104 245.6830 252.6934 265.6452 30.2543 -6.9366 245.8144 252.7510 265.7868 31.1055 -6.8551 245.9552 252.8103 265.9127 31.8675 -6.7852 246.0608 252.8460 266.0646 32.6895 -6.7180 246.1828 252.9008 266.1886 33.4815 -6.6503 246.2985 252.9488 266.3377 34.2733 -6.5811 246.4347 253.0158 266.4688 35.0955 -6.5084 246.5613 253.0697 266.6213 35.8875 -6.4435 246.6878 253.1313 266.7765 36.7093 -6.3753 246.8102 253.1855 266.9539 37.4975 -6.3084 246.9259 253.2343 267.1139 38.3085 -6.2458 247.0352 253.2810 267.2891 39.1003 -6.1844 247.1349 253.3192 267.4416 39.9223 -6.1198 247.2583 253.3781 267.6164 40.6840 -6.0663 247.3783 253.4446 267.7800 41.5363 -6.0033 247.5009 253.5042 267.9672 42.3280 -5.9455 247.6129 253.5584 268.1119 43.1195 -5.8836 247.7107 253.5943 268.2898 43.9420 -5.8260 247.8472 253.6731 268.4547 44.7035 -5.7707 247.9731 253.7438 268.6323 45.5560 -5.7094 248.0799 253.7893 268.8009 46.3480 -5.6580 248.1987 253.8567 268.9755 47.1405 -5.6053 248.2945 253.8998 269.1301 47.9530 -5.5519 248.4255 253.9774 269.3149 48.7450 -5.4995 248.5394 254.0388 269.4609 49.5365 -5.4530 248.6241 254.0772 269.6308 50.3895 -5.3950 248.7451 254.1401 269.7987 51.1518 -5.3511 248.8459 254.1969 269.9575 51.9738 -5.3024 248.9571 254.2595 270.1154 52.7658 -5.2506 249.0665 254.3172 270.2759 53.5575 -5.2068 249.1743 254.3811 270.4235 54.4095 -5.1577 249.2841 254.4418 270.5688 55.1680 -5.1137 249.3978 254.5115 270.7330 55.9860 -5.0711 249.5082 254.5793 270.8922 56.7745 -5.0244 249.6062 254.6305 271.0425 57.5818 -4.9792 249.7298 254.7090 271.1778 58.3660 -4.9401 249.8229 254.7630 271.3104 59.1845 -4.8981 249.9399 254.8380 271.4647 59.9733 -4.8609 250.0270 254.8879 271.6014 60.7935 -4.8202 250.1530 254.9733 271.7522 61.5825 -4.7828 250.2691 255.0519 271.8956 62.3710 -4.7440 250.3647 255.1086 272.0276 63.1920 -4.7038 250.4367 255.1405 272.1653 63.9535 -4.6669 250.5151 255.1820 272.3054 64.8060 -4.6262 250.6449 255.2711 272.4567 65.5980 -4.5882 250.7766 255.3648 272.5926 66.3895 -4.5556 250.8902 255.4458 272.7230 67.2120 -4.5181 251.0081 255.5262 272.8480 68.0123 -4.4809 251.0927 255.5737 272.9690 68.7795 -4.4489 251.1758 255.6247 273.0741 69.6320 -4.4137 251.2581 255.6718 273.2102 70.3938 -4.3800 251.3924 255.7724 273.3226 71.2158 -4.3504 251.4850 255.8353 273.4627 72.0080 -4.3197 251.5846 255.9043 273.5875 72.7995 -4.2866 251.6650 255.9517 273.6988 73.6520 -4.2515 251.7803 256.0318 273.7980 74.4138 -4.2191 251.9010 256.1201 273.9085 75.2358 -4.1871 252.0088 256.1959 274.0241 76.0280 -4.1599 252.1065 256.2663 274.1291 76.8195 -4.1324 252.1847 256.3172 274.2369 77.6420 -4.1028 252.2920 256.3949 274.3528 78.4633 -4.0710 252.4005 256.4715 274.4467 79.2145 -4.0429 252.4775 256.5204 274.5632 80.0668 -4.0125 252.5732 256.5857 274.6792 80.8588 -3.9845 252.6884 256.6729 274.7876 81.6505 -3.9608 252.7793 256.7402 274.9014 82.4728 -3.9344 252.8688 256.8032 275.0012 83.2345 -3.9097 252.9726 256.8822 275.1071 84.0873 -3.8807 253.0574 256.9381 275.2318 84.8495 -3.8570 253.1589 257.0159 275.3307 85.6715 -3.8312 253.2637 257.0949 275.4368 86.4933 -3.8046 253.3655 257.1702 275.5497 87.2518 -3.7801 253.4374 257.2175 275.6503 88.1000 -3.7597 253.5512 257.3109 275.7654 88.9073 -3.7359 253.6466 257.3825 275.8712 89.6650 -3.6978 253.7539 257.4516 275.9574 90.4830 -3.6826 253.8355 257.5180 276.0785 91.2713 -3.6663 253.9254 257.5918 276.1957 92.0600 -3.6635 254.0316 257.6951 276.3097 92.9085 -3.6730 254.1458 257.8188 276.4273 93.6673 -3.6627 254.2304 257.8930 276.5541 94.4873 -3.6342 254.3150 257.9493 276.6738 95.2773 -3.5745 254.4022 257.9767 276.7574 96.0685 -3.5357 254.4910 258.0267 276.8786 96.9210 -3.5086 254.6090 258.1176 277.0179 97.6825 -3.4881 254.6865 258.1745 277.1177 98.5538 -3.4691 254.8207 258.2898 277.2615 99.4948 -3.4485 254.9277 258.3762 277.3852 100.2865 -3.4289 254.9892 258.4181 277.5148 101.1088 -3.4087 255.0984 258.5071 277.6462 101.9005 -3.3919 255.1983 258.5902 277.7703 102.7228 -3.3736 255.3053 258.6788 277.8763 103.5150 -3.3508 255.3719 258.7227 277.9913 104.3065 -3.3370 255.4793 258.8163 278.1222 105.1285 -3.3221 255.5671 258.8892 278.2422 105.9205 -3.3058 255.6609 258.9667 278.3778 106.7428 -3.2892 255.7650 259.0542 278.4862 107.5348 -3.2706 255.8433 259.1139 278.6042 108.3265 -3.2553 255.9318 259.1872 278.7429 109.1495 -3.2405 256.0397 259.2801 278.8511 109.9425 -3.2267 256.1261 259.3529 278.9917 110.7645 -3.2082 256.2219 259.4302 279.1409 111.5565 -3.1954 256.3010 259.4964 279.2753 112.3485 -3.1829 256.4141 259.5970 279.3862 113.2010 -3.1638 256.5182 259.6820 279.5313 113.9635 -3.1490 256.5896 259.7386 279.6554 114.7863 -3.1345 256.6779 259.8123 279.7735 115.5785 -3.1220 256.7683 259.8903 279.9002 116.3705 -3.1112 256.8604 259.9716 280.0495 117.2225 -3.0992 256.9710 260.0701 280.1842 117.9845 -3.0868 257.0714 260.1582 280.3075 118.8048 -3.0737 257.1707 260.2444 280.4404 119.5930 -3.0597 257.2459 260.3057 280.5884 120.3820 -3.0450 257.3272 260.3722 280.7237 121.2300 -3.0343 257.4483 260.4826 280.8657 121.9880 -3.0271 257.5376 260.5648 280.9900 122.8060 -3.0165 257.6249 260.6415 281.1254 123.6243 -3.0053 257.7045 260.7098 281.2559 124.3840 -2.9939 257.7962 260.7901 281.3840 125.2325 -2.9794 257.8860 260.8654 281.5172 126.0220 -2.9697 257.9850 260.9546 281.6677 126.8120 -2.9644 258.1040 261.0683 281.8125 127.6335 -2.9557 258.1860 261.1417 281.9446 128.3955 -2.9446 258.2893 261.2339 282.0691 129.2603 -2.9331 258.3620 261.2951 282.1944 130.0325 -2.9254 258.4557 261.3811 282.3256 130.8545 -2.9138 258.5399 261.4537 282.4945 131.6165 -2.9034 258.6445 261.5479 282.6173 132.4685 -2.8952 258.7398 261.6349 282.7480 133.2305 -2.8879 258.8300 261.7180 282.8795 134.0525 -2.8797 258.9338 261.8136 283.0175 134.8748 -2.8668 259.0178 261.8846 283.1765 135.6365 -2.8567 259.0876 261.9442 283.2618 136.4885 -2.8487 259.2011 262.0498 283.3906 137.2505 -2.8433 259.3008 262.1440 283.5341 138.0725 -2.8374 259.3976 262.2350 283.6769 138.8945 -2.8277 259.4979 262.3257 283.8109 139.6943 -2.8198 259.5817 262.4015 283.9528 140.4645 -2.8125 259.6643 262.4768 284.0580 141.3165 -2.8008 259.7675 262.5682 284.2199 142.1085 -2.7946 259.8824 262.6770 284.3670 142.9015 -2.7882 259.9618 262.7500 284.4947 143.7235 -2.7818 260.0575 262.8393 284.6131 144.4855 -2.7749 260.1543 262.9292 284.7449 145.3373 -2.7682 260.2680 263.0362 284.8682 146.1295 -2.7627 260.3403 263.1030 285.0070 146.9223 -2.7554 260.4315 263.1869 285.1199 147.7443 -2.7476 260.5491 263.2966 285.2467 148.5055 -2.7409 260.6081 263.3490 285.3689 149.3580 -2.7318 260.7170 263.4488 285.5152 150.1513 -2.7289 260.8310 263.5599 285.6352 150.9313 -2.7230 260.9272 263.6502 285.7517 151.7500 -2.7159 261.0438 263.7596 285.8968 152.5385 -2.7076 261.1050 263.8126 286.0345 153.3263 -2.6986 261.1754 263.8740 286.1399 154.1748 -2.6934 261.2768 263.9702 286.2611 154.9325 -2.6909 261.3766 264.0675 286.3826 155.7510 -2.6840 261.4918 264.1758 286.5205 156.5693 -2.6836 261.5819 264.2655 286.6511 157.3293 -2.6755 261.6892 264.3648 286.7515 158.1793 -2.6695 261.7836 264.4532 286.8884 158.9398 -2.6650 261.8555 264.5206 287.0140 159.7615 -2.6574 261.9663 264.6237 287.1511 160.5675 -2.6559 262.0995 264.7554 287.2675 161.3595 -2.6533 262.1554 264.8088 287.3865 162.1515 -2.6483 262.2668 264.9151 287.4852 163.0035 -2.6413 262.3741 265.0154 287.6216 163.7655 -2.6378 262.4500 265.0878 287.7357 164.5875 -2.6314 262.5476 265.1790 287.8791 165.3795 -2.6248 262.6374 265.2622 287.9800 166.1715 -2.6242 262.7248 265.3490 288.0958 166.9935 -2.6209 262.8379 265.4588 288.2084 167.7855 -2.6155 262.9342 265.5498 288.3357 168.6073 -2.6094 263.0583 265.6677 288.4751 169.3995 -2.6059 263.1455 265.7514 288.5756 170.2105 -2.5988 263.2270 265.8258 288.7051 170.9983 -2.5989 263.3395 265.9384 288.8191 171.8205 -2.5970 263.4326 266.0296 288.9606 172.6120 -2.5915 263.5269 266.1185 289.0947 173.4338 -2.5904 263.6178 266.2081 289.2160 174.2260 -2.5855 263.7210 266.3065 289.3302 175.0185 -2.5805 263.8141 266.3947 289.4724 175.8410 -2.5780 263.9188 266.4968 289.6105 176.6025 -2.5749 264.0197 266.5946 289.7379 177.4550 -2.5698 264.1393 266.7091 289.8614 178.2470 -2.5656 264.2271 266.7926 290.0130 179.0385 -2.5636 264.3124 266.8760 290.1334 179.8610 -2.5603 264.4085 266.9688 290.2688 180.6658 -2.5559 264.4998 267.0558 290.3749 181.4415 -2.5547 264.5844 267.1392 290.5232 182.2943 -2.5496 264.7036 267.2531 290.6624 183.0565 -2.5508 264.8099 267.3607 290.7839 183.8770 -2.5482 264.9050 267.4532 290.9222 184.6650 -2.5443 264.9993 267.5437 291.0590 185.4530 -2.5375 265.0900 267.6275 291.1904 186.2713 -2.5382 265.2003 267.7384 291.3260 187.0593 -2.5339 265.3100 267.8439 291.4707 187.8780 -2.5296 265.4150 267.9446 291.5963 188.6665 -2.5287 265.5213 268.0500 291.7154 189.4550 -2.5266 265.6022 268.1288 291.8592 190.2738 -2.5231 265.7122 268.2353 291.9887 191.0880 -2.5186 265.8104 268.3289 292.1422 191.8675 -2.5108 265.9197 268.4305 292.2688 192.6890 -2.5156 266.0155 268.5311 292.3957 193.4803 -2.5139 266.1109 268.6248 292.5252 194.2715 -2.5109 266.2136 268.7245 292.6571 195.0943 -2.5112 266.3260 268.8372 292.7910 195.8555 -2.5104 266.4247 268.9351 292.9387 196.7080 -2.5087 266.5150 269.0237 293.0763 197.4698 -2.5079 266.6217 269.1296 293.2009 198.2918 -2.5027 266.7220 269.2247 293.3345 199.1140 -2.4995 266.8135 269.3130 293.4951 199.8755 -2.5008 266.9052 269.4060 293.6082 200.7318 -2.5002 267.0166 269.5168 293.7565 201.5353 -2.4959 267.1268 269.6227 293.8700 202.2978 -2.4947 267.2145 269.7092 293.9939 203.1198 -2.4937 267.3040 269.7977 294.1427 203.9120 -2.4937 267.4327 269.9264 294.2785 204.7035 -2.4927 267.5385 270.0311 294.3985 205.5560 -2.4920 267.6461 270.1382 294.5279 206.3178 -2.4904 267.7481 270.2385 294.6525 207.1398 -2.4868 267.8503 270.3372 294.8066 207.9320 -2.4864 267.9586 270.4450 294.9563 208.7235 -2.4837 268.0316 270.5153 295.0456 209.5758 -2.4799 268.1524 270.6323 295.1811 210.3375 -2.4777 268.2639 270.7416 295.3006 211.1798 -2.4785 268.3749 270.8534 295.4376 211.9705 -2.4788 268.4735 270.9523 295.5689 212.7628 -2.4770 268.5780 271.0550 295.6906 213.5555 -2.4782 268.6843 271.1625 295.8228 214.3775 -2.4739 268.7947 271.2686 295.9634 215.1695 -2.4684 268.8686 271.3370 296.0971 215.9900 -2.4667 268.9819 271.4486 296.2128 216.7780 -2.4675 269.1100 271.5775 296.3440 217.5660 -2.4692 269.2083 271.6775 296.4882 218.3830 -2.4710 269.3198 271.7908 296.6045 219.1720 -2.4705 269.4204 271.8909 296.7262 219.9900 -2.4678 269.4991 271.9669 296.8564 220.7783 -2.4691 269.6084 272.0775 296.9973 221.6055 -2.4664 269.7313 272.1977 297.1036 222.3758 -2.4681 269.8400 272.3081 297.2063 223.1953 -2.4671 269.9268 272.3940 297.3624 223.9565 -2.4669 270.0335 272.5004 297.4832 224.8090 -2.4635 270.1519 272.6154 297.6294 225.6003 -2.4610 270.2464 272.7074 297.7654 226.3915 -2.4630 270.3693 272.8323 297.8669 227.2140 -2.4636 270.4616 272.9251 297.9913 227.9758 -2.4638 270.5775 273.0414 298.1132 228.8280 -2.4636 270.6864 273.1501 298.2280 229.6200 -2.4588 270.8035 273.2624 298.3578 230.4115 -2.4575 270.8957 273.3532 298.5005 231.2340 -2.4530 271.0078 273.4608 298.6023 232.0485 -2.4518 271.1125 273.5644 298.7369 232.7985 -2.4550 271.2234 273.6783 298.8532 233.6508 -2.4514 271.3474 273.7988 298.9742 234.4428 -2.4578 271.4448 273.9026 299.0964 235.2345 -2.4527 271.5334 273.9862 299.2090 236.0568 -2.4550 271.6529 274.1079 299.3304 236.8485 -2.4564 271.7812 274.2376 299.4590 237.6708 -2.4553 271.8631 274.3185 299.6093 238.4625 -2.4555 271.9858 274.4413 299.7310 239.2545 -2.4572 272.0809 274.5381 299.8509 240.0765 -2.4553 272.2021 274.6574 299.9874 240.8685 -2.4560 272.2889 274.7449 300.1214 241.6905 -2.4518 272.4137 274.8655 300.2610 242.5040 -2.4500 272.5352 274.9852 300.3939 243.2965 -2.4532 272.6376 275.0908 300.5135 244.0885 -2.4543 272.7312 275.1854 300.6578 244.9105 -2.4542 272.8506 275.3048 300.7963 245.7025 -2.4532 272.9737 275.4269 300.9084 246.5245 -2.4562 273.0716 275.5278 301.0725 247.3163 -2.4529 273.1752 275.6281 301.1921 248.1058 -2.4507 273.2881 275.7387 301.3324 248.9245 -2.4509 273.4010 275.8518 301.4667 249.7130 -2.4496 273.4833 275.9329 301.6032 250.5310 -2.4498 273.5926 276.0424 301.7496 251.3190 -2.4536 273.7287 276.1823 301.8773 252.1283 -2.4567 273.8513 276.3080 301.9970 252.9145 -2.4520 273.9393 276.3913 302.1337 253.7340 -2.4568 274.0808 276.5376 302.2854 254.5230 -2.4572 274.1967 276.6539 302.4375 255.3420 -2.4582 274.2885 276.7467 302.5812 256.1330 -2.4578 274.4048 276.8626 302.7205 256.9240 -2.4541 274.4991 276.9532 302.8392 257.7755 -2.4523 274.6100 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