DTA measure 1pbupdown4 Date: 2024109:1019 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.25 s Mass = 959.100 mg data_number = 1583 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2615 -1.6494 228.3569 230.0064 261.7061 2.0835 -1.6436 228.4902 230.1338 261.6776 2.8755 -1.6416 228.6203 230.2619 261.6634 3.6978 -1.6388 228.7524 230.3912 261.6793 4.4895 -1.6385 228.8895 230.5280 261.6737 5.2815 -1.6376 229.0193 230.6569 261.6720 6.1035 -1.6339 229.1506 230.7845 261.6637 6.8655 -1.6310 229.2771 230.9081 261.7065 7.7175 -1.6290 229.4325 231.0616 261.6830 8.5095 -1.6279 229.5632 231.1911 261.7093 9.3023 -1.6241 229.7020 231.3261 261.7364 10.1245 -1.6210 229.8331 231.4541 261.7712 10.9165 -1.6176 229.9616 231.5792 261.8068 11.7385 -1.6169 230.0941 231.7110 261.8444 12.5305 -1.6166 230.2157 231.8323 261.8988 13.3225 -1.6141 230.3591 231.9732 261.9415 14.1445 -1.6113 230.5020 232.1133 262.0062 14.9365 -1.6087 230.6366 232.2454 262.0542 15.7585 -1.6082 230.7615 232.3697 262.1445 16.5505 -1.6069 230.8972 232.5041 262.2021 17.3418 -1.6078 231.0202 232.6280 262.2930 18.1643 -1.6056 231.1540 232.7597 262.3662 18.9560 -1.6010 231.2868 232.8879 262.4724 19.7778 -1.5974 231.4117 233.0091 262.5717 20.5700 -1.5941 231.5407 233.1348 262.6532 21.3615 -1.5926 231.6843 233.2770 262.7531 22.1840 -1.5938 231.8165 233.4104 262.8736 22.9758 -1.5944 231.9352 233.5296 262.9873 23.7978 -1.5919 232.0686 233.6605 263.1060 24.5898 -1.5867 232.1995 233.7862 263.2258 25.3825 -1.5860 232.3196 233.9056 263.3600 26.2050 -1.5850 232.4528 234.0379 263.4906 26.9968 -1.5883 232.5772 234.1655 263.6218 27.8198 -1.5855 232.7090 234.2945 263.7606 28.5908 -1.5863 232.8403 234.4266 263.8886 29.4125 -1.5857 232.9665 234.5522 264.0494 30.2348 -1.5834 233.0936 234.6769 264.2045 30.9965 -1.5845 233.2366 234.8211 264.3332 31.8485 -1.5839 233.3631 234.9470 264.5002 32.6105 -1.5816 233.4914 235.0730 264.6306 33.4325 -1.5813 233.6262 235.2075 264.7901 34.2545 -1.5841 233.7785 235.3626 264.9410 35.0165 -1.5844 233.8808 235.4653 265.0994 35.8670 -1.5799 234.0081 235.5880 265.2624 36.6248 -1.5774 234.1250 235.7024 265.3852 37.4438 -1.5774 234.2593 235.8367 265.5501 38.2320 -1.5786 234.3809 235.9594 265.7015 39.0200 -1.5800 234.5046 236.0846 265.8518 39.8680 -1.5787 234.6738 236.2525 266.0118 40.6260 -1.5812 234.7898 236.3710 266.1446 41.4453 -1.5794 234.9170 236.4964 266.3083 42.2340 -1.5812 235.0314 236.6126 266.4636 43.0230 -1.5796 235.1674 236.7470 266.5831 43.8720 -1.5785 235.3026 236.8811 266.7573 44.6310 -1.5817 235.4237 237.0054 266.8946 45.4498 -1.5830 235.5553 237.1383 267.0391 46.2683 -1.5810 235.6897 237.2707 267.1880 47.0280 -1.5839 235.8022 237.3861 267.3130 47.8765 -1.5849 235.9458 237.5307 267.4760 48.6658 -1.5818 236.0697 237.6515 267.6007 49.4550 -1.5828 236.2069 237.7897 267.7175 50.2733 -1.5863 236.3185 237.9048 267.8683 51.0638 -1.5892 236.4402 238.0295 267.9783 51.8843 -1.5890 236.5701 238.1591 268.1024 52.6745 -1.5879 236.7116 238.2995 268.2288 53.4660 -1.5883 236.8455 238.4338 268.3558 54.2875 -1.5869 236.9768 238.5637 268.4913 55.0795 -1.5899 237.0888 238.6787 268.5950 55.9015 -1.5937 237.2177 238.8114 268.7087 56.6935 -1.5955 237.3563 238.9518 268.8087 57.4855 -1.5965 237.4651 239.0616 268.9299 58.3075 -1.5955 237.5907 239.1862 269.0495 59.0995 -1.5946 237.7262 239.3208 269.1478 59.9213 -1.5968 237.8581 239.4549 269.2779 60.7135 -1.5967 237.9951 239.5918 269.3806 61.5055 -1.5977 238.1363 239.7340 269.4884 62.3275 -1.5990 238.2653 239.8643 269.5920 63.1193 -1.5995 238.3888 239.9882 269.6881 63.9415 -1.5999 238.5079 240.1077 269.7907 64.7343 -1.6046 238.6300 240.2346 269.8667 65.5255 -1.6028 238.7739 240.3767 269.9745 66.3483 -1.6023 238.8979 240.5002 270.0696 67.1398 -1.6069 239.0104 240.6173 270.1606 67.9618 -1.6077 239.1418 240.7496 270.2470 68.7540 -1.6045 239.2607 240.8652 270.3412 69.5458 -1.6024 239.3989 241.0013 270.4244 70.3680 -1.6045 239.5147 241.1192 270.5220 71.1598 -1.6045 239.6551 241.2596 270.6084 71.9818 -1.6074 239.7836 241.3910 270.6835 72.7740 -1.6076 239.9014 241.5090 270.7768 73.5655 -1.6078 240.0063 241.6140 270.8479 74.3880 -1.6059 240.1452 241.7511 270.9440 75.1495 -1.6078 240.2696 241.8774 271.0137 76.0020 -1.6070 240.4242 242.0312 271.1153 76.7940 -1.6078 240.5606 242.1684 271.1938 77.5855 -1.6097 240.6710 242.2807 271.2733 78.4078 -1.6085 240.7983 242.4068 271.3516 79.1695 -1.6119 240.9180 242.5300 271.4351 80.0315 -1.6127 241.0426 242.6553 271.5237 80.7935 -1.6140 241.1625 242.7765 271.6027 81.6158 -1.6127 241.3033 242.9161 271.6890 82.4075 -1.6135 241.4234 243.0369 271.7781 83.1995 -1.6140 241.5533 243.1673 271.8708 84.0215 -1.6166 241.6612 243.2777 271.9484 84.8135 -1.6172 241.7921 243.4093 272.0463 85.6355 -1.6162 241.9265 243.5427 272.1600 86.4275 -1.6187 242.0523 243.6709 272.2392 87.2195 -1.6205 242.1601 243.7807 272.3304 88.0415 -1.6204 242.3062 243.9266 272.4200 88.8335 -1.6224 242.4303 244.0527 272.5172 89.6555 -1.6222 242.5562 244.1784 272.6187 90.4475 -1.6237 242.6747 244.2984 272.7240 91.2395 -1.6249 242.8031 244.4280 272.8110 92.0615 -1.6234 242.9316 244.5550 272.9362 92.8535 -1.6239 243.0552 244.6790 273.0153 93.6755 -1.6257 243.1816 244.8073 273.1099 94.4670 -1.6271 243.3106 244.9377 273.2185 95.2585 -1.6295 243.4172 245.0467 273.3269 96.0810 -1.6264 243.5479 245.1743 273.4385 96.8728 -1.6273 243.6706 245.2979 273.5419 97.6955 -1.6272 243.8069 245.4342 273.6550 98.4880 -1.6267 243.9316 245.5583 273.7755 99.2795 -1.6269 244.0733 245.7003 273.8645 100.0980 -1.6306 244.1867 245.8173 273.9642 100.8870 -1.6330 244.2984 245.9314 274.0719 101.7055 -1.6330 244.4200 246.0530 274.1825 102.4935 -1.6342 244.5598 246.1940 274.3098 103.2823 -1.6357 244.6722 246.3079 274.4168 104.1305 -1.6365 244.7718 246.4083 274.5387 104.8883 -1.6374 244.8970 246.5344 274.6398 105.7070 -1.6411 245.0230 246.6642 274.7305 106.4955 -1.6410 245.1560 246.7969 274.8446 107.2835 -1.6459 245.2980 246.9439 274.9723 108.1323 -1.6445 245.4169 247.0614 275.0872 108.8903 -1.6445 245.5279 247.1725 275.1772 109.7095 -1.6438 245.6827 247.3266 275.2997 110.5288 -1.6461 245.7909 247.4370 275.4132 111.2870 -1.6476 245.9227 247.5703 275.5131 112.1368 -1.6467 246.0353 247.6820 275.6460 112.9268 -1.6500 246.1489 247.7989 275.7517 113.7178 -1.6503 246.2806 247.9309 275.8754 114.5403 -1.6488 246.4114 248.0602 275.9882 115.3010 -1.6483 246.5051 248.1534 276.0954 116.1530 -1.6504 246.6358 248.2862 276.2206 116.9148 -1.6541 246.7649 248.4191 276.3484 117.7368 -1.6580 246.8946 248.5526 276.4530 118.5590 -1.6611 247.0013 248.6624 276.5518 119.3205 -1.6602 247.1149 248.7750 276.6598 120.1730 -1.6616 247.2491 248.9107 276.7853 120.9348 -1.6606 247.3772 249.0377 276.8832 121.7568 -1.6611 247.5120 249.1731 277.0064 122.5490 -1.6643 247.6329 249.2972 277.1203 123.3405 -1.6621 247.7376 249.3997 277.2189 124.1630 -1.6658 247.8581 249.5239 277.3449 124.9545 -1.6682 247.9941 249.6624 277.4780 125.7768 -1.6677 248.1252 249.7929 277.5759 126.5690 -1.6690 248.2291 249.8981 277.6875 127.3605 -1.6704 248.3849 250.0553 277.8092 128.1828 -1.6735 248.4936 250.1671 277.9462 128.9445 -1.6722 248.6008 250.2730 278.0573 129.7965 -1.6747 248.7365 250.4112 278.1713 130.5623 -1.6754 248.8356 250.5110 278.2680 131.3968 -1.6787 248.9590 250.6378 278.3726 132.1885 -1.6782 249.0825 250.7607 278.4953 132.9805 -1.6797 249.2006 250.8803 278.6053 133.8025 -1.6804 249.3264 251.0069 278.7317 134.5645 -1.6850 249.4539 251.1389 278.8393 135.4165 -1.6868 249.5643 251.2511 278.9715 136.2085 -1.6888 249.6970 251.3858 279.0849 137.0005 -1.6873 249.8180 251.5053 279.1759 137.8225 -1.6892 249.9479 251.6371 279.3045 138.5845 -1.6908 250.0406 251.7314 279.4273 139.4365 -1.6893 250.1863 251.8756 279.5413 140.1985 -1.6889 250.3041 251.9931 279.6148 141.0205 -1.6931 250.4481 252.1412 279.7367 141.8425 -1.6957 250.5575 252.2531 279.8477 142.6045 -1.7002 250.6710 252.3713 279.9626 143.4565 -1.7003 250.8095 252.5098 280.0616 144.2183 -1.7010 250.9285 252.6295 280.1670 145.0398 -1.6989 251.0377 252.7366 280.2598 145.8620 -1.7022 251.1617 252.8639 280.3757 146.6235 -1.7018 251.2870 252.9888 280.4551 147.4760 -1.7032 251.3997 253.1029 280.5636 148.2378 -1.7035 251.5057 253.2092 280.6556 149.0598 -1.7063 251.6365 253.3428 280.7489 149.8820 -1.7080 251.7591 253.4671 280.8533 150.6435 -1.7130 251.8761 253.5892 280.9411 151.4960 -1.7085 251.9927 253.7013 281.0590 152.2880 -1.7112 252.1006 253.8118 281.1339 153.0795 -1.7139 252.2290 253.9429 281.2248 153.9020 -1.7137 252.3533 254.0670 281.3191 154.6635 -1.7151 252.4958 254.2109 281.4200 155.5163 -1.7160 252.6276 254.3436 281.5194 156.3088 -1.7143 252.7500 254.4643 281.6091 157.1005 -1.7150 252.8452 254.5602 281.6905 157.9233 -1.7151 252.9533 254.6684 281.7876 158.6855 -1.7174 253.0914 254.8088 281.8710 159.5400 -1.7230 253.2269 254.9499 281.9685 160.3325 -1.7258 253.3380 255.0638 282.0602 161.1270 -1.7251 253.4499 255.1750 282.1753 161.9275 -1.7215 253.5645 255.2860 282.2534 162.7195 -1.7248 253.6729 255.3977 282.3577 163.5708 -1.7271 253.8192 255.5463 282.4522 164.3290 -1.7279 253.9365 255.6643 282.5324 165.1470 -1.7308 254.0845 255.8153 282.6489 165.9650 -1.7290 254.1892 255.9182 282.7577 166.7230 -1.7300 254.3034 256.0334 282.8435 167.5715 -1.7325 254.4238 256.1563 282.9454 168.3300 -1.7360 254.5386 256.2746 283.0150 169.1488 -1.7367 254.6682 256.4049 283.1446 169.9678 -1.7387 254.7835 256.5222 283.2336 170.7260 -1.7387 254.8914 256.6301 283.3392 171.5740 -1.7389 255.0371 256.7760 283.4474 172.3320 -1.7432 255.1389 256.8821 283.5410 173.1508 -1.7454 255.2663 257.0117 283.6591 173.9693 -1.7446 255.3862 257.1308 283.7521 174.7280 -1.7442 255.4797 257.2239 283.8546 175.5775 -1.7451 255.5885 257.3336 283.9713 176.3665 -1.7501 255.7335 257.4836 284.0642 177.1568 -1.7499 255.8497 257.5996 284.1549 177.9765 -1.7485 255.9799 257.7284 284.2840 178.7385 -1.7526 256.0993 257.8519 284.3913 179.5903 -1.7500 256.2049 257.9549 284.5069 180.3815 -1.7551 256.3227 258.0778 284.5989 181.1733 -1.7544 256.4543 258.2087 284.6980 181.9945 -1.7545 256.5622 258.3167 284.8087 182.7560 -1.7576 256.6666 258.4242 284.8862 183.6075 -1.7585 256.8133 258.5718 284.9934 184.3695 -1.7598 256.9259 258.6856 285.1067 185.1915 -1.7643 257.0297 258.7940 285.2263 185.9835 -1.7656 257.1315 258.8971 285.3195 186.7755 -1.7674 257.2447 259.0122 285.4100 187.5975 -1.7685 257.3746 259.1431 285.5053 188.3895 -1.7697 257.4923 259.2619 285.6057 189.2115 -1.7700 257.6375 259.4075 285.7270 190.0033 -1.7731 257.7372 259.5104 285.8457 190.7955 -1.7755 257.8870 259.6625 285.9523 191.6175 -1.7746 258.0020 259.7766 286.0541 192.3788 -1.7712 258.1094 259.8806 286.1727 193.2313 -1.7725 258.2451 260.0176 286.2641 194.0233 -1.7745 258.3631 260.1375 286.3622 194.8145 -1.7733 258.4582 260.2315 286.4610 195.6373 -1.7763 258.5764 260.3527 286.5795 196.3985 -1.7772 258.7004 260.4775 286.6726 197.2510 -1.7824 258.8092 260.5917 286.7730 198.0430 -1.7850 258.9252 260.7102 286.8849 198.8345 -1.7837 259.0470 260.8306 286.9969 199.6570 -1.7853 259.1636 260.9489 287.1080 200.4185 -1.7889 259.2712 261.0602 287.1936 201.2710 -1.7949 259.3792 261.1741 287.2976 202.0630 -1.7939 259.5034 261.2973 287.4084 202.8545 -1.7930 259.6332 261.4262 287.5161 203.6770 -1.7934 259.7615 261.5549 287.6076 204.4385 -1.7989 259.8712 261.6702 287.7135 205.2910 -1.7988 259.9877 261.7866 287.8291 206.0828 -1.7965 260.0986 261.8952 287.9230 206.8745 -1.8009 260.2028 262.0038 288.0373 207.6968 -1.7973 260.3312 262.1285 288.1303 208.4885 -1.7985 260.4502 262.2487 288.2282 209.3115 -1.7974 260.5732 262.3706 288.3379 210.1035 -1.8002 260.6977 262.4979 288.4595 210.8955 -1.8059 260.8003 262.6062 288.5357 211.7175 -1.8062 260.9200 262.7261 288.6464 212.5108 -1.8071 261.0374 262.8445 288.7319 213.3365 -1.8148 261.1533 262.9681 288.8356 214.1285 -1.8125 261.2737 263.0862 288.9564 214.9205 -1.8116 261.4036 263.2152 289.0530 215.7425 -1.8148 261.5042 263.3190 289.1692 216.5345 -1.8167 261.6345 263.4512 289.2748 217.3583 -1.8195 261.7588 263.5783 289.3855 218.1505 -1.8211 261.8742 263.6953 289.5057 218.9425 -1.8209 261.9851 263.8060 289.6128 219.7645 -1.8207 262.1035 263.9242 289.7284 220.5565 -1.8237 262.2098 264.0335 289.8286 221.3783 -1.8254 262.3264 264.1518 289.9563 222.1705 -1.8275 262.4569 264.2844 290.0864 222.9618 -1.8264 262.5698 264.3961 290.2165 223.8140 -1.8298 262.6653 264.4950 290.3233 224.5758 -1.8317 262.7951 264.6268 290.4338 225.3978 -1.8304 262.9126 264.7430 290.5537 226.1900 -1.8320 263.0272 264.8593 290.6916 226.9815 -1.8333 263.1347 264.9680 290.8118 227.8328 -1.8359 263.2691 265.1050 290.9211 228.5890 -1.8396 263.3823 265.2220 291.0294 229.4080 -1.8406 263.4830 265.3236 291.1407 230.2263 -1.8436 263.6161 265.4598 291.2791 230.9840 -1.8419 263.7224 265.5643 291.3912 231.8323 -1.8434 263.8580 265.7014 291.5182 232.5903 -1.8437 263.9726 265.8163 291.6309 233.4090 -1.8462 264.0761 265.9224 291.7329 234.2280 -1.8520 264.2002 266.0522 291.8674 234.9863 -1.8535 264.3181 266.1716 291.9538 235.8355 -1.8545 264.4481 266.3026 292.0728 236.5943 -1.8575 264.5385 266.3961 292.1683 237.4130 -1.8557 264.6531 266.5087 292.2805 238.2320 -1.8604 264.7911 266.6515 292.4004 238.9930 -1.8597 264.8960 266.7556 292.5174 239.8430 -1.8589 265.0139 266.8728 292.6142 240.6013 -1.8642 265.1143 266.9785 292.7213 241.4218 -1.8673 265.2359 267.1033 292.8353 242.2135 -1.8687 265.3520 267.2207 292.9291 243.0038 -1.8702 265.4710 267.3412 293.0555 243.8358 -1.8710 265.5806 267.4516 293.1422 244.5968 -1.8719 265.7003 267.5722 293.2366 245.4490 -1.8757 265.8274 267.7031 293.3502 246.2410 -1.8792 265.9465 267.8257 293.4536 247.0325 -1.8815 266.0624 267.9439 293.5539 247.8550 -1.8838 266.1696 268.0535 293.6388 248.6158 -1.8859 266.2856 268.1716 293.7313 249.4680 -1.8855 266.4096 268.2951 293.8463 250.2298 -1.8893 266.5033 268.3926 293.9318 251.0518 -1.8941 266.6147 268.5089 294.0341 251.8740 -1.8945 266.7439 268.6383 294.1386 252.6355 -1.8932 266.8639 268.7572 294.2397 253.4880 -1.8972 266.9784 268.8757 294.3731 254.2495 -1.9003 267.0714 268.9717 294.4531 255.0718 -1.9037 267.2273 269.1310 294.5352 255.8938 -1.9063 267.3323 269.2386 294.6334 256.6555 -1.9089 267.4405 269.3494 294.7482 257.5078 -1.9052 267.5495 269.4547 294.8329 258.2695 -1.9090 267.6692 269.5782 294.9218 259.0918 -1.9113 267.8003 269.7117 295.0315 259.9138 -1.9124 267.9330 269.8454 295.1231 260.6755 -1.9156 268.0096 269.9252 295.2012 261.5275 -1.9170 268.1270 270.0441 295.3096 262.2895 -1.9180 268.2346 270.1526 295.3909 263.1115 -1.9206 268.3668 270.2874 295.4997 263.9335 -1.9219 268.4749 270.3968 295.5845 264.6955 -1.9208 268.5857 270.5065 295.6898 265.5475 -1.9195 268.7173 270.6368 295.7986 266.3395 -1.9254 268.8424 270.7678 295.9134 267.1315 -1.9264 268.9405 270.8669 295.9950 267.9535 -1.9287 269.0576 270.9863 296.0885 268.7155 -1.9339 269.1623 271.0962 296.1720 269.5675 -1.9322 269.2751 271.2072 296.2860 270.3595 -1.9366 269.3972 271.3338 296.4026 271.1515 -1.9372 269.5353 271.4725 296.5002 271.9733 -1.9363 269.6520 271.5882 296.6096 272.7655 -1.9388 269.7505 271.6893 296.7101 273.5868 -1.9381 269.8593 271.7974 296.8233 274.3790 -1.9403 269.9580 271.8982 296.9203 275.1705 -1.9441 270.0863 272.0304 297.0278 275.9930 -1.9457 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