DTA measure 2pb2updown Date: 2024109:930 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1647.94 s Mass = 959.100 mg data_number = 1021 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2605 -4.4908 401.7312 406.2220 418.8409 3.8748 -4.4895 401.9604 406.4498 418.8901 5.4745 -4.4878 402.1585 406.6464 418.9244 7.0740 -4.4834 402.3577 406.8411 418.9765 8.7043 -4.4824 402.5677 407.0501 419.0132 10.3020 -4.4758 402.7679 407.2436 419.0418 11.9089 -4.4692 402.9650 407.4342 419.0754 13.5000 -4.4720 403.1623 407.6344 419.0566 15.0923 -4.4657 403.3740 407.8397 419.0233 16.7149 -4.4599 403.5601 408.0200 418.9841 18.3088 -4.4606 403.7675 408.2281 418.9237 19.9205 -4.4537 403.9415 408.3951 418.8490 21.5195 -4.4519 404.1306 408.5825 418.7357 23.1185 -4.4469 404.3364 408.7832 418.6239 24.7175 -4.4427 404.5267 408.9694 418.4809 26.3465 -4.4346 404.7145 409.1490 418.3271 27.9455 -4.4253 404.8927 409.3180 418.1607 29.5445 -4.4197 405.0674 409.4871 417.9526 31.1435 -4.4129 405.2201 409.6330 417.7523 32.7581 -4.4009 405.4229 409.8239 417.5404 34.3725 -4.3896 405.5840 409.9736 417.3391 35.9865 -4.3798 405.7606 410.1404 417.1209 37.5854 -4.3708 405.9056 410.2764 416.9162 39.1959 -4.3614 406.0905 410.4519 416.6765 40.7969 -4.3504 406.2380 410.5883 416.4556 42.4114 -4.3394 406.4049 410.7443 416.2128 44.0228 -4.3309 406.5556 410.8866 416.0107 45.6144 -4.3167 406.7064 411.0231 415.7522 47.2205 -4.3050 406.8507 411.1558 415.5148 48.8123 -4.2907 406.9884 411.2791 415.2999 50.4359 -4.2777 407.1361 411.4137 415.0874 52.0461 -4.2647 407.2642 411.5290 414.8622 53.6568 -4.2540 407.3899 411.6439 414.6328 55.2705 -4.2429 407.5221 411.7650 414.4193 56.8845 -4.2352 407.6635 411.8987 414.1828 58.4985 -4.2253 407.7825 412.0079 413.9610 60.0975 -4.2079 407.9043 412.1122 413.7747 61.6960 -4.1972 408.0503 412.2475 413.5482 63.3101 -4.1863 408.1676 412.3538 413.3652 64.9239 -4.1751 408.2504 412.4255 413.1697 66.5380 -4.1608 408.3578 412.5186 412.9632 68.1378 -4.1511 408.4833 412.6344 412.7705 69.7373 -4.1420 408.5642 412.7062 412.5783 71.3518 -4.1265 408.6850 412.8115 412.4059 72.9658 -4.1074 408.7698 412.8772 412.2230 74.5800 -4.1047 408.8718 412.9765 412.0373 76.1760 -4.0945 408.9662 413.0606 411.8674 77.7671 -4.0811 409.0477 413.1288 411.6922 79.3581 -4.0691 409.1383 413.2074 411.5179 80.9793 -4.0597 409.2125 413.2722 411.3337 82.5874 -4.0464 409.2950 413.3414 411.1630 84.1814 -4.0357 409.3584 413.3941 410.9949 85.7798 -4.0235 409.4278 413.4513 410.8200 87.3793 -4.0134 409.5242 413.5376 410.6382 89.0089 -4.0007 409.5918 413.5925 410.4540 90.8140 -3.9897 409.6640 413.6537 410.2533 92.4128 -3.9794 409.7291 413.7085 410.0899 94.0118 -3.9678 409.7895 413.7573 409.9035 95.6258 -3.9539 409.8563 413.8102 409.7204 97.2248 -3.9392 409.9284 413.8676 409.5300 98.8540 -3.9348 409.9673 413.9021 409.3616 100.4528 -3.9218 410.0220 413.9437 409.1809 102.0518 -3.9132 410.0611 413.9743 408.9908 103.6656 -3.9002 410.1089 414.0091 408.7886 105.2795 -3.8883 410.1455 414.0338 408.6142 106.8936 -3.8757 410.1778 414.0535 408.4214 108.4890 -3.8659 410.2219 414.0878 408.2353 110.0950 -3.8618 410.2448 414.1066 408.0572 111.6860 -3.8538 410.2851 414.1389 407.8785 113.2930 -3.8466 410.3069 414.1535 407.7146 114.9025 -3.8362 410.3623 414.1985 407.5164 116.5141 -3.8246 410.3803 414.2048 407.3358 118.1128 -3.8188 410.3889 414.2077 407.1475 119.7118 -3.8103 410.4036 414.2140 406.9592 121.3409 -3.7988 410.4230 414.2218 406.7692 122.9399 -3.7884 410.4480 414.2365 406.5699 124.5536 -3.7769 410.4730 414.2499 406.3781 126.1526 -3.7671 410.4751 414.2422 406.1759 127.7525 -3.7572 410.4757 414.2329 406.0053 129.3816 -3.7490 410.4783 414.2273 405.8148 130.9806 -3.7428 410.4926 414.2354 405.6120 132.5948 -3.7319 410.4871 414.2190 405.4309 134.1945 -3.7255 410.4726 414.1981 405.2490 135.7935 -3.7138 410.4820 414.1958 405.0774 137.4225 -3.7058 410.4889 414.1946 404.8593 139.0213 -3.6927 410.4645 414.1572 404.6843 140.6146 -3.6838 410.4631 414.1469 404.4772 142.2210 -3.6796 410.4463 414.1259 404.2750 143.8131 -3.6709 410.4290 414.1000 404.0697 145.4200 -3.6611 410.3958 414.0569 403.8707 147.0280 -3.6527 410.3931 414.0458 403.6762 148.6248 -3.6435 410.3662 414.0097 403.4714 150.2376 -3.6353 410.3437 413.9790 403.2582 151.8371 -3.6291 410.3215 413.9506 403.0663 153.4516 -3.6168 410.2995 413.9163 402.8339 155.0655 -3.6046 410.2557 413.8603 402.6583 156.6645 -3.5950 410.2439 413.8390 402.4637 158.2785 -3.5912 410.2064 413.7976 402.2619 159.8775 -3.5816 410.1801 413.7617 402.0464 161.4915 -3.5733 410.1286 413.7019 401.8418 163.1055 -3.5651 410.1092 413.6743 401.6681 164.7195 -3.5588 410.0474 413.6062 401.4773 166.3189 -3.5458 410.0216 413.5675 401.2908 167.9184 -3.5339 409.9761 413.5100 401.1000 169.5469 -3.5268 409.9471 413.4740 400.9135 171.1868 -3.5181 409.8706 413.3887 400.7109 172.9635 -3.5074 409.8326 413.3399 400.4927 174.5556 -3.4985 409.7846 413.2831 400.3018 176.1474 -3.4915 409.7093 413.2009 400.1222 177.7715 -3.4837 409.6452 413.1289 399.9053 179.3660 -3.4740 409.6040 413.0780 399.7066 180.9763 -3.4659 409.5354 413.0013 399.5036 182.5734 -3.4578 409.4993 412.9571 399.3041 184.1725 -3.4498 409.4372 412.8870 399.1119 185.7865 -3.4447 409.3792 412.8239 398.9169 187.4005 -3.4373 409.2973 412.7346 398.7162 188.9994 -3.4266 409.2148 412.6415 398.5308 190.5983 -3.4186 409.1647 412.5833 398.3399 192.2121 -3.4132 409.0983 412.5116 398.1485 193.8111 -3.4007 409.0195 412.4202 397.9535 195.4400 -3.3935 408.9529 412.3464 397.7592 197.0388 -3.3865 408.8756 412.2621 397.5803 198.6378 -3.3795 408.8102 412.1897 397.3850 200.2518 -3.3710 408.7238 412.0948 397.1880 201.8514 -3.3656 408.6392 412.0048 397.0091 203.4716 -3.3556 408.5788 411.9344 396.8180 205.0821 -3.3454 408.4858 411.8312 396.6086 206.6733 -3.3349 408.4044 411.7393 396.4210 208.2646 -3.3302 408.3100 411.6402 396.2333 209.8725 -3.3218 408.2442 411.5660 396.0366 211.4961 -3.3126 408.1352 411.4477 395.8260 213.0910 -3.3035 408.0769 411.3804 395.6443 214.6880 -3.3029 407.9751 411.2780 395.4359 216.2868 -3.2947 407.8746 411.1692 395.2394 217.9008 -3.2855 407.7891 411.0747 395.0491 219.5149 -3.2785 407.6807 410.9592 394.8324 221.1309 -3.2719 407.5791 410.8510 394.6460 222.8030 -3.2615 407.4901 410.7515 394.4406 224.5388 -3.2527 407.3859 410.6386 394.2191 226.1378 -3.2488 407.2825 410.5313 394.0428 227.7670 -3.2383 407.1962 410.4346 393.8514 229.3658 -3.2301 407.1134 410.3435 393.6664 230.9796 -3.2251 406.9861 410.2112 393.4708 232.5794 -3.2075 406.8881 410.0956 393.2560 234.1839 -3.2097 406.7870 409.9967 393.0630 235.8126 -3.2063 406.6769 409.8832 392.8486 237.4074 -3.1975 406.5812 409.7787 392.6667 238.9990 -3.1901 406.4631 409.6532 392.4579 240.6055 -3.1813 406.3599 409.5413 392.2546 242.1983 -3.1758 406.2670 409.4429 392.0524 243.8211 -3.1697 406.1413 409.3110 391.8491 245.4163 -3.1661 406.0339 409.2000 391.6647 247.0138 -3.1566 405.9416 409.0981 391.4520 248.6128 -3.1512 405.7956 408.9468 391.2302 250.2268 -3.1427 405.6798 408.8225 391.0407 251.8409 -3.1168 405.5599 408.6767 390.8280 253.4548 -3.1270 405.4534 408.5805 390.6368 255.0538 -3.1219 405.3424 408.4643 390.4257 256.6528 -3.1154 405.2181 408.3335 390.2124 258.2665 -3.1072 405.0720 408.1792 390.0120 259.8814 -3.1015 404.9601 408.0616 389.8149 261.4815 -3.0949 404.8628 407.9577 389.6356 263.0955 -3.0856 404.7390 407.8246 389.4396 264.6949 -3.0794 404.6053 407.6847 389.2209 266.3095 -3.0732 404.4802 407.5535 389.0230 267.9241 -3.0659 404.3349 407.4008 388.8317 269.5329 -3.0587 404.2269 407.2856 388.6256 271.1243 -3.0546 404.1012 407.1558 388.4554 272.7160 -3.0442 403.9815 407.0257 388.2682 274.3226 -3.0378 403.8522 406.8901 388.0513 275.9448 -3.0338 403.7065 406.7403 387.8597 277.5399 -3.0247 403.5899 406.6146 387.6557 279.1378 -3.0156 403.4735 406.4891 387.4699 280.7515 -3.0064 403.3362 406.3426 387.2628 282.3506 -2.9998 403.1908 406.1906 387.0508 283.9795 -2.9983 403.0743 406.0725 386.8468 285.5785 -2.9916 402.9307 405.9223 386.6377 287.1775 -2.9888 402.7895 405.7783 386.4362 288.7915 -2.9796 402.6411 405.6207 386.2241 290.4055 -2.9734 402.5246 405.4980 386.0143 292.0195 -2.9646 402.3806 405.3453 385.8188 293.6185 -2.9575 402.2432 405.2007 385.6077 295.2258 -2.9506 402.1059 405.0565 385.4016 296.8264 -2.9455 401.9549 404.9004 385.1984 298.4268 -2.9418 401.8109 404.7528 384.9817 300.0569 -2.9371 401.6746 404.6117 384.7835 301.6548 -2.9292 401.5356 404.4648 384.5767 303.2466 -2.9239 401.3979 404.3218 384.3889 304.9450 -2.9165 401.2394 404.1559 384.1677 306.6431 -2.9085 401.0891 403.9975 383.9493 308.2513 -2.9041 400.9473 403.8514 383.7643 309.8584 -2.9011 400.7781 403.6792 383.5706 311.4548 -2.8911 400.6302 403.5213 383.3691 313.0526 -2.8829 400.4985 403.3814 383.1689 314.6514 -2.8811 400.3407 403.2218 382.9891 316.2805 -2.8754 400.2174 403.0928 382.7681 317.8795 -2.8658 400.0558 402.9216 382.5771 319.4931 -2.8612 399.8975 402.7587 382.3720 321.0920 -2.8569 399.7448 402.6018 382.1795 322.6908 -2.8505 399.6001 402.4506 381.9836 324.3199 -2.8454 399.4559 402.3013 381.7925 325.9189 -2.8431 399.3060 402.1491 381.5617 327.5328 -2.8362 399.1434 401.9796 381.3466 329.1318 -2.8293 399.0032 401.8325 381.1517 330.7458 -2.8248 398.8321 401.6568 380.9457 332.3599 -2.8206 398.6759 401.4965 380.7339 333.9725 -2.8157 398.5377 401.3535 380.5300 335.5705 -2.8080 398.3815 401.1895 380.3354 337.1695 -2.8026 398.2367 401.0393 380.1146 338.7835 -2.7972 398.0529 400.8501 379.9205 340.3975 -2.7899 397.9029 400.6928 379.7000 342.0115 -2.7856 397.7410 400.5266 379.5050 343.6103 -2.7796 397.5886 400.3682 379.2977 345.2095 -2.7715 397.4390 400.2105 379.0914 346.8129 -2.7652 397.2757 400.0409 378.9014 348.4420 -2.7595 397.0926 399.8521 378.6886 350.0409 -2.7556 396.9472 399.7028 378.4838 351.6548 -2.7465 396.7861 399.5326 378.2816 353.2538 -2.7428 396.6190 399.3618 378.0847 354.8528 -2.7363 396.4549 399.1912 377.8916 356.6131 -2.7271 396.2837 399.0108 377.6644 358.2759 -2.7233 396.1263 398.8496 377.4624 359.8746 -2.7182 395.9638 398.6820 377.2547 361.4886 -2.7114 395.7877 398.4991 377.0635 363.0875 -2.7035 395.6311 398.3347 376.8685 364.7015 -2.6999 395.4611 398.1610 376.6653 366.3155 -2.6915 395.2863 397.9778 376.4730 367.9146 -2.6844 395.1395 397.8238 376.2671 369.5148 -2.6798 394.9615 397.6413 376.0910 371.1300 -2.6770 394.7969 397.4739 375.8847 372.7295 -2.6730 394.6276 397.3007 375.6801 374.3585 -2.6686 394.4708 397.1394 375.4727 375.9573 -2.6638 394.2963 396.9600 375.2663 377.5559 -2.6577 394.1488 396.8066 375.0709 379.1698 -2.6474 393.9684 396.6158 374.8693 380.7839 -2.6438 393.7936 396.4374 374.6718 382.3979 -2.6381 393.6249 396.2630 374.4513 383.9968 -2.6321 393.4534 396.0855 374.2609 385.6111 -2.6265 393.2843 395.9107 374.0520 387.2113 -2.6263 393.1332 395.7595 373.8474 388.8263 -2.6196 392.9558 395.5753 373.6398 390.4415 -2.6118 392.7838 395.3956 373.4423 392.0555 -2.6078 392.6097 395.2176 373.2160 393.6549 -2.6020 392.4259 395.0279 373.0195 395.2550 -2.5984 392.2591 394.8575 372.8217 396.8846 -2.5906 392.0896 394.6802 372.6168 398.4800 -2.5869 391.9224 394.5094 372.4203 400.0703 -2.5802 391.7505 394.3307 372.2231 401.6774 -2.5750 391.5660 394.1410 372.0306 403.2690 -2.5695 391.4027 393.9723 371.8278 404.8915 -2.5670 391.2313 393.7983 371.6137 406.4851 -2.5615 391.0518 393.6133 371.4377 408.0934 -2.5578 390.8839 393.4417 371.2767 409.6869 -2.5567 390.7102 393.2669 371.0513 411.2956 -2.5525 390.5283 393.0808 370.8575 412.9073 -2.5467 390.3604 392.9070 370.6367 414.5184 -2.5435 390.1804 392.7239 370.4328 416.1165 -2.5372 390.0161 392.5533 370.2477 417.7150 -2.5288 389.8366 392.3654 370.0390 419.3284 -2.5301 389.6638 392.1938 369.8379 420.9423 -2.5239 389.4789 392.0028 369.6342 422.5559 -2.5181 389.3131 391.8312 369.4135 424.1549 -2.5159 389.1219 391.6379 369.1929 425.7538 -2.5126 388.9512 391.4638 368.9874 427.3679 -2.5045 388.7732 391.2777 368.7682 428.9819 -2.4992 388.5901 391.0893 368.5778 430.5959 -2.4983 388.4176 390.9159 368.3623 432.1948 -2.4943 388.2287 390.7230 368.1616 433.7938 -2.4908 388.0612 390.5520 367.9449 435.4076 -2.4846 387.8831 390.3677 367.7420 437.0369 -2.4811 387.6856 390.1666 367.5319 438.8159 -2.4762 387.4983 389.9745 367.2876 440.4405 -2.4679 387.3116 389.7795 367.0642 442.0545 -2.4611 387.1349 389.5959 366.8628 443.6543 -2.4553 386.9727 389.4280 366.6587 445.2835 -2.4492 386.7906 389.2399 366.4531 446.8826 -2.4443 386.6019 389.0462 366.2471 448.5119 -2.4349 386.4288 388.8636 366.0405 450.2933 -2.4173 386.2109 388.6281 365.7969 451.8953 -2.4087 386.0418 388.4506 365.5933 453.4941 -2.4188 385.8640 388.2829 365.4090 455.1078 -2.4176 385.6679 388.0856 365.1959 456.7370 -2.4152 385.4887 387.9039 365.0057 458.3358 -2.4133 385.3089 387.7222 364.7948 459.9348 -2.4089 385.1024 387.5113 364.5935 461.5469 -2.4067 384.9347 387.3414 364.3934 463.1396 -2.3986 384.7635 387.1621 364.1817 464.7623 -2.3952 384.5750 386.9702 363.9910 466.3548 -2.3920 384.3850 386.7770 363.8017 467.9475 -2.3834 384.1922 386.5756 363.6029 469.5546 -2.3796 384.0150 386.3947 363.4046 471.1620 -2.3792 383.8479 386.2271 363.2016 472.7708 -2.3710 383.6510 386.0220 363.0221 474.3788 -2.3701 383.4611 385.8312 362.8272 475.9744 -2.3660 383.2770 385.6430 362.6349 477.5728 -2.3618 383.1055 385.4673 362.4369 479.3029 -2.3548 382.9016 385.2564 362.2303 481.0029 -2.3471 382.7142 385.0613 361.9973 482.6018 -2.3454 382.5293 384.8746 361.8012 484.2008 -2.3416 382.3450 384.6866 361.6008 485.8146 -2.3362 382.1477 384.4839 361.3788 487.4285 -2.3305 381.9657 384.2963 361.1782 489.0276 -2.3269 381.7897 384.1166 360.9565 490.6415 -2.3214 381.6049 383.9263 360.7441 492.2405 -2.3173 381.4028 383.7200 360.5603 493.8395 -2.3167 381.2208 383.5376 360.3580 495.4685 -2.3143 381.0462 383.3606 360.1333 497.0675 -2.3079 380.8517 383.1596 359.9338 498.6815 -2.3040 380.6544 382.9583 359.7354 500.4873 -2.2999 380.4595 382.7595 359.4971 502.0865 -2.2935 380.2885 382.5820 359.2958 503.7000 -2.2899 380.0920 382.3820 359.0754 505.3141 -2.2869 379.8929 382.1798 358.8733 506.9128 -2.2811 379.7022 381.9832 358.6777 508.5268 -2.2749 379.5284 381.8033 358.4686 510.1258 -2.2749 379.3342 381.6091 358.2581 511.7399 -2.2677 379.1441 381.4118 358.0443 513.3539 -2.2636 378.9539 381.2175 357.8317 514.9528 -2.2586 378.7740 381.0325 357.6327 516.5666 -2.2530 378.5967 380.8498 357.4410 518.1656 -2.2452 378.4118 380.6571 357.2373 519.7796 -2.2406 378.1948 380.4354 357.0366 521.3935 -2.2378 378.0135 380.2514 356.8169 523.0075 -2.2320 377.8435 380.0756 356.6146 524.6065 -2.2245 377.6475 379.8720 356.4187 526.2050 -2.2215 377.4588 379.6802 356.2157 527.8281 -2.2182 377.2538 379.4720 356.0088 529.4203 -2.2158 377.0542 379.2700 355.8087 531.2114 -2.2103 376.8615 379.0719 355.5823 532.8199 -2.2053 376.6679 378.8733 355.3895 534.4143 -2.2021 376.4894 378.6915 355.1976 536.0276 -2.1941 376.2954 378.4895 354.9631 537.6360 -2.1911 376.1125 378.3036 354.7782 539.2310 -2.1900 375.9119 378.1018 354.5750 540.8266 -2.1835 375.7106 377.8941 354.3680 542.4384 -2.1779 375.5294 377.7072 354.1545 544.0498 -2.1759 375.3489 377.5248 353.9558 545.6475 -2.1717 375.1552 377.3269 353.7411 547.2615 -2.1659 374.9731 377.1390 353.5085 548.8605 -2.1611 374.7747 376.9358 353.3114 550.5329 -2.1576 374.5695 376.7271 353.1083 552.2840 -2.1504 374.3575 376.5079 352.8562 553.8831 -2.1452 374.1694 376.3146 352.6498 555.4970 -2.1405 373.9949 376.1354 352.4455 557.0958 -2.1352 373.8050 375.9402 352.2399 558.6948 -2.1300 373.6063 375.7364 352.0227 560.3089 -2.1245 373.4259 375.5504 351.8216 561.9229 -2.1222 373.2170 375.3391 351.6076 563.5218 -2.1164 373.0299 375.1463 351.4303 565.1358 -2.1133 372.8434 374.9567 351.1898 566.7346 -2.1110 372.6486 374.7595 350.9838 568.3485 -2.1024 372.4624 374.5648 350.7808 569.9626 -2.1017 372.2716 374.3733 350.5658 571.5615 -2.0964 372.0686 374.1650 350.3506 573.1755 -2.0918 371.8654 373.9572 350.1642 574.7745 -2.0869 371.6801 373.7670 349.9572 576.4035 -2.0858 371.4819 373.5677 349.7469 578.0025 -2.0781 371.2838 373.3620 349.5334 579.6165 -2.0727 371.0941 373.1668 349.3386 581.2834 -2.0658 370.8891 372.9549 349.1130 583.0414 -2.0620 370.6965 372.7585 348.8810 584.6399 -2.0597 370.5222 372.5819 348.6824 586.2538 -2.0527 370.3256 372.3783 348.4811 587.8528 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