DTA measure 16.1 Date: 2024109:859 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 810.31 s Mass = 954.500 mg data_number = 1008 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2913 -12.2444 253.4307 265.6751 267.3880 2.0803 -12.0991 253.6157 265.7148 267.3825 2.8993 -11.9459 253.8056 265.7514 267.3647 3.6580 -11.8090 253.9738 265.7828 267.3673 4.5075 -11.6559 254.1705 265.8264 267.3676 5.2960 -11.5174 254.3500 265.8674 267.3614 6.0850 -11.3959 254.5292 265.9251 267.3654 6.9045 -11.2514 254.7157 265.9671 267.3851 7.6940 -11.1100 254.8995 266.0096 267.3828 8.5138 -10.9708 255.0755 266.0464 267.4354 9.3040 -10.8416 255.2482 266.0898 267.4762 10.0965 -10.7120 255.4149 266.1269 267.5260 10.9175 -10.5825 255.5867 266.1693 267.5772 11.6793 -10.4617 255.7447 266.2063 267.6327 12.5305 -10.3288 255.9471 266.2759 267.6897 13.3218 -10.2024 256.1249 266.3273 267.7642 14.1135 -10.0733 256.2792 266.3525 267.8454 14.9355 -9.9552 256.4348 266.3901 267.9285 15.6975 -9.8444 256.6081 266.4525 268.0103 16.5490 -9.7205 256.7761 266.4966 268.1289 17.3113 -9.6118 256.9316 266.5434 268.2319 18.1330 -9.4952 257.0868 266.5820 268.3511 18.9550 -9.3774 257.2543 266.6318 268.5097 19.7165 -9.2735 257.4027 266.6763 268.6343 20.5688 -9.1593 257.5731 266.7324 268.7779 21.3308 -9.0551 257.7048 266.7599 268.9160 22.1528 -8.9490 257.8628 266.8118 269.0660 22.9748 -8.8439 258.0338 266.8777 269.1860 23.7365 -8.7440 258.1543 266.8983 269.3404 24.5888 -8.6344 258.3402 266.9746 269.5134 25.3808 -8.5335 258.4925 267.0260 269.6597 26.1725 -8.4360 258.6242 267.0602 269.8097 26.9948 -8.3385 258.7688 267.1074 269.9796 27.7565 -8.2504 258.9054 267.1558 270.1273 28.6088 -8.1474 259.0642 267.2116 270.2852 29.4008 -8.0562 259.1990 267.2552 270.4443 30.1925 -7.9646 259.3694 267.3341 270.5879 31.0148 -7.8748 259.5043 267.3791 270.7605 31.7765 -7.7935 259.6577 267.4511 270.9159 32.6285 -7.6978 259.7804 267.4782 271.0820 33.3905 -7.6142 259.9061 267.5203 271.2180 34.2125 -7.5283 260.0631 267.5914 271.3808 35.0345 -7.4413 260.1988 267.6401 271.5319 35.7965 -7.3619 260.3345 267.6964 271.6733 36.6485 -7.2728 260.4878 267.7606 271.8282 37.4105 -7.1978 260.6092 267.8070 271.9563 38.2325 -7.1143 260.7410 267.8553 272.0970 39.0545 -7.0379 260.8768 267.9147 272.2501 39.8163 -6.9641 261.0088 267.9729 272.3617 40.6685 -6.8811 261.1502 268.0313 272.5121 41.4305 -6.8121 261.2609 268.0730 272.6526 42.2518 -6.7395 261.4161 268.1555 272.7867 43.0440 -6.6645 261.5444 268.2089 272.9207 43.8355 -6.5842 261.6841 268.2683 273.0497 44.6883 -6.5204 261.8099 268.3303 273.1796 45.4505 -6.4574 261.9404 268.3978 273.2968 46.2735 -6.3867 262.0820 268.4687 273.4205 47.0658 -6.3190 262.2106 268.5296 273.5638 47.8575 -6.2522 262.3325 268.5846 273.6982 48.6798 -6.1859 262.4430 268.6289 273.8185 49.4715 -6.1220 262.5609 268.6828 273.9326 50.2938 -6.0580 262.6971 268.7552 274.0893 51.0858 -5.9974 262.8231 268.8206 274.2163 51.8775 -5.9369 262.9278 268.8647 274.3197 52.7000 -5.8720 263.0658 268.9379 274.4337 53.4925 -5.8156 263.2025 269.0181 274.5677 54.3165 -5.7531 263.3368 269.0899 274.6801 55.1085 -5.6964 263.4494 269.1458 274.7952 55.9015 -5.6437 263.5664 269.2101 274.9132 56.7265 -5.5847 263.6958 269.2805 275.0463 57.4925 -5.5303 263.7911 269.3214 275.1633 58.3438 -5.4685 263.9215 269.3900 275.2778 59.1023 -5.4180 264.0152 269.4332 275.3970 59.9210 -5.3622 264.1471 269.5093 275.5321 60.7093 -5.3116 264.2813 269.5929 275.6286 61.4980 -5.2633 264.3719 269.6352 275.7262 62.3460 -5.2103 264.4987 269.7090 275.8648 63.1040 -5.1642 264.6312 269.7954 276.0008 63.9220 -5.1132 264.7610 269.8742 276.1109 64.7103 -5.0646 264.8735 269.9381 276.2014 65.5000 -5.0176 264.9842 270.0018 276.3234 66.3488 -4.9657 265.1016 270.0673 276.4423 67.1080 -4.9228 265.2083 270.1311 276.5542 67.9268 -4.8755 265.3284 270.2039 276.6686 68.7155 -4.8305 265.4381 270.2687 276.7999 69.5068 -4.7875 265.5465 270.3339 276.9176 70.3555 -4.7412 265.6787 270.4199 277.0544 71.1150 -4.7033 265.7973 270.5006 277.1594 71.9358 -4.6639 265.9177 270.5816 277.2838 72.7265 -4.6188 266.0222 270.6410 277.4181 73.5168 -4.5781 266.1167 270.6949 277.5459 74.3668 -4.5336 266.2397 270.7732 277.6889 75.1278 -4.4945 266.3375 270.8319 277.8044 75.9493 -4.4533 266.4713 270.9247 277.9477 76.7410 -4.4164 266.5637 270.9801 278.0594 77.5325 -4.3796 266.6688 271.0484 278.1918 78.3550 -4.3380 266.7861 271.1241 278.3150 79.1468 -4.3008 266.8836 271.1843 278.4368 79.9690 -4.2656 267.0068 271.2724 278.5808 80.7610 -4.2286 267.1315 271.3601 278.7058 81.5525 -4.1945 267.2395 271.4340 278.8444 82.3750 -4.1576 267.3404 271.4980 278.9757 83.1665 -4.1236 267.4425 271.5661 279.1111 83.9888 -4.0910 267.5651 271.6561 279.2400 84.7808 -4.0579 267.6680 271.7259 279.3758 85.5725 -4.0242 267.7664 271.7905 279.5044 86.3948 -3.9925 267.8883 271.8807 279.6287 87.1565 -3.9609 268.0124 271.9733 279.7493 88.0095 -3.9237 268.1041 272.0279 279.9004 88.8015 -3.8941 268.2323 272.1264 280.0313 89.5935 -3.8658 268.3340 272.1998 280.1453 90.4158 -3.8333 268.4405 272.2739 280.2739 91.1775 -3.8034 268.5424 272.3458 280.3878 92.0295 -3.7756 268.6653 272.4409 280.5185 92.8215 -3.7453 268.7792 272.5245 280.6635 93.6135 -3.7171 268.8696 272.5868 280.7871 94.4355 -3.6881 268.9812 272.6692 280.9086 95.1975 -3.6609 269.0878 272.7488 281.0213 96.0495 -3.6345 269.2174 272.8519 281.1581 96.8415 -3.6075 269.3015 272.9089 281.2919 97.6335 -3.5811 269.4058 272.9869 281.4030 98.4555 -3.5552 269.5250 273.0802 281.5372 99.2475 -3.5260 269.6249 273.1508 281.6771 100.0695 -3.5016 269.7290 273.2306 281.7937 100.8615 -3.4780 269.8575 273.3355 281.9464 101.6533 -3.4528 269.9632 273.4160 282.0827 102.4750 -3.4261 270.0631 273.4892 282.2208 103.2668 -3.4011 270.1582 273.5594 282.3713 104.0888 -3.3792 270.2615 273.6407 282.4986 104.8810 -3.3566 270.3885 273.7451 282.6287 105.6725 -3.3336 270.4877 273.8213 282.7505 106.5248 -3.3111 270.6083 273.9194 282.9093 107.2865 -3.2899 270.7192 274.0091 283.0338 108.1095 -3.2667 270.7994 274.0661 283.1709 108.9018 -3.2451 270.9070 274.1522 283.3116 109.6945 -3.2247 271.0060 274.2307 283.4442 110.5473 -3.2045 271.1396 274.3440 283.6026 111.3095 -3.1861 271.2262 274.4124 283.7209 112.1318 -3.1651 271.3405 274.5055 283.8777 112.9238 -3.1446 271.4251 274.5698 284.0106 113.7155 -3.1231 271.5476 274.6707 284.1446 114.5680 -3.1022 271.6676 274.7698 284.2829 115.3305 -3.0851 271.7654 274.8504 284.4196 116.1525 -3.0638 271.8616 274.9255 284.5651 116.9748 -3.0453 271.9835 275.0288 284.6866 117.7375 -3.0304 272.0804 275.1107 284.8217 118.5900 -3.0136 272.1872 275.2007 284.9610 119.3525 -2.9962 272.2913 275.2875 285.0958 120.1745 -2.9792 272.4065 275.3857 285.2416 120.9968 -2.9597 272.5110 275.4707 285.3791 121.7590 -2.9412 272.6165 275.5577 285.4979 122.6110 -2.9229 272.7342 275.6571 285.6455 123.4015 -2.9103 272.8320 275.7424 285.7979 124.1898 -2.8937 272.9256 275.8193 285.9211 125.0078 -2.8769 273.0437 275.9207 286.0546 125.7653 -2.8617 273.1525 276.0142 286.1795 126.6150 -2.8441 273.2755 276.1196 286.3108 127.3730 -2.8307 273.3705 276.2012 286.4345 128.1910 -2.8138 273.4844 276.2982 286.5510 129.0100 -2.7971 273.5846 276.3817 286.6918 129.7685 -2.7847 273.7101 276.4948 286.8398 130.6170 -2.7683 273.8032 276.5715 286.9601 131.4055 -2.7549 273.9115 276.6664 287.0515 132.1948 -2.7435 274.0239 276.7674 287.1870 133.0138 -2.7267 274.1393 276.8660 287.3173 133.7728 -2.7134 274.2261 276.9395 287.4464 134.6218 -2.6994 274.3248 277.0242 287.5701 135.4103 -2.6890 274.4356 277.1246 287.6868 136.1993 -2.6748 274.5681 277.2429 287.8264 137.0193 -2.6615 274.6690 277.3305 287.9642 137.7795 -2.6495 274.7761 277.4256 288.0852 138.6308 -2.6342 274.8674 277.5016 288.2051 139.4215 -2.6235 274.9864 277.6099 288.3436 140.2125 -2.6148 275.0980 277.7127 288.4527 141.0333 -2.6014 275.1950 277.7964 288.5877 141.7945 -2.5899 275.3042 277.8942 288.7169 142.6470 -2.5771 275.4372 278.0143 288.8600 143.4085 -2.5654 275.5200 278.0854 288.9797 144.2308 -2.5511 275.6321 278.1833 289.0826 145.0228 -2.5409 275.7499 278.2909 289.1953 145.8145 -2.5309 275.8499 278.3808 289.3126 146.6420 -2.5195 275.9423 278.4618 289.4425 147.4043 -2.5084 276.0648 278.5732 289.5622 148.2568 -2.4974 276.1757 278.6731 289.6919 149.0485 -2.4860 276.2942 278.7802 289.8129 149.8405 -2.4767 276.4119 278.8886 289.9340 150.6625 -2.4654 276.5341 278.9995 290.0465 151.4245 -2.4557 276.6285 279.0843 290.1551 152.2765 -2.4449 276.7565 279.2015 290.2905 153.0685 -2.4330 276.8561 279.2891 290.4065 153.8605 -2.4242 276.9652 279.3894 290.5066 154.6825 -2.4157 277.0890 279.5047 290.6666 155.4445 -2.4087 277.1663 279.5750 290.7809 156.2965 -2.3979 277.2836 279.6815 290.9063 157.0585 -2.3884 277.3987 279.7871 291.0192 157.8805 -2.3773 277.5071 279.8844 291.1634 158.7025 -2.3696 277.6085 279.9781 291.3064 159.4643 -2.3614 277.7132 280.0746 291.4257 160.3165 -2.3517 277.8332 280.1849 291.5707 161.0780 -2.3422 277.9557 280.2979 291.7013 161.8998 -2.3380 278.0760 280.4140 291.8442 162.7218 -2.3306 278.1835 280.5141 292.0031 163.4835 -2.3253 278.2801 280.6054 292.1275 164.3358 -2.3147 278.3994 280.7141 292.2794 165.0975 -2.3047 278.5133 280.8180 292.4112 165.9198 -2.2923 278.6167 280.9090 292.5426 166.7118 -2.2859 278.7353 281.0212 292.6741 167.5035 -2.2786 278.8487 281.1273 292.8125 168.3558 -2.2689 278.9667 281.2357 292.9582 169.1175 -2.2606 279.0772 281.3378 293.0964 169.9398 -2.2553 279.1792 281.4345 293.2537 170.7318 -2.2492 279.2861 281.5352 293.3738 171.5235 -2.2417 279.4140 281.6557 293.5196 172.3758 -2.2346 279.5239 281.7584 293.6590 173.1375 -2.2277 279.6404 281.8681 293.7960 173.9598 -2.2200 279.7439 281.9639 293.9300 174.7515 -2.2145 279.8509 282.0653 294.0693 175.5435 -2.2059 279.9727 282.1786 294.2087 176.3955 -2.1987 280.0881 282.2868 294.3331 177.1575 -2.1947 280.1942 282.3890 294.4664 177.9803 -2.1882 280.3311 282.5193 294.6160 178.7725 -2.1841 280.4302 282.6143 294.7282 179.5655 -2.1798 280.5416 282.7214 294.8672 180.4180 -2.1722 280.6731 282.8453 294.9961 181.1805 -2.1638 280.7873 282.9510 295.1402 182.0023 -2.1576 280.8995 283.0571 295.2784 182.7940 -2.1524 281.0043 283.1567 295.3950 183.5855 -2.1473 281.1163 283.2635 295.5246 184.4080 -2.1411 281.2307 283.3718 295.6793 185.1995 -2.1359 281.3553 283.4912 295.7903 186.0225 -2.1297 281.4730 283.6027 295.9320 186.8148 -2.1212 281.5814 283.7026 296.0656 187.6040 -2.1183 281.7107 283.8290 296.1886 188.4230 -2.1107 281.8157 283.9264 296.3157 189.1810 -2.1045 281.9266 284.0311 296.4474 190.0295 -2.0974 282.0424 284.1397 296.5709 190.8170 -2.0943 282.1610 284.2553 296.7011 191.6050 -2.0877 282.2886 284.3763 296.8481 192.4233 -2.0819 282.4052 284.4871 296.9520 193.2110 -2.0775 282.5109 284.5885 297.0882 194.0300 -2.0736 282.6362 284.7097 297.2155 194.8183 -2.0689 282.7422 284.8111 297.3400 195.6070 -2.0651 282.8549 284.9200 297.4657 196.4558 -2.0643 282.9694 285.0338 297.6038 197.2158 -2.0630 283.0847 285.1477 297.7197 198.0358 -2.0586 283.2024 285.2611 297.8493 198.8260 -2.0534 283.3238 285.3772 297.9669 199.6158 -2.0476 283.4456 285.4932 298.0984 200.4648 -2.0427 283.5809 285.6236 298.2303 201.2233 -2.0365 283.6811 285.7176 298.3518 202.0438 -2.0315 283.8054 285.8369 298.4985 202.8350 -2.0276 283.9227 285.9503 298.5954 203.6253 -2.0235 284.0535 286.0771 298.7277 204.4758 -2.0165 284.1680 286.1845 298.8730 205.2375 -2.0139 284.2825 286.2964 298.9762 206.0595 -2.0066 284.3976 286.4042 299.1088 206.8518 -2.0063 284.5056 286.5119 299.2413 207.6435 -2.0004 284.6248 286.6252 299.3664 208.4658 -1.9975 284.7507 286.7482 299.4944 209.2575 -1.9951 284.8750 286.8701 299.6183 210.0795 -1.9887 285.0101 286.9989 299.7547 210.8715 -1.9837 285.1142 287.0979 299.8809 211.6635 -1.9802 285.2057 287.1859 300.0109 212.4855 -1.9772 285.3494 287.3266 300.1259 213.2775 -1.9718 285.4665 287.4383 300.2396 214.0995 -1.9667 285.5921 287.5588 300.3721 214.8915 -1.9622 285.7069 287.6691 300.5106 215.6835 -1.9544 285.8417 287.7962 300.6097 216.5055 -1.9523 285.9643 287.9165 300.7399 217.2970 -1.9495 286.0878 288.0372 300.8616 218.1193 -1.9465 286.1804 288.1269 300.9644 218.9113 -1.9388 286.3073 288.2461 301.0986 219.7033 -1.9345 286.4540 288.3885 301.2212 220.5250 -1.9343 286.5538 288.4881 301.3622 221.3173 -1.9320 286.6703 288.6022 301.4889 222.1388 -1.9268 286.8032 288.7300 301.6130 222.9310 -1.9233 286.9131 288.8364 301.7322 223.7225 -1.9201 287.0394 288.9595 301.8747 224.5750 -1.9135 287.1746 289.0882 302.0144 225.3365 -1.9064 287.2918 289.1981 302.1321 226.1588 -1.9059 287.4242 289.3300 302.2693 226.9508 -1.9028 287.5556 289.4584 302.4000 227.7425 -1.9005 287.6670 289.5675 302.5335 228.5948 -1.8950 287.7969 289.6919 302.6902 229.3565 -1.8932 287.9094 289.8025 302.8153 230.1788 -1.8907 288.0289 289.9196 302.9680 231.0008 -1.8867 288.1516 290.0383 303.1002 231.7625 -1.8810 288.2896 290.1706 303.2286 232.6145 -1.8793 288.3988 290.2781 303.3945 233.3765 -1.8766 288.5185 290.3951 303.5209 234.1985 -1.8740 288.6384 290.5124 303.6686 235.0208 -1.8697 288.7536 290.6233 303.8168 235.7835 -1.8712 288.8744 290.7456 303.9705 236.6355 -1.8691 289.0035 290.8726 304.1046 237.4275 -1.8658 289.1272 290.9930 304.2437 238.2195 -1.8636 289.2637 291.1273 304.3671 239.0415 -1.8611 289.3890 291.2502 304.5164 239.8335 -1.8573 289.5090 291.3663 304.6881 240.6555 -1.8550 289.6234 291.4785 304.8161 241.4475 -1.8549 289.7549 291.6098 304.9423 242.2395 -1.8564 289.8796 291.7360 305.0764 243.0623 -1.8560 290.0090 291.8650 305.2187 243.8545 -1.8519 290.1236 291.9755 305.3698 244.6775 -1.8477 290.2385 292.0862 305.5072 245.4698 -1.8456 290.3870 292.2326 305.6534 246.2625 -1.8445 290.4987 292.3432 305.7877 247.0850 -1.8406 290.6305 292.4711 305.9104 247.8775 -1.8406 290.7672 292.6078 306.0426 248.7005 -1.8360 290.9094 292.7453 306.1648 249.4928 -1.8355 291.0312 292.8667 306.2808 250.2855 -1.8342 291.1411 292.9753 306.4094 251.1073 -1.8338 291.2548 293.0886 306.5284 251.8660 -1.8295 291.3739 293.2035 306.6432 252.7150 -1.8270 291.5054 293.3324 306.7890 253.5030 -1.8250 291.6343 293.4593 306.8863 254.2910 -1.8215 291.7684 293.5899 306.9900 255.1090 -1.8212 291.9007 293.7219 307.1228 255.8670 -1.8181 291.9958 293.8139 307.2198 256.7150 -1.8144 292.1413 293.9557 307.3334 257.5035 -1.8161 292.2451 294.0612 307.4544 258.2920 -1.8158 292.3763 294.1920 307.5716 259.1105 -1.8117 292.5211 294.3328 307.6905 259.8690 -1.8114 292.6594 294.4707 307.8249 260.7180 -1.8097 292.7737 294.5834 307.9531 261.5088 -1.8068 292.8987 294.7055 308.0774 262.3000 -1.8031 292.9956 294.7987 308.1899 263.1183 -1.8051 293.1454 294.9504 308.3071 263.8788 -1.8050 293.2651 295.0701 308.4388 264.7288 -1.8001 293.4110 295.2111 308.5968 265.4895 -1.7992 293.5427 295.3419 308.6908 266.3113 -1.7980 293.6669 295.4649 308.8056 267.1303 -1.7955 293.8028 295.5982 308.9480 267.8910 -1.7948 293.9138 295.7086 309.0633 268.7418 -1.7960 294.0384 295.8344 309.2187 269.5035 -1.7935 294.1519 295.9454 309.3353 270.3255 -1.7876 294.2937 296.0814 309.4660 271.1175 -1.7885 294.4246 296.2131 309.5946 271.9095 -1.7855 294.5562 296.3417 309.7191 272.7615 -1.7863 294.6968 296.4831 309.8809 273.5235 -1.7858 294.8105 296.5964 309.9962 274.3455 -1.7854 294.9434 296.7288 310.1265 275.1375 -1.7851 295.0673 296.8524 310.2428 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