DTA measure 16.2 Date: 2024109:1019 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.15 s Mass = 954.500 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2455 -0.6457 244.8157 245.4614 266.3305 2.0653 -0.6425 244.9535 245.5960 266.3226 2.8240 -0.6386 245.1149 245.7536 266.3472 3.6725 -0.6332 245.2877 245.9209 266.3671 4.4620 -0.6312 245.4312 246.0624 266.3766 5.2535 -0.6269 245.5850 246.2118 266.3981 6.0748 -0.6193 245.7471 246.3665 266.4054 6.8365 -0.6145 245.8994 246.5139 266.4364 7.6883 -0.6099 246.0429 246.6527 266.4646 8.4495 -0.6092 246.1857 246.7948 266.5192 9.2715 -0.6056 246.3560 246.9616 266.5479 10.0935 -0.5998 246.5211 247.1209 266.5910 10.8553 -0.5967 246.6702 247.2669 266.6226 11.7075 -0.5932 246.8115 247.4047 266.6729 12.4690 -0.5890 246.9581 247.5471 266.7282 13.2910 -0.5815 247.1080 247.6895 266.8019 14.0830 -0.5791 247.2709 247.8500 266.8757 14.8745 -0.5768 247.4277 248.0045 266.9558 15.7268 -0.5706 247.5657 248.1362 267.0506 16.4885 -0.5686 247.7057 248.2743 267.1282 17.3108 -0.5660 247.8710 248.4370 267.2159 18.1028 -0.5605 248.0263 248.5867 267.3278 18.8945 -0.5553 248.1729 248.7282 267.4242 19.7473 -0.5544 248.3288 248.8833 267.5359 20.5095 -0.5526 248.4749 249.0274 267.6383 21.3318 -0.5469 248.6178 249.1647 267.7567 22.1238 -0.5451 248.7661 249.3112 267.8917 22.9248 -0.5411 248.9278 249.4689 268.0114 23.7468 -0.5371 249.0675 249.6047 268.1286 24.5085 -0.5375 249.2039 249.7414 268.2461 25.3608 -0.5327 249.3788 249.9115 268.4018 26.1225 -0.5305 249.5068 250.0373 268.5265 26.9445 -0.5285 249.6545 250.1830 268.6728 27.7665 -0.5234 249.8021 250.3255 268.8332 28.5285 -0.5222 249.9434 250.4656 268.9496 29.3805 -0.5190 250.0999 250.6189 269.1092 30.1425 -0.5170 250.2351 250.7521 269.2152 30.9645 -0.5145 250.4029 250.9174 269.3471 31.7565 -0.5152 250.5330 251.0482 269.4659 32.5485 -0.5155 250.6858 251.2013 269.5963 33.4003 -0.5096 250.8208 251.3304 269.7367 34.1625 -0.5075 250.9578 251.4652 269.8578 34.9843 -0.5071 251.1229 251.6300 269.9844 35.7760 -0.5065 251.2621 251.7685 270.1062 36.5675 -0.5062 251.3960 251.9022 270.2180 37.4200 -0.5043 251.5613 252.0656 270.3437 38.1815 -0.5040 251.6955 252.1996 270.4601 39.0038 -0.5022 251.8392 252.3414 270.5804 39.7958 -0.4993 251.9940 252.4933 270.6942 40.5875 -0.4978 252.1323 252.6301 270.7971 41.4398 -0.4975 252.2931 252.7906 270.9118 42.2015 -0.4957 252.4167 252.9123 271.0001 43.0250 -0.4962 252.5581 253.0543 271.1266 43.8198 -0.4938 252.7000 253.1938 271.2387 44.6115 -0.4940 252.8547 253.3487 271.3407 45.4340 -0.4950 252.9943 253.4894 271.4370 46.2265 -0.4932 253.1214 253.6146 271.5412 47.0495 -0.4944 253.2756 253.7700 271.6484 47.8415 -0.4941 253.4161 253.9101 271.7333 48.6335 -0.4917 253.5714 254.0631 271.8524 49.4555 -0.4900 253.7140 254.2040 271.9476 50.2475 -0.4888 253.8473 254.3362 272.0401 51.0693 -0.4922 254.0083 254.5004 272.1460 51.8580 -0.4935 254.1478 254.6413 272.2418 52.6470 -0.4941 254.2735 254.7676 272.3515 53.4650 -0.4919 254.4176 254.9096 272.4479 54.2530 -0.4920 254.5605 255.0525 272.5603 55.0710 -0.4914 254.6798 255.1712 272.6714 55.8590 -0.4918 254.8324 255.3242 272.7630 56.6468 -0.4906 254.9785 255.4690 272.8642 57.4955 -0.4913 255.1309 255.6222 272.9714 58.2540 -0.4908 255.2650 255.7558 273.0743 59.0728 -0.4866 255.4131 255.8997 273.1654 59.8913 -0.4884 255.5523 256.0407 273.2769 60.6510 -0.4894 255.6891 256.1786 273.3724 61.4995 -0.4904 255.8387 256.3291 273.4613 62.2590 -0.4912 255.9531 256.4443 273.5681 63.0775 -0.4929 256.1104 256.6033 273.6668 63.8995 -0.4921 256.2503 256.7425 273.7840 64.6595 -0.4906 256.3869 256.8775 273.8696 65.5105 -0.4908 256.5270 257.0179 273.9586 66.2725 -0.4922 256.6503 257.1425 274.0599 67.0945 -0.4915 256.8132 257.3047 274.1606 67.8865 -0.4915 256.9360 257.4275 274.2722 68.6768 -0.4946 257.0743 257.5689 274.3550 69.5283 -0.4927 257.2215 257.7142 274.4638 70.2900 -0.4937 257.3520 257.8457 274.5665 71.1118 -0.4931 257.4883 257.9814 274.6693 71.9038 -0.4951 257.6212 258.1163 274.7598 72.6955 -0.4940 257.7613 258.2553 274.8665 73.5478 -0.4953 257.9174 258.4127 274.9711 74.3095 -0.4957 258.0476 258.5433 275.0851 75.1318 -0.4967 258.1895 258.6861 275.1715 75.9240 -0.5028 258.3271 258.8298 275.2917 76.7165 -0.5028 258.4691 258.9719 275.3766 77.5688 -0.5018 258.5954 259.0972 275.5041 78.3305 -0.5034 258.7218 259.2253 275.6044 79.1528 -0.5047 258.8612 259.3659 275.7292 79.9448 -0.5057 259.0017 259.5074 275.8335 80.7365 -0.5040 259.1276 259.6315 275.9548 81.5888 -0.5081 259.3028 259.8109 276.0737 82.3505 -0.5109 259.4224 259.9334 276.1730 83.1728 -0.5121 259.5532 260.0652 276.2915 83.9645 -0.5135 259.6762 260.1897 276.4146 84.7565 -0.5142 259.8286 260.3428 276.5412 85.6085 -0.5148 259.9708 260.4856 276.6745 86.3705 -0.5146 260.1028 260.6174 276.7867 87.1925 -0.5161 260.2326 260.7487 276.9098 87.9845 -0.5170 260.3863 260.9033 277.0240 88.7765 -0.5167 260.5169 261.0337 277.1254 89.5985 -0.5209 260.6490 261.1699 277.2439 90.3905 -0.5201 260.7761 261.2962 277.3783 91.2125 -0.5201 260.9253 261.4454 277.4904 92.0045 -0.5215 261.0592 261.5807 277.5790 92.7960 -0.5232 261.1865 261.7097 277.6784 93.6183 -0.5256 261.3142 261.8397 277.8067 94.4100 -0.5268 261.4310 261.9577 277.8987 95.2318 -0.5285 261.5751 262.1036 277.9990 96.0240 -0.5296 261.7202 262.2498 278.1113 96.8155 -0.5306 261.8620 262.3926 278.2171 97.6380 -0.5334 261.9826 262.5160 278.3218 98.4295 -0.5341 262.1130 262.6471 278.4179 99.2518 -0.5364 262.2659 262.8023 278.5181 100.0438 -0.5368 262.3846 262.9214 278.6271 100.8365 -0.5387 262.5088 263.0474 278.7217 101.6588 -0.5403 262.6515 263.1918 278.8062 102.4505 -0.5415 262.7880 263.3295 278.9357 103.2728 -0.5425 262.9321 263.4746 279.0333 104.0648 -0.5476 263.0531 263.6007 279.1117 104.8565 -0.5476 263.1773 263.7250 279.2023 105.6785 -0.5494 263.3184 263.8678 279.3047 106.4705 -0.5509 263.4621 264.0130 279.4071 107.2935 -0.5538 263.5870 264.1408 279.5073 108.0855 -0.5553 263.7163 264.2716 279.6077 108.8785 -0.5574 263.8436 264.4010 279.7030 109.7005 -0.5577 263.9811 264.5387 279.8106 110.4925 -0.5592 264.1189 264.6780 279.9106 111.3145 -0.5598 264.2530 264.8128 279.9829 112.1065 -0.5649 264.3772 264.9421 280.0839 112.8998 -0.5657 264.5089 265.0746 280.1885 113.7228 -0.5677 264.6566 265.2243 280.2881 114.5153 -0.5698 264.7860 265.3558 280.3791 115.3375 -0.5795 264.9153 265.4948 280.4799 116.1295 -0.5839 265.0461 265.6300 280.5937 116.9180 -0.5881 265.1621 265.7502 280.7005 117.7368 -0.5875 265.2979 265.8853 280.8201 118.5240 -0.5897 265.4257 266.0154 280.9219 119.3428 -0.5908 265.5759 266.1667 281.0327 120.1303 -0.5936 265.7088 266.3024 281.1395 120.9185 -0.5952 265.8231 266.4183 281.2643 121.7368 -0.6022 265.9520 266.5542 281.3775 122.5245 -0.6054 266.0918 266.6972 281.4737 123.3423 -0.6060 266.2160 266.8220 281.5862 124.1308 -0.6063 266.3451 266.9514 281.7080 124.9228 -0.6085 266.4675 267.0760 281.8380 125.7455 -0.6105 266.5882 267.1987 281.9504 126.5353 -0.6140 266.7366 267.3506 282.0544 127.3540 -0.6160 266.8499 267.4659 282.1732 128.1433 -0.6167 266.9719 267.5886 282.2940 128.9325 -0.6170 267.1113 267.7283 282.4089 129.7820 -0.6197 267.2473 267.8670 282.5231 130.5423 -0.6244 267.3723 267.9967 282.6335 131.3638 -0.6270 267.5094 268.1365 282.7481 132.1558 -0.6277 267.6472 268.2749 282.8694 132.9468 -0.6284 267.7763 268.4046 282.9953 133.7978 -0.6332 267.9129 268.5461 283.1056 134.5578 -0.6345 268.0231 268.6576 283.2173 135.3908 -0.6356 268.1496 268.7852 283.3584 136.1555 -0.6384 268.2825 268.9209 283.4621 136.9778 -0.6407 268.4308 269.0715 283.5780 137.7998 -0.6383 268.5584 269.1967 283.6868 138.5615 -0.6402 268.6850 269.3252 283.7831 139.4135 -0.6453 268.8226 269.4679 283.8938 140.2058 -0.6454 268.9369 269.5823 283.9876 140.9975 -0.6487 269.0826 269.7313 284.1016 141.8195 -0.6524 269.1943 269.8467 284.1993 142.6115 -0.6536 269.3119 269.9655 284.2948 143.4335 -0.6546 269.4476 270.1021 284.4012 144.2255 -0.6569 269.5614 270.2183 284.5042 145.0175 -0.6603 269.6882 270.3485 284.5919 145.8395 -0.6598 269.8494 270.5092 284.6818 146.6315 -0.6641 269.9648 270.6289 284.7719 147.4535 -0.6679 270.0941 270.7620 284.8667 148.2455 -0.6684 270.2214 270.8898 284.9576 149.0375 -0.6711 270.3522 271.0233 285.0407 149.8595 -0.6743 270.4856 271.1599 285.1517 150.6515 -0.6763 270.6069 271.2832 285.2431 151.4735 -0.6758 270.7256 271.4014 285.3634 152.2653 -0.6790 270.8575 271.5365 285.4494 153.0565 -0.6837 270.9759 271.6596 285.5224 153.8788 -0.6867 271.1259 271.8126 285.6365 154.6708 -0.6885 271.2517 271.9402 285.7391 155.4928 -0.6912 271.3877 272.0789 285.8343 156.2850 -0.6906 271.4962 272.1869 285.9328 157.0765 -0.6955 271.6112 272.3066 286.0509 157.8988 -0.6984 271.7388 272.4371 286.1586 158.6905 -0.6994 271.8674 272.5668 286.2498 159.5128 -0.7025 271.9915 272.6939 286.3683 160.3048 -0.7064 272.1248 272.8313 286.5002 161.0965 -0.7100 272.2620 272.9720 286.6207 161.9188 -0.7124 272.3931 273.1056 286.7218 162.7105 -0.7151 272.5038 273.2189 286.8268 163.5328 -0.7151 272.6253 273.3404 286.9429 164.3245 -0.7166 272.7552 273.4718 287.0642 165.1165 -0.7161 272.8890 273.6051 287.1750 165.9385 -0.7227 273.0032 273.7259 287.2971 166.7305 -0.7141 273.1396 273.8537 287.3966 167.5533 -0.7135 273.2621 273.9756 287.5204 168.3455 -0.7155 273.3881 274.1036 287.6339 169.1375 -0.7194 273.5139 274.2333 287.7418 169.9595 -0.7218 273.6447 274.3665 287.8573 170.7215 -0.7236 273.7732 274.4968 287.9637 171.5735 -0.7252 273.8923 274.6175 288.0908 172.3655 -0.7290 274.0284 274.7575 288.2015 173.1573 -0.7324 274.1423 274.8747 288.3103 173.9790 -0.7319 274.2738 275.0057 288.4204 174.7405 -0.7346 274.3985 275.1330 288.5116 175.5930 -0.7396 274.5464 275.2860 288.6330 176.3848 -0.7407 274.6715 275.4123 288.7440 177.1765 -0.7430 274.7805 275.5235 288.8539 177.9988 -0.7432 274.9050 275.6481 288.9792 178.7605 -0.7480 275.0267 275.7746 289.0962 179.6133 -0.7511 275.1486 275.8997 289.1992 180.4043 -0.7514 275.2856 276.0370 289.2978 181.1930 -0.7559 275.3954 276.1513 289.4127 182.0110 -0.7595 275.5265 276.2860 289.5131 182.7690 -0.7597 275.6391 276.3988 289.6136 183.6170 -0.7630 275.7988 276.5618 289.7243 184.3750 -0.7658 275.9190 276.6848 289.8231 185.1940 -0.7669 276.0354 276.8023 289.9459 186.0120 -0.7715 276.1504 276.9219 290.0582 186.7700 -0.7736 276.2709 277.0445 290.1480 187.6180 -0.7736 276.3933 277.1669 290.2601 188.4060 -0.7774 276.5163 277.2937 290.3900 189.1940 -0.7796 276.6467 277.4264 290.4948 190.0120 -0.7840 276.7820 277.5660 290.5920 190.8000 -0.7856 276.9015 277.6871 290.6826 191.6198 -0.7883 277.0302 277.8185 290.7825 192.4093 -0.7889 277.1548 277.9437 290.8679 193.1988 -0.7922 277.2601 278.0523 290.9575 194.0180 -0.7931 277.3814 278.1745 291.0495 194.8078 -0.7970 277.5205 278.3175 291.1314 195.6275 -0.8024 277.6554 278.4578 291.2467 196.4188 -0.8048 277.7653 278.5701 291.3151 197.2093 -0.8070 277.8894 278.6964 291.4019 198.0305 -0.8082 278.0240 278.8322 291.5079 198.8225 -0.8093 278.1616 278.9709 291.5984 199.6448 -0.8125 278.2807 279.0932 291.6707 200.4358 -0.8147 278.4116 279.2263 291.7787 201.2275 -0.8164 278.5329 279.3493 291.8701 202.0495 -0.8202 278.6480 279.4682 291.9791 202.8415 -0.8225 278.7726 279.5950 292.0772 203.6635 -0.8232 278.8937 279.7170 292.2023 204.4555 -0.8265 279.0155 279.8420 292.2956 205.2475 -0.8293 279.1439 279.9732 292.3781 206.0695 -0.8310 279.2748 280.1058 292.4843 206.8615 -0.8329 279.3940 280.2270 292.5745 207.6835 -0.8373 279.5255 280.3628 292.6842 208.4760 -0.8396 279.6308 280.4703 292.7765 209.2685 -0.8415 279.7505 280.5920 292.8826 210.0903 -0.8445 279.8629 280.7074 292.9963 210.8818 -0.8469 279.9946 280.8415 293.0875 211.7040 -0.8485 280.1155 280.9640 293.2035 212.4963 -0.8515 280.2308 281.0823 293.3214 213.2875 -0.8551 280.3531 281.2082 293.4029 214.1100 -0.8591 280.4821 281.3411 293.5003 214.9015 -0.8622 280.6026 281.4647 293.6190 215.7238 -0.8649 280.7254 281.5903 293.7282 216.5158 -0.8633 280.8602 281.7235 293.8148 217.3075 -0.8670 280.9840 281.8510 293.9098 218.1598 -0.8688 281.1146 281.9834 294.0344 218.9215 -0.8719 281.2261 282.0980 294.1303 219.7438 -0.8753 281.3457 282.2210 294.2462 220.5358 -0.8783 281.4663 282.3446 294.3426 221.3275 -0.8812 281.5918 282.4730 294.4557 222.1495 -0.8806 281.7035 282.5841 294.5656 222.9415 -0.8840 281.8213 282.7053 294.6774 223.7635 -0.8862 281.9400 282.8262 294.7663 224.5555 -0.8899 282.0703 282.9602 294.8845 225.3475 -0.8948 282.2145 283.1093 294.9918 226.1995 -0.8950 282.3380 283.2330 295.0995 226.9615 -0.8991 282.4491 283.3482 295.1968 227.7835 -0.9009 282.5687 283.4695 295.3191 228.5755 -0.9021 282.6834 283.5855 295.4402 229.3685 -0.9049 282.7960 283.7008 295.5436 230.1905 -0.9074 282.9202 283.8276 295.6744 230.9825 -0.9118 283.0557 283.9674 295.7936 231.8043 -0.9126 283.1725 284.0851 295.9285 232.5960 -0.9120 283.2888 284.2008 296.0406 233.3885 -0.9183 283.4230 284.3413 296.1809 234.2110 -0.9208 283.5354 284.4562 296.3004 235.0328 -0.9253 283.6457 284.5710 296.4175 235.8245 -0.9286 283.7729 284.7015 296.5361 236.6468 -0.9286 283.8888 284.8174 296.6579 237.4385 -0.9324 284.0113 284.9436 296.7767 238.2608 -0.9348 284.1340 285.0687 296.8707 239.0528 -0.9361 284.2699 285.2060 296.9862 239.8445 -0.9393 284.3867 285.3261 297.0818 240.6670 -0.9416 284.5038 285.4455 297.1805 241.4595 -0.9443 284.6103 285.5546 297.2830 242.2818 -0.9483 284.7456 285.6939 297.4008 243.0735 -0.9483 284.8558 285.8041 297.4908 243.8655 -0.9534 284.9650 285.9185 297.5986 244.6850 -0.9564 285.1110 286.0674 297.7030 245.4430 -0.9577 285.2275 286.1852 297.7957 246.2910 -0.9605 285.3363 286.2968 297.9034 247.0790 -0.9638 285.4528 286.4166 298.0000 247.8670 -0.9655 285.5907 286.5562 298.1140 248.6853 -0.9667 285.7037 286.6704 298.2112 249.4440 -0.9716 285.8117 286.7833 298.3039 250.2920 -0.9720 285.9415 286.9135 298.4017 251.0800 -0.9733 286.0633 287.0367 298.4988 251.8680 -0.9770 286.1793 287.1563 298.5997 252.6863 -0.9760 286.3128 287.2888 298.6930 253.4750 -0.9795 286.4093 287.3888 298.7911 254.2938 -0.9820 286.5337 287.5157 298.8829 255.0820 -0.9865 286.6492 287.6356 298.9856 255.8715 -0.9899 286.7837 287.7737 299.0967 256.6908 -0.9921 286.9037 287.8958 299.1785 257.4818 -0.9953 287.0257 288.0210 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