DTA measure 26.1 Date: 2024109:929 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.18 s Mass = 954.500 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3595 -4.1009 420.9537 425.0545 423.9768 3.9585 -4.1012 421.2142 425.3154 423.9649 5.5730 -4.1045 421.4762 425.5808 423.9536 7.1725 -4.1080 421.7216 425.8297 423.9184 8.8015 -4.1068 421.9887 426.0955 423.8285 10.4016 -4.1090 422.2518 426.3608 423.7322 12.0011 -4.1098 422.4960 426.6058 423.5914 13.6148 -4.1112 422.7300 426.8412 423.4586 15.2143 -4.1143 422.9736 427.0879 423.2818 16.8243 -4.1136 423.2278 427.3414 423.0836 18.4313 -4.1144 423.4675 427.5819 422.8596 20.0221 -4.1164 423.6811 427.7976 422.6480 21.6144 -4.1180 423.9041 428.0221 422.4122 23.2224 -4.1212 424.1500 428.2712 422.1833 24.8314 -4.1232 424.3805 428.5037 421.9427 26.4381 -4.1212 424.5935 428.7147 421.7052 28.0335 -4.1239 424.8085 428.9324 421.4593 29.6301 -4.1274 425.0107 429.1381 421.2389 31.2288 -4.1278 425.2092 429.3370 421.0266 32.8556 -4.1263 425.4241 429.5504 420.8126 34.4533 -4.1283 425.6197 429.7480 420.6243 36.0516 -4.1336 425.8218 429.9554 420.4546 37.6505 -4.1330 426.0157 430.1487 420.2730 39.2645 -4.1350 426.1956 430.3306 420.0996 40.8635 -4.1401 426.3676 430.5077 419.9190 42.4925 -4.1397 426.5520 430.6917 419.7348 44.0921 -4.1418 426.7283 430.8701 419.5387 45.7005 -4.1466 426.8916 431.0382 419.3425 47.2994 -4.1476 427.0626 431.2102 419.1714 48.9133 -4.1498 427.2270 431.3768 419.0031 50.5121 -4.1523 427.3838 431.5362 418.8247 52.1409 -4.1554 427.5316 431.6870 418.6458 53.7396 -4.1580 427.6762 431.8342 418.4654 55.3386 -4.1592 427.8228 431.9821 418.2774 56.9526 -4.1645 427.9676 432.1321 418.0685 58.5516 -4.1696 428.1099 432.2795 417.8719 60.1808 -4.1722 428.2584 432.4307 417.6852 61.7806 -4.1739 428.3922 432.5661 417.4974 63.3950 -4.1755 428.4938 432.6693 417.3035 64.9945 -4.1808 428.6195 432.8004 417.1174 66.6085 -4.1840 428.7415 432.9256 416.9062 68.2234 -4.1876 428.8570 433.0446 416.7208 69.8376 -4.1918 428.9595 433.1513 416.5298 71.4375 -4.1944 429.0669 433.2613 416.3114 73.0373 -4.1989 429.1730 433.3719 416.1203 74.6674 -4.2051 429.2741 433.4792 415.9085 76.2676 -4.2075 429.3660 433.5735 415.7049 77.8829 -4.2093 429.4598 433.6691 415.4834 79.4829 -4.2145 429.5548 433.7693 415.3009 81.0784 -4.2194 429.6348 433.8542 415.1011 82.6859 -4.2190 429.7195 433.9386 414.8868 84.2931 -4.2222 429.7993 434.0215 414.7074 85.8850 -4.2294 429.8677 434.0971 414.5215 87.4768 -4.2315 429.9326 434.1641 414.3422 89.0850 -4.2369 429.9884 434.2253 414.1497 90.6805 -4.2410 430.0565 434.2975 413.9597 92.3048 -4.2519 430.1295 434.3814 413.7781 93.8980 -4.2631 430.1734 434.4364 413.5993 95.4983 -4.2630 430.2171 434.4801 413.3929 97.1011 -4.2571 430.2757 434.5328 413.2002 98.6988 -4.2631 430.3087 434.5718 412.9991 100.3118 -4.2691 430.3371 434.6063 412.8055 101.9255 -4.2719 430.4008 434.6727 412.6043 103.5245 -4.2769 430.4381 434.7149 412.4001 105.1235 -4.2817 430.4681 434.7498 412.2099 106.7370 -4.2880 430.5112 434.7993 412.0198 108.3359 -4.2927 430.5261 434.8188 411.8254 109.9349 -4.2973 430.5540 434.8513 411.6442 111.5638 -4.3048 430.5758 434.8806 411.4452 113.1626 -4.3092 430.5947 434.9039 411.2615 114.7616 -4.3176 430.5950 434.9126 411.0692 116.3756 -4.3227 430.6141 434.9368 410.8718 117.9746 -4.3301 430.6212 434.9513 410.6723 119.5886 -4.3320 430.6402 434.9721 410.4967 121.2035 -4.3331 430.6278 434.9609 410.2907 122.8025 -4.3379 430.6229 434.9608 410.0800 124.4165 -4.3442 430.6171 434.9613 409.8486 126.0155 -4.3456 430.6335 434.9791 409.6477 127.6294 -4.3517 430.6125 434.9642 409.4654 129.2433 -4.3578 430.6043 434.9620 409.2515 130.8570 -4.3625 430.5963 434.9587 409.0511 132.4560 -4.3658 430.5725 434.9383 408.8857 134.0563 -4.3716 430.5600 434.9316 408.6804 135.6864 -4.3721 430.5244 434.8965 408.4741 137.3008 -4.3736 430.5013 434.8749 408.2944 138.8996 -4.3812 430.4728 434.8539 408.1068 140.4986 -4.3860 430.4444 434.8304 407.8967 142.1133 -4.3910 430.4249 434.8159 407.7018 143.7425 -4.3937 430.3848 434.7785 407.5071 145.3398 -4.4006 430.3607 434.7612 407.3105 146.9318 -4.4000 430.3288 434.7288 407.1014 148.5390 -4.4075 430.2745 434.6820 406.9033 150.1306 -4.4107 430.2313 434.6420 406.7143 151.7536 -4.4110 430.1895 434.6005 406.5152 153.3464 -4.4146 430.1405 434.5550 406.3162 154.9394 -4.4162 430.0888 434.5050 406.1281 156.5488 -4.4179 430.0437 434.4616 405.9319 158.1566 -4.4216 429.9744 434.3960 405.7305 159.7660 -4.4265 429.9221 434.3486 405.5258 161.3611 -4.4297 429.8783 434.3081 405.3374 162.9604 -4.4334 429.8269 434.2603 405.1543 164.5749 -4.4361 429.7692 434.2054 404.9636 166.1739 -4.4399 429.6890 434.1289 404.7513 167.7879 -4.4405 429.6177 434.0582 404.5544 169.3868 -4.4457 429.5505 433.9962 404.3388 171.0006 -4.4470 429.4858 433.9328 404.1073 172.5996 -4.4490 429.4159 433.8649 403.8829 174.1986 -4.4519 429.3422 433.7941 403.6845 175.8126 -4.4541 429.2581 433.7122 403.4528 177.4268 -4.4556 429.1859 433.6415 403.2417 179.0255 -4.4602 429.1177 433.5778 403.0324 180.6395 -4.4618 429.0289 433.4908 402.8120 182.2385 -4.4635 428.9471 433.4106 402.6082 183.8375 -4.4643 428.8617 433.3260 402.4036 185.4665 -4.4680 428.7918 433.2598 402.1935 187.0654 -4.4689 428.6767 433.1457 401.9797 188.6640 -4.4700 428.5952 433.0652 401.7709 190.2778 -4.4712 428.5263 432.9974 401.5770 191.8768 -4.4712 428.4139 432.8851 401.3836 193.5064 -4.4737 428.3181 432.7918 401.1714 195.1068 -4.4757 428.2116 432.6873 400.9961 196.7220 -4.4776 428.1187 432.5963 400.8065 198.3216 -4.4770 428.0347 432.5117 400.5976 199.9356 -4.4775 427.9249 432.4023 400.4096 201.5505 -4.4778 427.8197 432.2975 400.2085 203.1505 -4.4812 427.7111 432.1923 400.0094 204.7645 -4.4793 427.6024 432.0817 399.8292 206.3635 -4.4813 427.5095 431.9907 399.6555 207.9924 -4.4801 427.3943 431.8744 399.4292 209.6036 -4.4822 427.2680 431.7502 399.2218 211.1946 -4.4822 427.1826 431.6649 399.0190 212.7854 -4.4817 427.0566 431.5383 398.8248 214.3923 -4.4815 426.9517 431.4333 398.6149 215.9994 -4.4833 426.8417 431.3250 398.4093 217.6078 -4.4832 426.7191 431.2023 398.1972 219.2016 -4.4830 426.5976 431.0807 397.9985 220.8094 -4.4856 426.4916 430.9772 397.7882 222.4028 -4.4871 426.3741 430.8612 397.5706 224.0141 -4.4848 426.2483 430.7331 397.3715 225.6268 -4.4883 426.1451 430.6334 397.1679 227.2256 -4.4883 426.0134 430.5017 396.9642 228.8246 -4.4837 425.8820 430.3658 396.7652 230.4238 -4.4864 425.7515 430.2379 396.5626 232.0376 -4.4862 425.6293 430.1155 396.3591 233.6516 -4.4843 425.5149 429.9992 396.1551 235.2506 -4.4837 425.3780 429.8617 395.9591 236.8495 -4.4849 425.2573 429.7421 395.7765 238.4635 -4.4841 425.1098 429.5939 395.5961 240.0625 -4.4796 424.9739 429.4534 395.3840 241.6765 -4.4783 424.8341 429.3124 395.1794 243.2905 -4.4768 424.7035 429.1803 394.9940 244.8895 -4.4775 424.5750 429.0526 394.7575 246.4883 -4.4770 424.4332 428.9102 394.5371 248.1068 -4.4736 424.2994 428.7731 394.3311 249.7081 -4.4735 424.1601 428.6336 394.1181 251.3076 -4.4704 424.0378 428.5082 393.9030 252.9369 -4.4709 423.8812 428.3522 393.6872 254.5356 -4.4703 423.7472 428.2175 393.4713 256.1346 -4.4683 423.6014 428.0698 393.2668 257.7486 -4.4659 423.4640 427.9299 393.0483 259.3475 -4.4641 423.3194 427.7836 392.8281 260.9765 -4.4633 423.1682 427.6315 392.6236 262.5768 -4.4622 423.0179 427.4801 392.4197 264.1765 -4.4590 422.8709 427.3299 392.2076 265.7905 -4.4573 422.7361 427.1934 391.9964 267.4044 -4.4540 422.5783 427.0324 391.8020 269.0190 -4.4533 422.4203 426.8736 391.5862 270.6178 -4.4505 422.2803 426.7308 391.3911 272.2320 -4.4473 422.1243 426.5716 391.1862 273.8273 -4.4449 421.9698 426.4147 391.0103 275.4331 -4.4427 421.8249 426.2676 390.8027 277.0390 -4.4396 421.6818 426.1213 390.6077 278.6306 -4.4395 421.5193 425.9587 390.4097 280.2395 -4.4384 421.3610 425.7994 390.2129 281.8339 -4.4347 421.1971 425.6318 390.0186 283.4428 -4.4340 421.0531 425.4871 389.8261 285.0513 -4.4329 420.8938 425.3267 389.6523 286.6613 -4.4297 420.7452 425.1748 389.4432 288.2573 -4.4291 420.5921 425.0213 389.2529 289.8540 -4.4248 420.4369 424.8617 389.0395 291.4805 -4.4273 420.2556 424.6830 388.8284 293.0796 -4.4238 420.0849 424.5087 388.6097 294.6786 -4.4183 419.9442 424.3625 388.3969 296.2925 -4.4134 419.7852 424.1986 388.1719 297.8915 -4.4108 419.6042 424.0150 387.9765 299.4905 -4.4066 419.4651 423.8717 387.7558 301.1195 -4.4040 419.3080 423.7121 387.5357 302.7184 -4.4010 419.1381 423.5392 387.3404 304.3171 -4.3990 418.9541 423.3531 387.1145 305.9158 -4.3943 418.8046 423.1989 386.9034 307.5299 -4.3910 418.6410 423.0320 386.6910 309.1438 -4.3897 418.4698 422.8594 386.4901 310.7428 -4.3861 418.2981 422.6842 386.2659 312.3569 -4.3835 418.1315 422.5150 386.0700 313.9566 -4.3826 417.9601 422.3427 385.8480 315.5556 -4.3791 417.7991 422.1782 385.6179 317.1846 -4.3775 417.6246 422.0020 385.4285 318.7845 -4.3722 417.4739 421.8461 385.2337 320.3985 -4.3673 417.2926 421.6598 385.0094 321.9975 -4.3644 417.1151 421.4796 384.8133 323.5965 -4.3629 416.9395 421.3024 384.6069 325.2255 -4.3592 416.7799 421.1391 384.4047 326.8245 -4.3566 416.6046 420.9613 384.2055 328.4380 -4.3505 416.4251 420.7756 383.9986 330.0390 -4.3498 416.2542 420.6040 383.7829 331.6516 -4.3437 416.0946 420.4383 383.6049 333.2520 -4.3386 415.9172 420.2557 383.4149 334.8715 -4.3313 415.7563 420.0876 383.2090 336.4855 -4.3329 415.5672 419.9002 383.0038 338.0790 -4.3295 415.3773 419.7068 382.8140 339.6706 -4.3237 415.2047 419.5284 382.6095 341.2770 -4.3192 415.0290 419.3482 382.4078 342.8843 -4.3170 414.8571 419.1742 382.2106 344.4933 -4.3151 414.6721 418.9873 382.0186 346.0866 -4.3123 414.5160 418.8283 381.7998 347.6949 -4.3072 414.3249 418.6321 381.5972 349.2895 -4.3030 414.1492 418.4522 381.3779 350.9131 -4.2972 413.9758 418.2730 381.1738 352.5090 -4.2937 413.7904 418.0841 380.9410 354.1038 -4.2899 413.6121 417.9020 380.7208 355.7165 -4.2874 413.4376 417.7250 380.5092 357.3155 -4.2836 413.2576 417.5412 380.2807 358.9445 -4.2816 413.0710 417.3526 380.0624 360.5435 -4.2778 412.8965 417.1743 379.8503 362.1425 -4.2755 412.7135 416.9890 379.6369 363.7413 -4.2712 412.5343 416.8055 379.4152 365.3551 -4.2649 412.3454 416.6103 379.2017 366.9688 -4.2625 412.1661 416.4286 378.9770 368.5828 -4.2587 411.9757 416.2344 378.7514 370.1816 -4.2544 411.8030 416.0574 378.5490 371.7806 -4.2497 411.6125 415.8622 378.3358 373.3946 -4.2468 411.4417 415.6885 378.1254 375.0086 -4.2416 411.2519 415.4934 377.9131 376.6228 -4.2373 411.0566 415.2939 377.6947 378.2215 -4.2337 410.8663 415.1000 377.4956 379.8210 -4.2303 410.6762 414.9065 377.2727 381.4205 -4.2251 410.5144 414.7395 377.0817 383.0495 -4.2211 410.3138 414.5349 376.8464 384.6494 -4.2164 410.1269 414.3433 376.6541 386.2484 -4.2106 409.9420 414.1526 376.4575 387.8625 -4.2095 409.7501 413.9596 376.2555 389.4616 -4.2053 409.5658 413.7711 376.0520 391.0756 -4.2003 409.3715 413.5718 375.8473 392.6906 -4.1943 409.1952 413.3895 375.6573 394.2908 -4.1912 409.0155 413.2067 375.4438 395.9060 -4.1867 408.8167 413.0034 375.2499 397.5061 -4.1806 408.6307 412.8113 375.0549 399.1213 -4.1782 408.4387 412.6169 374.8715 400.7355 -4.1756 408.2458 412.4214 374.6561 402.3320 -4.1697 408.0523 412.2220 374.4661 403.9390 -4.1633 407.8707 412.0340 374.2820 405.5313 -4.1604 407.6807 411.8411 374.0932 407.1394 -4.1558 407.4902 411.6460 373.8939 408.7469 -4.1517 407.3012 411.4529 373.6849 410.3543 -4.1477 407.1163 411.2640 373.4869 411.9471 -4.1425 406.9352 411.0777 373.2936 413.5418 -4.1388 406.7300 410.8689 373.0876 415.1666 -4.1354 406.5404 410.6758 372.8644 416.7610 -4.1316 406.3446 410.4762 372.6541 418.3723 -4.1254 406.1579 410.2833 372.4288 419.9694 -4.1214 405.9565 410.0779 372.2340 421.5821 -4.1168 405.7829 409.8997 372.0165 423.1955 -4.1139 405.5954 409.7094 371.8093 424.7939 -4.1102 405.4021 409.5123 371.6024 426.4079 -4.1043 405.2260 409.3303 371.3892 428.0108 -4.1012 405.0196 409.1207 371.1810 429.6126 -4.0975 404.8262 408.9237 370.9819 431.2266 -4.0896 404.6184 408.7081 370.7668 432.8415 -4.0839 404.4396 408.5235 370.5621 434.4426 -4.0819 404.2428 408.3247 370.3445 436.0566 -4.0773 404.0640 408.1412 370.1312 437.6555 -4.0738 403.8655 407.9393 369.9286 439.2695 -4.0689 403.6605 407.7295 369.7178 440.8835 -4.0647 403.4539 407.5186 369.5348 442.4835 -4.0591 403.2748 407.3338 369.3222 444.0979 -4.0537 403.0781 407.1318 369.1275 445.6975 -4.0504 402.8739 406.9243 368.9226 447.3110 -4.0441 402.6944 406.7385 368.7194 448.9248 -4.0402 402.5047 406.5449 368.5286 450.5236 -4.0349 402.2912 406.3261 368.3250 452.1376 -4.0312 402.1037 406.1348 368.1308 453.7371 -4.0245 401.8973 405.9219 367.9303 455.3666 -4.0209 401.7034 405.7243 367.7300 456.9658 -4.0180 401.5158 405.5337 367.5201 458.5805 -4.0133 401.3193 405.3325 367.3055 460.1799 -4.0090 401.1291 405.1381 367.1013 461.7795 -4.0053 400.9376 404.9429 366.8805 463.3983 -3.9999 400.7490 404.7489 366.6712 465.0113 -3.9954 400.5414 404.5368 366.4670 466.6218 -3.9885 400.3577 404.3462 366.2280 468.2131 -3.9811 400.1648 404.1459 366.0192 469.8049 -3.9772 399.9669 403.9441 365.7975 471.4116 -3.9698 399.7585 403.7283 365.5747 473.0195 -3.9657 399.5692 403.5349 365.3625 474.6276 -3.9607 399.3686 403.3293 365.1491 476.2201 -3.9564 399.1700 403.1264 364.9372 477.8289 -3.9527 398.9867 402.9394 364.7134 479.4233 -3.9443 398.7869 402.7312 364.5030 481.0475 -3.9403 398.5992 402.5395 364.2909 482.6454 -3.9359 398.3883 402.3242 364.0729 484.2438 -3.9311 398.1843 402.1155 363.8759 485.8576 -3.9256 397.9980 401.9237 363.6638 487.4568 -3.9197 397.7926 401.7122 363.4488 489.0706 -3.9150 397.5916 401.5066 363.2298 490.6848 -3.9097 397.3848 401.2945 363.0154 492.2835 -3.9057 397.1955 401.1012 362.8082 493.8825 -3.9013 397.0069 400.9082 362.6140 495.4965 -3.8938 396.7968 400.6905 362.3966 497.1105 -3.8888 396.6020 400.4908 362.1915 498.7245 -3.8841 396.4162 400.3003 361.9947 500.3235 -3.8768 396.2052 400.0819 361.7749 501.9225 -3.8727 396.0084 399.8810 361.5745 503.5364 -3.8692 395.8101 399.6793 361.3736 505.1653 -3.8630 395.6141 399.4772 361.1728 506.7638 -3.8600 395.4013 399.2613 360.9577 508.3636 -3.8542 395.2011 399.0552 360.7570 509.9776 -3.8486 394.9987 398.8473 360.5623 511.5916 -3.8426 394.8045 398.6471 360.3513 513.2058 -3.8343 394.6115 398.4459 360.1548 514.8046 -3.8311 394.4087 398.2398 359.9682 516.4190 -3.8249 394.2160 398.0409 359.7709 518.0185 -3.8181 394.0185 397.8367 359.5655 519.6475 -3.8132 393.8068 397.6200 359.3687 521.2474 -3.8073 393.6127 397.4200 359.1941 522.8615 -3.8014 393.4171 397.2185 358.9726 524.4604 -3.7980 393.2049 397.0029 358.7876 526.0744 -3.7942 393.0030 396.7972 358.5706 527.6885 -3.7891 392.8146 396.6036 358.3788 529.3029 -3.7842 392.6203 396.4046 358.1593 530.8974 -3.7785 392.4209 396.1994 357.9584 532.4886 -3.7727 392.2046 395.9773 357.7376 534.0954 -3.7681 392.0038 395.7720 357.5266 535.7163 -3.7645 391.8147 395.5792 357.3043 537.3085 -3.7592 391.6195 395.3787 357.0921 538.9006 -3.7535 391.4202 395.1737 356.8833 540.5093 -3.7480 391.2350 394.9831 356.6668 542.1190 -3.7422 391.0076 394.7499 356.4363 543.7276 -3.7366 390.7998 394.5365 356.2155 545.3241 -3.7318 390.6132 394.3450 356.0168 546.9366 -3.7280 390.4183 394.1464 355.8016 548.5336 -3.7226 390.2125 393.9351 355.5986 550.1326 -3.7161 390.0035 393.7197 355.3807 551.7618 -3.7122 389.8002 393.5124 355.1608 553.3606 -3.7071 389.5968 393.3040 354.9612 554.9595 -3.7018 389.3925 393.0943 354.7619 556.5735 -3.6960 389.1874 392.8835 354.5513 558.1731 -3.6875 388.9972 392.6847 354.3442 559.8045 -3.6830 388.7835 392.4665 354.1246 561.4034 -3.6803 388.5898 392.2700 353.9216 563.0023 -3.6763 388.3901 392.0664 353.7290 564.6159 -3.6709 388.1886 391.8595 353.5154 566.2153 -3.6648 388.0040 391.6688 353.3081 567.8449 -3.6594 387.7943 391.4538 353.1123 569.4436 -3.6534 387.5910 391.2444 352.9216 571.0580 -3.6505 387.3765 391.0270 352.6974 572.6576 -3.6431 387.1642 390.8074 352.4926 574.2716 -3.6380 386.9735 390.6115 352.3056 575.8858 -3.6317 386.7717 390.4034 352.1135 577.4855 -3.6267 386.5683 390.1950 351.9126 579.0995 -3.6243 386.3718 389.9961 351.7200 580.6990 -3.6201 386.1773 389.7974 351.5179 582.3140 -3.6138 385.9700 389.5838 351.3248 583.9285 -3.6087 385.7607 389.3693 351.1232 585.5433 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252.8615 253.9179 219.4401 1632.1166 -1.0525 252.6738 253.7263 219.2718 1633.7253 -1.0507 252.4782 253.5289 219.1021 1635.3203 -1.0475 252.2859 253.3334 218.9378 1636.9320 -1.0496 252.0896 253.1392 218.7483 1638.5293 -1.0460 251.8997 252.9457 218.5636 1640.1416 -1.0474 251.7116 252.7589 218.4073 1641.7550 -1.0475 251.5135 252.5610 218.2265 1643.3525 -1.0466 251.3204 252.3670 218.0522 1644.9660 -1.0455 251.1431 252.1886 217.8849 1646.5645 -1.0419 250.9231 251.9650 217.7132 1648.1784 -1.0398 250.7139 251.7538 217.5302