DTA measure 1pb_updown_4 Date: 2025101:1042 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1444.13 s Mass = 1111.600 mg data_number = 1795 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2513 -0.6038 263.6032 264.2070 257.6102 2.1100 -0.6010 263.6371 264.2380 257.3489 2.8458 -0.5912 263.6631 264.2543 257.1064 3.7045 -0.5791 263.7092 264.2883 256.8245 4.4710 -0.5745 263.7284 264.3029 256.5734 5.2990 -0.5701 263.8114 264.3815 256.3492 6.0853 -0.5599 263.8529 264.4128 256.1174 6.8925 -0.5508 263.8659 264.4167 255.8795 7.7103 -0.5378 263.9086 264.4464 255.6248 8.4768 -0.5292 263.9749 264.5040 255.3822 9.3355 -0.5188 264.0407 264.5594 255.1208 10.1020 -0.5095 264.0959 264.6054 254.8733 10.9300 -0.5043 264.1391 264.6434 254.6294 11.7170 -0.4942 264.1587 264.6529 254.3987 12.5245 -0.4692 264.1635 264.6326 254.1995 13.3420 -0.4492 264.1875 264.6368 253.9862 14.1180 -0.4349 264.2365 264.6714 253.7977 14.9665 -0.4166 264.2672 264.6838 253.5840 15.7433 -0.3942 264.3174 264.7117 253.4297 16.5610 -0.3681 264.3765 264.7446 253.2573 17.3275 -0.3536 264.3975 264.7510 253.0959 18.1555 -0.3482 264.3966 264.7448 252.9068 18.9523 -0.3363 264.4548 264.7911 252.7953 19.7490 -0.3254 264.4499 264.7754 252.7102 20.5668 -0.3167 264.4757 264.7924 252.6171 21.3435 -0.3102 264.5106 264.8208 252.5473 22.1920 -0.2990 264.5405 264.8395 252.5413 22.9585 -0.2860 264.5740 264.8599 252.5348 23.7863 -0.2706 264.6149 264.8855 252.5886 24.5828 -0.2593 264.6482 264.9075 252.7081 25.3800 -0.2512 264.6826 264.9338 252.8364 26.1978 -0.2376 264.7179 264.9555 252.9840 26.9745 -0.2270 264.7563 264.9833 253.1543 27.8230 -0.2257 264.8018 265.0275 253.3710 28.5895 -0.2269 264.8304 265.0572 253.6391 29.4170 -0.2221 264.8584 265.0804 253.9727 30.2138 -0.2149 264.9235 265.1384 254.2678 31.0110 -0.2062 264.9507 265.1569 254.6103 31.8288 -0.1967 264.9538 265.1504 254.9978 32.6055 -0.1924 264.9578 265.1503 255.3490 33.4540 -0.1830 264.9983 265.1813 255.7673 34.2508 -0.1785 265.0227 265.2013 256.1593 35.0475 -0.1786 265.0549 265.2334 256.5291 35.8448 -0.1758 265.0875 265.2634 256.9030 36.6420 -0.1766 265.1684 265.3450 257.2901 37.5008 -0.1771 265.2184 265.3955 257.7220 38.2365 -0.1716 265.2548 265.4264 258.0378 39.0953 -0.1605 265.2682 265.4287 258.3817 39.8618 -0.1609 265.2889 265.4498 258.6531 40.6785 -0.1642 265.3265 265.4907 258.9046 41.4860 -0.1655 265.3852 265.5507 259.1633 42.2730 -0.1616 265.3996 265.5612 259.3734 43.1113 -0.1566 265.4061 265.5628 259.5827 43.8675 -0.1603 265.4409 265.6012 259.7046 44.7365 -0.1617 265.4724 265.6342 259.8532 45.4925 -0.1627 265.5012 265.6639 259.9982 46.3200 -0.1641 265.5264 265.6905 260.1159 47.1170 -0.1699 265.5335 265.7034 260.1874 47.9143 -0.1780 265.5666 265.7446 260.2319 48.7320 -0.1829 265.6307 265.8136 260.2657 49.4985 -0.1854 265.6693 265.8547 260.2615 50.3470 -0.1904 265.7139 265.9044 260.2681 51.0725 -0.1950 265.7333 265.9283 260.2501 51.9308 -0.2000 265.6993 265.8993 260.1674 52.6865 -0.2000 265.7439 265.9438 260.0781 53.5145 -0.1987 265.7643 265.9630 260.0326 54.3015 -0.1958 265.7710 265.9668 259.9510 55.0885 -0.1955 265.8139 266.0095 259.8471 55.9165 -0.1931 265.8260 266.0191 259.7482 56.6830 -0.1930 265.8465 266.0395 259.6525 57.5315 -0.1915 265.9089 266.1004 259.5142 58.3073 -0.1904 265.9404 266.1308 259.4168 59.1250 -0.1855 265.9818 266.1673 259.2996 59.8813 -0.1864 265.9962 266.1826 259.1706 60.7195 -0.1889 266.0508 266.2397 259.0614 61.5065 -0.1850 266.1383 266.3234 258.9727 62.3038 -0.1833 266.1863 266.3696 258.8775 63.1310 -0.1751 266.1813 266.3564 258.8430 63.8973 -0.1738 266.2372 266.4110 258.8251 64.7560 -0.1628 266.2775 266.4403 258.8223 65.5123 -0.1582 266.3095 266.4677 258.8098 66.3505 -0.1612 266.3297 266.4909 258.8500 67.1375 -0.1596 266.3753 266.5349 258.9217 67.9348 -0.1574 266.4315 266.5888 258.9829 68.7628 -0.1577 266.4668 266.6245 259.0587 69.5288 -0.1595 266.5119 266.6714 259.1672 70.3870 -0.1539 266.5819 266.7358 259.3365 71.1433 -0.1525 266.6450 266.7975 259.5209 71.9815 -0.1495 266.6868 266.8363 259.7375 72.7685 -0.1455 266.7619 266.9075 259.9412 73.5760 -0.1426 266.7722 266.9147 260.1582 74.3630 -0.1392 266.7512 266.8904 260.4044 75.1705 -0.1421 266.7831 266.9252 260.7123 75.9880 -0.1438 266.8184 266.9622 261.0044 76.7538 -0.1472 266.8891 267.0363 261.2687 77.6125 -0.1471 266.9399 267.0870 261.5789 78.3893 -0.1416 266.9959 267.1375 261.8468 79.2070 -0.1391 267.0120 267.1511 262.1460 80.0043 -0.1383 267.0586 267.1968 262.4404 80.8015 -0.1352 267.1069 267.2420 262.7456 81.6285 -0.1303 267.1696 267.2999 263.0539 82.3848 -0.1278 267.2047 267.3325 263.3721 83.2128 -0.1258 267.2360 267.3618 263.6451 83.9690 -0.1281 267.2524 267.3805 263.8725 84.8278 -0.1257 267.3057 267.4314 264.1256 85.5943 -0.1287 267.3400 267.4688 264.3095 86.4213 -0.1374 267.3789 267.5163 264.4799 87.2185 -0.1376 267.4198 267.5574 264.6654 88.0055 -0.1333 267.4533 267.5866 264.7962 88.8438 -0.1329 267.5182 267.6511 264.9260 89.6000 -0.1338 267.5379 267.6717 265.0272 90.4280 -0.1355 267.5805 267.7160 265.1079 91.1940 -0.1376 267.6333 267.7708 265.1734 92.0420 -0.1403 267.6881 267.8283 265.2158 92.8085 -0.1376 267.6909 267.8285 265.2423 93.6365 -0.1404 267.7316 267.8720 265.2974 94.4338 -0.1438 267.7551 267.8989 265.2865 95.2310 -0.1451 267.8045 267.9495 265.2563 96.0488 -0.1459 267.8152 267.9611 265.2215 96.8248 -0.1451 267.8490 267.9940 265.2027 97.6730 -0.1431 267.9037 268.0469 265.1840 98.4395 -0.1399 267.9473 268.0873 265.1209 99.2675 -0.1371 268.0258 268.1629 265.0794 100.0443 -0.1376 268.0845 268.2220 265.0303 100.8620 -0.1381 268.1617 268.2998 264.9681 101.6593 -0.1385 268.2500 268.3885 264.8975 102.4558 -0.1378 268.2914 268.4292 264.8099 103.2835 -0.1360 268.3390 268.4750 264.7452 104.0500 -0.1345 268.3832 268.5177 264.7041 104.8985 -0.1341 268.4414 268.5755 264.6874 105.6753 -0.1336 268.4676 268.6013 264.6657 106.4930 -0.1333 268.5150 268.6483 264.6541 107.2900 -0.1330 268.5887 268.7217 264.6778 108.0868 -0.1315 268.6492 268.7807 264.6739 108.9145 -0.1323 268.7005 268.8328 264.6942 109.6810 -0.1325 268.7415 268.8740 264.7468 110.5090 -0.1325 268.7588 268.8913 264.8673 111.2755 -0.1321 268.8069 268.9390 264.9820 112.1343 -0.1306 268.9052 269.0358 265.1230 112.9000 -0.1273 268.9440 269.0713 265.2479 113.7175 -0.1275 268.9772 269.1047 265.3691 114.5148 -0.1256 269.0047 269.1303 265.5071 115.3120 -0.1166 269.0625 269.1792 265.6981 116.0990 -0.1062 269.1111 269.2173 265.9020 116.8963 -0.0985 269.1569 269.2554 266.1500 117.7140 -0.0877 269.2196 269.3072 266.3908 118.4800 -0.0744 269.2638 269.3382 266.6278 119.3383 -0.0649 269.2853 269.3502 266.9285 120.0945 -0.0654 269.3256 269.3910 267.1836 120.9225 -0.0615 269.3754 269.4368 267.4527 121.7198 -0.0515 269.4265 269.4780 267.6951 122.5170 -0.0460 269.4446 269.4906 267.9471 123.3345 -0.0487 269.4988 269.5474 268.1893 124.1105 -0.0477 269.5673 269.6150 268.4266 124.9590 -0.0442 269.5922 269.6365 268.6797 125.7255 -0.0460 269.6474 269.6934 268.9106 126.5535 -0.0494 269.7428 269.7922 269.1269 127.3508 -0.0578 269.8124 269.8703 269.3097 128.1480 -0.0657 269.8650 269.9307 269.5028 128.9650 -0.0719 269.9159 269.9878 269.6807 129.7415 -0.0731 269.9657 270.0387 269.8388 130.5900 -0.0743 270.0205 270.0948 269.9879 131.3360 -0.0744 270.0845 270.1589 270.0962 132.1845 -0.0872 270.1530 270.2403 270.2554 132.9613 -0.0885 270.1877 270.2761 270.3364 133.7780 -0.0874 270.2483 270.3357 270.4147 134.5753 -0.0903 270.2728 270.3631 270.4283 135.3725 -0.0939 270.3352 270.4291 270.4818 136.2005 -0.0971 270.4188 270.5160 270.5143 136.9670 -0.0955 270.4794 270.5749 270.5414 137.8258 -0.0953 270.5156 270.6109 270.5210 138.5913 -0.0962 270.5456 270.6418 270.5249 139.4193 -0.0972 270.5821 270.6793 270.5213 140.2165 -0.0969 270.6507 270.7475 270.5189 141.0035 -0.1020 270.7354 270.8374 270.4953 141.8418 -0.1047 270.8221 270.9269 270.4460 142.5980 -0.1071 270.8552 270.9623 270.4438 143.4563 -0.1093 270.9418 271.0510 270.3884 144.2223 -0.1169 271.0172 271.1340 270.3628 145.0503 -0.1158 271.0605 271.1763 270.3459 145.8373 -0.1137 271.0877 271.2015 270.3339 146.6345 -0.1141 271.1327 271.2468 270.3145 147.4625 -0.1145 271.2067 271.3211 270.2673 148.2280 -0.1142 271.2330 271.3472 270.2577 149.0458 -0.1119 271.2748 271.3867 270.2653 149.8123 -0.1042 271.3756 271.4798 270.3110 150.6710 -0.1022 271.4576 271.5597 270.3388 151.4273 -0.1026 271.5198 271.6225 270.3829 152.2553 -0.1007 271.5773 271.6780 270.4705 153.0515 -0.0969 271.6200 271.7169 270.5865 153.8385 -0.0954 271.6625 271.7579 270.7122 154.6768 -0.0983 271.7570 271.8553 270.8576 155.4330 -0.1004 271.8407 271.9412 270.9845 156.2918 -0.1094 271.8868 271.9962 271.1607 157.0583 -0.1089 271.9321 272.0410 271.3368 157.8855 -0.1114 271.9698 272.0811 271.5483 158.6825 -0.1150 272.0078 272.1228 271.7501 159.4695 -0.1156 272.0529 272.1685 271.9615 160.3078 -0.1187 272.1066 272.2253 272.2325 161.0640 -0.1164 272.1668 272.2831 272.4446 161.9328 -0.1151 272.2700 272.3851 272.7238 162.6883 -0.1154 272.3341 272.4495 272.9324 163.5265 -0.1186 272.3974 272.5159 273.1688 164.3135 -0.1140 272.4799 272.5939 273.4122 165.1108 -0.1121 272.5429 272.6549 273.6607 165.9388 -0.1112 272.5921 272.7033 273.9115 166.7053 -0.1136 272.6363 272.7499 274.1293 167.5635 -0.1161 272.7069 272.8230 274.3624 168.3295 -0.1132 272.7731 272.8863 274.5539 169.1575 -0.1126 272.8343 272.9469 274.7450 169.9548 -0.1142 272.9091 273.0233 274.9578 170.7520 -0.1154 273.0012 273.1167 275.1157 171.5698 -0.1196 273.0885 273.2081 275.2439 172.3465 -0.1243 273.1727 273.2969 275.3685 173.1950 -0.1291 273.2120 273.3411 275.5041 173.9615 -0.1271 273.2747 273.4018 275.5994 174.7888 -0.1280 273.3538 273.4818 275.6486 175.5858 -0.1262 273.4048 273.5309 275.7046 176.3830 -0.1251 273.4319 273.5570 275.7786 177.2008 -0.1232 273.5141 273.6374 275.8280 177.9775 -0.1263 273.6099 273.7363 275.8468 178.7953 -0.1272 273.6795 273.8067 275.8713 179.5618 -0.1268 273.7372 273.8640 275.8864 180.4198 -0.1240 273.8274 273.9514 275.8780 181.1758 -0.1202 273.8518 273.9720 275.8858 181.9935 -0.1206 273.9266 274.0473 275.8479 182.8010 -0.1246 273.9986 274.1231 275.8286 183.5880 -0.1241 274.0616 274.1856 275.8100 184.4058 -0.1287 274.1438 274.2725 275.7566 185.1823 -0.1293 274.2070 274.3363 275.7313 186.0300 -0.1307 274.2765 274.4072 275.7048 186.7965 -0.1273 274.3502 274.4775 275.6805 187.6245 -0.1289 274.4045 274.5333 275.6910 188.3910 -0.1291 274.4794 274.6085 275.6632 189.2190 -0.1294 274.6089 274.7383 275.6421 190.0060 -0.1277 274.6794 274.8071 275.6432 190.8125 -0.1248 274.7569 274.8817 275.6661 191.6303 -0.1250 274.8472 274.9721 275.7284 192.3968 -0.1304 274.9037 275.0341 275.8494 193.2555 -0.1297 274.9800 275.1097 275.9142 194.0220 -0.1286 275.0468 275.1754 276.0148 194.8500 -0.1291 275.1046 275.2337 276.1667 195.6365 -0.1308 275.1927 275.3235 276.3054 196.4435 -0.1303 275.2984 275.4287 276.4546 197.2613 -0.1301 275.3382 275.4684 276.6153 198.0380 -0.1285 275.4361 275.5645 276.7970 198.8865 -0.1297 275.5101 275.6398 277.0106 199.6633 -0.1330 275.5891 275.7222 277.2309 200.4810 -0.1320 275.6626 275.7947 277.4520 201.2465 -0.1335 275.7131 275.8466 277.6727 202.0745 -0.1327 275.7816 275.9143 277.8891 202.8718 -0.1315 275.8405 275.9720 278.1223 203.6690 -0.1291 275.8744 276.0035 278.3642 204.4868 -0.1293 275.9163 276.0455 278.6325 205.2635 -0.1280 276.0255 276.1535 278.8963 206.1120 -0.1300 276.1353 276.2653 279.1434 206.8880 -0.1337 276.1766 276.3104 279.3581 207.7055 -0.1346 276.2366 276.3712 279.5623 208.5130 -0.1350 276.3084 276.4435 279.7897 209.3000 -0.1332 276.3570 276.4902 280.0036 210.1178 -0.1388 276.4452 276.5839 280.1879 210.8843 -0.1391 276.5284 276.6675 280.3296 211.7013 -0.1400 276.6117 276.7517 280.4591 212.4675 -0.1391 276.6839 276.8230 280.5831 213.3263 -0.1376 276.7509 276.8885 280.6802 214.0825 -0.1392 276.8179 276.9571 280.8015 214.9105 -0.1411 276.8813 277.0224 280.8999 215.7078 -0.1452 276.9502 277.0955 280.9540 216.5048 -0.1437 277.0377 277.1814 281.0218 217.3218 -0.1420 277.1127 277.2548 281.0669 218.0985 -0.1451 277.1786 277.3237 281.1086 218.9470 -0.1477 277.3008 277.4485 281.1264 219.7135 -0.1474 277.3502 277.4976 281.1169 220.5415 -0.1442 277.4440 277.5882 281.1408 221.3080 -0.1449 277.5777 277.7226 281.1474 222.1350 -0.1455 277.6633 277.8088 281.1469 222.9220 -0.1482 277.7525 277.9007 281.1161 223.7295 -0.1472 277.8243 277.9715 281.0968 224.5473 -0.1438 277.9108 278.0547 281.0532 225.3138 -0.1421 278.0129 278.1549 281.0336 226.1725 -0.1423 278.0978 278.2402 281.0224 226.9390 -0.1420 278.1655 278.3075 281.0447 227.7660 -0.1417 278.2424 278.3841 281.0690 228.5530 -0.1443 278.3277 278.4720 281.0876 229.3605 -0.1467 278.3805 278.5272 281.0925 230.1783 -0.1458 278.4399 278.5857 281.0798 230.9448 -0.1439 278.5351 278.6790 281.0493 231.8035 -0.1413 278.6264 278.7678 281.1238 232.5700 -0.1412 278.7294 278.8706 281.1876 233.3980 -0.1398 278.8323 278.9722 281.2703 234.1943 -0.1407 278.8981 279.0389 281.3880 234.9915 -0.1416 278.9600 279.1016 281.5036 235.7888 -0.1437 279.0623 279.2061 281.6455 236.5860 -0.1421 279.1438 279.2859 281.7774 237.4038 -0.1429 279.2144 279.3573 281.9292 238.1805 -0.1415 279.2515 279.3930 282.0934 239.0290 -0.1425 279.2995 279.4420 282.2504 239.7945 -0.1427 279.3509 279.4936 282.4435 240.6225 -0.1401 279.4817 279.6218 282.6647 241.4198 -0.1417 279.5835 279.7251 282.8810 242.2170 -0.1421 279.6664 279.8084 283.1170 243.0348 -0.1443 279.7478 279.8920 283.3617 243.8008 -0.1425 279.8334 279.9759 283.6009 244.6590 -0.1422 279.8881 280.0303 283.8752 245.4153 -0.1426 280.0033 280.1459 284.0869 246.2433 -0.1431 280.1143 280.2574 284.2861 247.0405 -0.1425 280.1721 280.3146 284.5181 247.8275 -0.1419 280.2469 280.3888 284.7353 248.6555 -0.1448 280.3360 280.4808 284.9459 249.4213 -0.1506 280.4181 280.5686 285.1404 250.2695 -0.1486 280.5019 280.6505 285.3228 251.0463 -0.1464 280.5812 280.7276 285.4990 251.8640 -0.1459 280.6756 280.8214 285.6757 252.6613 -0.1508 280.7323 280.8830 285.8205 253.4585 -0.1502 280.8032 280.9534 285.9369 254.2865 -0.1533 280.8630 281.0163 286.0169 255.0530 -0.1592 280.9413 281.1005 286.1265 255.8708 -0.1593 281.0357 281.1950 286.2295 256.6468 -0.1593 281.1499 281.3092 286.3113 257.4950 -0.1619 281.2511 281.4130 286.3575 258.2615 -0.1621 281.3251 281.4872 286.3859 259.0895 -0.1581 281.4233 281.5814 286.4505 259.8868 -0.1555 281.5319 281.6874 286.4792 260.6840 -0.1509 281.6452 281.7961 286.5071 261.5008 -0.1517 281.7581 281.9099 286.4910 262.2775 -0.1569 281.8393 281.9962 286.4836 263.1260 -0.1572 281.9403 282.0975 286.4489 263.8925 -0.1543 282.0141 282.1683 286.4669 264.7205 -0.1545 282.1100 282.2645 286.4323 265.5178 -0.1575 282.2007 282.3582 286.3882 266.3150 -0.1560 282.2780 282.4340 286.3946 267.1328 -0.1556 282.3680 282.5237 286.4006 267.9088 -0.1559 282.4769 282.6328 286.3818 268.7570 -0.1539 282.5650 282.7189 286.3838 269.5235 -0.1507 282.6632 282.8139 286.3945 270.3515 -0.1490 282.7469 282.8959 286.4256 271.1795 -0.1498 282.8466 282.9964 286.4737 271.9460 -0.1536 282.9176 283.0712 286.5188 272.7945 -0.1555 283.0014 283.1569 286.5947 273.5710 -0.1527 283.0694 283.2221 286.6656 274.3880 -0.1523 283.1619 283.3142 286.7684 275.1853 -0.1514 283.2508 283.4023 286.8865 275.9825 -0.1487 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