DTA measure 2pb_updown_3 Date: 2025101:948 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.43 s Mass = 1111.600 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2708 -0.0594 280.4114 280.4708 275.1208 2.0675 -0.0579 280.4709 280.5288 275.0376 2.8743 -0.0530 280.5391 280.5921 274.9378 3.6708 -0.0553 280.5921 280.6474 274.8375 4.4675 -0.0536 280.6285 280.6821 274.7617 5.2848 -0.0506 280.6519 280.7025 274.6472 6.0503 -0.0503 280.6969 280.7471 274.5620 6.8983 -0.0512 280.7475 280.7987 274.4738 7.6643 -0.0509 280.7848 280.8356 274.4017 8.4913 -0.0519 280.8322 280.8841 274.3472 9.2778 -0.0507 280.8793 280.9300 274.2868 10.0745 -0.0471 280.9169 280.9640 274.2856 10.9015 -0.0451 280.9919 281.0371 274.3732 11.6675 -0.0447 281.0704 281.1151 274.4068 12.4848 -0.0429 281.1086 281.1515 274.4543 13.2605 -0.0428 281.1537 281.1965 274.5308 14.1085 -0.0443 281.2265 281.2707 274.6311 14.8745 -0.0443 281.2882 281.3325 274.7503 15.7015 -0.0393 281.3297 281.3690 274.9003 16.4983 -0.0370 281.3473 281.3843 275.0753 17.2950 -0.0336 281.3816 281.4153 275.3075 18.1118 -0.0315 281.4388 281.4703 275.5746 18.8880 -0.0282 281.5217 281.5499 275.8351 19.7360 -0.0307 281.6088 281.6395 276.1344 20.5015 -0.0289 281.6533 281.6823 276.4322 21.3290 -0.0281 281.6939 281.7221 276.7679 22.1258 -0.0349 281.7462 281.7810 277.0831 22.9428 -0.0393 281.8073 281.8466 277.4153 23.7293 -0.0360 281.8596 281.8956 277.7453 24.5360 -0.0379 281.8807 281.9186 278.0875 25.3530 -0.0399 281.9187 281.9586 278.4262 26.1290 -0.0380 281.9629 282.0010 278.7722 26.9770 -0.0392 282.0338 282.0730 279.1494 27.7425 -0.0429 282.1312 282.1741 279.4343 28.5700 -0.0462 282.1803 282.2265 279.7716 29.3463 -0.0497 282.2027 282.2524 280.0450 30.1630 -0.0516 282.2701 282.3217 280.3260 30.9598 -0.0502 282.3059 282.3560 280.5966 31.7565 -0.0471 282.3470 282.3941 280.8399 32.5938 -0.0490 282.4091 282.4581 281.0530 33.3495 -0.0525 282.4260 282.4785 281.2215 34.2078 -0.0550 282.4729 282.5279 281.3628 34.9733 -0.0534 282.5502 282.6035 281.4934 35.8110 -0.0541 282.6055 282.6596 281.6245 36.5975 -0.0581 282.6632 282.7214 281.7438 37.3938 -0.0577 282.7684 282.8261 281.8090 38.2215 -0.0610 282.8443 282.9053 281.8615 38.9975 -0.0621 282.8934 282.9556 281.8937 39.8453 -0.0588 282.9439 283.0028 281.9084 40.6113 -0.0616 283.0226 283.0842 281.9038 41.4385 -0.0659 283.0938 283.1597 281.8709 42.2453 -0.0668 283.1423 283.2091 281.8194 43.0318 -0.0693 283.1977 283.2670 281.7850 43.8590 -0.0712 283.2400 283.3112 281.7444 44.6248 -0.0753 283.2817 283.3570 281.6756 45.4933 -0.0720 283.3594 283.4314 281.5996 46.2488 -0.0721 283.4401 283.5122 281.5314 47.0760 -0.0734 283.4950 283.5684 281.4819 47.8730 -0.0757 283.5140 283.5896 281.4170 48.6693 -0.0799 283.5536 283.6335 281.3656 49.4968 -0.0834 283.6453 283.7288 281.2972 50.2525 -0.0847 283.7105 283.7952 281.2516 51.1205 -0.0891 283.7406 283.8296 281.2116 51.8763 -0.0879 283.8033 283.8912 281.2189 52.7140 -0.0898 283.8814 283.9712 281.2180 53.5000 -0.0874 283.9803 284.0677 281.2847 54.3068 -0.0880 284.0443 284.1323 281.3692 55.1243 -0.0879 284.0729 284.1608 281.4386 55.8898 -0.0924 284.0804 284.1728 281.5433 56.7480 -0.0930 284.1581 284.2511 281.7274 57.5240 -0.0930 284.2473 284.3403 281.9231 58.3410 -0.0972 284.3378 284.4350 282.1050 59.1375 -0.0984 284.3955 284.4939 282.3257 59.9343 -0.0954 284.4392 284.5346 282.5907 60.7615 -0.0954 284.4983 284.5937 282.8804 61.5273 -0.0986 284.5409 284.6395 283.1644 62.3855 -0.0991 284.6096 284.7088 283.5267 63.1513 -0.0986 284.6770 284.7757 283.8435 63.9785 -0.0976 284.7063 284.8039 284.1905 64.7753 -0.0972 284.7710 284.8682 284.5173 65.5718 -0.1015 284.8543 284.9558 284.8362 66.3990 -0.1070 284.9166 285.0237 285.1596 67.1650 -0.1096 284.9819 285.0915 285.4574 68.0230 -0.1182 285.0641 285.1823 285.8048 68.7785 -0.1204 285.1145 285.2349 286.0997 69.5958 -0.1191 285.1904 285.3095 286.4257 70.3820 -0.1207 285.2940 285.4147 286.6925 71.1785 -0.1229 285.3486 285.4715 286.9565 71.9650 -0.1251 285.4295 285.5546 287.1937 72.7615 -0.1314 285.4858 285.6173 287.4074 73.5785 -0.1368 285.5327 285.6696 287.6220 74.3343 -0.1362 285.5726 285.7088 287.7586 75.2025 -0.1419 285.6513 285.7932 287.9383 75.9273 -0.1455 285.7222 285.8677 288.0431 76.7753 -0.1474 285.7660 285.9135 288.1535 77.5513 -0.1550 285.8384 285.9934 288.2086 78.3683 -0.1548 285.9196 286.0744 288.2786 79.1648 -0.1529 286.0103 286.1633 288.3314 79.9615 -0.1488 286.0905 286.2393 288.3371 80.7785 -0.1476 286.1375 286.2851 288.2972 81.5445 -0.1500 286.1699 286.3199 288.2789 82.4025 -0.1496 286.2627 286.4124 288.2801 83.1683 -0.1509 286.3372 286.4881 288.2646 83.9958 -0.1528 286.4038 286.5565 288.2401 84.7820 -0.1538 286.4670 286.6208 288.1957 85.5888 -0.1516 286.5545 286.7061 288.1776 86.3753 -0.1543 286.6429 286.7973 288.1254 87.1718 -0.1498 286.7274 286.8773 288.0848 87.9990 -0.1477 286.8029 286.9506 288.0300 88.7650 -0.1448 286.8580 287.0028 287.9998 89.6230 -0.1479 286.9551 287.1030 287.9807 90.3785 -0.1481 287.0176 287.1657 287.9861 91.2163 -0.1514 287.0997 287.2510 287.9625 92.0025 -0.1483 287.1470 287.2953 287.9782 92.7993 -0.1516 287.2359 287.3874 288.0245 93.6268 -0.1485 287.2754 287.4240 288.1150 94.3925 -0.1554 287.3171 287.4725 288.1585 95.2508 -0.1606 287.4052 287.5657 288.2378 96.0165 -0.1654 287.4734 287.6389 288.3513 96.8440 -0.1638 287.5358 287.6996 288.5080 97.6408 -0.1666 287.6659 287.8325 288.6650 98.4373 -0.1663 287.7159 287.8822 288.8655 99.2545 -0.1653 287.8093 287.9745 289.0759 100.0305 -0.1686 287.8893 288.0579 289.3132 100.8578 -0.1727 287.9400 288.1127 289.5803 101.6238 -0.1739 288.0152 288.1891 289.8547 102.4715 -0.1759 288.0824 288.2583 290.1783 103.2478 -0.1740 288.1536 288.3276 290.4646 104.0650 -0.1738 288.2444 288.4182 290.7849 104.8613 -0.1733 288.3383 288.5116 291.0595 105.6580 -0.1755 288.4078 288.5833 291.3638 106.4855 -0.1753 288.4839 288.6592 291.6868 107.2513 -0.1751 288.5251 288.7002 291.9809 108.0993 -0.1766 288.6133 288.7899 292.2548 108.8753 -0.1771 288.6754 288.8525 292.5512 109.6923 -0.1800 288.7663 288.9463 292.8279 110.4583 -0.1865 288.8231 289.0097 293.0530 111.2855 -0.1870 288.8817 289.0687 293.3199 112.0818 -0.1889 288.9654 289.1543 293.5411 112.8788 -0.1931 289.0181 289.2112 293.7463 113.6958 -0.1957 289.0513 289.2470 293.9560 114.4718 -0.1995 289.1568 289.3562 294.1295 115.3095 -0.1975 289.2278 289.4253 294.2802 116.0753 -0.1983 289.3311 289.5295 294.3958 116.9333 -0.1995 289.4256 289.6251 294.4754 117.6890 -0.2003 289.5224 289.7227 294.5307 118.5265 -0.2022 289.6299 289.8321 294.5973 119.3230 -0.2034 289.7029 289.9063 294.6419 120.1198 -0.2048 289.7834 289.9882 294.6942 120.9368 -0.2046 289.8886 290.0932 294.7381 121.7128 -0.2095 289.9856 290.1951 294.7507 122.5403 -0.2134 290.0913 290.3047 294.7651 123.3060 -0.2148 290.1542 290.3690 294.7700 124.1538 -0.2107 290.2446 290.4553 294.7384 124.8993 -0.2126 290.3065 290.5191 294.7280 125.7675 -0.2164 290.4002 290.6167 294.6788 126.5435 -0.2185 290.4966 290.7151 294.6297 127.3608 -0.2199 290.5749 290.7947 294.6170 128.1573 -0.2167 290.6581 290.8748 294.5736 128.9538 -0.2199 290.7113 290.9312 294.5359 129.7813 -0.2256 290.8109 291.0365 294.5125 130.5470 -0.2261 290.8971 291.1232 294.5126 131.4050 -0.2269 290.9956 291.2224 294.5239 132.1713 -0.2219 291.1090 291.3309 294.5280 132.9983 -0.2211 291.1976 291.4188 294.5785 133.7643 -0.2180 291.2691 291.4871 294.6423 134.5815 -0.2201 291.3372 291.5573 294.7273 135.3678 -0.2231 291.4247 291.6479 294.8263 136.1953 -0.2253 291.5133 291.7386 294.9750 137.0020 -0.2287 291.5920 291.8206 295.1633 137.7883 -0.2266 291.6898 291.9164 295.3735 138.6260 -0.2282 291.7726 292.0007 295.5777 139.3815 -0.2289 291.8530 292.0819 295.8045 140.2498 -0.2275 291.9596 292.1871 296.0646 141.0055 -0.2288 292.0663 292.2950 296.3068 141.8430 -0.2299 292.1578 292.3876 296.5925 142.6295 -0.2291 292.2566 292.4856 296.8843 143.4365 -0.2319 292.3449 292.5768 297.1905 144.2533 -0.2338 292.4393 292.6731 297.5106 145.0295 -0.2291 292.5243 292.7533 297.8165 145.8775 -0.2307 292.6199 292.8506 298.1261 146.6533 -0.2310 292.7033 292.9343 298.3738 147.4708 -0.2304 292.8128 293.0432 298.6582 148.2673 -0.2330 292.8854 293.1183 298.9280 149.0638 -0.2344 292.9730 293.2074 299.1906 149.8915 -0.2386 293.0496 293.2881 299.4593 150.6570 -0.2409 293.1096 293.3504 299.7158 151.5155 -0.2409 293.2088 293.4497 299.9935 152.2813 -0.2396 293.2969 293.5365 300.1888 153.1088 -0.2433 293.4019 293.6452 300.4118 153.9055 -0.2421 293.4706 293.7128 300.5717 154.7018 -0.2391 293.5802 293.8193 300.7125 155.5293 -0.2424 293.6607 293.9031 300.8738 156.2953 -0.2461 293.7640 294.0101 300.9579 157.1530 -0.2536 293.8578 294.1114 301.0557 157.9193 -0.2553 293.9196 294.1749 301.1043 158.7465 -0.2537 293.9918 294.2455 301.1345 159.5430 -0.2601 294.1005 294.3605 301.1834 160.3398 -0.2555 294.1804 294.4359 301.1749 161.1568 -0.2519 294.2909 294.5429 301.1631 161.9330 -0.2486 294.4237 294.6723 301.1556 162.7913 -0.2503 294.5393 294.7896 301.0845 163.5568 -0.2554 294.6757 294.9311 301.0699 164.3740 -0.2579 294.8145 295.0724 301.0354 165.1808 -0.2604 294.9462 295.2066 301.0133 165.9670 -0.2612 295.0487 295.3099 300.9957 166.7638 -0.2617 295.1247 295.3864 300.9717 167.5605 -0.2604 295.2075 295.4678 300.9675 168.3773 -0.2607 295.3110 295.5716 300.9999 169.1433 -0.2573 295.4131 295.6704 301.0189 170.0015 -0.2602 295.5194 295.7796 301.0420 170.7568 -0.2624 295.6044 295.8668 301.0711 171.5740 -0.2669 295.7193 295.9862 301.1127 172.3810 -0.2677 295.8151 296.0828 301.1498 173.1670 -0.2614 295.9430 296.2043 301.2527 173.9843 -0.2599 296.0041 296.2641 301.3578 174.7605 -0.2608 296.1192 296.3799 301.4677 175.6080 -0.2622 296.2278 296.4900 301.6137 176.3638 -0.2645 296.3200 296.5845 301.7946 177.2015 -0.2690 296.4078 296.6767 301.9992 177.9670 -0.2676 296.4703 296.7379 302.1860 178.8150 -0.2669 296.5919 296.8588 302.4404 179.5913 -0.2625 296.6804 296.9428 302.7007 180.4080 -0.2638 296.7777 297.0415 302.9626 181.2050 -0.2666 296.8540 297.1206 303.1955 182.0015 -0.2696 296.9654 297.2349 303.4653 182.8285 -0.2691 297.0709 297.3400 303.7900 183.5945 -0.2705 297.1497 297.4201 304.0755 184.4425 -0.2701 297.2295 297.4996 304.3638 185.2185 -0.2725 297.3656 297.6381 304.6486 186.0358 -0.2777 297.4871 297.7648 304.9262 186.8323 -0.2799 297.5931 297.8730 305.2028 187.6490 -0.2837 297.6841 297.9678 305.4691 188.4458 -0.2857 297.7860 298.0717 305.7091 189.2425 -0.2883 297.8851 298.1733 305.9565 190.0388 -0.2882 297.9876 298.2758 306.1871 190.8355 -0.2876 298.1080 298.3956 306.3948 191.6528 -0.2864 298.2219 298.5083 306.5929 192.4285 -0.2877 298.3272 298.6149 306.7760 193.2765 -0.2866 298.3977 298.6843 306.9182 194.0425 -0.2898 298.4783 298.7681 307.0295 194.8695 -0.2944 298.5781 298.8726 307.1818 195.6663 -0.2976 298.7104 299.0080 307.2522 196.4630 -0.2993 298.8045 299.1038 307.3250 197.2798 -0.3014 298.8857 299.1872 307.3914 198.0560 -0.3005 298.9829 299.2834 307.4185 198.9143 -0.3003 299.0548 299.3551 307.4633 199.6798 -0.3003 299.1950 299.4953 307.4561 200.4970 -0.3025 299.3377 299.6401 307.4827 201.3040 -0.3022 299.4764 299.7785 307.5022 202.0900 -0.2975 299.5465 299.8440 307.4995 202.9175 -0.2969 299.6625 299.9594 307.4706 203.6835 -0.3021 299.8076 300.1097 307.4674 204.5413 -0.3053 299.9208 300.2261 307.4400 205.3073 -0.3067 300.0123 300.3190 307.4123 206.1245 -0.3058 300.1106 300.4164 307.4349 206.9313 -0.3062 300.2342 300.5404 307.4347 207.7278 -0.3057 300.3271 300.6328 307.4419 208.5245 -0.3073 300.4351 300.7424 307.4865 209.3108 -0.3057 300.5571 300.8628 307.5231 210.1485 -0.3043 300.6845 300.9888 307.5692 210.9143 -0.3039 300.7968 301.1006 307.6305 211.7723 -0.3034 300.9221 301.2256 307.6630 212.5280 -0.3058 301.0365 301.3423 307.7347 213.3655 -0.3021 301.1686 301.4707 307.8630 214.1620 -0.3017 301.2624 301.5640 307.9863 214.9588 -0.3029 301.3786 301.6814 308.1343 215.7758 -0.3059 301.4865 301.7924 308.2953 216.5515 -0.3097 301.5845 301.8943 308.4969 217.3998 -0.3092 301.6635 301.9727 308.7249 218.1450 -0.3107 301.7627 302.0734 308.9435 218.9928 -0.3086 301.8976 302.2062 309.2014 219.7690 -0.3108 302.0345 302.3454 309.4697 220.5860 -0.3130 302.1478 302.4609 309.7336 221.3828 -0.3136 302.2349 302.5486 310.0235 222.1795 -0.3170 302.3208 302.6378 310.3024 223.0065 -0.3188 302.4232 302.7420 310.6045 223.7725 -0.3060 302.5269 302.8328 310.8783 224.6205 -0.3047 302.6359 302.9406 311.1866 225.3965 -0.3079 302.7419 303.0498 311.4777 226.2240 -0.3136 302.8541 303.1677 311.7611 227.0205 -0.3156 302.9548 303.2703 312.0228 227.8068 -0.3164 303.0616 303.3780 312.2841 228.6445 -0.3157 303.1947 303.5105 312.5566 229.4103 -0.3167 303.3305 303.6472 312.7751 230.2583 -0.3195 303.4699 303.7894 312.9760 230.9935 -0.3213 303.5606 303.8818 313.1622 231.8410 -0.3219 303.6855 304.0075 313.3438 232.6070 -0.3218 303.8246 304.1464 313.4768 233.4345 -0.3244 303.9408 304.2652 313.6100 234.2208 -0.3312 304.0696 304.4009 313.7183 235.0178 -0.3306 304.2007 304.5312 313.8023 235.8448 -0.3309 304.3073 304.6382 313.8442 236.6108 -0.3362 304.4360 304.7722 313.8731 237.4690 -0.3437 304.5778 304.9216 313.9102 238.2140 -0.3447 304.6867 305.0314 313.9432 239.0415 -0.3440 304.7988 305.1428 313.9299 239.8075 -0.3453 304.8713 305.2165 313.9416 240.6653 -0.3407 304.9834 305.3241 313.9152 241.4210 -0.3444 305.0983 305.4426 313.8896 242.2485 -0.3459 305.2380 305.5840 313.8626 243.0450 -0.3461 305.3056 305.6517 313.8520 243.8418 -0.3454 305.4544 305.7998 313.8220 244.6588 -0.3462 305.5841 305.9303 313.8169 245.4348 -0.3492 305.6767 306.0259 313.7920 246.2830 -0.3494 305.8017 306.1511 313.7924 247.0178 -0.3457 305.9287 306.2744 313.8282 247.8760 -0.3493 306.0550 306.4043 313.8437 248.6420 -0.3509 306.1542 306.5051 313.8781 249.4690 -0.3515 306.2514 306.6029 313.9052 250.2555 -0.3500 306.3495 306.6996 313.9577 251.0625 -0.3528 306.4692 306.8220 314.0436 251.8793 -0.3512 306.6201 306.9713 314.1601 252.6453 -0.3469 306.7658 307.1127 314.3107 253.5035 -0.3495 306.8981 307.2476 314.4800 254.2690 -0.3517 307.0025 307.3541 314.6419 255.0968 -0.3510 307.1054 307.4564 314.8563 255.8830 -0.3498 307.1658 307.5156 315.0692 256.6898 -0.3486 307.2921 307.6407 315.2871 257.5070 -0.3556 307.4350 307.7906 315.5382 258.2728 -0.3635 307.5427 307.9062 315.7874 259.1308 -0.3635 307.6297 307.9931 316.0812 259.8970 -0.3672 307.7476 308.1148 316.3475 260.7240 -0.3670 307.8915 308.2586 316.6594 261.5105 -0.3694 308.0177 308.3871 316.9435 262.3175 -0.3710 308.1724 308.5433 317.2677 263.1343 -0.3752 308.3175 308.6927 317.5439 263.9005 -0.3752 308.4519 308.8271 317.8321 264.7585 -0.3784 308.5759 308.9543 318.1361 265.5243 -0.3788 308.6778 309.0566 318.3986 266.3520 -0.3812 308.8348 309.2160 318.6535 267.1380 -0.3871 308.9723 309.3594 318.9314 267.9453 -0.3880 309.0708 309.4588 319.1574 268.7623 -0.3898 309.1555 309.5452 319.3570 269.5283 -0.3916 309.2664 309.6579 319.5463 270.3865 -0.3933 309.3631 309.7564 319.7059 271.1520 -0.3958 309.4830 309.8788 319.8135 271.9795 -0.3988 309.5917 309.9905 319.9331 272.7763 -0.4016 309.7487 310.1504 320.0850 273.5725 -0.4000 309.9004 310.3004 320.1681 274.4000 -0.3985 310.0436 310.4421 320.2451 275.1660 -0.3982 310.1396 310.5378 320.2854 276.0135 -0.3988 310.2686 310.6674 320.3263 276.7898 -0.3991 310.3955 310.7946 320.3607 277.6070 -0.4009 310.5401 310.9410 320.3730 278.4135 -0.3996 310.6435 311.0431 320.3664 279.2103 -0.3996 310.7633 311.1630 320.3707 280.0378 -0.3994 310.9012 311.3006 320.3412 280.8033 -0.3985 310.9808 311.3793 320.3083 281.6615 -0.3990 311.0898 311.4888 320.2852 282.4173 -0.3978 311.2012 311.5990 320.2486 283.2548 -0.3988 311.3375 311.7363 320.2102 284.0515 -0.4003 311.4701 311.8704 320.2236 284.8480 -0.4022 311.6135 312.0157 320.1912 285.6650 -0.4024 311.7599 312.1622 320.2347 286.4410 -0.4030 311.8884 312.2914 320.2501 287.2993 -0.4041 312.0369 312.4410 320.2941 288.0648 -0.4065 312.1439 312.5504 320.3182 288.8820 -0.4078 312.2887 312.6965 320.3696 289.6890 -0.4053 312.4326 312.8379 320.4464 290.4750 -0.4003 312.5551 312.9554 320.5544 291.3130 -0.4020 312.6701 313.0722 320.6826 292.0685 -0.4019 312.8073 313.2091 320.8333 292.9368 -0.3992 312.9302 313.3295 321.0141 293.6618 -0.3996 313.0309 313.4305 321.1775 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