DTA measure 3pb_updown_3 Date: 2025101:1016 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1573.13 s Mass = 1111.600 mg data_number = 1957 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2193 -2.4840 455.0159 457.4999 433.7021 2.0260 -2.4848 455.0896 457.5744 433.8927 2.8123 -2.4899 455.1360 457.6259 434.1009 3.6398 -2.4967 455.1657 457.6624 434.3191 4.4055 -2.4994 455.1869 457.6863 434.4922 5.2635 -2.5022 455.2420 457.7442 434.6314 6.0295 -2.5055 455.2524 457.7579 434.7462 6.8465 -2.5085 455.2701 457.7786 434.8305 7.6533 -2.5144 455.3409 457.8553 434.8764 8.4395 -2.5173 455.4064 457.9237 434.9001 9.2670 -2.5208 455.4602 457.9810 434.9116 10.0325 -2.5223 455.5005 458.0227 434.8901 10.8598 -2.5290 455.5526 458.0816 434.8332 11.6258 -2.5355 455.6096 458.1451 434.7534 12.4735 -2.5417 455.6877 458.2294 434.6637 13.2495 -2.5493 455.7564 458.3057 434.5190 14.0665 -2.5517 455.8480 458.3997 434.3364 14.8633 -2.5544 455.8817 458.4361 434.1731 15.6595 -2.5581 455.8822 458.4403 434.0018 16.4970 -2.5606 455.8906 458.4513 433.7606 17.2528 -2.5624 455.9634 458.5258 433.5403 18.1108 -2.5637 456.0504 458.6141 433.2973 18.8765 -2.5620 456.0806 458.6426 433.0416 19.7040 -2.5617 456.1105 458.6722 432.7122 20.5005 -2.5656 456.1454 458.7110 432.4150 21.2970 -2.5681 456.2064 458.7746 432.1143 22.0935 -2.5696 456.2443 458.8138 431.8380 22.8903 -2.5724 456.2916 458.8640 431.5422 23.7173 -2.5732 456.3230 458.8962 431.2513 24.4730 -2.5748 456.3312 458.9060 430.9835 25.3415 -2.5780 456.3554 458.9334 430.6826 26.1070 -2.5794 456.4212 459.0006 430.4348 26.9345 -2.5815 456.4796 459.0611 430.1810 27.7313 -2.5829 456.5336 459.1165 429.9249 28.5275 -2.5824 456.5734 459.1559 429.6583 29.3550 -2.5830 456.6004 459.1834 429.4420 30.1210 -2.5823 456.6182 459.2005 429.2345 30.9685 -2.5815 456.6340 459.2155 429.0130 31.7140 -2.5806 456.6375 459.2182 428.8470 32.5723 -2.5824 456.6796 459.2621 428.6937 33.3380 -2.5814 456.7365 459.3178 428.5570 34.1553 -2.5808 456.7761 459.3568 428.4215 34.9620 -2.5812 456.8060 459.3872 428.3014 35.7585 -2.5809 456.8558 459.4368 428.2246 36.5860 -2.5853 456.8625 459.4478 428.1803 37.3415 -2.5873 456.8687 459.4561 428.0998 38.2098 -2.5867 456.8972 459.4839 428.0407 38.9755 -2.5896 456.8873 459.4768 428.0379 39.8028 -2.5872 456.8879 459.4751 428.0132 40.5890 -2.5845 456.9373 459.5218 428.0246 41.3960 -2.5854 456.9451 459.5306 428.0493 42.2235 -2.5857 456.9485 459.5342 428.1002 42.9890 -2.5885 456.9704 459.5589 428.1575 43.8368 -2.5855 457.0248 459.6102 428.2109 44.5823 -2.5852 457.0631 459.6484 428.2536 45.4300 -2.5867 457.0686 459.6553 428.2804 46.2060 -2.5892 457.0526 459.6419 428.2883 47.0230 -2.5931 457.0680 459.6611 428.3220 47.8300 -2.5962 457.0845 459.6808 428.3156 48.6365 -2.5990 457.1126 459.7116 428.3336 49.4535 -2.6013 457.1522 459.7535 428.3616 50.2093 -2.6034 457.1730 459.7764 428.3604 51.0775 -2.6005 457.1936 459.7941 428.3649 51.8023 -2.6049 457.1765 459.7815 428.3307 52.6500 -2.6077 457.2003 459.8079 428.2667 53.4260 -2.6071 457.2054 459.8126 428.2189 54.2430 -2.6094 457.2160 459.8254 428.1328 55.0395 -2.6131 457.2534 459.8665 428.0013 55.8363 -2.6165 457.2800 459.8965 427.8754 56.6533 -2.6163 457.3112 459.9276 427.7574 57.4188 -2.6101 457.3522 459.9623 427.6548 58.2770 -2.6075 457.3634 459.9709 427.4909 59.0328 -2.6089 457.3521 459.9610 427.3306 59.8598 -2.6115 457.3510 459.9626 427.1669 60.6565 -2.6136 457.3646 459.9782 427.0053 61.4533 -2.6118 457.3521 459.9639 426.7771 62.2700 -2.6110 457.3764 459.9874 426.6074 63.0360 -2.6140 457.3851 459.9991 426.4271 63.8940 -2.6128 457.3968 460.0096 426.2003 64.6598 -2.6157 457.3845 460.0002 426.0046 65.4768 -2.6211 457.3888 460.0100 425.7912 66.2838 -2.6235 457.4095 460.0330 425.5844 67.0700 -2.6253 457.4125 460.0378 425.3619 67.8973 -2.6262 457.4369 460.0630 425.1474 68.6633 -2.6295 457.3775 460.0070 424.9573 69.5213 -2.6308 457.3576 459.9885 424.8039 70.2563 -2.6306 457.3563 459.9869 424.6625 71.1043 -2.6310 457.3579 459.9890 424.4736 71.8803 -2.6321 457.3646 459.9967 424.2930 72.7075 -2.6328 457.3325 459.9653 424.1259 73.5040 -2.6338 457.3354 459.9692 423.9936 74.2903 -2.6339 457.3452 459.9791 423.8731 75.1278 -2.6359 457.3588 459.9947 423.7382 75.8833 -2.6379 457.3953 460.0332 423.6245 76.7415 -2.6382 457.4074 460.0456 423.5180 77.5073 -2.6400 457.3961 460.0361 423.4226 78.3345 -2.6409 457.3854 460.0263 423.3240 79.1313 -2.6420 457.3959 460.0378 423.2607 79.9175 -2.6443 457.3880 460.0323 423.1931 80.7550 -2.6428 457.3815 460.0243 423.1342 81.5105 -2.6445 457.3755 460.0199 423.0980 82.3688 -2.6423 457.3400 459.9823 423.0449 83.1343 -2.6429 457.3497 459.9927 422.9808 83.9718 -2.6438 457.3268 459.9706 422.9411 84.7583 -2.6440 457.3258 459.9698 422.9055 85.5548 -2.6476 457.3123 459.9600 422.8294 86.3820 -2.6478 457.2762 459.9240 422.7779 87.1580 -2.6464 457.2570 459.9034 422.7214 88.0060 -2.6468 457.2299 459.8767 422.7006 88.7715 -2.6439 457.2192 459.8631 422.6643 89.5990 -2.6421 457.2041 459.8462 422.6083 90.3955 -2.6412 457.1718 459.8130 422.5496 91.1920 -2.6383 457.1389 459.7772 422.5262 92.0193 -2.6372 457.1156 459.7527 422.4788 92.7853 -2.6339 457.0907 459.7245 422.4391 93.6433 -2.6283 457.0635 459.6918 422.3742 94.4090 -2.6240 457.0554 459.6794 422.3102 95.2263 -2.6209 457.0531 459.6739 422.2570 96.0330 -2.6249 457.0471 459.6720 422.1905 96.8193 -2.6314 457.0011 459.6325 422.1193 97.6568 -2.6309 456.9556 459.5865 421.9996 98.4125 -2.6387 456.9276 459.5663 421.8806 99.2808 -2.6514 456.9111 459.5624 421.7687 100.0363 -2.6527 456.8956 459.5483 421.6592 100.8638 -2.6549 456.8950 459.5499 421.5146 101.6600 -2.6587 456.8821 459.5409 421.4010 102.4568 -2.6588 456.8617 459.5205 421.2810 103.2843 -2.6674 456.8544 459.5219 421.1408 104.0498 -2.6696 456.8342 459.5038 421.0051 104.9080 -2.6716 456.8342 459.5057 420.8518 105.6738 -2.6757 456.7973 459.4730 420.7027 106.5010 -2.6768 456.7622 459.4390 420.5676 107.2975 -2.6768 456.6970 459.3738 420.4038 108.0940 -2.6801 456.6782 459.3583 420.2416 108.8908 -2.6859 456.6458 459.3317 420.0765 109.6870 -2.6864 456.6235 459.3099 419.9200 110.5040 -2.6871 456.5618 459.2489 419.7795 111.2803 -2.6877 456.5148 459.2025 419.6517 112.1383 -2.6870 456.4823 459.1692 419.4656 112.9038 -2.6915 456.4569 459.1485 419.3357 113.7210 -2.6924 456.4331 459.1255 419.2162 114.5178 -2.6925 456.4065 459.0990 419.0780 115.3143 -2.6925 456.3503 459.0427 418.9746 116.1313 -2.6905 456.3336 459.0241 418.8585 116.8973 -2.6889 456.3086 458.9975 418.7102 117.7448 -2.6881 456.2854 458.9735 418.5515 118.5108 -2.6892 456.2232 458.9124 418.4329 119.3383 -2.6907 456.1924 458.8831 418.3139 120.0935 -2.6917 456.1395 458.8312 418.1975 120.9210 -2.6906 456.1075 458.7981 418.1028 121.7178 -2.6945 456.1169 458.8114 418.0009 122.5140 -2.6958 456.0644 458.7602 417.9000 123.3310 -2.6947 456.0051 458.6998 417.8044 124.1073 -2.6935 455.9947 458.6882 417.7029 124.9550 -2.6869 455.9219 458.6088 417.6175 125.7208 -2.6878 455.8746 458.5624 417.5506 126.5483 -2.6876 455.8527 458.5402 417.4773 127.3345 -2.6917 455.8135 458.5053 417.4233 128.1308 -2.6954 455.7628 458.4583 417.3530 128.9583 -2.6950 455.7053 458.4003 417.2677 129.7243 -2.6946 455.6768 458.3714 417.1838 130.5513 -2.6952 455.6375 458.3327 417.0738 131.3070 -2.6973 455.6083 458.3056 416.9993 132.1755 -2.6963 455.5665 458.2628 416.9310 132.9308 -2.6958 455.5247 458.2205 416.8980 133.7580 -2.6974 455.4844 458.1818 416.8027 134.5548 -2.6999 455.4558 458.1557 416.6918 135.3513 -2.7011 455.3932 458.0943 416.6035 136.1785 -2.7004 455.3312 458.0316 416.5031 136.9340 -2.7035 455.2879 457.9914 416.4124 137.8025 -2.7031 455.2391 457.9422 416.3321 138.5270 -2.7059 455.2064 457.9123 416.2592 139.3853 -2.7012 455.1800 457.8812 416.1750 140.1513 -2.6989 455.1191 457.8179 416.1304 140.9783 -2.6994 455.0386 457.7380 416.0654 141.7748 -2.7036 455.0226 457.7262 415.9936 142.5715 -2.7076 454.9684 457.6759 415.8650 143.3988 -2.7036 454.9069 457.6105 415.7766 144.1643 -2.7093 454.8503 457.5597 415.6754 145.0225 -2.7120 454.8029 457.5149 415.5605 145.7783 -2.7116 454.7511 457.4626 415.4429 146.6155 -2.7122 454.6923 457.4045 415.3211 147.4020 -2.7124 454.6188 457.3313 415.2339 148.2088 -2.7130 454.5710 457.2840 415.1185 149.0258 -2.7122 454.5342 457.2463 415.0244 149.8018 -2.7157 454.5188 457.2345 414.9029 150.6495 -2.7126 454.4928 457.2054 414.7692 151.3848 -2.7101 454.4467 457.1567 414.6626 152.2425 -2.7140 454.3833 457.0974 414.5350 153.0393 -2.7135 454.3225 457.0359 414.4093 153.8360 -2.7112 454.2510 456.9622 414.2625 154.6220 -2.7097 454.2070 456.9167 414.1390 155.4290 -2.7140 454.1517 456.8657 414.0258 156.2768 -2.7153 454.1189 456.8341 413.8854 157.0220 -2.7171 454.1002 456.8174 413.7597 157.8698 -2.7207 454.0617 456.7823 413.6228 158.6460 -2.7218 453.9877 456.7095 413.5075 159.4630 -2.7189 453.9148 456.6337 413.3632 160.2595 -2.7214 453.8451 456.5665 413.2368 161.0563 -2.7215 453.8013 456.5227 413.0890 161.8835 -2.7229 453.7605 456.4834 412.9686 162.6495 -2.7252 453.6932 456.4183 412.8553 163.5075 -2.7261 453.6431 456.3692 412.7287 164.2733 -2.7252 453.6233 456.3485 412.6005 165.1003 -2.7236 453.5435 456.2672 412.4816 165.8973 -2.7266 453.4833 456.2098 412.3762 166.6835 -2.7254 453.4242 456.1495 412.2626 167.5208 -2.7298 453.3671 456.0968 412.1551 168.2868 -2.7271 453.2986 456.0257 412.0594 169.1450 -2.7231 453.2506 455.9737 411.9375 169.9003 -2.7253 453.1993 455.9246 411.8504 170.7380 -2.7211 453.1292 455.8503 411.7439 171.5348 -2.7189 453.0531 455.7720 411.6498 172.3310 -2.7164 453.0072 455.7236 411.5611 173.1480 -2.7162 452.9277 455.6439 411.4760 173.9243 -2.7167 452.8508 455.5675 411.3718 174.7720 -2.7157 452.7783 455.4940 411.2768 175.5378 -2.7181 452.7063 455.4244 411.1983 176.3650 -2.7140 452.6585 455.3725 411.1017 177.1618 -2.7147 452.5814 455.2960 410.9980 177.9580 -2.7182 452.4920 455.2102 410.9455 178.7753 -2.7196 452.4272 455.1468 410.8680 179.5410 -2.7170 452.3515 455.0685 410.7616 180.3888 -2.7184 452.3019 455.0203 410.6725 181.1548 -2.7181 452.2445 454.9626 410.6029 181.9820 -2.7110 452.1754 454.8864 410.5471 182.7683 -2.7109 452.0990 454.8099 410.4543 183.5648 -2.7055 452.0444 454.7499 410.3957 184.3923 -2.6992 451.9935 454.6927 410.3105 185.1580 -2.6978 451.9591 454.6569 410.2167 186.0058 -2.6998 451.8774 454.5772 410.1422 186.7820 -2.7024 451.7836 454.4860 410.0608 187.5990 -2.7063 451.6913 454.3976 409.9255 188.3850 -2.7063 451.6097 454.3160 409.8279 189.1920 -2.7087 451.6026 454.3113 409.7180 189.9785 -2.7110 451.5382 454.2492 409.6096 190.7750 -2.7088 451.4466 454.1554 409.5054 191.6023 -2.6890 451.3686 454.0576 409.3879 192.3683 -2.6656 451.3159 453.9815 409.3186 193.2260 -2.6441 451.2422 453.8863 409.2090 193.9818 -2.6322 451.1593 453.7914 409.1050 194.8193 -2.6258 451.0997 453.7255 408.9962 195.6055 -2.6193 451.0209 453.6402 408.8845 196.4023 -2.6212 450.9402 453.5614 408.7543 197.2298 -2.6205 450.8846 453.5051 408.5949 197.9953 -2.6273 450.8423 453.4696 408.4721 198.8535 -2.6353 450.7765 453.4119 408.3360 199.6093 -2.6340 450.6908 453.3248 408.2369 200.4465 -2.6289 450.6361 453.2650 408.0998 201.2330 -2.6228 450.5718 453.1946 407.9632 202.0295 -2.6220 450.5127 453.1347 407.8304 202.8568 -2.6340 450.4138 453.0478 407.7259 203.6225 -2.6431 450.3231 452.9662 407.5909 204.4808 -2.6528 450.2706 452.9235 407.4478 205.2363 -2.6607 450.2306 452.8913 407.3190 206.0738 -2.6661 450.1522 452.8184 407.2181 206.8603 -2.6682 450.0808 452.7490 407.1093 207.6568 -2.6662 450.0017 452.6679 407.0118 208.4840 -2.6554 449.9199 452.5753 406.9101 209.2500 -2.6467 449.8392 452.4859 406.8228 210.1080 -2.6440 449.7566 452.4005 406.6726 210.8635 -2.6457 449.6942 452.3399 406.5569 211.7013 -2.6532 449.5993 452.2524 406.4326 212.4875 -2.6626 449.5207 452.1833 406.3425 213.2840 -2.6666 449.4323 452.0989 406.2271 214.1115 -2.6701 449.3362 452.0062 406.1189 214.8875 -2.6728 449.2853 451.9582 406.0114 215.7043 -2.6722 449.2398 451.9120 405.8706 216.4703 -2.6758 449.1558 451.8316 405.7983 217.3285 -2.6766 449.0896 451.7663 405.7164 218.0940 -2.6769 448.9988 451.6757 405.6195 218.9218 -2.6771 448.9262 451.6033 405.5702 219.7183 -2.6782 448.8467 451.5249 405.4767 220.5145 -2.6813 448.7289 451.4102 405.3978 221.3420 -2.6846 448.6364 451.3210 405.2968 222.1078 -2.6826 448.5578 451.2404 405.2034 222.9555 -2.6830 448.4766 451.1597 405.0695 223.7315 -2.6795 448.4118 451.0913 404.9850 224.5488 -2.6769 448.3198 450.9967 404.8839 225.3248 -2.6703 448.2511 450.9214 404.7634 226.1418 -2.6683 448.1785 450.8468 404.6554 226.9485 -2.6669 448.1182 450.7852 404.5690 227.7350 -2.6627 448.0344 450.6971 404.4780 228.5620 -2.6614 447.9457 450.6071 404.3706 229.3280 -2.6628 447.8457 450.5085 404.2581 230.1963 -2.6661 447.7475 450.4135 404.1676 230.9518 -2.6677 447.6541 450.3218 404.0910 231.7790 -2.6660 447.5451 450.2111 404.0128 232.5758 -2.6653 447.5186 450.1840 403.9309 233.3825 -2.6683 447.4615 450.1298 403.8387 234.1688 -2.6648 447.3979 450.0628 403.7429 234.9755 -2.6621 447.3098 449.9719 403.6337 235.7928 -2.6602 447.2119 449.8721 403.5532 236.5685 -2.6616 447.1609 449.8225 403.4251 237.4165 -2.6614 447.0845 449.7458 403.3108 238.1825 -2.6640 447.0032 449.6673 403.2091 239.0095 -2.6605 446.8851 449.5457 403.1198 239.8165 -2.6560 446.7750 449.4310 403.0154 240.6030 -2.6580 446.7009 449.3588 402.8936 241.4095 -2.6553 446.6615 449.3168 402.7975 242.1960 -2.6534 446.5785 449.2318 402.6848 243.0235 -2.6534 446.4928 449.1463 402.5805 243.7890 -2.6562 446.4149 449.0710 402.4628 244.6368 -2.6595 446.3235 448.9830 402.3513 245.4130 -2.6606 446.2254 448.8860 402.2653 246.2300 -2.6575 446.1435 448.8009 402.1430 247.0163 -2.6566 446.0827 448.7393 402.0372 247.8130 -2.6571 445.9969 448.6541 401.9043 248.6095 -2.6585 445.8942 448.5527 401.7704 249.3958 -2.6590 445.8084 448.4674 401.6498 250.2335 -2.6616 445.7433 448.4049 401.5546 250.9890 -2.6604 445.6574 448.3178 401.4458 251.8368 -2.6606 445.5764 448.2370 401.3320 252.6128 -2.6623 445.4777 448.1400 401.2438 253.4300 -2.6613 445.4117 448.0730 401.1363 254.2263 -2.6593 445.3364 447.9957 400.9960 255.0228 -2.6542 445.2653 447.9195 400.8740 255.8503 -2.6524 445.1711 447.8234 400.7309 256.6160 -2.6558 445.0961 447.7518 400.5884 257.4638 -2.6556 445.0086 447.6642 400.4647 258.2090 -2.6532 444.9111 447.5644 400.3776 259.0568 -2.6502 444.7903 447.4404 400.2643 259.8225 -2.6466 444.7317 447.3783 400.1755 260.6495 -2.6448 444.6326 447.2774 400.0977 261.4463 -2.6445 444.5250 447.1695 399.9969 262.2430 -2.6421 444.4380 447.0801 399.9264 263.0598 -2.6387 444.3602 446.9989 399.8376 263.8358 -2.6350 444.3010 446.9361 399.7395 264.6838 -2.6349 444.2183 446.8532 399.6407 265.4495 -2.6374 444.1380 446.7754 399.5397 266.2768 -2.6377 444.0282 446.6659 399.4213 267.0735 -2.6359 443.9233 446.5591 399.3174 267.8700 -2.6347 443.8173 446.4520 399.2143 268.6870 -2.6310 443.7035 446.3345 399.0963 269.4633 -2.6267 443.6422 446.2689 399.0163 270.3110 -2.6214 443.5534 446.1749 398.9118 271.0765 -2.6191 443.4793 446.0983 398.7922 271.9040 -2.6212 443.3727 445.9939 398.6732 272.7008 -2.6166 443.2834 445.9000 398.5732 273.4970 -2.6132 443.2220 445.8353 398.4840 274.3143 -2.6188 443.1478 445.7666 398.3420 275.0905 -2.6227 443.0497 445.6724 398.2441 275.9483 -2.6185 442.9486 445.5671 398.1449 276.7143 -2.6147 442.8627 445.4773 398.0612 277.5313 -2.6115 442.7841 445.3956 397.9547 278.3380 -2.6110 442.6946 445.3056 397.8490 279.1245 -2.6135 442.5965 445.2101 397.7450 279.9518 -2.6124 442.5094 445.1219 397.6065 280.7175 -2.6128 442.4414 445.0541 397.4996 281.5755 -2.6137 442.3825 444.9962 397.3850 282.3415 -2.6136 442.2914 444.9050 397.2694 283.1585 -2.6138 442.1802 444.7940 397.1821 283.9655 -2.6115 442.0740 444.6855 397.0787 284.7623 -2.6110 441.9847 444.5957 396.9919 285.5893 -2.6090 441.8604 444.4695 396.8996 286.3448 -2.6058 441.7536 444.3594 396.8083 287.2133 -2.6051 441.6011 444.2062 396.6824 287.9688 -2.6055 441.5641 444.1696 396.5749 288.8063 -2.6039 441.5196 444.1235 396.4865 289.5928 -2.6031 441.4686 444.0717 396.3944 290.3995 -2.6067 441.3858 443.9925 396.3234 291.1855 -2.6040 441.2844 443.8884 396.2341 291.9823 -2.6040 441.2002 443.8042 396.1234 292.8405 -2.6018 441.1068 443.7086 396.0117 293.5855 -2.6025 441.0365 443.6390 395.9443 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