DTA measure 1DTA1_SN3 Date: 202623:1522 Lower limit = 100.0 C Upper limit = 340.0 C Rate = 10.00 C/min Mtime = 1439.55 s Mass = 0.987 mg data_number = 1791 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1283 0.4398 199.9867 199.5469 170.8155 1.9460 0.4433 199.9124 199.4691 170.7404 2.7425 0.4420 199.8447 199.4028 170.6744 3.5395 0.4416 199.7870 199.3454 170.6133 4.3675 0.4430 199.7159 199.2729 170.5368 5.1340 0.4464 199.6553 199.2089 170.4699 5.9928 0.4505 199.5897 199.1392 170.4395 6.7285 0.4525 199.5534 199.1009 170.3750 7.5865 0.4528 199.5056 199.0528 170.3140 8.3528 0.4574 199.4389 198.9815 170.2662 9.1705 0.4574 199.3576 198.9002 170.1759 9.9780 0.4580 199.2599 198.8019 170.1076 10.7650 0.4559 199.1942 198.7383 170.0528 11.5930 0.4568 199.1173 198.6605 169.9801 12.3588 0.4603 199.0417 198.5814 169.9329 13.2070 0.4578 198.9384 198.4806 169.8732 13.9735 0.4574 198.8732 198.4158 169.8097 14.8015 0.4585 198.8047 198.3462 169.7475 15.5885 0.4564 198.7440 198.2876 169.6713 16.3755 0.4545 198.6706 198.2162 169.6290 17.2138 0.4586 198.5848 198.1262 169.5580 17.9693 0.4588 198.5186 198.0599 169.4968 18.8175 0.4569 198.4649 198.0080 169.4365 19.5635 0.4562 198.4125 197.9563 169.4112 20.4120 0.4569 198.3246 197.8677 169.3510 21.1785 0.4584 198.2499 197.7915 169.2824 22.0063 0.4602 198.1698 197.7096 169.2104 22.7925 0.4595 198.1059 197.6464 169.1354 23.5898 0.4580 198.0398 197.5818 169.0849 24.4178 0.4578 197.9685 197.5107 169.0336 25.1843 0.4602 197.9004 197.4402 168.9688 26.0428 0.4619 197.8210 197.3591 168.9068 26.7983 0.4665 197.7412 197.2746 168.8692 27.6365 0.4671 197.6691 197.2020 168.8102 28.4235 0.4688 197.6136 197.1448 168.7652 29.2208 0.4732 197.5520 197.0788 168.7096 30.0488 0.4732 197.5006 197.0274 168.6317 30.8153 0.4708 197.4150 196.9442 168.5590 31.6433 0.4672 197.3498 196.8826 168.4905 32.3988 0.4665 197.2751 196.8086 168.4535 33.2573 0.4657 197.2018 196.7361 168.3975 34.0238 0.4658 197.1159 196.6501 168.3142 34.8415 0.4677 197.0687 196.6011 168.2523 35.6490 0.4705 196.9886 196.5181 168.1940 36.4360 0.4719 196.9092 196.4374 168.1309 37.2635 0.4721 196.8387 196.3665 168.0580 38.0295 0.4691 196.7992 196.3300 168.0033 38.8883 0.4658 196.7297 196.2639 167.9573 39.6548 0.4620 196.6407 196.1787 167.9206 40.4725 0.4601 196.5680 196.1079 167.8491 41.2800 0.4593 196.5060 196.0468 167.7731 42.0668 0.4626 196.4344 195.9718 167.7096 42.8940 0.4685 196.3699 195.9014 167.6512 43.6605 0.4701 196.3137 195.8436 167.5872 44.5193 0.4747 196.2321 195.7574 167.5361 45.2858 0.4764 196.1664 195.6900 167.4813 46.1035 0.4768 196.0867 195.6099 167.3925 46.9105 0.4767 196.0094 195.5327 167.3563 47.6970 0.4780 195.9697 195.4916 167.3018 48.5250 0.4756 195.9151 195.4395 167.2525 49.2915 0.4746 195.8499 195.3753 167.1916 50.1503 0.4782 195.7693 195.2911 167.0897 50.9168 0.4763 195.7279 195.2516 167.0419 51.7338 0.4777 195.6397 195.1620 166.9868 52.5410 0.4791 195.5567 195.0775 166.9026 53.3280 0.4796 195.4854 195.0058 166.8463 54.1663 0.4786 195.4329 194.9542 166.7716 54.9225 0.4772 195.3474 194.8701 166.7244 55.7910 0.4803 195.2689 194.7886 166.6871 56.5775 0.4816 195.1884 194.7068 166.6418 57.3748 0.4802 195.1233 194.6432 166.5794 58.2028 0.4813 195.0508 194.5694 166.5181 58.9693 0.4818 194.9747 194.4929 166.4774 59.8280 0.4825 194.9029 194.4203 166.4257 60.5833 0.4850 194.8695 194.3845 166.3578 61.4215 0.4868 194.8196 194.3327 166.3105 62.2085 0.4874 194.7424 194.2550 166.2439 63.0058 0.4866 194.6680 194.1814 166.2177 63.8338 0.4858 194.5901 194.1043 166.1620 64.6003 0.4854 194.5076 194.0222 166.1120 65.4588 0.4867 194.4330 193.9463 166.0400 66.2245 0.4883 194.3706 193.8823 165.9886 67.0525 0.4882 194.2987 193.8105 165.9224 67.8190 0.4898 194.2403 193.7505 165.8533 68.6470 0.4898 194.1400 193.6502 165.7690 69.4340 0.4933 194.0772 193.5839 165.7071 70.2415 0.4939 194.0210 193.5271 165.6382 71.0690 0.4935 193.9574 193.4638 165.5798 71.8350 0.4946 193.9279 193.4334 165.5415 72.6835 0.4914 193.8440 193.3526 165.4780 73.4603 0.4915 193.7738 193.2823 165.4208 74.2780 0.4945 193.6946 193.2001 165.3646 75.0753 0.4957 193.6012 193.1055 165.2966 75.8725 0.4972 193.5246 193.0274 165.2249 76.6998 0.4977 193.4549 192.9571 165.1964 77.4558 0.4994 193.4019 192.9024 165.1481 78.3145 0.4996 193.3213 192.8216 165.0661 79.0708 0.4987 193.2679 192.7692 164.9805 79.8885 0.4992 193.2143 192.7151 164.9110 80.6858 0.4974 193.1790 192.6816 164.8305 81.4828 0.4972 193.1032 192.6061 164.7901 82.2793 0.4946 193.0196 192.5251 164.7285 83.0765 0.4921 192.9448 192.4527 164.6808 83.9045 0.4959 192.8981 192.4023 164.5971 84.6608 0.4986 192.8173 192.3187 164.5494 85.5195 0.4936 192.7057 192.2120 164.5066 86.2855 0.4926 192.6381 192.1455 164.4365 87.1028 0.4944 192.5919 192.0975 164.3775 87.8693 0.4950 192.5289 192.0339 164.3342 88.6973 0.4962 192.4385 191.9423 164.2960 89.4945 0.4972 192.3703 191.8731 164.2528 90.2815 0.4948 192.3229 191.8281 164.1911 91.1188 0.4957 192.2698 191.7741 164.1438 91.8750 0.4950 192.1980 191.7030 164.0932 92.7338 0.4987 192.1125 191.6138 164.0235 93.5003 0.4975 192.0397 191.5422 163.9538 94.3180 0.4970 191.9680 191.4710 163.8637 95.0840 0.5021 191.9214 191.4193 163.8308 95.9115 0.5092 191.8568 191.3476 163.7857 96.7088 0.5109 191.7804 191.2695 163.7309 97.5060 0.5110 191.7234 191.2124 163.6755 98.3238 0.5105 191.6486 191.1381 163.6261 99.1005 0.5089 191.5651 191.0562 163.5667 99.9488 0.5070 191.5052 190.9982 163.5056 100.7145 0.5058 191.4253 190.9194 163.4594 101.5425 0.5068 191.3548 190.8480 163.3965 102.3398 0.5013 191.2850 190.7837 163.3385 103.1370 0.4981 191.2003 190.7022 163.2753 103.9240 0.5005 191.1483 190.6478 163.2023 104.7315 0.5033 191.0852 190.5818 163.1358 105.5483 0.5069 191.0054 190.4985 163.0878 106.3148 0.5093 190.9346 190.4253 163.0131 107.1735 0.5117 190.8896 190.3778 162.9376 107.9400 0.5073 190.8508 190.3435 162.8869 108.7680 0.5052 190.7837 190.2785 162.8497 109.5550 0.5026 190.7062 190.2036 162.8151 110.3625 0.5050 190.6481 190.1431 162.7475 111.1793 0.5058 190.5892 190.0834 162.7062 111.9458 0.5030 190.5413 190.0383 162.6504 112.8045 0.5001 190.4892 189.9890 162.5714 113.5710 0.5003 190.4110 189.9107 162.5167 114.3990 0.5015 190.3462 189.8447 162.4420 115.1860 0.5030 190.2533 189.7503 162.3712 115.9928 0.5028 190.1836 189.6807 162.3122 116.8103 0.5052 190.1065 189.6013 162.2615 117.5768 0.5074 190.0354 189.5280 162.2190 118.4355 0.5103 189.9513 189.4410 162.1441 119.2020 0.5137 189.8609 189.3471 162.0919 120.0300 0.5140 189.7854 189.2714 162.0395 120.8160 0.5140 189.7297 189.2157 161.9939 121.6235 0.5130 189.6477 189.1348 161.9300 122.4413 0.5128 189.5796 189.0668 161.8748 123.2078 0.5135 189.5545 189.0410 161.8358 124.0665 0.5108 189.4917 188.9809 161.7469 124.8328 0.5107 189.4484 188.9377 161.6872 125.6600 0.5079 189.3616 188.8537 161.6471 126.4470 0.5081 189.2762 188.7680 161.6058 127.2545 0.5086 189.2064 188.6978 161.5595 128.0723 0.5077 189.1505 188.6429 161.4793 128.8385 0.5079 189.1062 188.5983 161.4063 129.6658 0.5080 189.0273 188.5193 161.3317 130.4425 0.5097 188.9575 188.4479 161.2900 131.2910 0.5117 188.8918 188.3801 161.2447 132.0575 0.5089 188.8484 188.3394 161.1725 132.8855 0.5105 188.7809 188.2704 161.1383 133.6823 0.5101 188.7284 188.2183 161.0754 134.4790 0.5102 188.6692 188.1590 161.0247 135.2968 0.5146 188.6025 188.0879 160.9757 136.0735 0.5160 188.5378 188.0217 160.9477 136.9220 0.5172 188.4879 187.9708 160.9033 137.6878 0.5183 188.4275 187.9092 160.8468 138.5155 0.5145 188.3696 187.8551 160.7741 139.3128 0.5139 188.3058 187.7920 160.7411 140.1100 0.5187 188.2150 187.6963 160.7123 140.9278 0.5173 188.1305 187.6132 160.6590 141.6943 0.5154 188.0521 187.5367 160.6234 142.5420 0.5142 187.9533 187.4391 160.5427 143.3083 0.5137 187.8941 187.3804 160.4645 144.1260 0.5144 187.8141 187.2997 160.4068 144.9233 0.5152 187.7563 187.2411 160.3591 145.7205 0.5175 187.7133 187.1959 160.2912 146.5383 0.5194 187.6401 187.1207 160.2435 147.3048 0.5224 187.5751 187.0527 160.1899 148.1633 0.5211 187.5140 186.9929 160.1036 148.9188 0.5212 187.4492 186.9280 160.0601 149.7468 0.5189 187.3794 186.8605 159.9854 150.5440 0.5194 187.3095 186.7902 159.9328 151.3310 0.5202 187.2512 186.7310 159.8705 152.1590 0.5225 187.1930 186.6706 159.8217 152.9255 0.5209 187.1373 186.6164 159.7857 153.7735 0.5207 187.0705 186.5498 159.7047 154.5395 0.5230 186.9999 186.4769 159.6199 155.3675 0.5229 186.9517 186.4287 159.5303 156.1648 0.5240 186.8700 186.3461 159.4827 156.9620 0.5263 186.8001 186.2738 159.4487 157.7488 0.5302 186.7421 186.2120 159.4050 158.5555 0.5305 186.6742 186.1438 159.3767 159.3733 0.5341 186.6098 186.0757 159.3216 160.1398 0.5337 186.5355 186.0018 159.2688 160.9985 0.5320 186.4736 185.9416 159.2057 161.7650 0.5305 186.4112 185.8807 159.1688 162.5920 0.5283 186.3339 185.8055 159.1268 163.3790 0.5282 186.2733 185.7450 159.0419 164.1865 0.5279 186.1883 185.6604 158.9859 165.0043 0.5297 186.1079 185.5782 158.9419 165.7708 0.5281 186.0479 185.5198 158.8918 166.6290 0.5289 185.9878 185.4589 158.8221 167.3950 0.5323 185.9424 185.4102 158.7603 168.2230 0.5308 185.8672 185.3364 158.7042 169.0100 0.5321 185.7949 185.2627 158.6546 169.8175 0.5354 185.7307 185.1953 158.6378 170.6353 0.5368 185.6555 185.1187 158.6073 171.4018 0.5374 185.5438 185.0064 158.5494 172.2598 0.5384 185.4699 184.9316 158.5013 173.0363 0.5373 185.4370 184.8996 158.4346 173.8540 0.5361 185.3854 184.8493 158.3563 174.6513 0.5352 185.3078 184.7727 158.2927 175.4485 0.5339 185.2324 184.6985 158.2507 176.2765 0.5331 185.1932 184.6602 158.1977 177.0425 0.5344 185.1333 184.5989 158.1397 177.8905 0.5387 185.0540 184.5152 158.0779 178.6673 0.5381 184.9691 184.4310 157.9999 179.4850 0.5382 184.9221 184.3839 157.9364 180.2515 0.5410 184.8725 184.3315 157.8968 181.0795 0.5413 184.7994 184.2581 157.8619 181.8758 0.5423 184.7408 184.1985 157.7867 182.6730 0.5430 184.6548 184.1118 157.7301 183.4908 0.5432 184.5882 184.0450 157.6642 184.2675 0.5416 184.5278 183.9862 157.6072 185.1160 0.5375 184.4684 183.9308 157.5413 185.8825 0.5390 184.4077 183.8687 157.4785 186.7105 0.5409 184.3522 183.8113 157.4094 187.5068 0.5440 184.2950 183.7510 157.3103 188.3040 0.5469 184.2229 183.6759 157.2714 189.1218 0.5479 184.1584 183.6105 157.2161 189.8985 0.5445 184.1029 183.5584 157.1809 190.7573 0.5398 184.0338 183.4940 157.1231 191.5238 0.5388 183.9494 183.4106 157.0949 192.3413 0.5374 183.8743 183.3369 157.0596 193.1173 0.5376 183.8305 183.2929 157.0150 193.9453 0.5412 183.7567 183.2155 156.9540 194.7425 0.5417 183.6890 183.1473 156.9232 195.5295 0.5370 183.6290 183.0920 156.8630 196.3678 0.5369 183.5655 183.0287 156.7999 197.1230 0.5345 183.4952 182.9607 156.7220 197.9818 0.5361 183.4440 182.9078 156.6749 198.7483 0.5410 183.3801 182.8391 156.6172 199.5763 0.5379 183.3140 182.7761 156.5572 200.3735 0.5403 183.2506 182.7103 156.4744 201.1708 0.5433 183.1525 182.6092 156.4500 201.9675 0.5447 183.1013 182.5566 156.4090 202.7643 0.5416 183.0424 182.5008 156.3482 203.5923 0.5414 182.9697 182.4283 156.2770 204.3485 0.5428 182.9174 182.3746 156.2180 205.2073 0.5472 182.8348 182.2876 156.1377 205.9635 0.5502 182.7838 182.2337 156.0926 206.7915 0.5473 182.7084 182.1611 156.0478 207.5885 0.5483 182.6405 182.0923 155.9892 208.3748 0.5484 182.5894 182.0411 155.9527 209.2028 0.5521 182.5358 181.9837 155.9192 209.9590 0.5511 182.4871 181.9360 155.8754 210.7870 0.5490 182.4206 181.8716 155.8127 211.5535 0.5474 182.3723 181.8249 155.7608 212.4020 0.5508 182.2971 181.7463 155.6882 213.1683 0.5520 182.2294 181.6775 155.6468 213.9955 0.5514 182.1538 181.6024 155.5904 214.7928 0.5490 182.0870 181.5379 155.5153 215.5798 0.5447 182.0155 181.4708 155.4600 216.4078 0.5442 181.9524 181.4082 155.3833 217.1738 0.5447 181.8924 181.3477 155.3253 218.0320 0.5476 181.8397 181.2921 155.2804 218.7575 0.5499 181.7682 181.2182 155.2490 219.6265 0.5518 181.6769 181.1251 155.1973 220.3828 0.5522 181.6142 181.0620 155.1399 221.2005 0.5529 181.5724 181.0195 155.0821 222.0078 0.5519 181.4981 180.9462 155.0467 222.7940 0.5518 181.4487 180.8969 155.0023 223.6220 0.5509 181.3847 180.8338 154.9420 224.3885 0.5509 181.3450 180.7941 154.8591 225.2473 0.5542 181.3090 180.7548 154.7964 226.0138 0.5573 181.2657 180.7084 154.7497 226.8315 0.5570 181.2227 180.6657 154.6935 227.6390 0.5533 181.1564 180.6032 154.6354 228.4258 0.5540 181.0840 180.5300 154.5908 229.2530 0.5525 181.0373 180.4847 154.5426 230.0195 0.5508 180.9779 180.4270 154.5141 230.8475 0.5525 180.8883 180.3358 154.4700 231.6140 0.5510 180.8131 180.2621 154.4340 232.4625 0.5530 180.7481 180.1950 154.3762 233.2393 0.5543 180.6808 180.1265 154.3117 234.0560 0.5564 180.5866 180.0302 154.2491 234.8533 0.5581 180.5265 179.9684 154.2223 235.6505 0.5573 180.4883 179.9310 154.1790 236.4785 0.5559 180.4271 179.8713 154.1270 237.2450 0.5560 180.3734 179.8174 154.0505 238.0935 0.5582 180.2789 179.7207 153.9752 238.8693 0.5563 180.1995 179.6432 153.9437 239.6870 0.5569 180.1203 179.5634 153.8918 240.4843 0.5604 180.0654 179.5050 153.8338 241.2815 0.5627 179.9915 179.4288 153.7758 242.1198 0.5588 179.9373 179.3785 153.7151 242.8760 0.5615 179.9003 179.3388 153.6524 243.7345 0.5605 179.8330 179.2724 153.6022 244.5003 0.5590 179.7718 179.2129 153.5657 245.3283 0.5566 179.7026 179.1460 153.5170 246.1255 0.5562 179.6632 179.1070 153.4755 246.9125 0.5575 179.5970 179.0396 153.4134 247.7508 0.5533 179.5251 178.9718 153.3446 248.5165 0.5514 179.4564 178.9050 153.2726 249.3750 0.5551 179.3692 178.8141 153.2188 250.1313 0.5589 179.3012 178.7423 153.1758 250.9695 0.5601 179.2671 178.7070 153.1318 251.7565 0.5586 179.2004 178.6418 153.1062 252.5538 0.5573 179.1393 178.5820 153.0669 253.3818 0.5574 179.0531 178.4957 152.9955 254.1478 0.5583 179.0045 178.4462 152.9274 255.0060 0.5544 178.9404 178.3860 152.8673 255.7623 0.5573 178.8695 178.3121 152.8244 256.6005 0.5606 178.8186 178.2580 152.7702 257.3978 0.5619 178.7533 178.1914 152.7171 258.1950 0.5615 178.6802 178.1188 152.6871 259.0128 0.5664 178.6125 178.0460 152.6443 259.7888 0.5656 178.5646 177.9990 152.6084 260.6370 0.5688 178.5037 177.9349 152.5563 261.4035 0.5684 178.4431 177.8747 152.4934 262.2315 0.5654 178.3696 177.8043 152.4232 263.0288 0.5598 178.2958 177.7360 152.3668 263.8260 0.5616 178.2387 177.6771 152.2994 264.6428 0.5643 178.2047 177.6404 152.2428 265.4195 0.5635 178.1160 177.5524 152.1749 266.2680 0.5616 178.0176 177.4560 152.1407 267.0448 0.5653 177.9528 177.3875 152.0758 267.8625 0.5659 177.8771 177.3112 152.0284 268.6598 0.5658 177.8091 177.2432 151.9903 269.4468 0.5653 177.7735 177.2082 151.9649 270.2745 0.5647 177.7124 177.1478 151.8957 271.0300 0.5609 177.6526 177.0917 151.8351 271.8785 0.5617 177.5957 177.0341 151.7711 272.6553 0.5633 177.5480 176.9847 151.7083 273.4730 0.5636 177.4963 176.9327 151.6642 274.2600 0.5646 177.4025 176.8378 151.6361 275.0565 0.5675 177.3358 176.7683 151.6004 275.8740 0.5667 177.2627 176.6960 151.5176 276.6405 0.5630 177.2276 176.6646 151.4555 277.4993 0.5628 177.1667 176.6039 151.3904 278.2555 0.5600 177.1149 176.5549 151.3377 279.0835 0.5622 177.0345 176.4723 151.3014 279.8800 0.5679 176.9574 176.3895 151.2995 280.6770 0.5698 176.8876 176.3178 151.2779 281.4640 0.5674 176.8085 176.2412 151.1905 282.2715 0.5637 176.7497 176.1860 151.1091 283.0893 0.5639 176.6925 176.1287 151.0299 283.8555 0.5680 176.6621 176.0941 150.9900 284.7135 0.5690 176.5912 176.0222 150.9350 285.4800 0.5673 176.5237 175.9565 150.8760 286.2978 0.5682 176.4521 175.8839 150.7748 287.0950 0.5697 176.4138 175.8441 150.7144 287.8923 0.5720 176.3727 175.8007 150.6729 288.6895 0.5691 176.3037 175.7346 150.6179 289.4758 0.5679 176.2309 175.6630 150.5861 290.3138 0.5700 176.1722 175.6021 150.5451 291.0700 0.5719 176.1294 175.5574 150.5025 291.9288 0.5737 176.0747 175.5009 150.4715 292.6953 0.5726 176.0084 175.4358 150.3920 293.5233 0.5742 175.9507 175.3764 150.3660 294.3205 0.5743 175.8846 175.3103 150.3319 295.1073 0.5756 175.7880 175.2124 150.2800 295.9448 0.5771 175.7332 175.1561 150.2434 296.7010 0.5775 175.6429 175.0653 150.1849 297.5598 0.5761 175.5869 175.0109 150.1377 298.2955 0.5711 175.5622 174.9910 150.0762 299.1543 0.5668 175.4878 174.9209 150.0182 299.9208 0.5677 175.4304 174.8627 149.9783 300.7380 0.5682 175.3666 174.7984 149.9051 301.5450 0.5689 175.3233 174.7544 149.8372 302.3320 0.5724 175.2692 174.6968 149.7712 303.1600 0.5738 175.1859 174.6121 149.7212 303.9265 0.5760 175.1239 174.5479 149.6945 304.7853 0.5784 175.0487 174.4703 149.6025 305.5518 0.5843 174.9873 174.4030 149.5512 306.3685 0.5854 174.9094 174.3240 149.5220 307.1760 0.5819 174.8412 174.2593 149.4883 307.9630 0.5779 174.7987 174.2208 149.4465 308.7910 0.5778 174.7036 174.1257 149.3687 309.5575 0.5808 174.6526 174.0718 149.2991 310.4163 0.5817 174.5933 174.0116 149.2558 311.1828 0.5782 174.5240 173.9458 149.2170 312.0098 0.5755 174.4406 173.8652 149.1820 312.7763 0.5729 174.3639 173.7910 149.1292 313.6043 0.5737 174.3104 173.7367 149.0819 314.4015 0.5754 174.2525 173.6771 149.0281 315.1885 0.5773 174.2013 173.6239 148.9647 316.0265 0.5755 174.1824 173.6069 148.9097 316.7820 0.5775 174.1387 173.5612 148.8885 317.6510 0.5797 174.0954 173.5157 148.8355 318.4073 0.5780 174.0560 173.4781 148.8205 319.2455 0.5785 173.9831 173.4046 148.8060 320.0325 0.5791 173.9259 173.3468 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