DTA measure 1DTA2_PB3 Date: 202623:1259 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.38 s Mass = 1163.400 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2718 -4.1853 183.4868 187.6721 247.1957 2.1100 -4.1759 183.7712 187.9471 247.1116 2.8963 -4.1710 184.0488 188.2197 247.0367 3.7035 -4.1668 184.2532 188.4201 247.0020 4.5213 -4.1504 184.5236 188.6740 246.9431 5.2873 -4.1380 184.7902 188.9282 246.8603 6.1455 -4.1341 185.0702 189.2043 246.7971 6.9018 -4.1234 185.3099 189.4333 246.7669 7.7188 -4.1080 185.5607 189.6687 246.7148 8.5158 -4.0990 185.8155 189.9146 246.6298 9.3335 -4.0883 186.0737 190.1620 246.5909 10.0993 -4.0764 186.3073 190.3837 246.5178 10.9270 -4.0666 186.5520 190.6186 246.4511 11.7140 -4.0513 186.7687 190.8201 246.3560 12.5208 -4.0360 187.0312 191.0672 246.3027 13.3383 -4.0275 187.3127 191.3402 246.2400 14.0945 -4.0149 187.5278 191.5426 246.1743 14.9628 -4.0007 187.8268 191.8275 246.1014 15.7290 -3.9895 188.0628 192.0523 246.0933 16.5468 -3.9790 188.3160 192.2950 246.0953 17.3435 -3.9641 188.5419 192.5059 246.0887 18.1403 -3.9516 188.7999 192.7515 246.0693 18.9375 -3.9415 189.0745 193.0160 246.0229 19.7650 -3.9325 189.3602 193.2927 246.0019 20.5515 -3.9219 189.6099 193.5317 245.9837 21.3488 -3.9170 189.8465 193.7635 245.9483 22.1763 -3.9042 190.0742 193.9784 245.9745 22.9423 -3.8895 190.3392 194.2287 246.0108 23.8010 -3.8749 190.6280 194.5028 246.0089 24.5565 -3.8646 190.8328 194.6975 246.0112 25.3945 -3.8522 191.1051 194.9573 246.0543 26.1815 -3.8420 191.3514 195.1934 246.0746 26.9885 -3.8296 191.5709 195.4005 246.0755 27.8058 -3.8144 191.7943 195.6086 246.0810 28.5825 -3.7999 192.0439 195.8437 246.1299 29.4405 -3.7825 192.2935 196.0760 246.1752 30.1965 -3.7721 192.5127 196.2848 246.2060 31.0143 -3.7605 192.7933 196.5538 246.2563 31.7798 -3.7503 193.0002 196.7505 246.3192 32.6385 -3.7360 193.2321 196.9681 246.3850 33.4153 -3.7230 193.4561 197.1790 246.4570 34.2320 -3.7110 193.6865 197.3975 246.5674 35.0293 -3.7019 193.9092 197.6112 246.6819 35.8265 -3.6885 194.1533 197.8418 246.7659 36.6535 -3.6757 194.4058 198.0815 246.8789 37.4098 -3.6606 194.6249 198.2854 246.9951 38.2683 -3.6422 194.8691 198.5113 247.0886 39.0033 -3.6285 195.0920 198.7205 247.1311 39.8723 -3.6191 195.3249 198.9440 247.2551 40.6078 -3.6085 195.5113 199.1198 247.3627 41.4555 -3.5915 195.7531 199.3445 247.5272 42.2323 -3.5766 196.0047 199.5814 247.6892 43.0498 -3.5672 196.2652 199.8324 247.8508 43.8360 -3.5543 196.4527 200.0070 248.0000 44.6435 -3.5411 196.6620 200.2031 248.0936 45.4610 -3.5245 196.8810 200.4054 248.2730 46.2268 -3.5137 197.0949 200.6086 248.4138 47.0855 -3.5050 197.3246 200.8295 248.6049 47.8415 -3.4958 197.4876 200.9833 248.7982 48.6688 -3.4842 197.7100 201.1943 248.9845 49.4353 -3.4740 197.9191 201.3931 249.1396 50.2835 -3.4640 198.1499 201.6139 249.2993 51.0493 -3.4595 198.3423 201.8018 249.5096 51.8773 -3.4511 198.5568 202.0078 249.7116 52.6745 -3.4416 198.7722 202.2138 249.9098 53.4708 -3.4302 198.9888 202.4190 250.0861 54.2988 -3.4227 199.2393 202.6620 250.2981 55.0653 -3.4118 199.4650 202.8768 250.4899 55.9233 -3.4003 199.6715 203.0718 250.6904 56.6793 -3.3902 199.8574 203.2475 250.8643 57.5175 -3.3823 200.0926 203.4749 251.0413 58.3038 -3.3731 200.3129 203.6859 251.2530 59.1008 -3.3625 200.5282 203.8906 251.4719 59.9390 -3.3501 200.7912 204.1413 251.6950 60.7250 -3.3429 200.9905 204.3333 251.8852 61.5120 -3.3350 201.2090 204.5440 252.0571 62.3195 -3.3264 201.4233 204.7497 252.2620 63.1465 -3.3159 201.6512 204.9671 252.4877 63.9130 -3.3066 201.8500 205.1566 252.6747 64.7615 -3.2975 202.0700 205.3675 252.8782 65.5375 -3.2892 202.2455 205.5347 253.0367 66.3550 -3.2842 202.4463 205.7305 253.2480 67.1523 -3.2824 202.6848 205.9672 253.4739 67.9488 -3.2767 202.8941 206.1709 253.6970 68.7765 -3.2684 203.0976 206.3661 253.8821 69.5430 -3.2602 203.3069 206.5671 254.0801 70.4013 -3.2527 203.5181 206.7708 254.2815 71.1468 -3.2467 203.7301 206.9768 254.4461 71.9748 -3.2389 203.9563 207.1953 254.6283 72.7413 -3.2275 204.1772 207.4047 254.7880 73.5890 -3.2253 204.3934 207.6187 254.9557 74.3553 -3.2156 204.5932 207.8087 255.1424 75.1730 -3.2040 204.8201 208.0241 255.3548 75.9693 -3.1940 205.0187 208.2127 255.5175 76.7665 -3.1846 205.2481 208.4327 255.6883 77.5943 -3.1820 205.4630 208.6450 255.8886 78.3600 -3.1781 205.6577 208.8358 256.0550 79.2085 -3.1763 205.9067 209.0830 256.2459 79.9853 -3.1713 206.0802 209.2515 256.4093 80.8123 -3.1608 206.2783 209.4391 256.5859 81.5685 -3.1515 206.4583 209.6098 256.7252 82.4170 -3.1447 206.6682 209.8129 256.8759 83.1825 -3.1406 206.8955 210.0361 256.9823 84.0105 -3.1316 207.1399 210.2715 257.1367 84.8075 -3.1251 207.3154 210.4405 257.3100 85.6040 -3.1211 207.4982 210.6194 257.4861 86.4218 -3.1133 207.6992 210.8125 257.6444 87.1980 -3.1087 207.9010 211.0097 257.7521 88.0460 -3.1010 208.0968 211.1978 257.9162 88.8228 -3.0943 208.3217 211.4159 258.0731 89.6400 -3.0871 208.5588 211.6459 258.2620 90.4470 -3.0839 208.7969 211.8808 258.3722 91.2545 -3.0795 208.9912 212.0706 258.5413 92.0613 -3.0715 209.2020 212.2736 258.6742 92.8480 -3.0696 209.3908 212.4604 258.8556 93.6760 -3.0636 209.6224 212.6860 259.0121 94.4420 -3.0607 209.8153 212.8760 259.1287 95.3003 -3.0562 210.0251 213.0812 259.2850 96.0668 -3.0484 210.1885 213.2370 259.3850 96.8943 -3.0384 210.3699 213.4084 259.5335 97.6910 -3.0341 210.5487 213.5828 259.6790 98.4883 -3.0294 210.7289 213.7584 259.8448 99.3160 -3.0294 210.9321 213.9615 259.9603 100.0715 -3.0257 211.0938 214.1195 260.0833 100.9405 -3.0223 211.3072 214.3295 260.2034 101.6965 -3.0194 211.4918 214.5111 260.3023 102.5545 -3.0152 211.6763 214.6915 260.4208 103.2800 -3.0100 211.8278 214.8378 260.5117 104.1283 -3.0058 212.0171 215.0229 260.6371 104.9043 -2.9988 212.2109 215.2097 260.7730 105.7220 -2.9926 212.4027 215.3953 260.8823 106.5193 -2.9832 212.6336 215.6168 260.9967 107.3155 -2.9777 212.8507 215.8284 261.1340 108.1435 -2.9704 213.0830 216.0535 261.2264 108.8998 -2.9645 213.2724 216.2369 261.3272 109.7578 -2.9610 213.4741 216.4351 261.4679 110.5240 -2.9544 213.6667 216.6211 261.6010 111.3418 -2.9492 213.8560 216.8051 261.7265 112.1383 -2.9452 214.0585 217.0037 261.8330 112.9455 -2.9429 214.2321 217.1750 261.9845 113.7633 -2.9364 214.4608 217.3972 262.0947 114.5185 -2.9332 214.6304 217.5636 262.2469 115.3875 -2.9282 214.8207 217.7489 262.3670 116.1438 -2.9210 214.9909 217.9119 262.4760 116.9708 -2.9124 215.1607 218.0731 262.6018 117.7680 -2.9096 215.3715 218.2811 262.7054 118.5653 -2.9046 215.5630 218.4676 262.8028 119.3923 -2.8978 215.7422 218.6400 262.9123 120.1588 -2.8951 215.9133 218.8084 263.0159 121.0175 -2.8953 216.1122 219.0075 263.1363 121.7833 -2.8914 216.3332 219.2246 263.2598 122.6110 -2.8836 216.5402 219.4238 263.3867 123.3980 -2.8778 216.7425 219.6203 263.4832 124.2053 -2.8728 216.9351 219.8079 263.5847 125.0223 -2.8663 217.1306 219.9969 263.7275 125.7888 -2.8606 217.3028 220.1635 263.8572 126.6473 -2.8590 217.5450 220.4040 263.9957 127.4130 -2.8552 217.7369 220.5921 264.0858 128.2410 -2.8461 217.9183 220.7644 264.2071 129.0075 -2.8361 218.1038 220.9399 264.2856 129.8345 -2.8360 218.3080 221.1441 264.4167 130.6318 -2.8391 218.4936 221.3328 264.5220 131.4288 -2.8351 218.6844 221.5195 264.6357 132.2355 -2.8284 218.8904 221.7188 264.7383 133.0430 -2.8222 219.0663 221.8885 264.8515 133.8603 -2.8162 219.2645 222.0807 264.9718 134.6263 -2.8160 219.4566 222.2725 265.1027 135.4748 -2.8078 219.6261 222.4339 265.1958 136.2413 -2.8045 219.8178 222.6223 265.2975 137.0580 -2.7972 220.0003 222.7975 265.4184 137.8553 -2.7944 220.1859 222.9803 265.5214 138.6523 -2.7916 220.3869 223.1785 265.6220 139.4795 -2.7851 220.5803 223.3654 265.7307 140.2358 -2.7844 220.7525 223.5369 265.8387 141.0943 -2.7749 220.9853 223.7602 265.9849 141.8703 -2.7689 221.1509 223.9198 266.0875 142.6880 -2.7629 221.3608 224.1237 266.2077 143.4748 -2.7606 221.5291 224.2897 266.3283 144.2815 -2.7597 221.7088 224.4684 266.4080 145.0993 -2.7548 221.8848 224.6396 266.5514 145.8655 -2.7491 222.0577 224.8067 266.6445 146.7235 -2.7396 222.2842 225.0238 266.7600 147.4900 -2.7361 222.4638 225.2000 266.8490 148.3175 -2.7337 222.6767 225.4103 267.0154 149.0733 -2.7293 222.8597 225.5891 267.1452 149.9115 -2.7235 223.0647 225.7882 267.2594 150.6983 -2.7197 223.2140 225.9337 267.3839 151.4948 -2.7152 223.3864 226.1016 267.5226 152.3228 -2.7102 223.4917 226.2019 267.6617 153.0890 -2.7072 223.6366 226.3438 267.7831 153.9470 -2.7059 223.8358 226.5418 267.9274 154.7033 -2.7010 224.0123 226.7133 268.0513 155.5415 -2.6952 224.2020 226.8971 268.1693 156.3275 -2.6933 224.3764 227.0697 268.2956 157.1248 -2.6881 224.5737 227.2618 268.4253 157.9525 -2.6818 224.7863 227.4681 268.5692 158.7183 -2.6783 224.9601 227.6385 268.6838 159.5770 -2.6732 225.1146 227.7878 268.8343 160.3333 -2.6663 225.2789 227.9452 268.9642 161.1705 -2.6595 225.4559 228.1154 269.1008 161.9575 -2.6550 225.6376 228.2926 269.2341 162.7548 -2.6510 225.8274 228.4784 269.4013 163.5818 -2.6507 226.0336 228.6843 269.5514 164.3483 -2.6482 226.1891 228.8373 269.6873 165.2070 -2.6466 226.4016 229.0483 269.8388 165.9315 -2.6466 226.5489 229.1955 269.9815 166.7903 -2.6415 226.7273 229.3688 270.1217 167.5568 -2.6390 226.9193 229.5583 270.2440 168.3738 -2.6331 227.0894 229.7225 270.3689 169.1708 -2.6291 227.2669 229.8960 270.4850 169.9680 -2.6259 227.4181 230.0440 270.6323 170.7853 -2.6244 227.5625 230.1868 270.7682 171.5513 -2.6207 227.7044 230.3251 270.9173 172.3793 -2.6154 227.8955 230.5110 271.0231 173.1348 -2.6096 228.0572 230.6669 271.1538 174.0035 -2.6092 228.2496 230.8589 271.2922 174.7598 -2.6114 228.4379 231.0493 271.4502 175.5768 -2.6105 228.5871 231.1975 271.5849 176.3840 -2.6065 228.7683 231.3748 271.7130 177.1710 -2.6006 228.9495 231.5501 271.8262 177.9983 -2.5961 229.1535 231.7496 271.9865 178.7645 -2.5963 229.3456 231.9419 272.1286 179.6130 -2.5917 229.5163 232.1080 272.2471 180.3790 -2.5848 229.6882 232.2730 272.3702 181.2065 -2.5821 229.8654 232.4475 272.5223 181.9833 -2.5779 230.0222 232.6001 272.6463 182.8008 -2.5756 230.1899 232.7655 272.7719 183.6075 -2.5712 230.3652 232.9363 272.9030 184.3945 -2.5683 230.5520 233.1203 273.0346 185.2325 -2.5640 230.7409 233.3049 273.1905 185.9880 -2.5621 230.9005 233.4626 273.3222 186.8468 -2.5595 231.0987 233.6583 273.4595 187.5820 -2.5523 231.2868 233.8390 273.5635 188.4403 -2.5454 231.4815 234.0269 273.6892 189.2068 -2.5492 231.6564 234.2056 273.8014 190.0243 -2.5439 231.8175 234.3614 273.9345 190.8310 -2.5405 231.9475 234.4880 274.0605 191.6180 -2.5406 232.1141 234.6547 274.1751 192.4458 -2.5417 232.2907 234.8324 274.3172 193.2218 -2.5381 232.4504 234.9885 274.4650 194.0600 -2.5367 232.6360 235.1726 274.6071 194.8263 -2.5358 232.8088 235.3446 274.7335 195.6843 -2.5395 232.9654 235.5049 274.8970 196.4508 -2.5392 233.1153 235.6545 275.0299 197.2683 -2.5385 233.3280 235.8664 275.1625 198.0443 -2.5337 233.4873 236.0210 275.3010 198.8620 -2.5283 233.6714 236.1997 275.4263 199.6593 -2.5269 233.8379 236.3648 275.5586 200.4555 -2.5229 233.9894 236.5123 275.7091 201.2733 -2.5189 234.1694 236.6883 275.8575 202.0295 -2.5190 234.3267 236.8458 275.9709 202.8975 -2.5160 234.5344 237.0504 276.1442 203.6333 -2.5162 234.6804 237.1966 276.2886 204.4713 -2.5133 234.8834 237.3966 276.4232 205.2370 -2.5110 235.0601 237.5712 276.5669 206.0855 -2.5012 235.2597 237.7608 276.6834 206.8623 -2.4961 235.3526 237.8487 276.8060 207.6790 -2.4957 235.4759 237.9716 276.9615 208.4763 -2.4988 235.6520 238.1508 277.1048 209.2735 -2.4982 235.7834 238.2816 277.2169 210.1005 -2.4969 235.9406 238.4376 277.3254 210.8670 -2.4927 236.1105 238.6032 277.4607 211.6845 -2.4917 236.2921 238.7838 277.6192 212.4605 -2.4878 236.4650 238.9529 277.7460 213.3090 -2.4830 236.6741 239.1571 277.8907 214.0648 -2.4810 236.8565 239.3375 277.9672 214.9025 -2.4802 237.0192 239.4994 278.0771 215.6690 -2.4823 237.1414 239.6237 278.1965 216.5173 -2.4796 237.2799 239.7595 278.3021 217.2933 -2.4797 237.4315 239.9112 278.4704 218.1110 -2.4806 237.6209 240.1015 278.6276 218.9080 -2.4802 237.8174 240.2976 278.7608 219.7045 -2.4744 237.9956 240.4700 278.8925 220.5325 -2.4751 238.1524 240.6275 279.0028 221.2988 -2.4742 238.2996 240.7738 279.0794 222.1465 -2.4675 238.4616 240.9291 279.1863 222.9233 -2.4579 238.6123 241.0702 279.3461 223.7405 -2.4563 238.7910 241.2473 279.5097 224.5373 -2.4550 238.9822 241.4372 279.6382 225.3550 -2.4492 239.1539 241.6031 279.7855 226.1520 -2.4497 239.3165 241.7663 279.9471 226.9485 -2.4484 239.4866 241.9351 280.0866 227.7765 -2.4367 239.6742 242.1110 280.2299 228.5425 -2.4368 239.7938 242.2306 280.3439 229.4008 -2.4366 239.9695 242.4061 280.4675 230.1673 -2.4338 240.1192 242.5530 280.6561 230.9945 -2.4328 240.2913 242.7241 280.8108 231.7813 -2.4305 240.4151 242.8457 280.9177 232.5785 -2.4311 240.5610 242.9921 281.0305 233.3653 -2.4264 240.7270 243.1534 281.1698 234.1720 -2.4257 240.9027 243.3284 281.2504 234.9693 -2.4276 241.0727 243.5003 281.3651 235.7660 -2.4273 241.2446 243.6720 281.5085 236.5935 -2.4305 241.4096 243.8401 281.6257 237.3498 -2.4311 241.5545 243.9855 281.7779 238.2083 -2.4293 241.7138 244.1431 281.9304 238.9740 -2.4283 241.8680 244.2963 282.0613 239.7918 -2.4253 242.0033 244.4286 282.2007 240.5888 -2.4196 242.1548 244.5744 282.2896 241.3853 -2.4190 242.3063 244.7254 282.3844 242.2133 -2.4161 242.4689 244.8850 282.5048 242.9690 -2.4169 242.6098 245.0267 282.6282 243.8273 -2.4208 242.8072 245.2280 282.8054 244.5938 -2.4206 242.9390 245.3596 282.9461 245.4113 -2.4188 243.1056 245.5245 283.0661 246.2180 -2.4167 243.2808 245.6974 283.1980 247.0050 -2.4219 243.4497 245.8717 283.3191 247.8328 -2.4169 243.6357 246.0526 283.4364 248.5985 -2.4160 243.7889 246.2049 283.5506 249.4573 -2.4167 244.0078 246.4245 283.6719 250.2238 -2.4106 244.1798 246.5904 283.8101 251.0405 -2.4053 244.3261 246.7314 283.9346 251.8480 -2.4054 244.4995 246.9049 284.0214 252.6348 -2.4037 244.6828 247.0866 284.1403 253.4620 -2.3990 244.8276 247.2266 284.2857 254.2285 -2.3977 244.9791 247.3768 284.3980 255.0973 -2.3918 245.1477 247.5396 284.5037 255.8425 -2.3892 245.3204 247.7097 284.6189 256.6910 -2.3830 245.4837 247.8668 284.7398 257.4675 -2.3835 245.6125 247.9961 284.8540 258.2845 -2.3878 245.7709 248.1588 285.0067 259.0920 -2.3872 245.9503 248.3375 285.1426 259.8785 -2.3867 246.1349 248.5217 285.2711 260.7060 -2.3830 246.3039 248.6868 285.3923 261.4725 -2.3775 246.4583 248.8358 285.5376 262.3308 -2.3756 246.6209 248.9965 285.6742 263.0865 -2.3733 246.7773 249.1506 285.7604 263.9145 -2.3758 246.9176 249.2934 285.8719 264.7115 -2.3752 247.0453 249.4205 285.9837 265.5285 -2.3738 247.2011 249.5750 286.1315 266.2848 -2.3751 247.3448 249.7199 286.2541 267.1125 -2.3736 247.5121 249.8857 286.3698 267.9090 -2.3731 247.6914 250.0645 286.4943 268.6960 -2.3699 247.8433 250.2132 286.6315 269.5240 -2.3694 248.0164 250.3858 286.7711 270.2895 -2.3679 248.1785 250.5464 286.9145 271.1380 -2.3687 248.3441 250.7128 287.0635 271.9043 -2.3670 248.5105 250.8775 287.2155 272.7315 -2.3671 248.6737 251.0408 287.3294 273.5288 -2.3657 248.8021 251.1678 287.4367 274.3260 -2.3656 248.9362 251.3018 287.5788 275.1530 -2.3682 249.1057 251.4739 287.7920 275.9400 -2.3708 249.2622 251.6330 287.9289 276.7578 -2.3681 249.4349 251.8030 288.0523 277.5335 -2.3657 249.5986 251.9643 288.1685 278.3820 -2.3635 249.7725 252.1361 288.3115 279.1485 -2.3639 249.9296 252.2935 288.4396 279.9755 -2.3631 250.1287 252.4917 288.5774 280.7728 -2.3621 250.2756 252.6377 288.7264 281.5700 -2.3617 250.4320 252.7937 288.8845 282.3870 -2.3598 250.5637 252.9235 289.0621 283.1635 -2.3564 250.7029 253.0593 289.1921 284.0120 -2.3581 250.8659 253.2241 289.3397 284.7780 -2.3588 251.0182 253.3769 289.4719 285.6158 -2.3594 251.1535 253.5129 289.5895 286.3720 -2.3588 251.2991 253.6579 289.7236 287.2200 -2.3560 251.4594 253.8154 289.8786 287.9963 -2.3551 251.5673 253.9223 290.0150 288.8140 -2.3547 251.6891 254.0438 290.1299 289.6108 -2.3581 251.8338 254.1920 290.2896 290.4075 -2.3580 251.9902 254.3483 290.4066 291.2355 -2.3560 252.1459 254.5019 290.5349 292.0015 -2.3556 252.2935 254.6491 290.6645 292.8495 -2.3553 252.4975 254.8528 290.8156 293.6263 -2.3526 252.6875 255.0401 290.9685 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