DTA measure 3DTA1_PB3 Date: 202623:1326 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.02 s Mass = 1173.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3014 -5.0031 460.0333 465.0364 433.1332 3.9100 -5.0154 460.0556 465.0710 433.3847 5.5084 -5.0266 460.0656 465.0922 433.5923 7.1166 -5.0408 460.0714 465.1122 433.7300 8.7049 -5.0536 460.0635 465.1171 433.7636 10.3083 -5.0645 460.0672 465.1317 433.6899 11.9168 -5.0732 460.0815 465.1547 433.5349 13.5355 -5.0828 460.0888 465.1716 433.2891 15.1440 -5.0885 460.1073 465.1958 433.0113 16.7474 -5.0906 460.1307 465.2212 432.6099 18.3561 -5.0959 460.1315 465.2274 432.1706 19.9596 -5.0981 460.1048 465.2029 431.7055 21.5680 -5.1020 460.0931 465.1951 431.2093 23.1765 -5.1043 460.0960 465.2004 430.7204 24.7953 -5.1083 460.1132 465.2214 430.2210 26.4038 -5.1067 460.1315 465.2382 429.7664 27.9970 -5.1027 460.1162 465.2189 429.3566 29.6055 -5.1001 460.1242 465.2242 428.9744 31.2089 -5.1018 460.1108 465.2125 428.6589 32.8175 -5.0995 460.0817 465.1812 428.3859 34.4209 -5.0966 460.0163 465.1129 428.1942 36.0191 -5.0976 459.9584 465.0560 428.0611 37.6278 -5.1048 459.9473 465.0521 427.9698 39.2260 -5.1063 459.9482 465.0545 427.8705 40.8345 -5.1053 459.9061 465.0113 427.8312 42.4380 -5.1045 459.8941 464.9986 427.8363 44.0414 -5.1098 459.8341 464.9439 427.8259 45.6499 -5.1097 459.7888 464.8985 427.7884 47.2585 -5.1103 459.7192 464.8295 427.7259 48.8671 -5.1112 459.6575 464.7687 427.7227 50.4550 -5.1169 459.6266 464.7435 427.6359 52.0790 -5.1238 459.5812 464.7050 427.4984 53.6824 -5.1300 459.5284 464.6584 427.2965 55.2959 -5.1307 459.4675 464.5982 427.0683 56.8994 -5.1316 459.4019 464.5335 426.8044 58.5128 -5.1340 459.3541 464.4881 426.5110 60.1163 -5.1302 459.3004 464.4306 426.2068 61.7248 -5.1347 459.2520 464.3867 425.8853 63.3485 -5.1359 459.1999 464.3357 425.5630 64.9573 -5.1379 459.1189 464.2569 425.2333 66.5553 -5.1373 459.0600 464.1973 424.8977 68.1588 -5.1370 459.0118 464.1488 424.5357 69.7671 -5.1378 458.9623 464.1001 424.2371 71.3550 -5.1325 458.9085 464.0410 423.9456 72.9585 -5.1320 458.8681 464.0001 423.6858 74.5620 -5.1266 458.7850 463.9116 423.4673 76.1806 -5.1259 458.6889 463.8148 423.2623 77.7893 -5.1299 458.5828 463.7128 423.0706 79.3976 -5.1316 458.4992 463.6308 422.9055 81.0063 -5.1277 458.4052 463.5329 422.7595 82.6098 -5.1297 458.3068 463.4365 422.6321 84.2181 -5.1304 458.2135 463.3438 422.5412 85.8215 -5.1338 458.1128 463.2467 422.4141 87.4506 -5.1379 458.0479 463.1858 422.2933 89.0540 -5.1334 457.9884 463.1218 422.1517 90.6575 -5.1332 457.8827 463.0160 421.9852 92.2816 -5.1334 457.7647 462.8981 421.8292 93.8900 -5.1304 457.6382 462.7686 421.6598 95.4986 -5.1329 457.5515 462.6844 421.4927 97.1174 -5.1341 457.4688 462.6029 421.2908 98.7001 -5.1336 457.3776 462.5112 421.0715 100.3036 -5.1382 457.2754 462.4136 420.8321 101.9071 -5.1334 457.1587 462.2921 420.5756 103.5154 -5.1313 457.0512 462.1825 420.3503 105.1189 -5.1323 456.9512 462.0836 420.1101 106.7271 -5.1331 456.8700 462.0030 419.8194 108.3306 -5.1333 456.7924 461.9257 419.5833 109.9188 -5.1302 456.6433 461.7735 419.3087 111.5425 -5.1236 456.5298 461.6535 419.0072 113.1460 -5.1197 456.4348 461.5545 418.7730 114.7545 -5.1166 456.2958 461.4124 418.5549 116.3579 -5.1228 456.1643 461.2871 418.3126 117.9665 -5.1334 456.0463 461.1797 418.1020 119.5700 -5.1287 455.9345 461.0632 417.9046 121.1784 -5.1271 455.8313 460.9584 417.7186 122.8023 -5.1227 455.7204 460.8431 417.5249 124.3900 -5.1228 455.5899 460.7127 417.3635 125.9986 -5.1261 455.4412 460.5673 417.1716 127.6073 -5.1297 455.3140 460.4437 416.9617 129.2155 -5.1267 455.1724 460.2992 416.7420 130.8139 -5.1247 454.9859 460.1106 416.5915 132.4069 -5.1205 454.8317 459.9522 416.4249 134.0103 -5.1211 454.7116 459.8326 416.2193 135.6086 -5.1214 454.5725 459.6940 416.0425 137.2324 -5.1211 454.4512 459.5722 415.8506 138.8359 -5.1251 454.3145 459.4396 415.6963 140.4290 -5.1177 454.1807 459.2984 415.5084 142.0323 -5.1141 454.0432 459.1573 415.2898 143.6358 -5.1137 453.9194 459.0332 415.0612 145.2440 -5.1082 453.7599 458.8682 414.8588 146.8475 -5.1058 453.6066 458.7124 414.6180 148.4561 -5.1061 453.4892 458.5953 414.3886 150.0748 -5.1020 453.3468 458.4487 414.1406 151.6885 -5.1038 453.2061 458.3100 413.9020 153.2920 -5.0995 453.0546 458.1541 413.6668 154.9005 -5.0896 452.8736 457.9632 413.4699 156.5040 -5.0888 452.7418 457.8306 413.2575 158.1178 -5.0922 452.5949 457.6871 413.0118 159.7210 -5.0882 452.4163 457.5045 412.7674 161.3245 -5.0844 452.2414 457.3258 412.5218 162.9280 -5.0824 452.1046 457.1870 412.2912 164.5314 -5.0769 451.9488 457.0257 412.0884 166.1296 -5.0735 451.8069 456.8804 411.9153 167.7383 -5.0708 451.6540 456.7249 411.7087 169.3416 -5.0687 451.5263 456.5950 411.5106 170.9501 -5.0665 451.3873 456.4538 411.3068 172.5535 -5.0614 451.2493 456.3107 411.1161 174.1774 -5.0537 451.0724 456.1261 410.9075 175.7808 -5.0523 450.9144 455.9667 410.7003 177.3843 -5.0493 450.7373 455.7865 410.5163 178.9926 -5.0502 450.6095 455.6597 410.3149 180.6013 -5.0466 450.4621 455.5087 410.1227 182.2096 -5.0484 450.2976 455.3459 409.9512 183.8130 -5.0442 450.1370 455.1812 409.7703 185.4369 -5.0405 449.9268 454.9672 409.5630 187.0403 -5.0397 449.7801 454.8198 409.3688 188.6489 -5.0339 449.6322 454.6661 409.1611 190.2523 -5.0283 449.4720 454.5003 408.9628 191.8658 -5.0287 449.3174 454.3461 408.7549 193.4693 -5.0224 449.1738 454.1962 408.5259 195.0675 -5.0130 449.0045 454.0174 408.3136 196.6913 -5.0119 448.8080 453.8199 408.0708 198.2948 -5.0081 448.6197 453.6277 407.8646 199.8930 -5.0058 448.4350 453.4407 407.6523 201.5015 -4.9997 448.2534 453.2531 407.4223 203.1049 -4.9983 448.0774 453.0757 407.1767 204.7133 -4.9943 447.9069 452.9012 406.9218 206.3168 -4.9934 447.7220 452.7153 406.6913 207.9254 -4.9915 447.5321 452.5237 406.4983 209.5440 -4.9859 447.3938 452.3797 406.2779 211.1475 -4.9841 447.2172 452.2013 406.0634 212.7561 -4.9808 447.0476 452.0284 405.8510 214.3593 -4.9768 446.8760 451.8528 405.6426 215.9730 -4.9745 446.6981 451.6726 405.4408 217.5766 -4.9680 446.5316 451.4996 405.2439 219.1849 -4.9632 446.3462 451.3095 405.0354 220.8038 -4.9598 446.1721 451.1319 404.8295 222.4125 -4.9602 445.9619 450.9221 404.6186 224.0055 -4.9610 445.7765 450.7375 404.4441 225.6193 -4.9582 445.5914 450.5497 404.2382 227.2125 -4.9515 445.4174 450.3689 404.0482 228.8106 -4.9453 445.2302 450.1755 403.8579 230.4193 -4.9372 445.0756 450.0129 403.6405 232.0226 -4.9298 444.8885 449.8183 403.4109 233.6260 -4.9303 444.6535 449.5838 403.2132 235.2345 -4.9285 444.4923 449.4208 403.0114 236.8379 -4.9266 444.3142 449.2408 402.7970 238.4463 -4.9191 444.0972 449.0163 402.6016 240.0345 -4.9166 443.9047 448.8214 402.3967 241.6429 -4.9154 443.7114 448.6268 402.1750 243.2464 -4.9044 443.5527 448.4571 401.9544 244.8499 -4.9002 443.3676 448.2678 401.7344 246.4789 -4.8977 443.1883 448.0860 401.5090 248.0874 -4.8922 442.9910 447.8832 401.2896 249.6808 -4.8830 442.7788 447.6618 401.0751 251.2893 -4.8767 442.6159 447.4926 400.8672 252.9028 -4.8699 442.4456 447.3155 400.6629 254.5114 -4.8656 442.2797 447.1452 400.4512 256.1045 -4.8667 442.0958 446.9625 400.2045 257.7130 -4.8612 441.8926 446.7539 399.9972 259.3165 -4.8591 441.7153 446.5745 399.7979 260.9301 -4.8537 441.5004 446.3541 399.5869 262.5385 -4.8483 441.2998 446.1481 399.4057 264.1369 -4.8489 441.1373 445.9862 399.1910 265.7401 -4.8488 440.9533 445.8021 399.0132 267.3335 -4.8479 440.7347 445.5826 398.8103 268.9369 -4.8383 440.5504 445.3887 398.5807 270.5453 -4.8284 440.3619 445.1902 398.3691 272.1488 -4.8190 440.1850 445.0040 398.1677 273.7726 -4.8108 439.9660 444.7768 397.9403 275.3810 -4.8083 439.7768 444.5851 397.7001 276.9896 -4.8062 439.6086 444.4148 397.4881 278.5929 -4.8022 439.4054 444.2076 397.3051 280.2014 -4.7955 439.2054 444.0009 397.1115 281.8099 -4.7888 439.0234 443.8122 396.9077 283.4183 -4.7839 438.8090 443.5929 396.7010 285.0423 -4.7792 438.5857 443.3648 396.4749 286.6456 -4.7763 438.3898 443.1661 396.2591 288.2591 -4.7683 438.2027 442.9710 396.0347 289.8626 -4.7666 438.0036 442.7703 395.8433 291.4505 -4.7610 437.8287 442.5898 395.6498 293.0540 -4.7586 437.6387 442.3973 395.4413 294.6524 -4.7538 437.3960 442.1498 395.2243 296.2608 -4.7496 437.2177 441.9673 395.0233 297.8796 -4.7444 437.0762 441.8206 394.7901 299.4880 -4.7428 436.8631 441.6059 394.5649 301.0915 -4.7377 436.6612 441.3990 394.3383 302.7001 -4.7292 436.4683 441.1975 394.1175 304.3034 -4.7249 436.2898 441.0147 393.9049 305.9068 -4.7199 436.0929 440.8128 393.6794 307.5154 -4.7113 435.8659 440.5772 393.4904 309.1341 -4.7042 435.6788 440.3830 393.2877 310.7478 -4.7046 435.4859 440.1904 393.0834 312.3514 -4.6944 435.2930 439.9874 392.8891 313.9598 -4.6846 435.1007 439.7853 392.6911 315.5681 -4.6793 434.8868 439.5660 392.4739 317.1769 -4.6742 434.6765 439.3508 392.2363 318.7854 -4.6700 434.4499 439.1199 392.0169 320.4093 -4.6668 434.2337 438.9005 391.8412 322.0179 -4.6594 434.0326 438.6920 391.6443 323.6264 -4.6516 433.8510 438.5026 391.4472 325.2041 -4.6458 433.6463 438.2922 391.2267 326.8078 -4.6393 433.4315 438.0708 391.0160 328.4161 -4.6347 433.2509 437.8856 390.7793 330.0195 -4.6336 433.0627 437.6964 390.5850 331.6230 -4.6241 432.8606 437.4847 390.3542 333.2420 -4.6197 432.6316 437.2513 390.1206 334.8350 -4.6137 432.4474 437.0611 389.9063 336.4435 -4.6091 432.2380 436.8472 389.6835 338.0469 -4.6072 432.0105 436.6177 389.4733 339.6554 -4.6045 431.8050 436.4094 389.2894 341.2590 -4.6029 431.6100 436.2128 389.0341 342.8676 -4.5967 431.4047 436.0014 388.8175 344.4709 -4.5865 431.2149 435.8014 388.6565 346.0949 -4.5834 431.0188 435.6021 388.4645 347.7035 -4.5797 430.8094 435.3891 388.2510 349.2915 -4.5734 430.6108 435.1841 388.0925 350.9051 -4.5650 430.4122 434.9772 387.9084 352.5086 -4.5606 430.2070 434.7676 387.6869 354.1221 -4.5505 429.9986 434.5491 387.4777 355.7204 -4.5439 429.7645 434.3084 387.2605 357.3085 -4.5400 429.5935 434.1335 387.0308 358.9119 -4.5339 429.3857 433.9196 386.8067 360.5256 -4.5310 429.1919 433.7229 386.5891 362.1341 -4.5281 428.9922 433.5203 386.3740 363.7374 -4.5232 428.7743 433.2975 386.1865 365.3308 -4.5152 428.5658 433.0810 385.9937 366.9343 -4.5030 428.3619 432.8649 385.7890 368.5426 -4.4969 428.1765 432.6735 385.5450 370.1513 -4.4849 427.9683 432.4532 385.3081 371.7546 -4.4838 427.7645 432.2484 385.0383 373.3785 -4.4794 427.5540 432.0334 384.8240 374.9718 -4.4796 427.3527 431.8322 384.6201 376.5803 -4.4752 427.1312 431.6064 384.4318 378.1835 -4.4675 426.9646 431.4320 384.2540 379.7973 -4.4631 426.7444 431.2075 384.0476 381.4004 -4.4580 426.5192 430.9772 383.8338 383.0141 -4.4562 426.2982 430.7544 383.5938 384.6175 -4.4511 426.0512 430.5023 383.3595 386.2464 -4.4432 425.8703 430.3134 383.1780 387.8448 -4.4382 425.6769 430.1151 382.9977 389.4379 -4.4318 425.5056 429.9374 382.8141 391.0463 -4.4276 425.3148 429.7424 382.6019 392.6496 -4.4227 425.1430 429.5657 382.3918 394.2580 -4.4228 424.9114 429.3342 382.1729 395.8615 -4.4133 424.6764 429.0897 381.9466 397.4803 -4.4055 424.4999 428.9054 381.7540 399.0886 -4.4043 424.2963 428.7005 381.5399 400.6919 -4.3966 424.0655 428.4621 381.3141 402.3004 -4.3854 423.8204 428.2058 381.0838 403.9039 -4.3832 423.6063 427.9895 380.8662 405.5124 -4.3795 423.3833 427.7629 380.6235 407.1158 -4.3701 423.1514 427.5215 380.4005 408.7449 -4.3630 422.9657 427.3288 380.1767 410.3483 -4.3602 422.8170 427.1772 379.9978 411.9516 -4.3548 422.6046 426.9593 379.7273 413.5655 -4.3481 422.3959 426.7440 379.5095 415.1690 -4.3459 422.1850 426.5309 379.3461 416.7825 -4.3394 421.9558 426.2952 379.1257 418.3706 -4.3346 421.7655 426.1000 378.9360 419.9790 -4.3266 421.5601 425.8868 378.7553 421.5926 -4.3236 421.3270 425.6506 378.5642 423.2013 -4.3239 421.0763 425.4002 378.3742 424.8046 -4.3189 420.8562 425.1751 378.1520 426.3925 -4.3177 420.6423 424.9599 377.9339 427.9960 -4.3105 420.4212 424.7318 377.6876 429.5993 -4.3008 420.2326 424.5334 377.4694 431.2080 -4.2936 420.0361 424.3297 377.3027 432.8115 -4.2849 419.8326 424.1176 377.1117 434.4303 -4.2802 419.6393 423.9196 376.9004 436.0439 -4.2723 419.4103 423.6826 376.6873 437.6473 -4.2655 419.1925 423.4581 376.4506 439.2608 -4.2606 419.0187 423.2793 376.2628 440.8643 -4.2521 418.8339 423.0860 376.0634 442.4778 -4.2519 418.6351 422.8870 375.8811 444.0658 -4.2484 418.4234 422.6718 375.6406 445.6795 -4.2453 418.2143 422.4597 375.4262 447.2980 -4.2375 417.9770 422.2144 375.2209 448.9066 -4.2325 417.7103 421.9429 375.0183 450.5101 -4.2234 417.5744 421.7979 374.8284 452.1184 -4.2082 417.3833 421.5915 374.6208 453.7219 -4.2003 417.1641 421.3644 374.3569 455.3096 -4.1916 416.9807 421.1723 374.1024 456.9131 -4.1859 416.7615 420.9474 373.8869 458.5166 -4.1814 416.5388 420.7202 373.6874 460.1404 -4.1768 416.2918 420.4686 373.4758 461.7438 -4.1728 416.0526 420.2254 373.2479 463.3523 -4.1635 415.8188 419.9824 373.0573 464.9556 -4.1545 415.6415 419.7960 372.8590 466.5438 -4.1483 415.4352 419.5836 372.6422 468.1676 -4.1398 415.2193 419.3591 372.4373 469.7710 -4.1330 415.0198 419.1528 372.2113 471.3644 -4.1246 414.7916 418.9162 372.0120 472.9881 -4.1176 414.6032 418.7208 371.7848 474.5966 -4.1116 414.4247 418.5363 371.6036 476.2053 -4.1129 414.2411 418.3540 371.3840 477.8138 -4.1107 414.0176 418.1282 371.1641 479.4171 -4.1022 413.7895 417.8917 370.9555 481.0258 -4.0964 413.5857 417.6821 370.7473 482.6343 -4.0887 413.3884 417.4771 370.5261 484.2581 -4.0788 413.1397 417.2185 370.2913 485.8564 -4.0747 412.8944 416.9692 370.0486 487.4649 -4.0702 412.6806 416.7508 369.8713 489.0581 -4.0663 412.5207 416.5871 369.6968 490.6616 -4.0603 412.2990 416.3593 369.4984 492.2701 -4.0582 412.0345 416.0927 369.2974 493.8735 -4.0522 411.7987 415.8509 369.0821 495.4666 -4.0457 411.6121 415.6577 368.8371 497.0699 -4.0351 411.3874 415.4225 368.6492 498.6889 -4.0262 411.1897 415.2159 368.4212 500.2974 -4.0191 411.0183 415.0375 368.2324 501.9009 -4.0156 410.8137 414.8293 367.9890 503.5299 -4.0133 410.5999 414.6133 367.7270 505.1180 -4.0071 410.4038 414.4109 367.4920 506.7315 -3.9975 410.1834 414.1809 367.3050 508.3400 -3.9942 409.9942 413.9885 367.1097 509.9640 -3.9891 409.7783 413.7675 366.9195 511.5673 -3.9829 409.5351 413.5181 366.7325 513.1760 -3.9746 409.3121 413.2867 366.5237 514.7846 -3.9725 409.1131 413.0855 366.2848 516.3931 -3.9669 408.9086 412.8755 366.0750 517.9914 -3.9566 408.6797 412.6363 365.8975 519.5896 -3.9485 408.4761 412.4246 365.6959 521.2136 -3.9425 408.2506 412.1931 365.5051 522.8119 -3.9406 407.9977 411.9382 365.2966 524.4103 -3.9364 407.7441 411.6805 365.1043 526.0185 -3.9376 407.5470 411.4846 364.8757 527.6220 -3.9307 407.3368 411.2675 364.6955 529.2254 -3.9174 407.1267 411.0441 364.4962 530.8286 -3.9052 406.9330 410.8382 364.2743 532.4373 -3.9026 406.7647 410.6673 364.0609 534.0610 -3.8974 406.5566 410.4539 363.8323 535.6695 -3.8884 406.3389 410.2274 363.6091 537.2781 -3.8836 406.1054 409.9890 363.3997 538.8865 -3.8799 405.8773 409.7571 363.2102 540.4951 -3.8755 405.6377 409.5132 363.0043 542.1038 -3.8653 405.4297 409.2950 362.8116 543.6966 -3.8616 405.2067 409.0683 362.5599 545.3053 -3.8522 404.9788 408.8309 362.3505 546.9289 -3.8471 404.7645 408.6116 362.1573 548.5375 -3.8455 404.5689 408.4144 361.9250 550.1308 -3.8401 404.3491 408.1893 361.7166 551.7340 -3.8345 404.1687 408.0032 361.4962 553.3426 -3.8294 404.0010 407.8303 361.2584 554.9460 -3.8202 403.8052 407.6254 361.0737 556.5493 -3.8134 403.5615 407.3749 360.8601 558.1683 -3.8101 403.3609 407.1710 360.6430 559.7715 -3.8048 403.1337 406.9384 360.4333 561.3800 -3.7916 402.9424 406.7340 360.2485 562.9835 -3.7833 402.7329 406.5162 360.0032 564.5920 -3.7795 402.4888 406.2683 359.8014 566.1954 -3.7732 402.2643 406.0376 359.6068 567.8040 -3.7655 402.0588 405.8243 359.4235 569.4279 -3.7619 401.8370 405.5989 359.2356 571.0313 -3.7554 401.6295 405.3849 359.0200 572.6399 -3.7473 401.4085 405.1558 358.7883 574.2484 -3.7466 401.1701 404.9168 358.5759 575.8568 -3.7445 400.9639 404.7084 358.3661 577.4654 -3.7398 400.7706 404.5103 358.1341 579.0736 -3.7272 400.5751 404.3023 357.9311 580.6976 -3.7196 400.3600 404.0795 357.7153 582.3009 -3.7162 400.1502 403.8664 357.5234 583.8940 -3.7075 399.9484 403.6559 357.3236 585.4975 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