DTA measure 1gyors Date: 202691:1618 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.34 s Mass = 100.000 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5966 -1.0366 218.0689 219.1055 198.9274 4.1954 -1.0338 217.9943 219.0282 198.9157 5.8049 -1.0303 217.9132 218.9435 198.9034 7.4090 -1.0273 217.8208 218.8481 198.8851 9.0134 -1.0245 217.7467 218.7712 198.8601 10.6329 -1.0227 217.6475 218.6703 198.8396 12.2369 -1.0222 217.5625 218.5846 198.8438 13.8464 -1.0222 217.4797 218.5018 198.8191 15.4451 -1.0202 217.4104 218.4306 198.8254 17.0495 -1.0200 217.3306 218.3506 198.8455 18.6536 -1.0163 217.2561 218.2724 198.8631 20.2578 -1.0159 217.1775 218.1934 198.8985 21.8621 -1.0135 217.0952 218.1087 198.9495 23.4763 -1.0108 217.0246 218.0353 198.9773 25.0808 -1.0065 216.9481 217.9546 199.0277 26.6744 -1.0050 216.8653 217.8703 199.0745 28.2785 -1.0044 216.8027 217.8071 199.1454 29.8880 -1.0010 216.7299 217.7308 199.2145 31.4918 -0.9991 216.6524 217.6515 199.2995 33.0910 -1.0014 216.5721 217.5735 199.3688 34.7156 -0.9985 216.5066 217.5050 199.4403 36.3195 -0.9954 216.4305 217.4260 199.5392 37.9290 -0.9919 216.3545 217.3463 199.6501 39.5279 -0.9905 216.2750 217.2655 199.7469 41.1319 -0.9914 216.2059 217.1973 199.8574 42.7260 -0.9890 216.1431 217.1321 199.9909 44.3299 -0.9889 216.0838 217.0728 200.1255 45.9393 -0.9893 216.0181 217.0074 200.2691 47.5640 -0.9878 215.9465 216.9343 200.4068 49.1679 -0.9874 215.8750 216.8624 200.5459 50.7723 -0.9868 215.8115 216.7983 200.6875 52.3763 -0.9839 215.7245 216.7084 200.8181 53.9699 -0.9840 215.6378 216.6218 200.9553 55.5744 -0.9810 215.5740 216.5550 201.0944 57.1834 -0.9790 215.5129 216.4919 201.2187 58.7875 -0.9816 215.4455 216.4271 201.3744 60.4073 -0.9862 215.3587 216.3449 201.5195 62.0161 -0.9877 215.2871 216.2748 201.6738 63.6203 -0.9868 215.2272 216.2141 201.8323 65.2296 -0.9870 215.1802 216.1672 201.9955 66.8233 -0.9865 215.1385 216.1250 202.1492 68.4326 -0.9861 215.0949 216.0810 202.3046 70.0369 -0.9872 215.0396 216.0267 202.4635 71.6459 -0.9896 214.9796 215.9691 202.6299 73.2503 -0.9911 214.9408 215.9320 202.8055 74.8549 -0.9915 214.8870 215.8786 202.9712 76.4651 -0.9907 214.8243 215.8150 203.1137 78.0699 -0.9941 214.7614 215.7555 203.2746 79.6746 -0.9958 214.7211 215.7168 203.4251 81.2753 -0.9940 214.6827 215.6766 203.5589 82.8800 -0.9919 214.6452 215.6371 203.6964 84.4899 -0.9907 214.6026 215.5933 203.8735 86.0801 -0.9918 214.5543 215.5461 204.0358 87.6953 -0.9942 214.5234 215.5177 204.2116 89.3051 -0.9941 214.5043 215.4984 204.3869 90.9099 -0.9951 214.4623 215.4574 204.5454 92.5154 -0.9967 214.4065 215.4032 204.7082 94.1204 -0.9952 214.3596 215.3549 204.8790 95.7251 -0.9938 214.3357 215.3296 205.0537 97.3299 -0.9937 214.3114 215.3051 205.2408 98.9356 -0.9947 214.2904 215.2851 205.4217 100.5404 -0.9939 214.2722 215.2661 205.5822 102.1451 -0.9929 214.2416 215.2345 205.7510 103.7503 -0.9932 214.2186 215.2118 205.9177 105.3556 -0.9940 214.1973 215.1913 206.0792 106.9604 -0.9945 214.1833 215.1779 206.2689 108.5600 -0.9949 214.1633 215.1582 206.4565 110.1699 -0.9948 214.1317 215.1265 206.6236 111.7910 -0.9935 214.0918 215.0852 206.8099 113.3906 -0.9944 214.0900 215.0844 206.9915 115.0005 -0.9963 214.0537 215.0500 207.1748 116.6058 -0.9927 214.0240 215.0167 207.3776 118.2110 -0.9937 213.9897 214.9835 207.5688 119.7953 -0.9948 213.9931 214.9879 207.7345 121.4000 -0.9957 213.9770 214.9726 207.9002 123.0058 -0.9936 213.9762 214.9698 208.0732 124.6259 -0.9924 213.9637 214.9561 208.2596 126.2255 -0.9913 213.9508 214.9421 208.4355 127.8363 -0.9920 213.9274 214.9193 208.6066 129.4360 -0.9920 213.9227 214.9148 208.7929 131.0408 -0.9918 213.9231 214.9149 208.9664 132.6460 -0.9908 213.9330 214.9239 209.1309 134.2513 -0.9890 213.9186 214.9076 209.3035 135.8714 -0.9870 213.9219 214.9089 209.4750 137.4761 -0.9899 213.9121 214.9020 209.6744 139.0768 -0.9898 213.9341 214.9239 209.8573 140.6866 -0.9873 213.9266 214.9139 210.0533 142.2863 -0.9865 213.9221 214.9087 210.2556 143.8911 -0.9849 213.9312 214.9161 210.4583 145.4968 -0.9840 213.9331 214.9171 210.6600 147.1169 -0.9855 213.9505 214.9360 210.8430 148.7216 -0.9841 213.9690 214.9531 211.0241 150.3268 -0.9797 213.9932 214.9729 211.2331 151.9321 -0.9764 214.0119 214.9883 211.4226 153.5318 -0.9754 214.0248 215.0002 211.5831 155.1365 -0.9754 214.0197 214.9952 211.7510 156.7421 -0.9756 214.0221 214.9977 211.9277 158.3573 -0.9756 214.0553 215.0309 212.0993 159.9671 -0.9748 214.0771 215.0518 212.2759 161.5668 -0.9753 214.1309 215.1061 212.4738 163.1776 -0.9736 214.1408 215.1144 212.6468 164.7773 -0.9724 214.1530 215.1254 212.8063 166.3769 -0.9710 214.1662 215.1372 212.9774 167.9818 -0.9688 214.1879 215.1567 213.1563 169.5874 -0.9673 214.2265 215.1938 213.3412 171.2126 -0.9663 214.2851 215.2514 213.5434 172.8125 -0.9661 214.3206 215.2867 213.7296 174.4129 -0.9643 214.3450 215.3094 213.9192 176.0279 -0.9651 214.3828 215.3480 214.1267 177.6275 -0.9651 214.4119 215.3771 214.3071 179.2380 -0.9625 214.4579 215.4204 214.4927 180.8431 -0.9623 214.5109 215.4732 214.7071 182.4325 -0.9623 214.5369 215.4992 214.8737 184.0529 -0.9583 214.5849 215.5432 215.0540 185.6738 -0.9544 214.6148 215.5692 215.2506 187.2580 -0.9514 214.6417 215.5931 215.4229 188.8628 -0.9502 214.7049 215.6550 215.6156 190.4679 -0.9479 214.7685 215.7164 215.8133 192.0784 -0.9474 214.8025 215.7499 215.9979 193.6780 -0.9470 214.8563 215.8033 216.1931 195.2981 -0.9460 214.9114 215.8574 216.3878 196.9088 -0.9467 214.9635 215.9101 216.5625 198.5086 -0.9463 215.0180 215.9643 216.7279 200.1083 -0.9459 215.0556 216.0015 216.9066 201.7183 -0.9475 215.1304 216.0780 217.1032 203.3085 -0.9467 215.1865 216.1332 217.2848 204.9081 -0.9428 215.2393 216.1821 217.4400 206.5180 -0.9379 215.3002 216.2381 217.6441 208.1340 -0.9330 215.3596 216.2926 217.8617 209.7336 -0.9294 215.4194 216.3488 218.0492 211.3435 -0.9284 215.4849 216.4133 218.2326 212.9485 -0.9292 215.5498 216.4790 218.4458 214.5540 -0.9309 215.6102 216.5411 218.6620 216.1434 -0.9302 215.6601 216.5903 218.8801 217.7584 -0.9267 215.7667 216.6934 219.0800 219.3585 -0.9263 215.8378 216.7641 219.2758 220.9791 -0.9256 215.9118 216.8374 219.4624 222.5839 -0.9231 215.9665 216.8896 219.6750 224.1835 -0.9221 216.0491 216.9712 219.8811 225.7891 -0.9207 216.1199 217.0407 220.0731 227.4043 -0.9194 216.1977 217.1171 220.2433 229.0193 -0.9192 216.2728 217.1921 220.4525 230.6189 -0.9209 216.3416 217.2625 220.6619 232.2296 -0.9166 216.3894 217.3060 220.8669 233.8499 -0.9132 216.4545 217.3678 221.0633 235.4546 -0.9127 216.5339 217.4466 221.2391 237.0594 -0.9089 216.6180 217.5269 221.4259 238.6496 -0.9073 216.6907 217.5980 221.6220 240.2545 -0.9050 216.7632 217.6682 221.7880 241.8746 -0.9041 216.8523 217.7564 221.9784 243.4640 -0.9036 216.9317 217.8353 222.1720 245.0695 -0.9019 217.0241 217.9260 222.3723 246.6899 -0.8961 217.1144 218.0105 222.5596 248.2946 -0.8928 217.1958 218.0886 222.7409 249.9048 -0.8919 217.3155 218.2074 222.9319 251.5103 -0.8897 217.4053 218.2950 223.1160 253.1099 -0.8868 217.4948 218.3816 223.3032 254.7146 -0.8860 217.5793 218.4654 223.4683 256.3196 -0.8848 217.6808 218.5657 223.6948 257.9405 -0.8817 217.7678 218.6495 223.9019 259.5453 -0.8794 217.8631 218.7424 224.0979 261.1508 -0.8767 217.9604 218.8371 224.2940 262.7558 -0.8735 218.0719 218.9454 224.4968 264.3605 -0.8751 218.1632 219.0383 224.7176 265.9653 -0.8756 218.2565 219.1321 224.9369 267.5704 -0.8750 218.3599 219.2350 225.1618 269.1911 -0.8767 218.4747 219.3514 225.3555 270.7805 -0.8756 218.5540 219.4296 225.5404 272.3904 -0.8724 218.6523 219.5246 225.7241 273.9958 -0.8687 218.7736 219.6423 225.9285 275.6009 -0.8654 218.8992 219.7646 226.1429 277.2056 -0.8619 218.9893 219.8511 226.3513 278.8106 -0.8591 219.0876 219.9466 226.5473 280.4161 -0.8546 219.2108 220.0655 226.7638 282.0055 -0.8535 219.3312 220.1848 226.9699 283.6308 -0.8525 219.4280 220.2805 227.1945 285.2309 -0.8476 219.5352 220.3828 227.4028 286.8361 -0.8459 219.6321 220.4781 227.6048 288.4409 -0.8440 219.7496 220.5936 227.7802 290.0461 -0.8411 219.8587 220.6998 227.9617 291.6514 -0.8378 219.9807 220.8186 228.1595 293.2561 -0.8389 220.1215 220.9604 228.3645 294.8609 -0.8373 220.2299 221.0673 228.5644 296.4718 -0.8373 220.3320 221.1693 228.7524 298.0714 -0.8357 220.4446 221.2803 228.9316 299.6813 -0.8349 220.5598 221.3947 229.1235 301.2865 -0.8367 220.6633 221.5000 229.3017 302.8866 -0.8334 220.7856 221.6189 229.4702 304.4863 -0.8321 220.9151 221.7471 229.6491 306.0910 -0.8306 221.0432 221.8737 229.8353 307.6966 -0.8266 221.1702 221.9968 230.0117 309.3169 -0.8261 221.2865 222.1126 230.1877 310.9216 -0.8214 221.4171 222.2385 230.3838 312.5268 -0.8196 221.5743 222.3940 230.5854 314.1168 -0.8170 221.7129 222.5299 230.7836 315.7369 -0.8124 221.8435 222.6558 230.9852 317.3213 -0.8110 221.9759 222.7869 231.1774 318.9421 -0.8118 222.1367 222.9485 231.3589 320.5419 -0.8104 222.2542 223.0646 231.5540 322.1518 -0.8083 222.3542 223.1625 231.7552 323.7516 -0.8061 222.4880 223.2941 231.9684 325.3623 -0.8006 222.6179 223.4185 232.2000 326.9670 -0.8003 222.7782 223.5785 232.4167 328.5666 -0.7995 222.8960 223.6955 232.6105 330.1775 -0.8006 223.0225 223.8232 232.7871 331.7823 -0.8033 223.1756 223.9790 233.0074 333.3973 -0.8023 223.2769 224.0792 233.2276 335.0074 -0.8002 223.4141 224.2143 233.4512 336.6078 -0.7991 223.5360 224.3351 233.6523 338.2176 -0.7999 223.6724 224.4723 233.8686 339.8173 -0.7974 223.8052 224.6026 234.0627 341.4228 -0.7948 223.9469 224.7416 234.2688 343.0278 -0.7923 224.1079 224.9002 234.4705 344.6479 -0.7919 224.2599 225.0518 234.7007 346.2535 -0.7902 224.3961 225.1863 234.9076 347.8635 -0.7886 224.5168 225.3054 235.1016 349.4631 -0.7866 224.6520 225.4386 235.3089 351.0685 -0.7856 224.7851 225.5707 235.5169 352.6736 -0.7845 224.9421 225.7265 235.7146 354.2784 -0.7877 225.1003 225.8880 235.9057 355.8986 -0.7891 225.2627 226.0519 236.1273 357.5043 -0.7881 225.4317 226.2198 236.3491 359.1039 -0.7819 225.5767 226.3586 236.5409 360.7138 -0.7793 225.7227 226.5021 236.7305 362.3185 -0.7784 225.8556 226.6340 236.9158 363.9233 -0.7783 226.0062 226.7845 237.1234 365.5288 -0.7770 226.1645 226.9415 237.3130 367.1440 -0.7766 226.3467 227.1234 237.4947 368.7539 -0.7763 226.4801 227.2565 237.6961 370.3541 -0.7780 226.6326 227.4106 237.8974 371.9593 -0.7780 226.8051 227.5831 238.0869 373.5691 -0.7773 226.9465 227.7237 238.2724 375.1589 -0.7766 227.1225 227.8991 238.4471 376.7745 -0.7728 227.2590 228.0319 238.6277 378.3690 -0.7698 227.4093 228.1792 238.8109 379.9844 -0.7687 227.5630 228.3317 238.9918 381.5898 -0.7673 227.7080 228.4753 239.1778 383.1945 -0.7651 227.8401 228.6052 239.3551 384.7993 -0.7662 228.0101 228.7763 239.5478 386.4099 -0.7680 228.1795 228.9475 239.7381 388.0098 -0.7681 228.3167 229.0848 239.9495 389.5940 -0.7667 228.4669 229.2336 240.1609 391.2040 -0.7641 228.6353 229.3993 240.3460 392.8199 -0.7682 228.8154 229.5837 240.5394 394.4246 -0.7690 228.9839 229.7529 240.7559 396.0345 -0.7698 229.1436 229.9133 240.9691 397.6341 -0.7707 229.3046 230.0753 241.1695 399.2399 -0.7701 229.4828 230.2529 241.3835 400.8446 -0.7705 229.6505 230.4210 241.5936 402.4340 -0.7701 229.7949 230.5650 241.8067 404.0390 -0.7724 229.9496 230.7220 242.0121 405.6599 -0.7704 230.1099 230.8802 242.2302 407.2595 -0.7716 230.2692 231.0407 242.4319 408.8749 -0.7717 230.4395 231.2112 242.6186 410.4751 -0.7704 230.5925 231.3628 242.8294 412.0901 -0.7720 230.7612 231.5332 243.0429 413.6954 -0.7693 230.9401 231.7094 243.2215 415.3058 -0.7660 231.1193 231.8853 243.4097 416.9105 -0.7654 231.2918 232.0571 243.6049 418.5258 -0.7661 231.4443 232.2104 243.7869 420.1364 -0.7661 231.6309 232.3971 244.0106 421.7360 -0.7687 231.7889 232.5576 244.2327 423.3356 -0.7666 231.9383 232.7048 244.4225 424.9463 -0.7652 232.1159 232.8811 244.6015 426.5513 -0.7659 232.2842 233.0501 244.8026 428.1663 -0.7674 232.4496 233.2170 245.0091 429.7771 -0.7679 232.6351 233.4031 245.2125 431.3768 -0.7678 232.8024 233.5702 245.4190 432.9866 -0.7671 232.9580 233.7251 245.6212 434.5864 -0.7671 233.1369 233.9040 245.8331 436.1920 -0.7675 233.3062 234.0736 246.0255 437.7968 -0.7672 233.4678 234.2350 246.2168 439.4169 -0.7637 233.6393 234.4030 246.4118 441.0223 -0.7621 233.8382 234.6003 246.6207 442.6274 -0.7626 234.0045 234.7671 246.8339 444.2321 -0.7644 234.1851 234.9495 247.0567 445.8318 -0.7642 234.3698 235.1340 247.2567 447.4366 -0.7627 234.5495 235.3122 247.4503 449.0423 -0.7636 234.7149 235.4785 247.6317 450.6624 -0.7658 234.8954 235.6612 247.8332 452.2673 -0.7689 235.0810 235.8499 248.0191 453.8729 -0.7721 235.2425 236.0147 248.2165 455.4828 -0.7747 235.4351 236.2098 248.3965 457.0824 -0.7746 235.6510 236.4257 248.6102 458.6820 -0.7758 235.8316 236.6074 248.8265 460.2878 -0.7743 236.0186 236.7929 249.0436 461.9079 -0.7729 236.1969 236.9697 249.2588 463.5126 -0.7722 236.3756 237.1478 249.4764 465.1178 -0.7737 236.5700 237.3437 249.6668 466.7231 -0.7720 236.7466 237.5186 249.8726 468.3279 -0.7728 236.9090 237.6818 250.1098 469.9326 -0.7714 237.0907 237.8621 250.3334 471.5326 -0.7744 237.2839 238.0583 250.5664 473.1585 -0.7775 237.4547 238.2322 250.8070 474.7581 -0.7797 237.6221 238.4017 251.0256 476.3635 -0.7820 237.7978 238.5798 251.2433 477.9738 -0.7840 237.9874 238.7714 251.4656 479.5888 -0.7849 238.1794 238.9643 251.6958 481.1938 -0.7854 238.3529 239.1382 251.9267 482.7839 -0.7856 238.5436 239.3292 252.1615 484.4040 -0.7895 238.7456 239.5352 252.3796 486.0141 -0.7894 238.9469 239.7363 252.5832 487.6196 -0.7886 239.1355 239.9241 252.7940 489.2193 -0.7907 239.3105 240.1013 253.0300 490.8291 -0.7887 239.4823 240.2710 253.2657 492.4348 -0.7873 239.6854 240.4727 253.4604 494.0396 -0.7884 239.8802 240.6686 253.6756 495.6599 -0.7887 240.0732 240.8619 253.9094 497.2604 -0.7871 240.2483 241.0354 254.1350 498.8651 -0.7889 240.4177 241.2066 254.3673 500.4699 -0.7910 240.5903 241.3813 254.5744 502.0698 -0.7922 240.7808 241.5730 254.7921 503.6958 -0.7955 240.9741 241.7696 254.9926 505.3159 -0.7961 241.1788 241.9749 255.2008 506.9155 -0.7943 241.3849 242.1792 255.4171 508.5254 -0.7952 241.5996 242.3948 255.6460 510.1255 -0.7970 241.7997 242.5967 255.8580 511.7256 -0.7961 241.9847 242.7809 256.0677 513.3355 -0.7968 242.1887 242.9856 256.2630 514.9404 -0.7992 242.3719 243.1710 256.4668 516.5563 -0.8039 242.5743 243.3783 256.6989 518.1661 -0.8036 242.7778 243.5814 256.9280 519.7660 -0.8017 242.9574 243.7592 257.1248 521.3715 -0.8047 243.1291 243.9337 257.3224 522.9763 -0.8065 243.3374 244.1439 257.5165 524.5810 -0.8086 243.5249 244.3336 257.7065 526.1918 -0.8103 243.7274 244.5377 257.8946 527.7915 -0.8132 243.9502 244.7633 258.0798 529.3963 -0.8146 244.1683 244.9828 258.3154 531.0069 -0.8173 244.3711 245.1885 258.5113 532.6119 -0.8214 244.5598 245.3812 258.6983 534.2218 -0.8216 244.7511 245.5726 258.8962 535.8219 -0.8239 244.9262 245.7501 259.0801 537.4220 -0.8253 245.1059 245.9312 259.2826 539.0319 -0.8273 245.3166 246.1439 259.4802 540.6520 -0.8278 245.5227 246.3505 259.6855 542.2519 -0.8303 245.6941 246.5244 259.8885 543.8625 -0.8300 245.8720 246.7020 260.0923 545.4621 -0.8303 246.0684 246.8986 260.2842 547.0675 -0.8305 246.2899 247.1204 260.4760 548.6726 -0.8330 246.5166 247.3496 260.6665 550.2723 -0.8357 246.6949 247.5306 260.8512 551.8821 -0.8354 246.8941 247.7295 261.0435 553.4819 -0.8358 247.0938 247.9297 261.2473 555.0875 -0.8377 247.3003 248.1380 261.4464 556.6923 -0.8407 247.5038 248.3446 261.6413 558.2920 -0.8452 247.7075 248.5527 261.8528 559.8976 -0.8473 247.9064 248.7537 262.0687 561.5024 -0.8479 248.0952 248.9432 262.2566 563.1071 -0.8516 248.3093 249.1609 262.4411 564.7223 -0.8524 248.4998 249.3522 262.6330 566.3330 -0.8508 248.6945 249.5453 262.8263 567.9275 -0.8542 248.8945 249.7487 263.0085 569.5323 -0.8547 249.1018 249.9565 263.2047 571.1431 -0.8561 249.3094 250.1656 263.3904 572.7479 -0.8564 249.5086 250.3650 263.5720 574.3475 -0.8556 249.7125 250.5681 263.7471 575.9729 -0.8581 249.9290 250.7871 263.9440 577.5734 -0.8629 250.1258 250.9887 264.1336 579.1833 -0.8647 250.3182 251.1829 264.3154 580.7830 -0.8677 250.5024 251.3701 264.4807 582.3886 -0.8695 250.7082 251.5778 264.6811 583.9934 -0.8714 250.9229 251.7943 264.8829 585.5828 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