DTA measure 1lassu Date: 202691:1514 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1078.98 s Mass = 100.000 mg data_number = 1343 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2410 0.4523 195.3757 194.9234 247.5133 2.0895 0.4530 195.6585 195.2054 247.5131 2.8550 0.4512 195.9126 195.4613 247.5286 3.6830 0.4526 196.2034 195.7508 247.5412 4.4393 0.4553 196.4467 195.9914 247.5476 5.2768 0.4568 196.7488 196.2920 247.5398 6.0635 0.4588 197.0189 196.5602 247.5662 6.8505 0.4609 197.2889 196.8280 247.5935 7.6883 0.4585 197.5633 197.1048 247.6100 8.4440 0.4560 197.8179 197.3619 247.6327 9.3028 0.4558 198.0947 197.6389 247.6714 10.0693 0.4563 198.3499 197.8936 247.7089 10.8860 0.4568 198.6103 198.1535 247.7546 11.6833 0.4580 198.8884 198.4303 247.7807 12.4805 0.4592 199.1717 198.7125 247.8175 13.3080 0.4634 199.4371 198.9737 247.8689 14.0740 0.4620 199.6904 199.2284 247.9222 14.9225 0.4615 199.9669 199.5054 247.9883 15.6883 0.4582 200.2175 199.7593 248.0461 16.5160 0.4581 200.5041 200.0460 248.1211 17.3030 0.4561 200.7762 200.3201 248.1737 18.1100 0.4568 201.0263 200.5694 248.2135 18.9273 0.4551 201.2797 200.8246 248.2896 19.6835 0.4570 201.5362 201.0792 248.3863 20.5523 0.4553 201.8220 201.3667 248.4847 21.3078 0.4560 202.0643 201.6084 248.5832 22.1358 0.4597 202.3299 201.8702 248.6807 22.9330 0.4609 202.6029 202.1420 248.7609 23.7293 0.4612 202.8611 202.3999 248.8718 24.5573 0.4617 203.1303 202.6686 248.9729 25.3135 0.4605 203.3680 202.9074 249.0683 26.1818 0.4597 203.6343 203.1746 249.1803 26.9070 0.4589 203.8635 203.4046 249.3086 27.7658 0.4582 204.1229 203.6647 249.4494 28.5315 0.4581 204.3605 203.9024 249.5566 29.3490 0.4583 204.6108 204.1525 249.6705 30.1463 0.4567 204.8531 204.3964 249.7804 30.9433 0.4569 205.0922 204.6353 249.9287 31.7705 0.4539 205.3605 204.9066 250.0768 32.5370 0.4526 205.6011 205.1486 250.1828 33.3855 0.4514 205.8676 205.4162 250.3127 34.1615 0.4507 206.1094 205.6588 250.4486 34.9790 0.4512 206.3468 205.8956 250.5896 35.7763 0.4522 206.5985 206.1463 250.7150 36.5728 0.4515 206.8526 206.4011 250.8588 37.4005 0.4480 207.0922 206.6442 251.0063 38.1568 0.4473 207.3167 206.8694 251.1528 39.0153 0.4447 207.5793 207.1346 251.2957 39.7810 0.4435 207.8197 207.3762 251.4096 40.6090 0.4416 208.0918 207.6502 251.5661 41.3960 0.4403 208.3152 207.8749 251.7021 42.2028 0.4389 208.5566 208.1177 251.8331 43.0203 0.4381 208.7767 208.3386 251.9687 43.7765 0.4355 208.9935 208.5580 252.0824 44.6450 0.4340 209.3035 208.8695 252.2197 45.4008 0.4306 209.5497 209.1191 252.3449 46.2288 0.4267 209.8042 209.3776 252.4811 47.0260 0.4242 210.0264 209.6021 252.6275 47.8120 0.4192 210.2453 209.8261 252.7743 48.6400 0.4157 210.4750 210.0593 252.9184 49.4065 0.4134 210.7238 210.3105 253.0551 50.2548 0.4092 210.9990 210.5898 253.1835 51.0205 0.4081 211.2071 210.7990 253.3323 51.8485 0.4098 211.4603 211.0505 253.4803 52.6458 0.4080 211.6828 211.2748 253.6100 53.4420 0.4048 211.9129 211.5081 253.7470 54.2598 0.3989 212.1412 211.7423 253.8805 55.0365 0.3972 212.3606 211.9634 254.0073 55.8843 0.3934 212.6354 212.2419 254.1412 56.6505 0.3916 212.8580 212.4664 254.2811 57.4785 0.3892 213.1066 212.7174 254.4209 58.2750 0.3897 213.3351 212.9454 254.5526 59.0618 0.3848 213.5512 213.1664 254.6926 59.8898 0.3799 213.7836 213.4036 254.8422 60.6560 0.3756 213.9978 213.6223 254.9764 61.5140 0.3718 214.2404 213.8686 255.1306 62.2395 0.3702 214.4658 214.0956 255.2312 63.1083 0.3701 214.7361 214.3660 255.3578 63.8740 0.3662 214.9685 214.6023 255.4884 64.6918 0.3659 215.1891 214.8232 255.6113 65.5198 0.3636 215.4226 215.0590 255.7472 66.2855 0.3603 215.6343 215.2739 255.8744 67.1133 0.3574 215.8557 215.4982 256.0272 67.8695 0.3547 216.0749 215.7202 256.1703 68.7380 0.3509 216.3279 215.9770 256.3319 69.4938 0.3465 216.5418 216.1953 256.4708 70.3218 0.3417 216.7675 216.4259 256.5992 71.1185 0.3395 217.0005 216.6610 256.7202 71.9153 0.3361 217.2336 216.8974 256.8530 72.7433 0.3303 217.4581 217.1279 256.9888 73.4993 0.3261 217.6675 217.3413 257.1243 74.3573 0.3212 217.9074 217.5861 257.2897 75.1238 0.3181 218.1170 217.7990 257.4254 75.9415 0.3181 218.3319 218.0138 257.5533 76.7483 0.3146 218.5511 218.2365 257.6925 77.5350 0.3121 218.7591 218.4470 257.8428 78.3528 0.3088 218.9804 218.6716 257.9778 79.1293 0.3038 219.2010 218.8972 258.1113 79.9770 0.2997 219.4304 219.1307 258.2605 80.7435 0.2962 219.6419 219.3458 258.3921 81.5715 0.2925 219.8595 219.5670 258.5281 82.3678 0.2893 220.0758 219.7865 258.6411 83.1650 0.2848 220.2870 220.0022 258.7619 83.9828 0.2817 220.5111 220.2294 258.9069 84.7483 0.2776 220.7370 220.4594 259.0338 85.6070 0.2770 220.9578 220.6808 259.1798 86.3633 0.2728 221.1744 220.9016 259.3028 87.2010 0.2683 221.4049 221.1366 259.4298 87.9568 0.2649 221.6168 221.3519 259.5494 88.7848 0.2642 221.8387 221.5745 259.6981 89.5820 0.2603 222.0564 221.7961 259.8544 90.3680 0.2534 222.2871 222.0337 259.9982 91.1960 0.2463 222.5128 222.2665 260.1249 91.9625 0.2414 222.7135 222.4721 260.2355 92.8208 0.2405 222.9282 222.6877 260.3694 93.5868 0.2374 223.1459 222.9085 260.5000 94.4045 0.2313 223.3579 223.1266 260.6416 95.2118 0.2244 223.5952 223.3708 260.7786 95.9980 0.2215 223.8035 223.5820 260.9027 96.8158 0.2179 224.0253 223.8074 261.0295 97.5923 0.2148 224.2115 223.9966 261.1392 98.4195 0.2099 224.4300 224.2201 261.2662 99.1860 0.2048 224.6156 224.4109 261.3929 100.0345 0.1996 224.8437 224.6441 261.5370 100.8103 0.1975 225.0608 224.8632 261.6739 101.6280 0.1927 225.2770 225.0843 261.7990 102.4150 0.1884 225.4800 225.2916 261.9297 103.2215 0.1860 225.6715 225.4854 262.0407 104.0393 0.1851 225.8752 225.6901 262.1931 104.8058 0.1815 226.0759 225.8944 262.3206 105.6640 0.1782 226.3012 226.1231 262.4716 106.4300 0.1743 226.4916 226.3173 262.6015 107.2580 0.1689 226.7065 226.5376 262.7353 108.0135 0.1641 226.8932 226.7291 262.8797 108.8515 0.1607 227.1250 226.9643 263.0340 109.6385 0.1535 227.3442 227.1907 263.1673 110.4253 0.1486 227.5463 227.3977 263.2940 111.2628 0.1434 227.7549 227.6114 263.4427 112.0190 0.1378 227.9486 227.8108 263.5944 112.8778 0.1348 228.1644 228.0296 263.7427 113.6433 0.1288 228.3560 228.2272 263.8631 114.4713 0.1216 228.5752 228.4536 264.0101 115.2583 0.1135 228.7835 228.6700 264.1334 116.0550 0.1131 228.9872 228.8741 264.2632 116.8825 0.1085 229.2063 229.0979 264.4023 117.6490 0.1056 229.4144 229.3088 264.5302 118.4973 0.1002 229.6267 229.5265 264.7040 119.2733 0.0951 229.8305 229.7354 264.8355 120.0910 0.0898 230.0359 229.9461 264.9386 120.8880 0.0860 230.2463 230.1603 265.0805 121.6845 0.0824 230.4513 230.3689 265.2149 122.4818 0.0779 230.6486 230.5707 265.3260 123.2790 0.0757 230.8434 230.7677 265.4376 124.0958 0.0698 231.0495 230.9798 265.5523 124.8725 0.0648 231.2360 231.1712 265.6704 125.7210 0.0619 231.4589 231.3970 265.8087 126.4868 0.0561 231.6717 231.6156 265.9536 127.3145 0.0513 231.8983 231.8469 266.1036 128.1118 0.0486 232.0960 232.0473 266.2281 128.9085 0.0454 232.2864 232.2411 266.3495 129.6950 0.0391 232.4835 232.4444 266.4877 130.5025 0.0348 232.6831 232.6482 266.6152 131.3508 0.0318 232.8885 232.8566 266.7898 132.0755 0.0256 233.0733 233.0477 266.9201 132.9445 0.0202 233.2712 233.2510 267.0636 133.7005 0.0157 233.4597 233.4440 267.1863 134.5175 0.0120 233.6864 233.6745 267.3126 135.3558 0.0079 233.9072 233.8993 267.4558 136.1118 0.0060 234.1007 234.0946 267.5844 136.9698 0.0027 234.3198 234.3171 267.7275 137.7055 -0.0005 234.4953 234.4959 267.8687 138.5538 -0.0057 234.6948 234.7005 268.0249 139.3195 -0.0101 234.8742 234.8844 268.1526 140.1475 -0.0162 235.0737 235.0899 268.3025 140.9445 -0.0231 235.2752 235.2983 268.4200 141.7410 -0.0294 235.4716 235.5010 268.5635 142.5588 -0.0323 235.6658 235.6981 268.6951 143.3353 -0.0330 235.8399 235.8728 268.8447 144.1830 -0.0380 236.0443 236.0824 268.9870 144.9495 -0.0424 236.2339 236.2763 269.1237 145.7775 -0.0490 236.4368 236.4858 269.2702 146.5738 -0.0569 236.6369 236.6938 269.4153 147.3710 -0.0633 236.8082 236.8715 269.5460 148.1885 -0.0680 237.0074 237.0754 269.6901 148.9645 -0.0732 237.1885 237.2617 269.8103 149.8130 -0.0771 237.3779 237.4550 269.9687 150.5693 -0.0825 237.5597 237.6422 270.0957 151.4065 -0.0882 237.7685 237.8566 270.2201 152.1935 -0.0900 237.9707 238.0607 270.3427 152.9908 -0.0940 238.1536 238.2476 270.4781 153.8183 -0.0996 238.3325 238.4321 270.6274 154.5843 -0.1031 238.5020 238.6051 270.7487 155.4328 -0.1100 238.6968 238.8068 270.8835 156.1990 -0.1168 238.8965 239.0133 271.0054 157.0263 -0.1229 239.1037 239.2266 271.1323 157.8235 -0.1283 239.2943 239.4226 271.2664 158.6105 -0.1341 239.4602 239.5943 271.4116 159.4480 -0.1374 239.6673 239.8047 271.5660 160.2040 -0.1432 239.8446 239.9878 271.7030 161.0525 -0.1480 240.0595 240.2075 271.8676 161.8285 -0.1523 240.2423 240.3946 272.0122 162.6460 -0.1552 240.4307 240.5859 272.1510 163.4433 -0.1595 240.6060 240.7656 272.2933 164.2403 -0.1666 240.7951 240.9617 272.4206 165.0675 -0.1721 240.9973 241.1694 272.5442 165.8340 -0.1776 241.1728 241.3504 272.6766 166.6820 -0.1849 241.3765 241.5614 272.8083 167.4583 -0.1921 241.5705 241.7626 272.9526 168.2760 -0.1951 241.7927 241.9879 273.0874 169.0733 -0.2002 241.9809 242.1810 273.2272 169.8695 -0.2073 242.1747 242.3820 273.3755 170.6975 -0.2130 242.3608 242.5738 273.5119 171.4538 -0.2175 242.5345 242.7520 273.6150 172.3120 -0.2212 242.7241 242.9454 273.7558 173.0780 -0.2252 242.9023 243.1275 273.8718 173.8958 -0.2312 243.1332 243.3644 274.0021 174.6930 -0.2380 243.3034 243.5414 274.1264 175.4895 -0.2420 243.5005 243.7425 274.2518 176.3173 -0.2439 243.6772 243.9211 274.3929 177.0735 -0.2462 243.8619 244.1081 274.5155 177.9423 -0.2504 244.0753 244.3258 274.6579 178.6978 -0.2550 244.2572 244.5122 274.7844 179.5258 -0.2625 244.4624 244.7249 274.9169 180.3228 -0.2690 244.6535 244.9225 275.0545 181.1090 -0.2750 244.8287 245.1036 275.1789 181.9370 -0.2797 245.0096 245.2893 275.3290 182.7035 -0.2846 245.1876 245.4722 275.4499 183.5513 -0.2869 245.3903 245.6772 275.5763 184.3175 -0.2902 245.5691 245.8593 275.7243 185.1455 -0.2952 245.7703 246.0655 275.8473 185.9420 -0.3030 245.9495 246.2525 275.9771 186.7390 -0.3058 246.1207 246.4265 276.1025 187.5568 -0.3121 246.2890 246.6010 276.2299 188.3328 -0.3168 246.4532 246.7699 276.3569 189.1810 -0.3246 246.6516 246.9761 276.4907 189.9065 -0.3269 246.8060 247.1329 276.6061 190.7750 -0.3316 246.9967 247.3283 276.7461 191.5308 -0.3349 247.1650 247.4999 276.8615 192.3588 -0.3354 247.3474 247.6827 276.9846 193.1558 -0.3406 247.5406 247.8813 277.1119 193.9523 -0.3437 247.7185 248.0621 277.2338 194.7700 -0.3473 247.9172 248.2645 277.3764 195.5365 -0.3489 248.0958 248.4447 277.4918 196.3948 -0.3544 248.2894 248.6438 277.6591 197.1608 -0.3600 248.4514 248.8114 277.8002 197.9785 -0.3649 248.6374 249.0022 277.9384 198.7753 -0.3689 248.8232 249.1921 278.0721 199.5720 -0.3751 249.0036 249.3786 278.2075 200.3898 -0.3800 249.1965 249.5764 278.3377 201.1665 -0.3829 249.3643 249.7472 278.4541 201.9833 -0.3882 249.5196 249.9077 278.5761 202.7498 -0.3934 249.7084 250.1018 278.7114 203.6085 -0.4016 249.9057 250.3073 278.8497 204.3740 -0.4058 250.0866 250.4924 278.9700 205.2020 -0.4101 250.2747 250.6848 279.1041 205.9993 -0.4136 250.4595 250.8731 279.2216 206.7960 -0.4157 250.6541 251.0697 279.3540 207.6235 -0.4204 250.8387 251.2590 279.4904 208.3900 -0.4258 251.0070 251.4328 279.6021 209.2380 -0.4296 251.1887 251.6183 279.7266 209.9733 -0.4346 251.3283 251.7629 279.8460 210.8320 -0.4384 251.5136 251.9519 279.9737 211.5883 -0.4421 251.6581 252.1002 280.0855 212.4255 -0.4446 251.8445 252.2891 280.2103 213.2125 -0.4499 252.0270 252.4770 280.3415 214.0095 -0.4546 252.2103 252.6649 280.4661 214.8368 -0.4592 252.3983 252.8575 280.5706 215.5930 -0.4618 252.5622 253.0240 280.6759 216.4518 -0.4673 252.7573 253.2246 280.7994 217.2173 -0.4706 252.9265 253.3971 280.9204 218.0453 -0.4748 253.0948 253.5696 281.0498 218.8425 -0.4785 253.2766 253.7550 281.1851 219.6285 -0.4826 253.4614 253.9440 281.2893 220.4565 -0.4861 253.6447 254.1308 281.3986 221.2230 -0.4897 253.8248 254.3146 281.5261 222.0710 -0.4924 254.0022 254.4945 281.6725 222.8473 -0.4984 254.1841 254.6825 281.8017 223.6650 -0.5051 254.3720 254.8772 281.9421 224.4615 -0.5090 254.5565 255.0655 282.0623 225.2585 -0.5118 254.7403 255.2521 282.1877 226.0763 -0.5152 254.9021 255.4173 282.3271 226.8425 -0.5195 255.0662 255.5857 282.4554 227.7005 -0.5236 255.2480 255.7716 282.6037 228.4568 -0.5305 255.4009 255.9314 282.7466 229.2848 -0.5330 255.5792 256.1122 282.9016 230.0813 -0.5372 255.7711 256.3083 283.0377 230.8783 -0.5425 255.9490 256.4915 283.1846 231.6755 -0.5493 256.1289 256.6782 283.3168 232.4618 -0.5541 256.2953 256.8494 283.4491 233.2998 -0.5574 256.4828 257.0402 283.5860 234.0560 -0.5608 256.6551 257.2159 283.7122 234.9043 -0.5639 256.8036 257.3675 283.8695 235.6803 -0.5682 256.9443 257.5125 284.0192 236.4980 -0.5713 257.1168 257.6882 284.1621 237.2948 -0.5762 257.2895 257.8657 284.3043 238.0915 -0.5815 257.4632 258.0447 284.4445 238.9195 -0.5844 257.6458 258.2302 284.5866 239.6858 -0.5867 257.8029 258.3895 284.7410 240.5335 -0.5918 257.9781 258.5698 284.9050 241.3103 -0.5965 258.1562 258.7528 285.0526 242.1280 -0.6006 258.3409 258.9415 285.1924 242.9143 -0.6086 258.4939 259.1025 285.3499 243.7215 -0.6154 258.6749 259.2903 285.5028 244.5393 -0.6211 258.8563 259.4774 285.6490 245.3053 -0.6239 259.0074 259.6313 285.7919 246.1635 -0.6292 259.1782 259.8073 285.9386 246.9198 -0.6324 259.3358 259.9682 286.0633 247.7475 -0.6365 259.5087 260.1452 286.2160 248.5440 -0.6386 259.6737 260.3123 286.3629 249.3413 -0.6433 259.8470 260.4903 286.5127 250.1590 -0.6461 260.0263 260.6724 286.6556 250.9248 -0.6510 260.1971 260.8480 286.7854 251.7833 -0.6529 260.3750 261.0279 286.9158 252.5498 -0.6574 260.5266 261.1841 287.0461 253.3673 -0.6636 260.6997 261.3632 287.1976 254.1740 -0.6657 260.8665 261.5322 287.3640 254.9610 -0.6705 261.0260 261.6964 287.4982 255.7888 -0.6727 261.2021 261.8748 287.6415 256.5545 -0.6768 261.3730 262.0498 287.7781 257.3825 -0.6820 261.5581 262.2401 287.8956 258.1488 -0.6866 261.7064 262.3930 288.0237 258.9965 -0.6897 261.8916 262.5813 288.1572 259.7733 -0.6959 262.0489 262.7448 288.2730 260.5910 -0.6999 262.2416 262.9415 288.3934 261.3773 -0.7027 262.4220 263.1247 288.5080 262.1845 -0.7077 262.6032 263.3109 288.6133 263.0023 -0.7137 262.7594 263.4731 288.7357 263.7685 -0.7160 262.9163 263.6323 288.8504 264.6265 -0.7187 263.0935 263.8122 289.0241 265.4135 -0.7225 263.2573 263.9798 289.1461 266.2108 -0.7271 263.4211 264.1482 289.2490 267.0383 -0.7317 263.6122 264.3439 289.3778 267.8043 -0.7340 263.7792 264.5132 289.4680 268.6323 -0.7397 263.9753 264.7151 289.5784 269.3878 -0.7446 264.1511 264.8957 289.6998 270.2463 -0.7498 264.3106 265.0604 289.8111 271.0128 -0.7542 264.4583 265.2126 289.8980 271.8295 -0.7577 264.6160 265.3736 290.0258 272.6370 -0.7625 264.7726 265.5351 290.1461 273.4240 -0.7655 264.9334 265.6989 290.2647 274.2413 -0.7703 265.0891 265.8594 290.3807 275.0175 -0.7726 265.2639 266.0366 290.4915 275.8660 -0.7789 265.4458 266.2246 290.6019 276.6320 -0.7841 265.6255 266.4095 290.7171 277.4595 -0.7853 265.8227 266.6081 290.8519 278.2568 -0.7877 265.9775 266.7651 290.9725 279.0538 -0.7898 266.1368 266.9266 291.0922 279.8708 -0.7943 266.3123 267.1066 291.2229 280.6373 -0.7993 266.4570 267.2564 291.3302 281.4960 -0.8022 266.6353 267.4376 291.4597 282.2513 -0.8054 266.7712 267.5766 291.5691 283.0895 -0.8083 266.9366 267.7449 291.6837 283.8765 -0.8100 267.0925 267.9024 291.7920 284.6625 -0.8156 267.2589 268.0745 291.9196 285.5008 -0.8201 267.4294 268.2495 292.0624 286.2570 -0.8238 267.5886 268.4124 292.1911 287.1055 -0.8289 267.7602 268.5890 292.3173 287.8813 -0.8346 267.9259 268.7605 292.4334 288.6990 -0.8387 268.1106 268.9493 292.5749 289.4963 -0.8423 268.2919 269.1342 292.7070 290.2930 -0.8460 268.4625 269.3085 292.8358 291.1205 -0.8488 268.6288 269.4776 292.9805 291.8870 -0.8535 268.7716 269.6251 293.1108 292.7350 -0.8566 268.9569 269.8135 293.2366 293.5113 -0.8582 269.1214 269.9796 293.3443 294.3290 -0.8622 269.2961 270.1583 293.4599 295.1255 -0.8657 269.4451 270.3108 293.5902 295.9225 -0.8683 269.6143 270.4826 293.7298 296.7505 -0.8695 269.7753 270.6448 293.8784 297.5163 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