DTA measure 2lassu Date: 202691:1545 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1649.16 s Mass = 100.000 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4205 -4.6279 428.4063 433.0342 406.3419 4.0299 -4.6367 428.3859 433.0227 406.3356 5.6290 -4.6432 428.3318 432.9750 406.3444 7.2484 -4.6487 428.2859 432.9346 406.3511 8.8426 -4.6571 428.2197 432.8768 406.3558 10.4465 -4.6625 428.1766 432.8390 406.3687 12.0460 -4.6712 428.1356 432.8068 406.3656 13.6549 -4.6781 428.0895 432.7677 406.3423 15.2591 -4.6848 428.0297 432.7145 406.2872 16.8685 -4.6914 428.0005 432.6919 406.2340 18.4674 -4.7000 427.9657 432.6657 406.2090 20.0873 -4.7011 427.8903 432.5914 406.1477 21.6961 -4.7060 427.8313 432.5374 406.0439 23.2851 -4.7144 427.7661 432.4805 405.9367 24.8893 -4.7203 427.7105 432.4308 405.8218 26.4934 -4.7268 427.6729 432.3997 405.6991 28.0926 -4.7299 427.6183 432.3482 405.5732 29.7016 -4.7337 427.5786 432.3123 405.4284 31.3010 -4.7383 427.5188 432.2571 405.3141 32.9203 -4.7391 427.4502 432.1893 405.1937 34.5300 -4.7418 427.3849 432.1267 405.0495 36.1339 -4.7468 427.3464 432.0932 404.8935 37.7431 -4.7466 427.2956 432.0422 404.7062 39.3321 -4.7512 427.2596 432.0108 404.5309 40.9308 -4.7551 427.1959 431.9510 404.3552 42.5404 -4.7572 427.1433 431.9005 404.1549 44.1444 -4.7597 427.0698 431.8295 403.9712 45.7640 -4.7626 426.9910 431.7536 403.7995 47.3683 -4.7609 426.9386 431.6995 403.6299 48.9670 -4.7599 426.8877 431.6477 403.4474 50.5768 -4.7615 426.8146 431.5761 403.2652 52.1806 -4.7649 426.7638 431.5287 403.1102 53.7901 -4.7662 426.7101 431.4762 402.9179 55.3890 -4.7692 426.6280 431.3972 402.7063 57.0084 -4.7710 426.5990 431.3700 402.5387 58.6024 -4.7709 426.5370 431.3079 402.3553 60.2064 -4.7707 426.4745 431.2452 402.1845 61.8108 -4.7688 426.3850 431.1538 402.0061 63.4149 -4.7679 426.3140 431.0819 401.8255 65.0138 -4.7707 426.2337 431.0044 401.6637 66.6234 -4.7696 426.1629 430.9325 401.4690 68.2275 -4.7694 426.0946 430.8640 401.2788 69.8473 -4.7706 426.0145 430.7852 401.0623 71.4563 -4.7714 425.9397 430.7111 400.8727 73.0604 -4.7678 425.8545 430.6223 400.6709 74.6646 -4.7688 425.7563 430.5251 400.4799 76.2635 -4.7688 425.6729 430.4418 400.2924 77.8680 -4.7660 425.5920 430.3580 400.0911 79.4771 -4.7637 425.5101 430.2738 399.9025 81.0970 -4.7591 425.4402 430.1993 399.7195 82.6956 -4.7586 425.3476 430.1062 399.5321 84.3053 -4.7601 425.2438 430.0039 399.3453 85.9093 -4.7593 425.1586 429.9179 399.1705 87.5186 -4.7598 425.0824 429.8422 398.9805 89.1229 -4.7593 424.9992 429.7585 398.7772 90.7218 -4.7557 424.9169 429.6726 398.5975 92.3414 -4.7514 424.8178 429.5692 398.3968 93.9454 -4.7503 424.7372 429.4875 398.2265 95.5496 -4.7502 424.6335 429.3837 398.0492 97.1539 -4.7478 424.5401 429.2879 397.8734 98.7581 -4.7474 424.4523 429.1997 397.6798 100.3624 -4.7459 424.3597 429.1056 397.4834 101.9666 -4.7479 424.2446 428.9924 397.3163 103.5863 -4.7458 424.1344 428.8803 397.1363 105.1951 -4.7419 424.0213 428.7632 396.9475 106.7996 -4.7389 423.9168 428.6557 396.7568 108.4036 -4.7387 423.7959 428.5346 396.5419 110.0079 -4.7365 423.6973 428.4338 396.3436 111.6070 -4.7365 423.5903 428.3267 396.1372 113.2160 -4.7352 423.4983 428.2334 395.9390 114.8051 -4.7321 423.3971 428.1293 395.7138 116.4193 -4.7272 423.2938 428.0210 395.5014 118.0286 -4.7264 423.1727 427.8991 395.3228 119.6329 -4.7238 423.0972 427.8210 395.1314 121.2419 -4.7212 422.9801 427.7013 394.9559 122.8464 -4.7163 422.8885 427.6048 394.7778 124.4451 -4.7172 422.7904 427.5076 394.5964 126.0546 -4.7141 422.6761 427.3902 394.3862 127.6690 -4.7122 422.5286 427.2408 394.1931 129.2785 -4.7101 422.4109 427.1210 394.0275 130.8775 -4.7089 422.2739 426.9828 393.8165 132.4714 -4.7037 422.1595 426.8631 393.6155 134.0809 -4.6984 422.0320 426.7304 393.4103 135.6848 -4.6968 421.9262 426.6229 393.2450 137.2943 -4.6933 421.8058 426.4991 393.0683 138.8931 -4.6889 421.6854 426.3742 392.8778 140.5128 -4.6860 421.5521 426.2381 392.6932 142.1068 -4.6833 421.4432 426.1265 392.5041 143.7108 -4.6818 421.3304 426.0122 392.3082 145.3204 -4.6788 421.2089 425.8877 392.1279 146.9190 -4.6754 421.0710 425.7464 391.9554 148.5236 -4.6745 420.9395 425.6140 391.7896 150.1275 -4.6750 420.7950 425.4700 391.6000 151.7320 -4.6729 420.6593 425.3321 391.4116 153.3514 -4.6701 420.5421 425.2122 391.2286 154.9555 -4.6695 420.4194 425.0889 391.0402 156.5599 -4.6677 420.2857 424.9534 390.8588 158.1689 -4.6653 420.1608 424.8261 390.6515 159.7733 -4.6614 420.0246 424.6861 390.4423 161.3721 -4.6591 419.8934 424.5525 390.2519 162.9815 -4.6538 419.7585 424.4124 390.0504 164.5858 -4.6487 419.6192 424.2679 389.8631 166.1899 -4.6446 419.4835 424.1281 389.6754 167.7943 -4.6415 419.3850 424.0265 389.5160 169.3983 -4.6382 419.2546 423.8928 389.3272 171.0028 -4.6376 419.0857 423.7233 389.1026 172.6065 -4.6383 418.9315 423.5698 388.9114 174.2161 -4.6371 418.7951 423.4322 388.7248 175.8201 -4.6319 418.6363 423.2682 388.5513 177.4396 -4.6275 418.4887 423.1161 388.3629 179.0440 -4.6249 418.3344 422.9593 388.1674 180.6479 -4.6196 418.2039 422.8235 387.9738 182.2575 -4.6155 418.0888 422.7043 387.7829 183.8614 -4.6157 417.9328 422.5484 387.6205 185.4656 -4.6143 417.7963 422.4105 387.4389 187.0750 -4.6134 417.6615 422.2748 387.2528 188.6943 -4.6129 417.5164 422.1293 387.0781 190.2985 -4.6089 417.3618 421.9707 386.8866 191.9026 -4.6060 417.2244 421.8304 386.6984 193.5019 -4.6017 417.0609 421.6626 386.5128 195.1111 -4.6009 416.9122 421.5130 386.3067 196.7153 -4.5951 416.7895 421.3846 386.0983 198.3248 -4.5911 416.6499 421.2409 385.9019 199.9133 -4.5890 416.4912 421.0802 385.6913 201.5281 -4.5828 416.3316 420.9144 385.4862 203.1370 -4.5801 416.1618 420.7420 385.2616 204.7414 -4.5795 416.0376 420.6171 385.0756 206.3455 -4.5735 415.8744 420.4480 384.8622 207.9494 -4.5704 415.7306 420.3009 384.6571 209.5539 -4.5661 415.6058 420.1720 384.4660 211.1629 -4.5626 415.4488 420.0114 384.2693 212.7774 -4.5575 415.2757 419.8332 384.0858 214.3611 -4.5539 415.1405 419.6943 383.8747 215.9754 -4.5513 414.9940 419.5454 383.6528 217.5850 -4.5486 414.8256 419.3743 383.4540 219.1888 -4.5478 414.6536 419.2014 383.2639 220.7880 -4.5471 414.5048 419.0519 383.0953 222.3973 -4.5433 414.3567 418.9000 382.8798 223.9965 -4.5373 414.1942 418.7315 382.6885 225.6058 -4.5336 414.0192 418.5528 382.4598 227.2099 -4.5303 413.8694 418.3997 382.2653 228.8143 -4.5264 413.7198 418.2462 382.0639 230.4233 -4.5262 413.5667 418.0929 381.8719 232.0278 -4.5217 413.4327 417.9544 381.6882 233.6316 -4.5191 413.2798 417.7988 381.5180 235.2306 -4.5171 413.1150 417.6321 381.3169 236.8350 -4.5128 412.9443 417.4571 381.1498 238.4441 -4.5036 412.7767 417.2803 380.9809 240.0589 -4.4969 412.6018 417.0986 380.7835 241.6628 -4.4918 412.4433 416.9351 380.5948 243.2725 -4.4917 412.2697 416.7614 380.4354 244.8711 -4.4885 412.0953 416.5838 380.2284 246.4808 -4.4827 411.9430 416.4256 380.0265 248.0848 -4.4803 411.7918 416.2721 379.8388 249.6735 -4.4769 411.6298 416.1067 379.6748 251.2779 -4.4706 411.4651 415.9356 379.5034 252.8970 -4.4679 411.2831 415.7510 379.3214 254.5016 -4.4655 411.1058 415.5714 379.1248 256.1055 -4.4620 410.9557 415.4177 378.9149 257.7099 -4.4626 410.7945 415.2571 378.7144 259.3191 -4.4584 410.6313 415.0897 378.5073 260.9230 -4.4515 410.4623 414.9138 378.3008 262.5225 -4.4448 410.3113 414.7561 378.1008 264.1468 -4.4429 410.1522 414.5951 377.9138 265.7514 -4.4393 409.9973 414.4366 377.7325 267.3553 -4.4362 409.8414 414.2776 377.5671 268.9596 -4.4296 409.6648 414.0944 377.3632 270.5433 -4.4242 409.4930 413.9172 377.1692 272.1679 -4.4240 409.3244 413.7484 376.9793 273.7723 -4.4220 409.1473 413.5693 376.7705 275.3658 -4.4187 408.9913 413.4100 376.5719 276.9858 -4.4141 408.8289 413.2430 376.3907 278.5896 -4.4105 408.6933 413.1038 376.1983 280.1991 -4.4042 408.5249 412.9292 376.0077 281.8033 -4.4008 408.3335 412.7343 375.8004 283.4124 -4.3979 408.1835 412.5815 375.6012 285.0169 -4.3944 407.9969 412.3913 375.4139 286.6258 -4.3890 407.8047 412.1938 375.2326 288.2404 -4.3857 407.6223 412.0080 375.0650 289.8445 -4.3828 407.4486 411.8314 374.8725 291.4538 -4.3766 407.2800 411.6566 374.6804 293.0581 -4.3708 407.0894 411.4602 374.5189 294.6570 -4.3685 406.9218 411.2903 374.3296 296.2615 -4.3652 406.7417 411.1069 374.1179 297.8655 -4.3606 406.5865 410.9471 373.9254 299.4905 -4.3556 406.4386 410.7943 373.7280 301.0943 -4.3503 406.2616 410.6120 373.5232 302.6936 -4.3447 406.1005 410.4452 373.3192 304.3028 -4.3408 405.9359 410.2767 373.1187 305.8915 -4.3343 405.7589 410.0932 372.9156 307.5010 -4.3311 405.5758 409.9069 372.7002 309.0998 -4.3294 405.3815 409.7109 372.5059 310.7043 -4.3248 405.1937 409.5185 372.3112 312.3235 -4.3206 405.0383 409.3589 372.0898 313.9281 -4.3141 404.8631 409.1772 371.8988 315.5269 -4.3085 404.6869 408.9955 371.7120 317.1366 -4.3059 404.4891 408.7949 371.5120 318.7405 -4.3008 404.3288 408.6296 371.3268 320.3499 -4.2968 404.1739 408.4707 371.1283 321.9490 -4.2932 403.9928 408.2861 370.9262 323.5684 -4.2904 403.8155 408.1060 370.7471 325.1626 -4.2837 403.6359 407.9196 370.5611 326.7614 -4.2826 403.4636 407.7463 370.3629 328.3608 -4.2816 403.2758 407.5574 370.1872 329.9698 -4.2791 403.1037 407.3829 370.0136 331.5741 -4.2714 402.9066 407.1781 369.8144 333.1834 -4.2655 402.7206 406.9862 369.6088 334.7874 -4.2638 402.5611 406.8249 369.4028 336.3918 -4.2593 402.3728 406.6320 369.2267 337.9956 -4.2547 402.1921 406.4468 369.0307 339.6003 -4.2482 402.0289 406.2771 368.8607 341.1990 -4.2432 401.8625 406.1056 368.6934 342.8085 -4.2372 401.6669 405.9041 368.5174 344.4075 -4.2312 401.4833 405.7145 368.3185 346.0168 -4.2265 401.2860 405.5124 368.1144 347.6210 -4.2252 401.1124 405.3376 367.9261 349.2198 -4.2187 400.9625 405.1812 367.7209 350.8398 -4.2123 400.7837 404.9961 367.5025 352.4385 -4.2085 400.5983 404.8068 367.3028 354.0479 -4.2066 400.4100 404.6166 367.0842 355.6521 -4.2034 400.2436 404.4470 366.8818 357.2560 -4.2001 400.0721 404.2722 366.6835 358.8606 -4.1964 399.9046 404.1010 366.4936 360.4644 -4.1900 399.7122 403.9022 366.2627 362.0841 -4.1846 399.5181 403.7027 366.0577 363.6883 -4.1819 399.3159 403.4978 365.8583 365.2769 -4.1768 399.1517 403.3285 365.6640 366.8864 -4.1729 398.9807 403.1536 365.4402 368.4903 -4.1669 398.8115 402.9784 365.2414 370.0995 -4.1619 398.6375 402.7994 365.0314 371.6988 -4.1589 398.4582 402.6172 364.8238 373.3028 -4.1556 398.2719 402.4275 364.6292 374.9224 -4.1490 398.0666 402.2156 364.4292 376.5264 -4.1438 397.8807 402.0244 364.2311 378.1309 -4.1367 397.6767 401.8134 364.0231 379.7349 -4.1337 397.5208 401.6545 363.8462 381.3341 -4.1311 397.3494 401.4806 363.6484 382.9434 -4.1261 397.1687 401.2948 363.4334 384.5474 -4.1226 397.0036 401.1262 363.2154 386.1670 -4.1196 396.8374 400.9570 363.0246 387.7761 -4.1140 396.6465 400.7606 362.8442 389.3805 -4.1086 396.4416 400.5502 362.6347 390.9846 -4.1075 396.2468 400.3542 362.4140 392.5888 -4.1029 396.0741 400.1771 362.2115 394.1931 -4.0970 395.8872 399.9842 362.0031 395.7969 -4.0905 395.6876 399.7781 361.7966 397.4166 -4.0876 395.5050 399.5926 361.6054 399.0156 -4.0824 395.2964 399.3788 361.4259 400.6253 -4.0779 395.1208 399.1987 361.2674 402.2293 -4.0714 394.9478 399.0192 361.0900 403.8386 -4.0660 394.7453 398.8114 360.9050 405.4429 -4.0627 394.5706 398.6333 360.7276 407.0418 -4.0586 394.3902 398.4487 360.5398 408.6668 -4.0533 394.2076 398.2609 360.3534 410.2551 -4.0473 394.0217 398.0689 360.1746 411.8598 -4.0432 393.8255 397.8687 359.9585 413.4585 -4.0408 393.6384 397.6792 359.7678 415.0629 -4.0415 393.4558 397.4973 359.5646 416.6721 -4.0389 393.2777 397.3166 359.3544 418.2760 -4.0307 393.0919 397.1226 359.1694 419.8856 -4.0265 392.9292 396.9556 358.9754 421.4998 -4.0208 392.7430 396.7637 358.7673 423.1041 -4.0141 392.5618 396.5759 358.5788 424.7083 -4.0059 392.3584 396.3643 358.3899 426.3124 -4.0005 392.1689 396.1694 358.2071 427.9014 -3.9943 391.9680 395.9622 357.9830 429.5104 -3.9921 391.7914 395.7834 357.7608 431.1099 -3.9855 391.5896 395.5751 357.5482 432.7188 -3.9833 391.4157 395.3990 357.3675 434.3385 -3.9785 391.2275 395.2060 357.1490 435.9375 -3.9742 391.0357 395.0100 356.9369 437.5469 -3.9647 390.8403 394.8051 356.7573 439.1511 -3.9609 390.6418 394.6027 356.5498 440.7498 -3.9563 390.4767 394.4330 356.3526 442.3594 -3.9523 390.3052 394.2575 356.1549 443.9634 -3.9496 390.1076 394.0572 355.9754 445.5830 -3.9490 389.9013 393.8502 355.7764 447.1719 -3.9436 389.7305 393.6740 355.5994 448.7759 -3.9403 389.5379 393.4782 355.3849 450.3854 -3.9332 389.3489 393.2821 355.1870 451.9893 -3.9299 389.1541 393.0841 355.0177 453.5935 -3.9252 388.9647 392.8899 354.8300 455.1978 -3.9184 388.7604 392.6788 354.6609 456.7965 -3.9127 388.5816 392.4943 354.4829 458.4213 -3.9117 388.3965 392.3081 354.2823 460.0254 -3.9036 388.1994 392.1030 354.0870 461.6243 -3.8963 388.0128 391.9091 353.9083 463.2339 -3.8888 387.7960 391.6848 353.6997 464.8376 -3.8867 387.6050 391.4916 353.4795 466.4423 -3.8823 387.4355 391.3178 353.2922 468.0308 -3.8818 387.2594 391.1413 353.0926 469.6608 -3.8775 387.0901 390.9676 352.9071 471.2546 -3.8717 386.8981 390.7698 352.7311 472.8588 -3.8663 386.6908 390.5571 352.5244 474.4631 -3.8650 386.4871 390.3522 352.3278 476.0670 -3.8554 386.3075 390.1629 352.0967 477.6715 -3.8507 386.1261 389.9767 351.9013 479.2805 -3.8482 385.9367 389.7849 351.6943 480.8796 -3.8428 385.7499 389.5927 351.4597 482.4993 -3.8397 385.5331 389.3728 351.2614 484.1083 -3.8359 385.3568 389.1926 351.0710 485.7126 -3.8296 385.1737 389.0033 350.8508 487.3218 -3.8255 384.9810 388.8065 350.6440 488.9261 -3.8207 384.7860 388.6067 350.4352 490.5251 -3.8165 384.6191 388.4355 350.2509 492.1343 -3.8085 384.4442 388.2527 350.0791 493.7490 -3.8054 384.2593 388.0647 349.8613 495.3579 -3.8008 384.0631 387.8639 349.6446 496.9573 -3.7961 383.8448 387.6408 349.4550 498.5459 -3.7910 383.6476 387.4386 349.2689 500.1554 -3.7848 383.4533 387.2382 349.0916 501.7595 -3.7784 383.2614 387.0399 348.8837 503.3686 -3.7755 383.0761 386.8516 348.6615 504.9731 -3.7718 382.8919 386.6638 348.4718 506.5874 -3.7666 382.7067 386.4732 348.2700 508.1968 -3.7597 382.5212 386.2809 348.0567 509.8008 -3.7536 382.3549 386.1084 347.8438 511.3998 -3.7513 382.1664 385.9177 347.6524 513.0041 -3.7494 381.9534 385.7028 347.4749 514.6079 -3.7434 381.7651 385.5085 347.2963 516.2175 -3.7351 381.5916 385.3267 347.1053 517.8369 -3.7304 381.3873 385.1177 346.9301 519.4413 -3.7294 381.1774 384.9068 346.7699 521.0505 -3.7265 380.9870 384.7135 346.5769 522.6545 -3.7201 380.7898 384.5099 346.3616 524.2641 -3.7137 380.6150 384.3287 346.1514 525.8628 -3.7108 380.4120 384.1228 345.9703 527.4619 -3.7061 380.2237 383.9297 345.7910 529.0866 -3.6946 380.0478 383.7424 345.5818 530.6856 -3.6885 379.8909 383.5794 345.4105 532.2899 -3.6855 379.6967 383.3822 345.1886 533.8938 -3.6814 379.5032 383.1846 344.9738 535.4981 -3.6780 379.3033 382.9813 344.7879 537.1074 -3.6746 379.0780 382.7527 344.5836 538.7113 -3.6685 378.8670 382.5355 344.3934 540.3259 -3.6665 378.6766 382.3431 344.1874 541.9350 -3.6627 378.4767 382.1394 343.9868 543.5393 -3.6602 378.2868 381.9470 343.7827 545.1435 -3.6575 378.0944 381.7519 343.5820 546.7474 -3.6526 377.9106 381.5633 343.3907 548.3519 -3.6466 377.7268 381.3734 343.2035 549.9558 -3.6436 377.5237 381.1673 342.9960 551.5755 -3.6368 377.3325 380.9694 342.8011 553.1796 -3.6336 377.1347 380.7683 342.5874 554.7840 -3.6300 376.9522 380.5821 342.3814 556.3881 -3.6235 376.7688 380.3923 342.1769 557.9924 -3.6175 376.5708 380.1882 341.9746 559.5966 -3.6110 376.3720 379.9830 341.7748 561.2009 -3.6050 376.1798 379.7848 341.5583 562.8205 -3.6004 375.9847 379.5852 341.3447 564.4194 -3.5971 375.8130 379.4101 341.1430 566.0239 -3.5901 375.6176 379.2077 340.9724 567.6328 -3.5838 375.4410 379.0249 340.7839 569.2370 -3.5792 375.2542 378.8334 340.6010 570.8464 -3.5755 375.0670 378.6425 340.4147 572.4505 -3.5713 374.8947 378.4660 340.2145 574.0549 -3.5663 374.6846 378.2509 340.0314 575.6638 -3.5623 374.4860 378.0484 339.8387 577.2785 -3.5596 374.2762 377.8358 339.6413 578.8723 -3.5557 374.0867 377.6423 339.4672 580.4715 -3.5523 373.9178 377.4701 339.3009 582.0756 -3.5490 373.7205 377.2695 339.0878 583.6850 -3.5456 373.5065 377.0521 338.8714 585.2841 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