DTA measure 1updown3 Date: 2025924:91 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.53 s Mass = 1115.700 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3343 -0.5837 233.4944 234.0781 271.7283 2.1618 -0.5804 233.7715 234.3519 271.6415 2.9175 -0.5785 234.0059 234.5844 271.6089 3.7855 -0.5802 234.2727 234.8529 271.5821 4.5415 -0.5835 234.5100 235.0935 271.5771 5.3688 -0.5890 234.7818 235.3709 271.5899 6.1655 -0.5897 235.0297 235.6194 271.6066 6.9623 -0.5821 235.2797 235.8619 271.7267 7.7893 -0.5789 235.5641 236.1430 271.8602 8.5453 -0.5693 235.7760 236.3453 272.0276 9.4135 -0.5617 236.0684 236.6300 272.1957 10.1795 -0.5580 236.3475 236.9055 272.4478 11.0070 -0.5537 236.5884 237.1422 272.7321 11.7930 -0.5566 236.8199 237.3765 273.0346 12.6000 -0.5596 237.0625 237.6221 273.3725 13.4173 -0.5599 237.3273 237.8871 273.7262 14.1828 -0.5606 237.6008 238.1614 274.0942 15.0413 -0.5600 237.8600 238.4200 274.5184 15.8070 -0.5638 238.1054 238.6692 274.9133 16.6343 -0.5637 238.3422 238.9060 275.3486 17.4003 -0.5646 238.6041 239.1687 275.7466 18.2275 -0.5674 238.8731 239.4405 276.1573 19.0243 -0.5707 239.1416 239.7124 276.5437 19.8210 -0.5716 239.3986 239.9702 276.9147 20.6378 -0.5756 239.6461 240.2217 277.2735 21.4143 -0.5780 239.8811 240.4591 277.5746 22.2620 -0.5814 240.0996 240.6810 277.8456 23.0278 -0.5855 240.3314 240.9169 278.0947 23.8555 -0.5896 240.5284 241.1180 278.3659 24.6518 -0.5952 240.7610 241.3562 278.5953 25.4383 -0.6013 241.0140 241.6153 278.7622 26.2658 -0.6078 241.2803 241.8882 278.9019 27.0313 -0.6111 241.5145 242.1256 279.0042 27.8898 -0.6125 241.7764 242.3888 279.1203 28.6453 -0.6138 241.9743 242.5880 279.1735 29.4723 -0.6126 242.2338 242.8464 279.1708 30.2693 -0.6017 242.4524 243.0541 279.1652 31.0555 -0.5921 242.7168 243.3089 279.1433 31.8930 -0.5947 242.9778 243.5725 279.1168 32.6488 -0.5998 243.1893 243.7891 279.0762 33.5068 -0.6076 243.4367 244.0443 279.0042 34.2725 -0.6118 243.6591 244.2708 278.9291 35.1000 -0.6165 243.9126 244.5291 278.8338 35.8965 -0.6213 244.1613 244.7826 278.7343 36.6828 -0.6225 244.3909 245.0134 278.6181 37.5205 -0.6225 244.6647 245.2873 278.4990 38.2760 -0.6240 244.8985 245.5225 278.4277 39.1340 -0.6225 245.1641 245.7866 278.3303 39.9003 -0.6172 245.3548 245.9720 278.2844 40.7375 -0.6208 245.5849 246.2057 278.2184 41.4930 -0.6217 245.7992 246.4209 278.1673 42.3205 -0.6269 246.0305 246.6575 278.1619 43.1478 -0.6310 246.2694 246.9004 278.1507 43.9138 -0.6305 246.4987 247.1292 278.1632 44.7720 -0.6263 246.7514 247.3777 278.2571 45.5070 -0.6305 246.9418 247.5723 278.3430 46.3653 -0.6318 247.1852 247.8169 278.5069 47.1310 -0.6310 247.4051 248.0361 278.6434 47.9585 -0.6377 247.6429 248.2807 278.8174 48.7553 -0.6418 247.8384 248.4801 279.0291 49.5515 -0.6439 248.0403 248.6842 279.2966 50.3790 -0.6461 248.2617 248.9078 279.5880 51.1450 -0.6477 248.4507 249.0984 279.8509 51.9928 -0.6524 248.6910 249.3435 280.1798 52.7690 -0.6590 248.9201 249.5791 280.5306 53.5860 -0.6618 249.1734 249.8352 280.9287 54.3930 -0.6683 249.3854 250.0538 281.3287 55.1795 -0.6740 249.5911 250.2650 281.6806 56.0170 -0.6786 249.8236 250.5021 282.0371 56.7728 -0.6813 250.0170 250.6983 282.3592 57.6205 -0.6846 250.2510 250.9356 282.7349 58.3965 -0.6865 250.4817 251.1682 283.0695 59.2140 -0.6902 250.7053 251.3955 283.4032 60.0000 -0.6942 250.9206 251.6148 283.7201 60.8070 -0.6971 251.1472 251.8444 284.0093 61.6243 -0.6982 251.3117 252.0100 284.2552 62.3900 -0.6997 251.5241 252.2239 284.4949 63.2483 -0.7093 251.7574 252.4668 284.6806 64.0140 -0.7143 252.0023 252.7166 284.8377 64.8413 -0.7210 252.2637 252.9846 284.9765 65.6278 -0.7231 252.4931 253.2162 285.0721 66.4345 -0.7189 252.7038 253.4227 285.1788 67.2515 -0.7284 252.9262 253.6546 285.2704 68.0175 -0.7370 253.1122 253.8492 285.2935 68.8755 -0.7431 253.3544 254.0975 285.3191 69.6415 -0.7464 253.5394 254.2859 285.3279 70.4690 -0.7497 253.7167 254.4664 285.3244 71.2550 -0.7504 253.9367 254.6871 285.2766 72.0623 -0.7567 254.1720 254.9286 285.2269 72.8793 -0.7589 254.3881 255.1470 285.1750 73.6453 -0.7633 254.5848 255.3481 285.1099 74.5035 -0.7647 254.8461 255.6108 285.0160 75.2793 -0.7706 255.0547 255.8252 284.9500 76.0965 -0.7739 255.2705 256.0444 284.8994 76.8933 -0.7783 255.4949 256.2732 284.8480 77.6898 -0.7818 255.7012 256.4830 284.8169 78.5173 -0.7851 255.9306 256.7158 284.7820 79.2830 -0.7895 256.1187 256.9082 284.7701 80.1000 -0.7892 256.3237 257.1129 284.7738 80.8765 -0.7981 256.5287 257.3268 284.7901 81.7343 -0.8034 256.7635 257.5669 284.8279 82.5003 -0.8067 256.9264 257.7331 284.8823 83.3175 -0.8034 257.1375 257.9409 284.9515 84.1243 -0.8009 257.3215 258.1224 285.0447 84.9108 -0.7948 257.5050 258.2998 285.1656 85.7380 -0.7958 257.7213 258.5171 285.3129 86.5040 -0.7949 257.9167 258.7116 285.4950 87.3623 -0.7972 258.1402 258.9374 285.7237 88.1278 -0.8003 258.3440 259.1443 285.9583 88.9450 -0.8020 258.5445 259.3465 286.1868 89.7418 -0.8064 258.7463 259.5527 286.4665 90.5383 -0.8086 258.9581 259.7667 286.7707 91.3555 -0.8138 259.1835 259.9973 287.0752 92.1315 -0.8202 259.3895 260.2098 287.3806 92.9793 -0.8248 259.5886 260.4134 287.7385 93.7148 -0.8314 259.7743 260.6057 288.0391 94.5725 -0.8393 259.9915 260.8308 288.3691 95.3385 -0.8440 260.1818 261.0258 288.6545 96.1558 -0.8494 260.3886 261.2380 288.9643 96.9520 -0.8583 260.5585 261.4168 289.2912 97.7488 -0.8680 260.7582 261.6262 289.5810 98.5763 -0.8741 260.9589 261.8330 289.8658 99.3318 -0.8756 261.1596 262.0352 290.1150 100.2005 -0.8798 261.3983 262.2782 290.3646 100.9558 -0.8860 261.6094 262.4954 290.5657 101.7835 -0.8973 261.8266 262.7239 290.7625 102.5493 -0.9007 262.0093 262.9100 290.9321 103.3868 -0.9017 262.2047 263.1064 291.0974 104.1733 -0.9013 262.4067 263.3079 291.2216 104.9698 -0.9061 262.5995 263.5056 291.3158 105.7868 -0.9081 262.7958 263.7039 291.3988 106.5733 -0.9140 262.9923 263.9063 291.4365 107.4108 -0.9205 263.1890 264.1096 291.4779 108.1663 -0.9249 263.3658 264.2907 291.5057 109.0348 -0.9244 263.5612 264.4856 291.4751 109.7903 -0.9307 263.7373 264.6680 291.4682 110.6280 -0.9365 263.9525 264.8890 291.4575 111.3835 -0.9377 264.1695 265.1072 291.4428 112.2210 -0.9392 264.3842 265.3234 291.4282 113.0073 -0.9437 264.5661 265.5097 291.3975 113.8143 -0.9521 264.7319 265.6840 291.3502 114.6313 -0.9529 264.9213 265.8742 291.3061 115.4075 -0.9536 265.1196 266.0732 291.3117 116.2555 -0.9513 265.3144 266.2657 291.2692 117.0313 -0.9519 265.5136 266.4655 291.2643 117.8485 -0.9502 265.6815 266.6316 291.2428 118.6453 -0.9532 265.8464 266.7995 291.2646 119.4418 -0.9564 266.0204 266.9767 291.2510 120.2690 -0.9551 266.1888 267.1439 291.3088 121.0350 -0.9637 266.3657 267.3294 291.3698 121.8520 -0.9674 266.5906 267.5580 291.4897 122.6180 -0.9716 266.7802 267.7518 291.6252 123.4760 -0.9751 267.0093 267.9845 291.7637 124.2318 -0.9756 267.1954 268.1709 291.9061 125.0695 -0.9683 267.3852 268.3534 292.0925 125.8353 -0.9731 267.5589 268.5320 292.2782 126.6628 -0.9760 267.7095 268.6855 292.5211 127.4490 -0.9785 267.8978 268.8763 292.7431 128.2558 -0.9830 268.1020 269.0850 292.9933 129.0733 -0.9850 268.3035 269.2885 293.2679 129.8285 -0.9886 268.4566 269.4452 293.5635 130.6970 -0.9943 268.6492 269.6435 293.9028 131.4528 -0.9984 268.8435 269.8419 294.1898 132.2800 -1.0018 269.0496 270.0514 294.4768 133.0768 -1.0059 269.2374 270.2433 294.7346 133.8733 -1.0135 269.4441 270.4576 295.0212 134.7008 -1.0221 269.6221 270.6442 295.3286 135.4565 -1.0327 269.7981 270.8308 295.5567 136.3245 -1.0415 270.0153 271.0568 295.8638 137.0805 -1.0480 270.2232 271.2712 296.1337 137.9180 -1.0513 270.4453 271.4967 296.4042 138.7043 -1.0577 270.6424 271.7001 296.6221 139.5113 -1.0619 270.8559 271.9179 296.8384 140.3283 -1.0684 271.0232 272.0916 297.0154 141.0940 -1.0747 271.2047 272.2794 297.1754 141.9523 -1.0801 271.4253 272.5054 297.3279 142.7180 -1.0832 271.5960 272.6792 297.4236 143.5455 -1.0863 271.7860 272.8723 297.4864 144.3423 -1.0901 271.9624 273.0525 297.5608 145.1388 -1.0928 272.1275 273.2202 297.6083 145.9665 -1.0963 272.3262 273.4225 297.6680 146.7320 -1.1053 272.4617 273.5671 297.6695 147.5490 -1.1161 272.6412 273.7574 297.6693 148.3255 -1.1191 272.7958 273.9149 297.6913 149.1730 -1.1211 272.9734 274.0945 297.7067 149.9495 -1.1183 273.1926 274.3110 297.7171 150.7665 -1.1168 273.3635 274.4804 297.6577 151.5733 -1.1214 273.5451 274.6665 297.6470 152.3598 -1.1244 273.7339 274.8583 297.6433 153.1768 -1.1270 273.9139 275.0409 297.6281 153.9530 -1.1325 274.0757 275.2082 297.5963 154.8010 -1.1400 274.2454 275.3854 297.5933 155.5665 -1.1441 274.3741 275.5182 297.6279 156.3943 -1.1426 274.5636 275.7062 297.6714 157.1805 -1.1292 274.7574 275.8867 297.7181 157.9770 -1.1175 274.9230 276.0405 297.7582 158.8043 -1.1145 275.1167 276.2312 297.8109 159.5600 -1.1119 275.2802 276.3920 297.8963 160.4178 -1.1204 275.5021 276.6225 298.0294 161.1838 -1.1273 275.6664 276.7937 298.1665 162.0113 -1.1381 275.8478 276.9859 298.3240 162.8078 -1.1458 276.0204 277.1662 298.4771 163.5943 -1.1528 276.1781 277.3310 298.6458 164.4318 -1.1581 276.3530 277.5111 298.8477 165.1875 -1.1638 276.5269 277.6907 299.0526 166.0458 -1.1677 276.7019 277.8696 299.3014 166.8113 -1.1730 276.8661 278.0391 299.5156 167.6490 -1.1716 277.0490 278.2206 299.8187 168.4150 -1.1711 277.2076 278.3788 300.0990 169.2420 -1.1805 277.3974 278.5779 300.4111 170.0285 -1.1808 277.5476 278.7284 300.7008 170.8355 -1.1826 277.7411 278.9237 300.9788 171.6833 -1.1892 277.9334 279.1225 301.2757 172.4493 -1.1876 278.1104 279.2980 301.5388 173.2765 -1.1961 278.2940 279.4901 301.7897 174.0833 -1.2080 278.4797 279.6876 302.0644 174.8700 -1.2151 278.6390 279.8541 302.3186 175.6970 -1.2200 278.8279 280.0478 302.5689 176.4630 -1.2246 279.0058 280.2303 302.7932 177.3213 -1.2362 279.1538 280.3899 303.0198 178.0870 -1.2466 279.2696 280.5162 303.1505 178.9043 -1.2535 279.4381 280.6915 303.2873 179.7110 -1.2588 279.5999 280.8587 303.4419 180.4975 -1.2645 279.7734 281.0379 303.5824 181.3250 -1.2688 279.9563 281.2251 303.6868 182.0908 -1.2667 280.1045 281.3712 303.7756 182.9490 -1.2742 280.3108 281.5850 303.8348 183.7148 -1.2789 280.4817 281.7606 303.8590 184.5318 -1.2839 280.6376 281.9215 303.8697 185.3288 -1.2889 280.8068 282.0957 303.8331 186.1250 -1.2942 280.9688 282.2630 303.8462 186.9423 -1.2962 281.1422 282.4384 303.8618 187.7083 -1.2995 281.3401 282.6396 303.8678 188.5660 -1.3029 281.5306 282.8336 303.8615 189.3218 -1.3084 281.6817 282.9901 303.8565 190.1493 -1.3147 281.9127 283.2274 303.8763 190.9455 -1.3158 282.0768 283.3926 303.8788 191.7320 -1.3178 282.2617 283.5794 303.9241 192.5390 -1.3199 282.4406 283.7605 303.9475 193.3253 -1.3218 282.5833 283.9051 303.9642 194.1528 -1.3216 282.7393 284.0608 303.9984 194.9185 -1.3265 282.8991 284.2255 304.0157 195.7765 -1.3259 283.0993 284.4252 304.0426 196.5428 -1.3262 283.2651 284.5913 304.1404 197.3595 -1.3267 283.4418 284.7685 304.2460 198.1668 -1.3266 283.6259 284.9525 304.3355 198.9633 -1.3256 283.8386 285.1642 304.4678 199.7905 -1.3293 283.9750 285.3042 304.6497 200.5463 -1.3305 284.0952 285.4257 304.7929 201.4145 -1.3373 284.2651 285.6023 305.0054 202.1395 -1.3393 284.4311 285.7703 305.1940 203.0080 -1.3426 284.6215 285.9642 305.4083 203.7633 -1.3485 284.7932 286.1417 305.6401 204.6010 -1.3538 284.9540 286.3078 305.9118 205.3875 -1.3560 285.1183 286.4743 306.1678 206.1838 -1.3568 285.2772 286.6340 306.4218 207.0115 -1.3597 285.4891 286.8488 306.6863 207.7875 -1.3591 285.6740 287.0331 306.9478 208.6353 -1.3633 285.8524 287.2157 307.2450 209.3705 -1.3702 286.0333 287.4035 307.4935 210.2285 -1.3632 286.2033 287.5664 307.7491 211.0045 -1.3700 286.3576 287.7276 307.9768 211.8218 -1.3811 286.5483 287.9294 308.2512 212.6183 -1.3879 286.6888 288.0767 308.4676 213.4150 -1.3907 286.8661 288.2568 308.7037 214.2528 -1.4020 287.0435 288.4455 308.9290 215.0080 -1.4093 287.2073 288.6166 309.0770 215.8663 -1.4112 287.3580 288.7692 309.2699 216.6323 -1.4111 287.5085 288.9197 309.4238 217.4593 -1.4170 287.6827 289.0998 309.5886 218.2148 -1.4205 287.8019 289.2224 309.7208 219.0423 -1.4224 287.9376 289.3600 309.8632 219.8388 -1.4299 288.1017 289.5316 309.9527 220.6353 -1.4355 288.2610 289.6965 310.0591 221.4525 -1.4421 288.4353 289.8774 310.1128 222.2285 -1.4446 288.5774 290.0221 310.1516 223.0763 -1.4508 288.7656 290.2164 310.1770 223.8423 -1.4555 288.9330 290.3885 310.1964 224.6695 -1.4558 289.1169 290.5727 310.2308 225.4353 -1.4575 289.2794 290.7369 310.2280 226.2628 -1.4626 289.3962 290.8588 310.1921 227.0490 -1.4690 289.5662 291.0352 310.1872 227.8560 -1.4692 289.7551 291.2243 310.1854 228.6733 -1.4660 289.9075 291.3735 310.1614 229.4490 -1.4644 290.0900 291.5543 310.1383 230.2765 -1.4002 290.2752 291.6754 310.1889 231.0425 -1.3617 290.4414 291.8031 310.2177 231.9003 -1.3329 290.6512 291.9842 310.2332 232.6663 -1.3201 290.7660 292.0861 310.2639 233.4835 -1.3390 290.9116 292.2506 310.3207 234.2900 -1.3687 291.0978 292.4664 310.3666 235.0768 -1.3914 291.2628 292.6543 310.4316 235.9040 -1.4201 291.4209 292.8410 310.5559 236.6698 -1.4474 291.5659 293.0133 310.6702 237.5383 -1.4717 291.7558 293.2275 310.8235 238.2938 -1.4874 291.9153 293.4027 310.9555 239.1210 -1.4922 292.0619 293.5541 311.2018 239.9178 -1.4906 292.2418 293.7324 311.4334 240.7245 -1.4950 292.4195 293.9145 311.6563 241.5415 -1.4967 292.5879 294.0846 311.9010 242.3075 -1.5002 292.7398 294.2401 312.1423 243.1655 -1.5033 292.9104 294.4137 312.4519 243.9110 -1.5000 293.0665 294.5665 312.7150 244.7590 -1.4842 293.2212 294.7054 313.0053 245.5245 -1.4523 293.3605 294.8129 313.2744 246.3520 -1.3901 293.5054 294.8955 313.5446 247.1488 -1.3573 293.6626 295.0199 313.8426 247.9450 -1.3550 293.8268 295.1818 314.1489 248.7728 -1.3674 294.0371 295.4044 314.4369 249.5385 -1.3686 294.2108 295.5794 314.6727 250.3865 -1.3596 294.3523 295.7119 314.9276 251.1423 -1.3701 294.4602 295.8304 315.1638 251.9795 -1.3820 294.5998 295.9818 315.3806 252.7660 -1.3931 294.7435 296.1367 315.5264 253.5628 -1.4179 294.8986 296.3165 315.6713 254.3900 -1.4415 295.0298 296.4712 315.8030 255.1458 -1.4448 295.1937 296.6385 315.9138 256.0038 -1.4380 295.3629 296.8009 316.0174 256.7695 -1.4437 295.5135 296.9572 316.1119 257.5970 -1.4533 295.6783 297.1316 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