DTA measure 1Gyors Date: 2025311:114 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1011.19 s Mass = 936.100 mg data_number = 1240 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2915 -0.1093 218.8970 219.0063 261.1462 2.1445 -0.1068 219.0972 219.2039 261.1629 2.9068 -0.1016 219.2677 219.3693 261.1468 3.7273 -0.0959 219.4696 219.5655 261.1486 4.5153 -0.0928 219.6520 219.7448 261.1709 5.3030 -0.0888 219.8207 219.9095 261.1703 6.1215 -0.0856 219.9809 220.0665 261.1895 6.9093 -0.0849 220.1303 220.2152 261.2051 7.7270 -0.0760 220.3119 220.3879 261.2494 8.5153 -0.0740 220.5148 220.5888 261.2922 9.3435 -0.0691 220.6926 220.7617 261.3231 10.1130 -0.0687 220.8464 220.9151 261.3975 10.9330 -0.0644 221.0287 221.0931 261.4484 11.6928 -0.0609 221.1757 221.2366 261.5156 12.5440 -0.0602 221.3799 221.4402 261.5818 13.3340 -0.0566 221.5579 221.6145 261.6410 14.1258 -0.0527 221.7174 221.7701 261.7105 14.9483 -0.0548 221.8924 221.9471 261.7884 15.7098 -0.0532 222.0646 222.1178 261.8824 16.5620 -0.0501 222.2388 222.2889 261.9887 17.3238 -0.0471 222.3909 222.4381 262.0979 18.1458 -0.0455 222.5739 222.6193 262.2067 18.9683 -0.0423 222.7609 222.8032 262.3207 19.7858 -0.0403 222.9405 222.9808 262.4520 20.5355 -0.0394 223.0877 223.1271 262.5621 21.3880 -0.0402 223.2765 223.3168 262.7287 22.1498 -0.0357 223.4410 223.4768 262.8502 22.9718 -0.0370 223.6152 223.6523 262.9892 23.7940 -0.0369 223.7964 223.8333 263.1445 24.5555 -0.0328 223.9359 223.9687 263.2939 25.4090 -0.0332 224.1102 224.1434 263.4409 26.1708 -0.0302 224.2824 224.3126 263.5978 26.9928 -0.0297 224.4548 224.4845 263.7673 27.8150 -0.0306 224.6318 224.6624 263.9367 28.5765 -0.0290 224.8008 224.8298 264.1056 29.4293 -0.0295 224.9732 225.0027 264.2945 30.3920 -0.0285 225.1662 225.1947 264.5098 31.2138 -0.0270 225.3436 225.3707 264.7013 32.0358 -0.0239 225.5159 225.5398 264.8908 32.7975 -0.0249 225.6676 225.6925 265.0535 33.6503 -0.0249 225.8424 225.8674 265.2338 34.4125 -0.0250 226.0063 226.0313 265.4065 35.2353 -0.0255 226.1853 226.2109 265.5939 36.0535 -0.0235 226.3489 226.3724 265.7898 36.8110 -0.0239 226.5080 226.5319 265.9393 37.6595 -0.0206 226.6554 226.6760 266.1363 38.4183 -0.0235 226.8253 226.8488 266.3283 39.2380 -0.0263 227.0200 227.0463 266.5221 40.0658 -0.0231 227.2039 227.2270 266.7173 40.8340 -0.0223 227.3207 227.3429 266.8768 41.6533 -0.0265 227.5069 227.5334 267.0657 42.4423 -0.0266 227.6826 227.7091 267.2264 43.2613 -0.0273 227.8455 227.8728 267.4170 44.0530 -0.0289 227.9968 228.0257 267.5748 44.8445 -0.0276 228.1693 228.1969 267.7242 45.6670 -0.0256 228.3280 228.3536 267.9285 46.4588 -0.0232 228.4949 228.5181 268.0891 47.2808 -0.0223 228.6841 228.7065 268.2710 48.0730 -0.0216 228.8379 228.8596 268.4315 48.8645 -0.0199 228.9945 229.0145 268.6055 49.6870 -0.0174 229.1683 229.1857 268.7630 50.5040 -0.0143 229.3186 229.3329 268.9209 51.2535 -0.0161 229.4790 229.4951 269.0617 52.1058 -0.0183 229.6558 229.6741 269.2264 52.8980 -0.0181 229.8271 229.8452 269.3652 53.6895 -0.0213 229.9876 230.0089 269.5181 54.5120 -0.0242 230.1621 230.1862 269.6796 55.2735 -0.0271 230.3342 230.3612 269.8064 56.1258 -0.0274 230.4968 230.5241 269.9500 56.9178 -0.0295 230.6375 230.6670 270.0807 57.7095 -0.0306 230.7898 230.8204 270.2193 58.5315 -0.0292 230.9584 230.9876 270.3637 59.2935 -0.0282 231.1317 231.1599 270.4753 60.1455 -0.0306 231.3130 231.3437 270.6133 60.9625 -0.0332 231.4773 231.5106 270.7632 61.7245 -0.0356 231.6171 231.6526 270.8918 62.5465 -0.0361 231.8040 231.8401 271.0156 63.3385 -0.0352 231.9779 232.0131 271.1567 64.1305 -0.0335 232.1338 232.1674 271.2749 64.9825 -0.0361 232.3032 232.3393 271.3877 65.7445 -0.0365 232.4497 232.4862 271.5086 66.5665 -0.0353 232.6204 232.6557 271.6346 67.3568 -0.0343 232.7751 232.8094 271.7615 68.1453 -0.0399 232.9506 232.9905 271.8852 68.9660 -0.0416 233.1027 233.1443 271.9976 69.7558 -0.0417 233.2501 233.2918 272.1197 70.5915 -0.0436 233.4435 233.4872 272.2410 71.3740 -0.0526 233.6045 233.6571 272.3428 72.1620 -0.0495 233.7631 233.8126 272.4460 72.9500 -0.0535 233.9157 233.9692 272.5655 73.7688 -0.0545 234.0996 234.1542 272.6900 74.5580 -0.0551 234.2481 234.3032 272.7955 75.3768 -0.0568 234.3988 234.4556 272.8871 76.1668 -0.0568 234.5615 234.6184 272.9959 76.9578 -0.0601 234.7208 234.7809 273.1346 77.7795 -0.0633 234.9024 234.9656 273.2469 78.5718 -0.0643 235.0447 235.1090 273.3317 79.3935 -0.0627 235.1879 235.2506 273.4377 80.1858 -0.0628 235.3793 235.4422 273.5763 81.0760 -0.0640 235.5661 235.6302 273.6819 81.9978 -0.0666 235.7318 235.7985 273.7929 82.7608 -0.0658 235.8767 235.9425 273.9151 83.6178 -0.0689 236.0585 236.1275 274.0350 84.3795 -0.0705 236.2039 236.2744 274.1206 85.2015 -0.0692 236.3714 236.4406 274.2282 86.0235 -0.0692 236.5296 236.5988 274.3570 86.7855 -0.0708 236.6709 236.7417 274.4619 87.6375 -0.0694 236.8611 236.9305 274.5817 88.4295 -0.0719 237.0197 237.0916 274.7058 89.2215 -0.0762 237.1837 237.2599 274.8327 90.0435 -0.0754 237.3376 237.4131 274.9257 90.8055 -0.0773 237.4921 237.5694 275.0730 91.6575 -0.0791 237.6732 237.7524 275.2114 92.4195 -0.0777 237.8375 237.9152 275.3021 93.2415 -0.0769 237.9867 238.0636 275.4327 94.0635 -0.0807 238.1350 238.2156 275.5629 94.8255 -0.0824 238.2797 238.3621 275.6579 95.6775 -0.0832 238.4393 238.5225 275.7989 96.4395 -0.0855 238.6008 238.6864 275.9248 97.2613 -0.0833 238.7725 238.8557 276.0453 98.0838 -0.0842 238.9252 239.0095 276.1793 98.8458 -0.0875 239.0720 239.1596 276.2967 99.6980 -0.0886 239.2357 239.3243 276.4258 100.4595 -0.0886 239.3664 239.4550 276.5513 101.2780 -0.0883 239.5413 239.6296 276.6788 102.0688 -0.0865 239.7028 239.7892 276.7851 102.8563 -0.0885 239.8634 239.9518 276.9363 103.7053 -0.0901 240.0300 240.1201 277.0688 104.4635 -0.0909 240.1770 240.2679 277.1696 105.2820 -0.0955 240.3475 240.4429 277.3393 106.0700 -0.0988 240.4975 240.5962 277.4896 106.8590 -0.0984 240.6372 240.7356 277.5968 107.7078 -0.0981 240.8188 240.9169 277.7519 108.4683 -0.1001 240.9595 241.0596 277.8722 109.2895 -0.0982 241.1031 241.2012 278.0361 110.0805 -0.1029 241.2666 241.3696 278.2077 110.8725 -0.1058 241.4302 241.5360 278.3064 111.7803 -0.1078 241.6097 241.7175 278.4656 112.6875 -0.1092 241.7745 241.8837 278.6336 113.4795 -0.1075 241.9210 242.0286 278.7895 114.3015 -0.1090 242.0888 242.1979 278.9302 115.0935 -0.1107 242.2472 242.3578 279.0790 115.9155 -0.1131 242.4095 242.5226 279.2157 116.7075 -0.1166 242.5654 242.6820 279.3594 117.4995 -0.1199 242.7025 242.8225 279.5213 118.3215 -0.1219 242.8763 242.9982 279.6764 119.1135 -0.1273 243.0143 243.1417 279.8274 119.9350 -0.1266 243.1644 243.2910 279.9924 120.7275 -0.1278 243.3290 243.4568 280.1273 121.5188 -0.1307 243.4839 243.6146 280.2864 122.3425 -0.1316 243.6551 243.7868 280.4228 123.1063 -0.1319 243.8045 243.9364 280.5566 123.9585 -0.1365 243.9507 244.0873 280.7134 124.7510 -0.1367 244.1186 244.2553 280.8457 125.5435 -0.1374 244.2547 244.3922 280.9996 126.3663 -0.1404 244.4248 244.5651 281.1432 127.1285 -0.1420 244.5577 244.6996 281.2704 127.9810 -0.1424 244.7268 244.8692 281.3969 128.7428 -0.1435 244.8764 245.0199 281.5516 129.5648 -0.1442 245.0397 245.1839 281.6929 130.3878 -0.1468 245.1982 245.3450 281.8282 131.1495 -0.1496 245.3541 245.5037 281.9444 132.0025 -0.1468 245.5188 245.6656 282.1085 132.7620 -0.1507 245.6590 245.8097 282.2326 133.5810 -0.1551 245.8116 245.9667 282.3724 134.3993 -0.1563 245.9735 246.1298 282.5097 135.1570 -0.1570 246.1207 246.2776 282.6442 136.0053 -0.1572 246.2698 246.4270 282.7917 136.7638 -0.1586 246.3727 246.5313 282.9032 137.5840 -0.1577 246.5582 246.7159 283.0314 138.4023 -0.1598 246.7384 246.8982 283.1689 139.1600 -0.1620 246.8814 247.0434 283.2925 140.0098 -0.1644 247.0225 247.1868 283.4368 140.7988 -0.1667 247.1972 247.3639 283.5632 141.5888 -0.1628 247.3458 247.5086 283.7056 142.4968 -0.1680 247.5013 247.6693 283.8424 143.4050 -0.1719 247.6794 247.8513 283.9804 144.1965 -0.1729 247.8408 248.0137 284.0897 145.0190 -0.1725 247.9908 248.1633 284.2279 145.7808 -0.1733 248.1464 248.3197 284.3779 146.6330 -0.1753 248.3098 248.4852 284.5097 147.4253 -0.1780 248.4500 248.6280 284.6109 148.2168 -0.1795 248.6026 248.7821 284.7453 149.0393 -0.1805 248.7647 248.9452 284.8676 149.8005 -0.1861 248.9110 249.0971 285.0008 150.6530 -0.1885 249.0652 249.2536 285.1311 151.4450 -0.1870 249.2210 249.4080 285.2743 152.2365 -0.1887 249.3825 249.5712 285.3974 153.0590 -0.1910 249.5479 249.7389 285.5042 153.8205 -0.1933 249.7028 249.8961 285.6330 154.6730 -0.1945 249.8590 250.0535 285.7661 155.4650 -0.1960 250.0063 250.2023 285.9054 156.2565 -0.1985 250.1506 250.3491 286.0199 157.0790 -0.2007 250.2801 250.4807 286.1530 157.8708 -0.1980 250.4238 250.6219 286.2695 158.6935 -0.2006 250.5968 250.7974 286.3791 159.4858 -0.2001 250.7567 250.9568 286.5150 160.2775 -0.2025 250.9046 251.1070 286.6363 161.0998 -0.2081 251.0535 251.2617 286.7655 161.8915 -0.2099 251.2102 251.4200 286.8723 162.7138 -0.2128 251.3780 251.5907 287.0062 163.5055 -0.2141 251.5256 251.7397 287.1219 164.2973 -0.2132 251.6613 251.8745 287.2459 165.1440 -0.2147 251.8339 252.0486 287.3841 165.9030 -0.2159 251.9869 252.2028 287.5062 166.7210 -0.2206 252.1296 252.3502 287.6289 167.5093 -0.2201 252.2791 252.4992 287.7531 168.2970 -0.2216 252.4376 252.6592 287.8639 169.1450 -0.2224 252.5910 252.8134 287.9913 169.9033 -0.2246 252.7208 252.9454 288.0948 170.7220 -0.2268 252.8692 253.0960 288.2290 171.5405 -0.2251 253.0399 253.2649 288.3634 172.3000 -0.2281 253.1788 253.4069 288.4897 173.2418 -0.2291 253.3530 253.5821 288.6233 174.1258 -0.2315 253.5364 253.7678 288.7478 174.9205 -0.2329 253.6953 253.9282 288.8842 175.7730 -0.2343 253.8344 254.0687 289.0156 176.5345 -0.2345 253.9568 254.1913 289.1184 177.3568 -0.2365 254.1231 254.3596 289.2847 178.1490 -0.2381 254.2797 254.5178 289.4218 178.9405 -0.2373 254.4101 254.6474 289.5431 179.7930 -0.2403 254.5919 254.8322 289.6749 180.5545 -0.2409 254.7360 254.9770 289.8137 181.3768 -0.2397 254.8784 255.1181 289.9502 182.1690 -0.2402 255.0391 255.2793 290.0869 182.9605 -0.2416 255.1832 255.4248 290.2173 183.8145 -0.2446 255.3404 255.5849 290.3599 184.5765 -0.2459 255.4646 255.7105 290.5039 185.3988 -0.2489 255.6416 255.8906 290.6520 186.1908 -0.2480 255.7754 256.0234 290.7694 186.9825 -0.2507 255.9117 256.1624 290.9351 187.8348 -0.2501 256.0865 256.3365 291.0712 188.5965 -0.2564 256.2264 256.4828 291.2063 189.4185 -0.2580 256.4023 256.6603 291.3273 190.2405 -0.2616 256.5498 256.8114 291.4899 191.0025 -0.2619 256.6804 256.9423 291.6300 191.8545 -0.2646 256.8374 257.1021 291.7637 192.6165 -0.2640 256.9709 257.2349 291.8893 193.4385 -0.2641 257.1334 257.3975 292.0383 194.2605 -0.2667 257.2728 257.5395 292.1835 195.0225 -0.2694 257.4252 257.6946 292.3188 195.8745 -0.2702 257.5865 257.8567 292.4723 196.6358 -0.2712 257.7401 258.0113 292.5963 197.4545 -0.2737 257.8784 258.1522 292.7436 198.2728 -0.2731 258.0292 258.3023 292.8651 199.0310 -0.2781 258.1871 258.4653 293.0229 199.8790 -0.2797 258.3334 258.6131 293.1655 200.6370 -0.2816 258.4905 258.7721 293.2926 201.4550 -0.2828 258.6397 258.9226 293.4273 202.2733 -0.2807 258.7736 259.0543 293.5719 203.0320 -0.2866 258.9074 259.1940 293.7254 203.9693 -0.2896 259.0861 259.3757 293.8711 204.8778 -0.2922 259.2669 259.5591 294.0252 205.6395 -0.2990 259.4274 259.7264 294.1666 206.4915 -0.2994 259.5752 259.8747 294.3153 207.2535 -0.3013 259.7013 260.0026 294.4546 208.0758 -0.3018 259.8483 260.1501 294.6086 208.8678 -0.3041 259.9995 260.3036 294.7227 209.6595 -0.3088 260.1415 260.4503 294.8598 210.4815 -0.3101 260.2888 260.5989 294.9953 211.2735 -0.3133 260.4494 260.7627 295.1326 212.0958 -0.3140 260.6196 260.9336 295.2548 212.8875 -0.3139 260.7530 261.0669 295.3892 213.6795 -0.3163 260.9082 261.2245 295.5219 214.5015 -0.3154 261.0465 261.3619 295.6610 215.2935 -0.3180 261.1944 261.5124 295.7828 216.1155 -0.3200 261.3552 261.6752 295.9104 216.9075 -0.3239 261.5068 261.8307 296.0386 217.6995 -0.3237 261.6374 261.9612 296.1586 218.5215 -0.3279 261.8057 262.1336 296.3129 219.3135 -0.3323 261.9399 262.2722 296.4218 220.1355 -0.3333 262.0811 262.4143 296.5399 220.9275 -0.3345 262.2416 262.5760 296.6454 221.7195 -0.3343 262.3737 262.7080 296.7386 222.5415 -0.3392 262.5603 262.8995 296.9013 223.3335 -0.3403 262.6991 263.0394 297.0239 224.1555 -0.3396 262.8465 263.1861 297.1505 224.9475 -0.3409 262.9924 263.3334 297.2817 225.7405 -0.3434 263.1379 263.4813 297.3991 226.5625 -0.3423 263.2889 263.6312 297.5137 227.3543 -0.3441 263.4507 263.7948 297.6462 228.1765 -0.3485 263.5860 263.9345 297.7751 228.9690 -0.3506 263.7304 264.0810 297.8841 229.7570 -0.3536 263.8695 264.2231 298.0075 230.5770 -0.3530 264.0326 264.3856 298.1214 231.3350 -0.3516 264.1680 264.5196 298.2347 232.1843 -0.3543 264.3069 264.6612 298.3852 232.9728 -0.3530 264.4497 264.8027 298.5122 233.7610 -0.3541 264.5949 264.9490 298.6418 234.6625 -0.3575 264.7731 265.1306 298.7856 235.5670 -0.3624 264.9612 265.3236 298.9097 236.3560 -0.3638 265.1170 265.4809 299.0617 237.2058 -0.3654 265.2714 265.6368 299.2099 237.9670 -0.3666 265.3875 265.7541 299.3247 238.7885 -0.3689 265.5513 265.9201 299.4503 239.5805 -0.3693 265.7247 266.0940 299.5848 240.3723 -0.3680 265.8523 266.2204 299.7214 241.1935 -0.3736 265.9821 266.3557 299.8605 241.9855 -0.3741 266.1414 266.5155 299.9984 242.8075 -0.3784 266.2870 266.6655 300.1384 243.5995 -0.3775 266.4268 266.8043 300.2649 244.3915 -0.3831 266.5657 266.9488 300.3946 245.2135 -0.3838 266.7338 267.1175 300.5168 246.0055 -0.3855 266.8882 267.2737 300.6536 246.8275 -0.3872 267.0390 267.4263 300.7844 247.6195 -0.3884 267.1865 267.5749 300.9139 248.4115 -0.3906 267.3094 267.7000 301.0598 249.2335 -0.3893 267.4669 267.8562 301.1899 250.0250 -0.3937 267.6224 268.0161 301.3149 250.8470 -0.3973 267.7676 268.1649 301.4485 251.6393 -0.3970 267.9152 268.3122 301.5750 252.4313 -0.3957 268.0534 268.4491 301.7108 253.2535 -0.3984 268.2239 268.6223 301.8386 254.0460 -0.4004 268.3648 268.7652 301.9884 254.8678 -0.4006 268.4971 268.8977 302.1235 255.6600 -0.4067 268.6593 269.0660 302.2471 256.4525 -0.4112 268.8112 269.2224 302.3768 257.2750 -0.4126 268.9401 269.3528 302.5241 258.0668 -0.4120 269.0939 269.5059 302.6619 258.8895 -0.4147 269.2379 269.6525 302.7937 259.6820 -0.4181 269.3805 269.7986 302.9164 260.4745 -0.4186 269.5409 269.9595 303.0483 261.2968 -0.4196 269.6940 270.1136 303.1651 262.0850 -0.4238 269.8333 270.2571 303.3087 262.9030 -0.4267 269.9748 270.4016 303.4392 263.6910 -0.4283 270.1124 270.5408 303.5610 264.4793 -0.4279 270.2473 270.6752 303.6981 265.3833 -0.4309 270.4317 270.8626 303.8367 266.2875 -0.4325 270.6040 271.0365 303.9729 267.0760 -0.4333 270.7428 271.1761 304.1010 267.9243 -0.4311 270.9137 271.3448 304.2579 268.6823 -0.4318 271.0491 271.4809 304.3870 269.5010 -0.4329 271.2121 271.6450 304.5081 270.3213 -0.4376 271.3731 271.8107 304.6431 271.0825 -0.4424 271.5015 271.9439 304.7617 271.9943 -0.4416 271.6542 272.0958 304.9158 272.8753 -0.4446 271.8257 272.2703 305.0562 273.6670 -0.4490 271.9569 272.4060 305.1878 274.4890 -0.4510 272.1149 272.5659 305.3366 275.3325 -0.4485 272.2599 272.7084 305.4593 276.2785 -0.4551 272.4309 272.8860 305.5804 277.1010 -0.4539 272.5922 273.0461 305.7539 277.8625 -0.4546 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