DTA measure 1Lassu Date: 2025311:124 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1617.37 s Mass = 936.100 mg data_number = 1000 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4468 0.9575 225.6030 224.6455 213.6749 4.0455 0.9412 225.4975 224.5563 213.5763 5.6445 0.9186 225.3906 224.4720 213.4304 7.2585 0.9113 225.2620 224.3507 213.3014 8.8575 0.9105 225.1582 224.2477 213.1550 10.6529 0.9150 225.0201 224.1051 212.9782 12.2905 0.9132 224.9032 223.9900 212.8027 13.8895 0.9041 224.7844 223.8802 212.6307 15.4885 0.9042 224.6720 223.7677 212.4640 17.1174 0.9587 224.5667 223.6081 212.2626 18.7171 0.9964 224.4610 223.4645 212.0688 20.3309 0.9764 224.3359 223.3595 211.8921 21.9298 1.0445 224.2176 223.1731 211.7076 23.5589 0.9558 224.1116 223.1558 211.4974 25.1738 0.9226 224.0000 223.0775 211.3237 26.7728 0.9179 223.8840 222.9661 211.1641 28.3871 0.9115 223.7963 222.8848 210.9846 29.9866 0.9390 223.6793 222.7404 210.8216 31.6006 0.9697 223.5486 222.5789 210.6900 33.2145 0.9577 223.4563 222.4987 210.5650 34.8075 0.9513 223.3412 222.3899 210.4583 36.4140 0.9597 223.2420 222.2823 210.3441 38.0050 0.9319 223.1252 222.1932 210.2535 39.5970 0.9568 223.0284 222.0716 210.1949 41.3924 0.9674 222.9145 221.9471 210.1434 43.0080 0.9644 222.7971 221.8327 210.1167 44.6148 0.9785 222.7026 221.7242 210.1127 46.2085 0.9734 222.5956 221.6222 210.1289 47.8328 1.0095 222.4912 221.4817 210.1527 49.4263 0.9350 222.3901 221.4552 210.2180 51.0244 0.9302 222.2678 221.3376 210.2985 52.6375 0.9287 222.1602 221.2315 210.3824 54.2361 0.9299 222.0825 221.1526 210.5019 55.8495 0.9391 221.9733 221.0343 210.6188 57.4635 0.9592 221.8721 220.9129 210.7749 59.0625 0.9529 221.7857 220.8328 210.9386 60.6615 0.9242 221.6802 220.7560 211.1343 62.2605 0.9147 221.5907 220.6760 211.3438 63.8895 0.9102 221.4933 220.5831 211.5485 65.4885 0.9059 221.4175 220.5116 211.7689 67.1019 0.9027 221.3243 220.4216 212.0037 68.7008 0.8959 221.2341 220.3382 212.2626 70.2998 0.8917 221.1488 220.2571 212.5129 72.1043 0.8859 221.0395 220.1537 212.8043 73.7238 0.8812 220.9426 220.0614 213.0815 75.3378 0.8778 220.8876 220.0098 213.3501 76.9368 0.8728 220.8016 219.9288 213.6300 78.5660 0.8674 220.7101 219.8427 213.9011 80.1656 0.8626 220.6297 219.7671 214.1801 81.7659 0.8589 220.5532 219.6942 214.4637 83.3821 0.8553 220.4941 219.6389 214.7187 84.9966 0.8516 220.4197 219.5680 214.9927 86.6105 0.8444 220.3348 219.4904 215.2459 88.2095 0.8395 220.2585 219.4189 215.5105 89.8235 0.8355 220.2265 219.3911 215.7539 91.4225 0.8299 220.1558 219.3259 216.0045 93.0365 0.8213 220.0837 219.2624 216.2283 94.6513 0.8146 220.0122 219.1976 216.4757 96.2514 0.8113 219.9505 219.1392 216.6902 97.8661 0.8057 219.9105 219.1048 216.9058 99.4610 0.8013 219.8640 219.0627 217.1272 101.0523 0.7952 219.8222 219.0270 217.3434 102.8440 0.7924 219.7623 218.9699 217.5817 104.4583 0.7869 219.6830 218.8961 217.8056 106.0649 0.7834 219.6327 218.8493 218.0223 107.6715 0.7780 219.6016 218.8237 218.2134 109.2781 0.7712 219.5661 218.7949 218.3960 110.8704 0.7659 219.5124 218.7465 218.5868 112.4669 0.7632 219.4746 218.7114 218.7792 114.0788 0.7590 219.4218 218.6628 218.9716 115.6748 0.7530 219.3913 218.6383 219.1458 117.3040 0.7458 219.3502 218.6044 219.3232 118.9028 0.7441 219.3171 218.5730 219.5059 120.5018 0.7394 219.2997 218.5603 219.6707 122.1525 0.7334 219.2656 218.5321 219.8526 123.9068 0.7272 219.2218 218.4946 220.0398 125.5058 0.7247 219.2078 218.4832 220.2128 127.1348 0.7205 219.1765 218.4560 220.3645 128.7336 0.7158 219.1534 218.4377 220.5038 130.3325 0.7127 219.1355 218.4228 220.6761 131.9465 0.7116 219.1191 218.4075 220.8353 133.5456 0.7084 219.0963 218.3879 221.0096 135.1745 0.7055 219.0656 218.3601 221.1863 136.7735 0.7028 219.0534 218.3507 221.3494 138.3725 0.6976 219.0488 218.3512 221.5108 139.9865 0.6944 219.0270 218.3326 221.6822 141.5855 0.6929 219.0169 218.3240 221.8484 143.2155 0.6901 219.0045 218.3144 222.0324 144.8145 0.6833 219.0034 218.3201 222.2085 146.4130 0.6790 218.9924 218.3134 222.3698 148.0268 0.6766 218.9845 218.3078 222.5607 149.6409 0.6751 218.9871 218.3120 222.7539 151.2549 0.6756 218.9789 218.3034 222.9431 152.8989 0.6722 218.9735 218.3013 223.1320 154.6638 0.6641 218.9640 218.2999 223.3301 156.2778 0.6634 218.9791 218.3156 223.5340 157.8918 0.6641 218.9902 218.3262 223.7254 159.4905 0.6580 218.9852 218.3272 223.9281 161.1050 0.6562 218.9988 218.3426 224.1558 162.7033 0.6512 219.0024 218.3513 224.3494 164.3099 0.6510 219.0057 218.3547 224.5648 165.9160 0.6487 219.0198 218.3712 224.7680 167.5070 0.6446 219.0484 218.4038 224.9888 169.0980 0.6409 219.0545 218.4136 225.1979 170.7045 0.6386 219.0697 218.4311 225.4183 172.3119 0.6345 219.1088 218.4743 225.6418 173.9180 0.6292 219.1067 218.4775 225.8571 175.5243 0.6295 219.1381 218.5086 226.0867 177.1173 0.6240 219.1591 218.5351 226.2912 178.7126 0.6192 219.1892 218.5700 226.5220 180.3393 0.6171 219.2024 218.5853 226.7309 181.9375 0.6124 219.2216 218.6091 226.9409 183.5815 0.6089 219.2790 218.6701 227.1609 185.3445 0.6053 219.3019 218.6966 227.4185 186.9435 0.6001 219.3261 218.7259 227.6356 188.5575 0.5965 219.3513 218.7548 227.8306 190.1715 0.5933 219.4000 218.8067 228.0537 191.7705 0.5892 219.4449 218.8558 228.2674 193.3694 0.5851 219.4694 218.8842 228.4809 194.9701 0.5834 219.5042 218.9208 228.6912 196.5989 0.5794 219.5644 218.9850 228.9017 198.1979 0.5765 219.5948 219.0183 229.1016 199.8118 0.5721 219.6216 219.0495 229.3035 201.4108 0.5709 219.6785 219.1076 229.5156 203.0098 0.5697 219.7259 219.1562 229.7188 204.6239 0.5777 219.7808 219.2031 229.9054 206.2379 0.5961 219.8167 219.2206 230.1228 207.8519 0.5826 219.8573 219.2747 230.3124 209.4516 0.6231 219.9051 219.2820 230.5160 211.0505 0.5884 219.9639 219.3755 230.7035 212.6796 0.5526 220.0411 219.4885 230.8973 214.2795 0.5478 220.0916 219.5438 231.0987 215.8935 0.5454 220.1490 219.6036 231.2752 217.4925 0.5443 220.1955 219.6512 231.4681 219.0915 0.5396 220.2606 219.7210 231.6532 220.7205 0.5368 220.3325 219.7957 231.8706 222.3195 0.5360 220.3920 219.8560 232.0348 223.9334 0.5302 220.4395 219.9093 232.2265 225.5336 0.5310 220.5075 219.9765 232.4012 227.1326 0.5260 220.5699 220.0439 232.5778 228.7544 0.5238 220.6376 220.1138 232.7585 230.3453 0.5246 220.7154 220.1908 232.9440 231.9511 0.5207 220.7870 220.2663 233.1339 233.5421 0.5180 220.8485 220.3305 233.3215 235.2370 0.5165 220.9283 220.4118 233.5041 236.9473 0.5133 221.0064 220.4931 233.7285 238.5545 0.5085 221.0665 220.5580 233.9200 240.1630 0.5061 221.1339 220.6278 234.1115 241.7559 0.5052 221.2161 220.7109 234.3069 243.3656 0.5030 221.2942 220.7912 234.5020 244.9766 0.5005 221.3724 220.8719 234.6999 246.5739 0.4976 221.4535 220.9559 234.8821 248.1883 0.4966 221.5490 221.0523 235.0965 249.7878 0.4958 221.6097 221.1139 235.2882 251.3868 0.4914 221.7013 221.2099 235.4813 253.0008 0.4901 221.7822 221.2921 235.6879 254.6148 0.4883 221.8749 221.3866 235.8905 256.2138 0.4811 221.9610 221.4800 236.0904 257.8125 0.4804 222.0496 221.5692 236.2978 259.4266 0.4784 222.1329 221.6545 236.5058 261.0256 0.4747 222.2247 221.7499 236.7181 262.6545 0.4708 222.3127 221.8419 236.9355 264.2535 0.4683 222.3968 221.9285 237.1762 265.8525 0.4663 222.5028 222.0364 237.3969 267.4515 0.4636 222.6010 222.1373 237.5992 269.0655 0.4585 222.6726 222.2140 237.8230 270.6795 0.4562 222.7855 222.3292 238.0541 272.2935 0.4560 222.8850 222.4290 238.2879 273.8925 0.4516 222.9884 222.5368 238.4998 275.5059 0.4492 223.0812 222.6320 238.7298 277.1048 0.4442 223.1688 222.7246 238.9516 278.7340 0.4410 223.2777 222.8368 239.1811 280.3339 0.4370 223.3683 222.9312 239.3969 281.9338 0.4364 223.4815 223.0451 239.6261 283.5483 0.4326 223.6072 223.1746 239.8419 285.1476 0.4270 223.6865 223.2595 240.0569 286.7768 0.4273 223.8010 223.3737 240.2827 288.3765 0.4251 223.8962 223.4712 240.4935 289.9910 0.4207 224.0090 223.5883 240.7188 291.5860 0.4215 224.1132 223.6917 240.9253 293.1769 0.4171 224.2359 223.8188 241.1353 294.7975 0.4128 224.3520 223.9392 241.3552 296.3890 0.4111 224.4663 224.0552 241.5724 297.9800 0.4084 224.5606 224.1522 241.7755 299.5860 0.4050 224.6905 224.2855 241.9927 301.1928 0.4007 224.7998 224.3990 242.1960 302.7999 0.3985 224.9113 224.5128 242.4289 304.4079 0.3994 225.0148 224.6155 242.6230 306.0023 0.3937 225.1601 224.7664 242.8235 307.6030 0.3897 225.2666 224.8769 243.0216 309.2160 0.3885 225.3895 225.0010 243.2227 310.8295 0.3864 225.5264 225.1400 243.4399 312.4285 0.3828 225.6482 225.2654 243.6534 314.0275 0.3769 225.7578 225.3809 243.8410 315.6265 0.3746 225.8694 225.4949 244.0374 317.3650 0.3702 226.0050 225.6349 244.2517 319.0535 0.3664 226.1550 225.7886 244.4686 320.6523 0.3637 226.2794 225.9157 244.6784 322.2660 0.3617 226.4106 226.0489 244.8460 323.8649 0.3575 226.5385 226.1810 245.0483 325.4639 0.3531 226.6578 226.3047 245.2507 327.0954 0.3522 226.7778 226.4256 245.4548 328.6989 0.3479 226.9036 226.5558 245.6386 330.2978 0.3441 227.0449 226.7008 245.8327 331.9116 0.3425 227.1832 226.8407 246.0218 333.5108 0.3409 227.3235 226.9827 246.2283 335.1248 0.3334 227.4483 227.1149 246.4236 336.7390 0.3306 227.5731 227.2424 246.5992 338.3396 0.3288 227.7196 227.3908 246.7779 339.9385 0.3227 227.8543 227.5316 246.9779 341.5525 0.3235 227.9774 227.6539 247.1519 343.1665 0.3181 228.1181 227.8000 247.3403 344.7814 0.3130 228.2372 227.9242 247.5412 346.3816 0.3115 228.3931 228.0816 247.7142 347.9965 0.3111 228.5318 228.2208 247.9033 349.5960 0.3075 228.6630 228.3555 248.1091 351.2104 0.3050 228.8078 228.5028 248.2975 352.8248 0.3029 228.9463 228.6434 248.5078 354.4248 0.3032 229.0988 228.7956 248.7268 356.0368 0.3009 229.2273 228.9264 248.9301 357.6294 0.2977 229.3957 229.0980 249.1283 359.2250 0.2972 229.5239 229.2266 249.3362 360.8458 0.2971 229.6643 229.3673 249.5347 362.4373 0.2919 229.8134 229.5215 249.7515 364.0281 0.2903 229.9582 229.6679 249.9735 365.6343 0.2849 230.0938 229.8089 250.2005 367.2410 0.2877 230.2357 229.9480 250.3881 369.0159 0.2824 230.4050 230.1226 250.6124 370.6538 0.2827 230.5476 230.2649 250.8305 372.2478 0.2793 230.6925 230.4132 251.0528 373.8599 0.2735 230.8429 230.5694 251.2471 375.4588 0.2728 231.0174 230.7446 251.4676 377.0729 0.2704 231.1599 230.8896 251.6748 378.6873 0.2681 231.3080 231.0399 251.8824 380.2868 0.2640 231.4417 231.1776 252.0819 381.8856 0.2607 231.5958 231.3351 252.3061 383.4845 0.2580 231.7479 231.4899 252.5076 385.1148 0.2563 231.9140 231.6577 252.7323 386.7136 0.2535 232.0588 231.8053 252.9227 388.3629 0.2507 232.2327 231.9821 253.1340 390.1285 0.2447 232.4177 232.1730 253.3745 391.7275 0.2446 232.5520 232.3074 253.5565 393.3415 0.2414 232.7059 232.4645 253.7687 394.9555 0.2390 232.8675 232.6285 253.9674 396.5545 0.2360 233.0138 232.7778 254.1746 398.1535 0.2341 233.1672 232.9331 254.3728 399.7674 0.2312 233.3304 233.0992 254.5828 401.3663 0.2298 233.4875 233.2577 254.7596 402.9951 0.2243 233.6461 233.4217 254.9861 404.5938 0.2254 233.8087 233.5833 255.1734 406.1928 0.2203 233.9773 233.7570 255.3867 407.8073 0.2142 234.1377 233.9236 255.6003 409.4219 0.2148 234.3199 234.1050 255.8175 411.0368 0.2131 234.4744 234.2613 256.0416 412.6368 0.2094 234.6416 234.4322 256.2526 414.2520 0.2037 234.7903 234.5866 256.4801 415.8516 0.2017 234.9517 234.7500 256.7025 417.4663 0.2017 235.1165 234.9147 256.9263 419.0815 0.1977 235.2726 235.0750 257.1447 420.6760 0.1961 235.4469 235.2508 257.3478 422.2670 0.1933 235.5988 235.4055 257.5755 423.8735 0.1909 235.7654 235.5745 257.8069 425.4665 0.1882 235.9471 235.7588 258.0401 427.0898 0.1837 236.0942 235.9105 258.2619 428.6825 0.1812 236.2681 236.0870 258.4983 430.2754 0.1748 236.4327 236.2579 258.7271 431.8839 0.1719 236.6043 236.4324 258.9458 433.4780 0.1712 236.7850 236.6138 259.1578 435.1038 0.1657 236.9475 236.7818 259.4122 436.7015 0.1594 237.1167 236.9573 259.6150 438.2998 0.1591 237.3014 237.1424 259.8194 440.0001 0.1547 237.4778 237.3231 260.0327 441.7015 0.1491 237.6464 237.4973 260.2626 443.3305 0.1484 237.8104 237.6620 260.4525 444.9295 0.1493 237.9913 237.8420 260.6674 446.5435 0.1420 238.1653 238.0233 260.8719 448.1425 0.1371 238.3484 238.2113 261.0412 449.7413 0.1375 238.5091 238.3715 261.2143 451.3703 0.1335 238.6942 238.5607 261.3964 452.9689 0.1297 238.8578 238.7281 261.5941 454.5828 0.1267 239.0477 238.9210 261.7815 456.1818 0.1215 239.2305 239.1091 261.9871 457.7808 0.1181 239.4100 239.2919 262.1576 459.4099 0.1172 239.5677 239.4505 262.3566 461.0089 0.1150 239.7629 239.6479 262.5479 462.6226 0.1089 239.9431 239.8342 262.7430 464.2216 0.1045 240.1198 240.0153 262.9318 465.8355 0.1041 240.2877 240.1837 263.1415 467.4496 0.1006 240.4453 240.3447 263.3416 469.0635 0.0958 240.6369 240.5411 263.5418 470.6628 0.0943 240.8091 240.7149 263.7441 472.2625 0.0927 240.9895 240.8968 263.9433 473.8771 0.0904 241.1691 241.0786 264.1611 475.4915 0.0858 241.3561 241.2703 264.3564 477.1056 0.0849 241.5557 241.4708 264.5516 478.7054 0.0806 241.7230 241.6424 264.7445 480.3040 0.0782 241.8893 241.8110 264.9572 481.9178 0.0760 242.0740 241.9980 265.1863 483.5311 0.0746 242.2730 242.1984 265.3741 485.1383 0.0736 242.4519 242.3783 265.5537 486.7295 0.0692 242.6203 242.5511 265.7560 488.3359 0.0646 242.7891 242.7245 265.9795 489.9280 0.0599 242.9757 242.9158 266.1814 491.5495 0.0588 243.1789 243.1201 266.3821 493.1425 0.0567 243.3476 243.2909 266.6205 494.7361 0.0532 243.5296 243.4764 266.8474 496.3438 0.0499 243.7364 243.6865 267.0674 497.9526 0.0484 243.9074 243.8590 267.2839 499.5630 0.0456 244.0930 244.0474 267.5109 501.2378 0.0467 244.2895 244.2428 267.7495 502.9718 0.0444 244.4796 244.4352 268.0109 504.5849 0.0479 244.6553 244.6074 268.2610 506.1838 0.0499 244.8410 244.7911 268.5010 507.7978 0.0413 245.0430 245.0017 268.7317 509.3966 0.0606 245.2242 245.1636 268.9475 510.9958 0.0538 245.4048 245.3510 269.1940 512.6248 0.0342 245.6199 245.5857 269.4177 514.2238 0.0440 245.7903 245.7463 269.6467 515.8375 0.0474 245.9691 245.9217 269.8316 517.4365 0.0291 246.1765 246.1474 270.0431 519.0355 0.0201 246.3681 246.3480 270.2548 520.6645 0.0215 246.5584 246.5369 270.4573 522.4191 0.0029 246.7513 246.7483 270.6660 524.0705 -0.0057 246.9481 246.9538 270.8631 525.6844 -0.0110 247.1345 247.1455 271.0556 527.2840 -0.0126 247.3396 247.3521 271.2405 528.8988 -0.0180 247.5353 247.5534 271.4323 530.5140 -0.0188 247.7199 247.7387 271.6212 532.1128 -0.0236 247.9055 247.9290 271.7935 533.7271 -0.0260 248.1074 248.1334 271.9936 535.3268 -0.0269 248.3055 248.3324 272.1705 536.9558 -0.0306 248.4954 248.5260 272.3718 538.5699 -0.0330 248.6793 248.7124 272.5701 540.1698 -0.0348 248.8664 248.9012 272.7775 541.7686 -0.0422 249.0678 249.1100 272.9638 543.3826 -0.0459 249.2616 249.3075 273.1737 544.9974 -0.0466 249.4716 249.5182 273.3887 546.6116 -0.0500 249.6558 249.7058 273.6021 548.2088 -0.0542 249.8449 249.8992 273.7922 549.8150 -0.0546 250.0361 250.0907 274.0094 551.4060 -0.0591 250.2228 250.2818 274.2078 553.1751 -0.0638 250.4357 250.4995 274.4622 554.8114 -0.0663 250.6360 250.7023 274.6899 556.4185 -0.0665 250.8348 250.9013 274.9258 558.0115 -0.0741 251.0215 251.0955 275.1294 559.6353 -0.0778 251.2091 251.2869 275.3468 561.2284 -0.0795 251.4125 251.4920 275.5534 562.9245 -0.0884 251.6099 251.6983 275.7785 564.6374 -0.0915 251.8268 251.9183 276.0090 566.2505 -0.0960 252.0366 252.1326 276.2283 567.8489 -0.0971 252.2179 252.3150 276.4364 569.4625 -0.0998 252.4345 252.5344 276.6666 571.0833 -0.1043 252.6331 252.7374 276.8829 572.6828 -0.1077 252.8334 252.9412 277.0840 574.2851 -0.1129 253.0293 253.1422 277.2967 575.9014 -0.1182 253.2039 253.3221 277.4944 577.5003 -0.1237 253.3994 253.5231 277.7064 579.1139 -0.1254 253.5903 253.7156 277.9181 580.7279 -0.1317 253.8074 253.9391 278.1293 582.3278 -0.1347 254.0108 254.1455 278.3295 583.9450 -0.1362 254.2142 254.3504 278.5339 585.5529 -0.1419 254.4145 254.5564 278.7567 587.1516 -0.1444 254.6167 254.7611 278.9645 588.7660 -0.1482 254.8165 254.9647 279.1551 590.3656 -0.1482 255.0225 255.1708 279.3462 591.9946 -0.1550 255.2238 255.3788 279.5437 593.6031 -0.1565 255.4116 255.5681 279.7551 595.1966 -0.1600 255.6321 255.7921 279.9407 596.8105 -0.1647 255.8244 255.9892 280.1346 598.4255 -0.1681 256.0278 256.1959 280.3576 600.0395 -0.1702 256.2224 256.3926 280.5338 601.6389 -0.1709 256.4296 256.6005 280.7575 603.2485 -0.1764 256.6376 256.8140 280.9405 604.8604 -0.1796 256.8342 257.0137 281.1265 606.4745 -0.1794 257.0316 257.2110 281.3484 608.0734 -0.1832 257.2243 257.4075 281.5649 609.6880 -0.1861 257.4411 257.6273 281.7580 611.3028 -0.1903 257.6279 257.8182 281.9520 612.9153 -0.1929 257.8477 258.0406 282.1824 614.4903 -0.1961 258.0297 258.2258 282.3971 616.1156 -0.2013 258.2546 258.4559 282.6192 617.7075 -0.2027 258.4569 258.6596 282.8380 619.3143 -0.1905 258.6676 258.8582 283.0651 620.9060 -0.1700 258.8705 259.0406 283.2780 622.5123 -0.2073 259.0492 259.2565 283.5126 624.1186 -0.2207 259.2597 259.4804 283.7468 625.7176 -0.2219 259.4688 259.6907 283.9748 627.3428 -0.2235 259.6776 259.9011 284.2188 628.9396 -0.2262 259.8691 260.0953 284.4466 630.5505 -0.2328 260.0995 260.3324 284.6627 632.1488 -0.2356 260.2855 260.5210 284.9042 633.7476 -0.2415 260.4931 260.7346 285.1275 635.3566 -0.2461 260.6971 260.9432 285.3925 636.9706 -0.2522 260.8971 261.1492 285.6135 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