DTA measure 11meres Date: 20241022:1511 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 804.92 s Mass = 958.000 mg data_number = 1000 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2558 -1.2194 280.3635 281.5829 267.7421 2.0175 -1.2202 280.3607 281.5809 267.7325 2.8698 -1.2187 280.3714 281.5902 267.7264 3.6318 -1.2107 280.3565 281.5672 267.7086 4.4538 -1.2185 280.3509 281.5694 267.7068 5.2758 -1.2138 280.3559 281.5697 267.7320 6.0375 -1.2146 280.3514 281.5661 267.7498 6.8898 -1.2171 280.3728 281.5899 267.7498 7.6818 -1.2196 280.3643 281.5838 267.7769 8.4735 -1.2204 280.3460 281.5664 267.7962 9.2958 -1.2200 280.3506 281.5706 267.8275 10.0575 -1.2180 280.3647 281.5827 267.8571 10.9098 -1.2189 280.3638 281.5828 267.9043 11.7018 -1.2130 280.3805 281.5936 267.9447 12.4945 -1.2023 280.3786 281.5809 268.0074 13.3168 -1.2145 280.3855 281.6001 268.0776 14.0785 -1.2208 280.3797 281.6005 268.1352 14.9305 -1.2195 280.3703 281.5898 268.2421 15.7225 -1.2199 280.3655 281.5855 268.3290 16.7145 -1.2219 280.3655 281.5874 268.4372 17.5365 -1.2165 280.3770 281.5934 268.5538 18.3285 -1.2181 280.3755 281.5936 268.6533 19.1205 -1.2138 280.3723 281.5861 268.7696 19.9725 -1.2108 280.3736 281.5845 268.8928 20.7345 -1.2200 280.3835 281.6035 268.9998 21.5563 -1.2258 280.3884 281.6142 269.1355 22.3783 -1.2259 280.3765 281.6024 269.2657 23.1395 -1.2277 280.3803 281.6080 269.3964 23.9925 -1.2304 280.3891 281.6195 269.5475 24.7545 -1.2233 280.3971 281.6203 269.7043 25.5768 -1.2250 280.3880 281.6130 269.8565 26.4715 -1.2215 280.3947 281.6162 270.0035 27.3970 -1.2214 280.4001 281.6215 270.1611 28.1595 -1.2302 280.4304 281.6605 270.2959 29.0118 -1.2297 280.4159 281.6456 270.4508 29.8038 -1.2308 280.4216 281.6524 270.6025 30.5965 -1.2329 280.4275 281.6604 270.7645 31.4190 -1.2351 280.4229 281.6581 270.9128 32.1815 -1.2392 280.4325 281.6717 271.0721 33.0335 -1.2364 280.4417 281.6781 271.2081 33.8255 -1.2374 280.4359 281.6733 271.3685 34.6175 -1.2429 280.4463 281.6892 271.5091 35.4395 -1.2451 280.4466 281.6917 271.6689 36.2015 -1.2444 280.4556 281.7000 271.8127 37.0528 -1.2400 280.4659 281.7059 271.9819 37.8410 -1.2488 280.4609 281.7097 272.1109 38.6290 -1.2505 280.4787 281.7292 272.2558 39.4475 -1.2533 280.4841 281.7374 272.3965 40.2060 -1.2559 280.4936 281.7495 272.5392 41.0548 -1.2605 280.5159 281.7764 272.6875 41.8130 -1.2661 280.5108 281.7769 272.8069 42.6320 -1.2659 280.5153 281.7813 272.9515 43.4503 -1.2656 280.5305 281.7961 273.0866 44.2090 -1.2615 280.5367 281.7982 273.2008 45.0573 -1.2550 280.5403 281.7953 273.3422 45.8160 -1.2687 280.5481 281.8168 273.4642 46.6358 -1.2768 280.5568 281.8336 273.5745 47.4543 -1.2733 280.5663 281.8395 273.7071 48.2130 -1.2748 280.6041 281.8789 273.8185 49.0618 -1.2781 280.6035 281.8816 273.9391 49.8220 -1.2845 280.6225 281.9070 274.0525 50.6425 -1.2854 280.6424 281.9279 274.1870 51.4633 -1.2905 280.6380 281.9285 274.2968 52.2245 -1.2904 280.6631 281.9534 274.4125 53.0753 -1.2921 280.6699 281.9619 274.5256 53.8365 -1.2976 280.6861 281.9838 274.6190 54.6578 -1.2976 280.6915 281.9891 274.7455 55.4520 -1.3002 280.7054 282.0056 274.8493 56.2438 -1.3032 280.7249 282.0281 274.9599 57.1465 -1.3041 280.7536 282.0577 275.0895 58.0803 -1.3059 280.7618 282.0677 275.2296 58.8415 -1.3066 280.7857 282.0923 275.3356 59.6938 -1.3106 280.8252 282.1358 275.4855 60.4555 -1.3066 280.8229 282.1295 275.5917 61.2778 -1.3013 280.8361 282.1374 275.7143 62.0998 -1.3129 280.8683 282.1812 275.8320 62.8615 -1.3183 280.8740 282.1923 275.9401 63.7138 -1.3252 280.8941 282.2193 276.0580 64.4755 -1.3258 280.9297 282.2556 276.1828 65.2978 -1.3277 280.9369 282.2645 276.3194 66.0898 -1.3278 280.9520 282.2798 276.4270 66.8815 -1.3301 280.9856 282.3157 276.5512 67.7345 -1.3350 281.0189 282.3539 276.6866 68.4965 -1.3359 281.0255 282.3614 276.8132 69.3188 -1.3346 281.0608 282.3954 276.9484 70.1105 -1.3336 281.0815 282.4152 277.0878 70.9025 -1.3356 281.1110 282.4466 277.2215 71.7545 -1.3394 281.1164 282.4558 277.3581 72.5165 -1.3436 281.1428 282.4864 277.4953 73.3385 -1.3453 281.1719 282.5172 277.6299 74.1305 -1.3468 281.1955 282.5423 277.7796 74.9225 -1.3454 281.2186 282.5640 277.9229 75.7745 -1.3512 281.2530 282.6042 278.0587 76.5365 -1.3564 281.2626 282.6190 278.1932 77.3585 -1.3565 281.2924 282.6489 278.3375 78.1805 -1.3589 281.3272 282.6862 278.4734 78.9425 -1.3630 281.3465 282.7095 278.6019 79.7943 -1.3631 281.3877 282.7507 278.7584 80.5865 -1.3598 281.4145 282.7743 278.8924 81.3775 -1.3555 281.4414 282.7969 279.0219 82.2003 -1.3577 281.4743 282.8320 279.1616 82.9625 -1.3617 281.5144 282.8761 279.2839 83.8148 -1.3680 281.5232 282.8911 279.4194 84.6068 -1.3707 281.5503 282.9210 279.5610 85.3995 -1.3739 281.5902 282.9641 279.6939 86.2218 -1.3763 281.6415 283.0177 279.8412 86.9835 -1.3777 281.6737 283.0515 279.9606 87.8613 -1.3796 281.6834 283.0629 280.1131 88.6185 -1.3838 281.7166 283.1004 280.2479 89.4408 -1.3821 281.7554 283.1375 280.3568 90.2025 -1.3828 281.7964 283.1792 280.4913 91.0553 -1.3872 281.8324 283.2196 280.6289 91.8478 -1.3891 281.8777 283.2668 280.7582 92.6405 -1.3911 281.9056 283.2967 280.8811 93.4630 -1.3908 281.9325 283.3233 281.0192 94.2555 -1.3918 281.9730 283.3648 281.1517 95.0783 -1.3785 282.0090 283.3875 281.2880 95.8705 -1.3833 282.0554 283.4387 281.4096 96.6625 -1.3882 282.0823 283.4705 281.5214 97.4848 -1.3930 282.1190 283.5120 281.6560 98.3075 -1.3983 282.1598 283.5581 281.7917 99.0595 -1.4000 282.2054 283.6055 281.9084 99.9115 -1.3991 282.2467 283.6458 282.0320 100.7030 -1.3993 282.2826 283.6819 282.1454 101.4923 -1.3938 282.3265 283.7203 282.2607 102.3110 -1.3864 282.3610 283.7474 282.3796 103.0700 -1.3834 282.3921 283.7755 282.5098 103.9178 -1.3762 282.4400 283.8163 282.6255 104.6755 -1.3834 282.4980 283.8813 282.7290 105.4950 -1.3858 282.5344 283.9202 282.8740 106.3138 -1.3903 282.5739 283.9642 282.9958 107.0723 -1.3897 282.6260 284.0157 283.1059 107.9205 -1.3928 282.6636 284.0564 283.2232 108.7190 -1.3878 282.7006 284.0885 283.3156 109.5075 -1.3824 282.7411 284.1235 283.4454 110.2965 -1.3876 282.7800 284.1676 283.5695 111.1150 -1.3944 282.8112 284.2056 283.6774 111.8740 -1.4117 282.8596 284.2713 283.7793 112.7230 -1.4178 282.9202 284.3380 283.9100 113.5123 -1.4139 282.9758 284.3897 284.0305 114.3020 -1.4070 283.0255 284.4325 284.1461 115.1230 -1.4017 283.0679 284.4696 284.2775 115.8838 -1.4180 283.1138 284.5319 284.3738 116.7350 -1.4183 283.1623 284.5806 284.5132 117.5258 -1.4099 283.2217 284.6317 284.6446 118.3413 -1.4103 283.2705 284.6807 284.7797 119.1248 -1.4055 283.3207 284.7262 284.8918 119.9468 -1.4097 283.3686 284.7783 285.0296 120.7085 -1.4133 283.4111 284.8244 285.1718 121.5608 -1.4288 283.4611 284.8899 285.2946 122.3225 -1.4321 283.5307 284.9627 285.4093 123.1448 -1.4290 283.5714 285.0004 285.5307 123.9368 -1.4201 283.6108 285.0309 285.6798 124.7285 -1.4221 283.6578 285.0799 285.8150 125.5508 -1.4294 283.7183 285.1477 285.9406 126.3425 -1.4341 283.7826 285.2167 286.0631 127.1648 -1.4346 283.8509 285.2854 286.2107 127.9565 -1.4348 283.8961 285.3309 286.3291 128.7840 -1.4398 283.9442 285.3840 286.4700 129.5525 -1.4404 283.9946 285.4350 286.5921 130.3745 -1.4326 284.0537 285.4863 286.7326 131.1665 -1.4297 284.1151 285.5448 286.8593 131.9885 -1.4315 284.1609 285.5924 286.9959 132.7805 -1.4297 284.2163 285.6459 287.1174 133.5725 -1.4347 284.2685 285.7032 287.2405 134.3945 -1.4340 284.3342 285.7682 287.3596 135.1865 -1.4352 284.3922 285.8274 287.4891 136.0085 -1.4397 284.4603 285.9000 287.6223 136.8005 -1.4420 284.5089 285.9508 287.7367 137.5923 -1.4401 284.5718 286.0119 287.8613 138.4145 -1.4421 284.6376 286.0797 288.0024 139.2300 -1.4450 284.6936 286.1386 288.1270 140.0108 -1.4488 284.7692 286.2180 288.2317 140.8328 -1.4492 284.8253 286.2745 288.3710 141.6250 -1.4488 284.8727 286.3215 288.4821 142.4165 -1.4490 284.9368 286.3859 288.5986 143.2688 -1.4479 284.9894 286.4373 288.7353 144.0305 -1.4456 285.0526 286.4983 288.8619 144.8528 -1.4494 285.1227 286.5721 288.9905 145.6748 -1.4479 285.1883 286.6361 289.1402 146.4365 -1.4481 285.2500 286.6981 289.2727 147.2888 -1.4446 285.3168 286.7615 289.4024 148.0505 -1.4453 285.3690 286.8144 289.5424 148.8728 -1.4497 285.4544 286.9041 289.6614 149.6860 -1.4458 285.5189 286.9647 289.8085 150.4788 -1.4476 285.5746 287.0222 289.9450 151.2715 -1.4509 285.6309 287.0818 290.0958 152.1235 -1.4492 285.6909 287.1401 290.2368 152.8855 -1.4499 285.7599 287.2098 290.3691 153.7075 -1.4506 285.8226 287.2732 290.5087 154.4995 -1.4485 285.8986 287.3471 290.6418 155.2925 -1.4490 285.9743 287.4233 290.7845 156.1450 -1.4491 286.0414 287.4905 290.9125 156.9075 -1.4525 286.0954 287.5479 291.0297 157.7303 -1.4521 286.1674 287.6195 291.1879 158.5225 -1.4579 286.2448 287.7027 291.3207 159.3338 -1.4588 286.3193 287.7781 291.4624 160.1265 -1.4596 286.3868 287.8465 291.6056 160.9493 -1.4593 286.4495 287.9088 291.7298 161.7415 -1.4597 286.5251 287.9848 291.8605 162.5638 -1.4457 286.5974 288.0431 292.0176 163.3558 -1.4343 286.6698 288.1041 292.1549 164.1475 -1.4355 286.7380 288.1735 292.2861 164.9700 -1.4491 286.8203 288.2693 292.4177 165.7623 -1.4578 286.8822 288.3401 292.5450 166.5813 -1.4606 286.9746 288.4351 292.6801 167.3693 -1.4618 287.0355 288.4972 292.8040 168.1580 -1.4635 287.0868 288.5503 292.9302 168.9768 -1.4632 287.1745 288.6377 293.0598 169.7723 -1.4623 287.2521 288.7144 293.1841 170.5360 -1.4633 287.3190 288.7824 293.3086 171.3840 -1.4637 287.4021 288.8658 293.4378 172.1720 -1.4649 287.4723 288.9372 293.5735 172.9600 -1.4656 287.5399 289.0055 293.7042 173.7785 -1.4678 287.6266 289.0944 293.8303 174.5370 -1.4709 287.7046 289.1755 293.9591 175.3850 -1.4694 287.7746 289.2440 294.0927 176.1733 -1.4700 287.8660 289.3360 294.2202 176.9625 -1.4700 287.9429 289.4129 294.3473 177.7813 -1.4677 288.0225 289.4902 294.4946 178.5418 -1.4717 288.0911 289.5628 294.6171 179.3915 -1.4706 288.1750 289.6457 294.7339 180.1828 -1.4665 288.2516 289.7181 294.8652 180.9618 -1.4705 288.3357 289.8062 294.9894 181.7820 -1.4623 288.4127 289.8750 295.1339 182.5735 -1.4616 288.4890 289.9506 295.2598 183.3653 -1.4691 288.5582 290.0273 295.3901 184.2168 -1.4709 288.6507 290.1216 295.5241 184.9785 -1.4729 288.7222 290.1952 295.6406 185.8005 -1.4737 288.8153 290.2889 295.7580 186.5925 -1.4742 288.8860 290.3602 295.8934 187.3845 -1.4754 288.9697 290.4451 296.0107 188.2065 -1.4757 289.0550 290.5307 296.1397 188.9985 -1.4762 289.1345 290.6107 296.2566 189.8205 -1.4788 289.2047 290.6835 296.3868 190.6198 -1.4772 289.2884 290.7656 296.5128 191.4125 -1.4750 289.3959 290.8710 296.6293 192.2045 -1.4756 289.4853 290.9609 296.7378 193.0265 -1.4779 289.5535 291.0315 296.8643 193.8185 -1.4795 289.6301 291.1096 296.9788 194.6405 -1.4789 289.7225 291.2014 297.0872 195.4320 -1.4785 289.8098 291.2884 297.2127 196.2235 -1.4787 289.9021 291.3808 297.3458 197.0460 -1.4795 290.0008 291.4804 297.4612 197.8375 -1.4803 290.0724 291.5527 297.5831 198.6598 -1.4800 290.1429 291.6229 297.7033 199.4518 -1.4789 290.2391 291.7180 297.8352 200.2623 -1.4781 290.3181 291.7962 297.9716 201.0498 -1.4786 290.4035 291.8821 298.0903 201.8718 -1.4787 290.4971 291.9758 298.2367 202.6635 -1.4777 290.5847 292.0625 298.3724 203.4858 -1.4800 290.6749 292.1550 298.4901 204.2778 -1.4825 290.7589 292.2414 298.6147 205.0695 -1.4827 290.8429 292.3256 298.7587 205.8920 -1.4825 290.9455 292.4280 298.9009 206.6845 -1.4807 291.0358 292.5164 299.0248 207.5075 -1.4790 291.1176 292.5966 299.1742 208.2995 -1.4811 291.2132 292.6942 299.3091 209.0915 -1.4828 291.2984 292.7811 299.4417 209.9435 -1.4839 291.3883 292.8723 299.6087 210.7153 -1.4826 291.4817 292.9643 299.7240 211.5165 -1.4836 291.5776 293.0612 299.8528 212.3385 -1.4840 291.6614 293.1454 299.9919 213.1305 -1.4835 291.7446 293.2282 300.1335 213.9235 -1.4843 291.8417 293.3260 300.2638 214.7455 -1.4847 291.9512 293.4359 300.4267 215.5375 -1.4861 292.0306 293.5167 300.5404 216.3603 -1.4850 292.1335 293.6185 300.6743 217.1525 -1.4842 292.2277 293.7119 300.8168 217.9438 -1.4845 292.3148 293.7992 300.9598 218.7663 -1.4853 292.4053 293.8907 301.1009 219.5585 -1.4837 292.4743 293.9581 301.2291 220.3808 -1.4849 292.5775 294.0624 301.3724 221.1770 -1.4868 292.6758 294.1625 301.5115 221.9898 -1.4885 292.7792 294.2677 301.6640 222.7825 -1.4892 292.8766 294.3658 301.7951 223.6048 -1.4883 292.9705 294.4588 301.9306 224.3665 -1.4901 293.0608 294.5509 302.0466 225.2193 -1.4918 293.1616 294.6534 302.1933 226.0118 -1.4937 293.2548 294.7485 302.3271 226.8035 -1.4930 293.3555 294.8485 302.4544 227.6258 -1.4936 293.4679 294.9615 302.5984 228.4175 -1.4933 293.5525 295.0458 302.7505 229.2395 -1.4931 293.6625 295.1556 302.8839 230.0308 -1.4930 293.7538 295.2468 303.0050 230.8190 -1.4932 293.8387 295.3320 303.1346 231.6225 -1.4948 293.9546 295.4494 303.2717 232.4413 -1.4945 294.0406 295.5350 303.3880 233.2000 -1.4952 294.1204 295.6156 303.5217 234.0488 -1.4972 294.2366 295.7338 303.6688 234.8070 -1.4975 294.3296 295.8270 303.7976 235.6258 -1.4997 294.4298 295.9296 303.9193 236.4143 -1.5004 294.5216 296.0220 304.0598 237.2030 -1.5000 294.6251 296.1251 304.1918 238.0518 -1.5017 294.7298 296.2315 304.3091 238.8110 -1.5030 294.8280 296.3310 304.4295 239.6298 -1.5040 294.9143 296.4183 304.5655 240.4183 -1.5023 295.0307 296.5330 304.6834 241.2255 -1.5040 295.1350 296.6389 304.8238 242.0080 -1.5052 295.2446 296.7498 304.9332 242.8578 -1.5030 295.3458 296.8488 305.0685 243.6190 -1.5013 295.4408 296.9422 305.2053 244.4405 -1.5026 295.5368 297.0394 305.3136 245.2320 -1.5049 295.6448 297.1498 305.4316 246.0233 -1.5081 295.7359 297.2440 305.5637 246.8445 -1.5099 295.8425 297.3524 305.6954 247.6365 -1.5106 295.9483 297.4589 305.8213 248.4585 -1.5108 296.0567 297.5675 305.9380 249.2505 -1.5102 296.1513 297.6615 306.0712 250.0423 -1.5120 296.2581 297.7701 306.1866 250.8645 -1.5132 296.3684 297.8816 306.3044 251.6588 -1.5132 296.4572 297.9703 306.4270 252.4528 -1.5159 296.5779 298.0938 306.5531 253.2748 -1.5175 296.6708 298.1883 306.6795 254.0673 -1.5150 296.7738 298.2888 306.8038 254.8585 -1.5147 296.8834 298.3981 306.9116 255.6810 -1.5155 296.9855 298.5010 307.0305 256.4425 -1.5138 297.0801 298.5940 307.1510 257.2950 -1.5139 297.1863 298.7002 307.2739 258.0868 -1.5170 297.2936 298.8106 307.3917 258.8785 -1.5165 297.4048 298.9213 307.5235 259.7008 -1.5205 297.5245 299.0451 307.6528 260.4625 -1.5221 297.6116 299.1338 307.7670 261.3153 -1.5216 297.7441 299.2657 307.9136 262.1035 -1.5231 297.8429 299.3660 308.0132 262.9108 -1.5250 297.9371 299.4621 308.1451 263.7025 -1.5253 298.0530 299.5783 308.2969 264.5248 -1.5278 298.1640 299.6918 308.4471 265.2865 -1.5264 298.2708 299.7972 308.5830 266.1385 -1.5240 298.3851 299.9092 308.7222 266.9305 -1.5249 298.4812 300.0061 308.8532 267.7225 -1.5260 298.5840 300.1100 309.0008 268.5445 -1.5272 298.7031 300.2303 309.1418 269.3365 -1.5301 298.8107 300.3409 309.2887 270.1585 -1.5280 298.9159 300.4439 309.4249 270.9505 -1.5292 299.0211 300.5503 309.5637 271.7438 -1.5308 299.1404 300.6711 309.7175 272.5570 -1.5325 299.2374 300.7699 309.8725 273.3795 -1.5325 299.3597 300.8922 310.0190 274.1415 -1.5342 299.4498 300.9840 310.1483 274.9935 -1.5336 299.5804 301.1140 310.3273 275.7555 -1.5339 299.6700 301.2039 310.4707 276.5768 -1.5346 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