DTA measure 31meres Date: 20241022:1541 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.09 s Mass = 958.000 mg data_number = 1023 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2946 -3.9843 417.5700 421.5543 423.6174 3.9916 -3.9894 417.9235 421.9129 423.6048 5.7025 -3.9911 418.2588 422.2499 423.5864 7.3116 -3.9996 418.5523 422.5518 423.5442 8.9199 -4.0015 418.8482 422.8497 423.4901 10.5179 -4.0105 419.1682 423.1787 423.3844 12.1164 -4.0111 419.4597 423.4707 423.2456 13.7406 -4.0133 419.7523 423.7657 423.0991 15.3379 -4.0167 420.0504 424.0671 422.9361 16.9358 -4.0222 420.3298 424.3520 422.7491 18.5496 -4.0274 420.6219 424.6493 422.5569 20.1488 -4.0263 420.9004 424.9266 422.3540 21.7626 -4.0260 421.1777 425.2037 422.1144 23.3768 -4.0281 421.4452 425.4733 421.8929 24.9755 -4.0303 421.7101 425.7403 421.6507 26.5896 -4.0339 421.9843 426.0182 421.4087 28.1885 -4.0344 422.2338 426.2682 421.1905 29.8025 -4.0378 422.4910 426.5289 420.9603 31.4165 -4.0397 422.7489 426.7886 420.7289 33.0156 -4.0393 422.9809 427.0202 420.5204 34.7165 -4.0440 423.2341 427.2780 420.3104 36.4320 -4.0463 423.4865 427.5328 420.1243 38.0459 -4.0486 423.7092 427.7578 419.9298 39.6448 -4.0537 423.9265 427.9802 419.7555 41.2436 -4.0575 424.1508 428.2083 419.5985 42.8581 -4.0584 424.3775 428.4359 419.4217 44.4576 -4.0631 424.5855 428.6486 419.2468 46.0716 -4.0683 424.7920 428.8603 419.0454 47.6859 -4.0724 424.9870 429.0594 418.8637 49.2855 -4.0802 425.1643 429.2445 418.6907 50.8849 -4.0845 425.3566 429.4411 418.5144 52.4995 -4.0846 425.5387 429.6233 418.3151 54.1143 -4.0923 425.7355 429.8278 418.1288 55.7135 -4.0953 425.9099 430.0052 417.9230 57.3241 -4.1008 426.0854 430.1862 417.7168 58.9159 -4.1040 426.2551 430.3591 417.5239 60.5063 -4.1085 426.4113 430.5197 417.3268 62.1285 -4.1130 426.5670 430.6800 417.1174 63.7209 -4.1186 426.7371 430.8556 416.9359 65.3276 -4.1223 426.8910 431.0133 416.7356 66.9205 -4.1273 427.0219 431.1492 416.5506 68.5140 -4.1358 427.1575 431.2932 416.3819 70.1395 -4.1417 427.2948 431.4365 416.2092 71.7496 -4.1469 427.4241 431.5710 416.0302 73.3463 -4.1532 427.5570 431.7102 415.8343 74.9446 -4.1597 427.6870 431.8467 415.6443 76.5439 -4.1648 427.7939 431.9588 415.4434 78.1736 -4.1704 427.9347 432.1051 415.2379 79.7728 -4.1745 428.0431 432.2176 415.0364 81.3866 -4.1819 428.1540 432.3360 414.8532 82.9856 -4.1872 428.2424 432.4296 414.6600 84.5845 -4.1940 428.3597 432.5537 414.4916 86.3629 -4.1996 428.4633 432.6629 414.2662 88.0115 -4.2065 428.5485 432.7550 414.0862 89.6255 -4.2138 428.6333 432.8471 413.8856 91.2245 -4.2182 428.7112 432.9294 413.6724 92.8384 -4.2258 428.7932 433.0190 413.4754 94.4523 -4.2343 428.8784 433.1128 413.2759 96.0659 -4.2386 428.9583 433.1970 413.0561 97.6658 -4.2458 429.0227 433.2685 412.8445 99.2648 -4.2561 429.0874 433.3435 412.6371 100.8786 -4.2642 429.1436 433.4077 412.4274 102.4926 -4.2740 429.2110 433.4850 412.2479 104.1076 -4.2844 429.2525 433.5369 412.0208 105.7065 -4.2873 429.3102 433.5975 411.8321 107.3055 -4.2881 429.3600 433.6481 411.6396 108.9503 -4.2925 429.4089 433.7014 411.4368 110.5495 -4.2977 429.4458 433.7435 411.2512 112.1638 -4.3031 429.4875 433.7907 411.0668 113.7639 -4.3097 429.5184 433.8281 410.8893 115.3633 -4.3180 429.5440 433.8620 410.7053 117.1291 -4.3237 429.5877 433.9114 410.5005 118.7899 -4.3309 429.6049 433.9358 410.3044 120.3895 -4.3347 429.6259 433.9606 410.1151 121.9830 -4.3404 429.6398 433.9802 409.8964 123.5891 -4.3459 429.6530 433.9989 409.7053 125.1960 -4.3540 429.6763 434.0303 409.5219 126.7885 -4.3577 429.6665 434.0242 409.3360 128.3994 -4.3659 429.6831 434.0490 409.1390 129.9915 -4.3769 429.6886 434.0655 408.9441 131.5993 -4.3839 429.6893 434.0732 408.7616 133.2094 -4.3875 429.6695 434.0570 408.5752 134.8193 -4.3924 429.6826 434.0750 408.3677 136.4424 -4.3995 429.6666 434.0661 408.1734 138.2186 -4.4043 429.6264 434.0307 407.9549 139.8175 -4.4099 429.6343 434.0441 407.7412 141.4315 -4.4148 429.6227 434.0375 407.5250 143.0455 -4.4192 429.5957 434.0149 407.3154 144.6445 -4.4255 429.5800 434.0054 407.0955 146.2585 -4.4294 429.5542 433.9836 406.8897 147.8606 -4.4333 429.5287 433.9620 406.6758 149.4604 -4.4375 429.4932 433.9307 406.4693 151.0891 -4.4427 429.4668 433.9095 406.2589 152.6880 -4.4487 429.4382 433.8869 406.0597 154.2868 -4.4525 429.3859 433.8384 405.8671 155.9006 -4.4546 429.3407 433.7953 405.6613 157.6006 -4.4585 429.3098 433.7683 405.4558 159.3308 -4.4648 429.2518 433.7167 405.2372 160.9296 -4.4707 429.2094 433.6801 405.0451 162.5436 -4.4726 429.1615 433.6341 404.8434 164.1431 -4.4771 429.1011 433.5782 404.6515 165.7575 -4.4824 429.0552 433.5377 404.4753 167.4238 -4.4893 428.9868 433.4761 404.2704 169.0235 -4.4935 428.9330 433.4266 404.0909 170.6225 -4.4993 428.8666 433.3660 403.8787 172.2515 -4.5040 428.8028 433.3068 403.6856 173.8511 -4.5089 428.7436 433.2525 403.4713 175.4668 -4.5122 428.6601 433.1723 403.2612 177.0661 -4.5196 428.5892 433.1088 403.0545 178.6758 -4.5192 428.5295 433.0487 402.8568 180.2856 -4.5201 428.4594 432.9796 402.6454 181.8846 -4.5238 428.3759 432.8998 402.4356 183.4991 -4.5297 428.3071 432.8368 402.2297 185.0966 -4.5300 428.2440 432.7740 402.0438 186.7030 -4.5315 428.1633 432.6947 401.8323 188.3034 -4.5355 428.0674 432.6029 401.6315 189.8878 -4.5366 427.9913 432.5279 401.4445 191.5104 -4.5416 427.9023 432.4439 401.2525 193.1181 -4.5446 427.8223 432.3669 401.0524 194.7121 -4.5463 427.7312 432.2775 400.8605 196.3060 -4.5485 427.6448 432.1932 400.6774 197.9265 -4.5505 427.5382 432.0887 400.4867 199.5246 -4.5538 427.4499 432.0037 400.3038 201.1225 -4.5567 427.3604 431.9171 400.1004 202.7189 -4.5592 427.2529 431.8121 399.8993 204.3475 -4.5629 427.1636 431.7265 399.6765 205.9465 -4.5636 427.0831 431.6466 399.4768 207.5454 -4.5632 426.9701 431.5333 399.2742 209.1520 -4.5627 426.8687 431.4314 399.0546 210.7639 -4.5658 426.7629 431.3287 398.8577 212.3778 -4.5673 426.6556 431.2229 398.6444 213.9768 -4.5666 426.5583 431.1250 398.4231 215.5756 -4.5680 426.4426 431.0106 398.2261 217.2046 -4.5707 426.3433 430.9140 398.0157 218.8015 -4.5674 426.2326 430.8000 397.8078 220.4165 -4.5704 426.1163 430.6867 397.6122 222.0306 -4.5736 425.9920 430.5655 397.3997 223.6448 -4.5723 425.8916 430.4639 397.2004 225.2445 -4.5746 425.7826 430.3572 397.0126 226.8435 -4.5743 425.6539 430.2282 396.8090 228.4581 -4.5733 425.5325 430.1059 396.6180 230.0759 -4.5767 425.4146 429.9914 396.4348 231.6786 -4.5769 425.2847 429.8616 396.2351 233.2768 -4.5771 425.1714 429.7484 396.0430 234.9056 -4.5769 425.0529 429.6298 395.8265 236.5048 -4.5778 424.9288 429.5066 395.6406 238.1189 -4.5779 424.8027 429.3806 395.4167 239.7081 -4.5794 424.6869 429.2663 395.2099 241.3368 -4.5796 424.5565 429.1361 394.9984 242.9365 -4.5794 424.4347 429.0141 394.7798 244.5505 -4.5793 424.2961 428.8754 394.5726 246.1500 -4.5788 424.1709 428.7497 394.3537 247.7495 -4.5767 424.0306 428.6073 394.1374 249.3700 -4.5765 423.8962 428.4726 393.9318 250.9698 -4.5734 423.7535 428.3269 393.7233 252.5608 -4.5731 423.6248 428.1980 393.5148 254.1669 -4.5744 423.5021 428.0765 393.2964 255.7744 -4.5718 423.3663 427.9381 393.0971 257.3701 -4.5719 423.2229 427.7948 392.8812 258.9771 -4.5699 423.0756 427.6455 392.6706 260.5833 -4.5671 422.9395 427.5066 392.4602 262.1819 -4.5671 422.8002 427.3673 392.2524 263.8055 -4.5676 422.6710 427.2386 392.0472 265.4184 -4.5678 422.5206 427.0883 391.8312 267.0168 -4.5619 422.3676 426.9295 391.6289 268.6291 -4.5627 422.2417 426.8044 391.4338 270.2276 -4.5611 422.0849 426.6460 391.2253 271.8266 -4.5594 421.9310 426.4904 391.0292 273.4406 -4.5556 421.7965 426.3521 390.8387 275.0546 -4.5572 421.6495 426.2067 390.6330 276.6536 -4.5542 421.5029 426.0572 390.4436 278.2676 -4.5529 421.3546 425.9075 390.2519 279.8718 -4.5509 421.2003 425.7512 390.0733 281.4725 -4.5472 421.0367 425.5839 389.8790 283.1015 -4.5461 420.8912 425.4372 389.6803 284.7005 -4.5431 420.7442 425.2873 389.4818 286.3145 -4.5424 420.5785 425.1209 389.2747 287.9135 -4.5396 420.4268 424.9664 389.0743 289.5123 -4.5361 420.2853 424.8214 388.8631 291.1409 -4.5339 420.1334 424.6673 388.6551 292.7549 -4.5332 419.9659 424.4991 388.4438 294.3546 -4.5301 419.7985 424.3286 388.2554 295.9536 -4.5288 419.6515 424.1804 388.0409 297.5676 -4.5245 419.4902 424.0146 387.8195 299.1968 -4.5211 419.3420 423.8631 387.6133 300.7886 -4.5192 419.1624 423.6816 387.3958 302.4095 -4.5159 418.9920 423.5080 387.1798 304.0085 -4.5151 418.8397 423.3548 386.9740 305.6078 -4.5112 418.6847 423.1959 386.7673 307.2225 -4.5068 418.5179 423.0247 386.5594 308.8221 -4.5057 418.3572 422.8630 386.3517 310.4513 -4.5043 418.1856 422.6899 386.1444 312.0510 -4.5012 418.0354 422.5366 385.9372 313.6503 -4.4991 417.8826 422.3816 385.7405 315.2431 -4.4957 417.7058 422.2015 385.5505 316.8491 -4.4917 417.5366 422.0283 385.3326 318.4560 -4.4906 417.3662 421.8568 385.1335 320.0621 -4.4873 417.2097 421.6970 384.9440 321.6454 -4.4858 417.0493 421.5351 384.7459 323.2613 -4.4829 416.8838 421.3667 384.5362 324.8545 -4.4804 416.6983 421.1786 384.3318 326.4490 -4.4780 416.5444 421.0225 384.1286 328.0721 -4.4767 416.3621 420.8387 383.9120 329.6830 -4.4720 416.1933 420.6653 383.6996 331.2806 -4.4665 416.0293 420.4958 383.4893 332.8786 -4.4635 415.8620 420.3255 383.2661 334.4775 -4.4590 415.7021 420.1611 383.0363 336.1066 -4.4582 415.5156 419.9738 382.8359 337.7055 -4.4550 415.3583 419.8133 382.6155 339.3195 -4.4508 415.1766 419.6274 382.3994 340.9185 -4.4501 415.0131 419.4632 382.1903 342.5208 -4.4427 414.8307 419.2734 381.9744 344.1345 -4.4400 414.6640 419.1039 381.7579 345.7335 -4.4360 414.4837 418.9197 381.5502 347.3621 -4.4305 414.3036 418.7341 381.3439 348.9610 -4.4283 414.1329 418.5612 381.1225 350.5598 -4.4185 413.9448 418.3633 380.9168 352.1741 -4.4155 413.7602 418.1757 380.7058 353.7888 -4.4131 413.5921 418.0052 380.4917 355.4028 -4.4073 413.4050 417.8124 380.2879 357.0016 -4.4019 413.2275 417.6294 380.0665 358.6156 -4.3985 413.0557 417.4541 379.8717 360.2145 -4.3947 412.8742 417.2689 379.6743 361.8323 -4.3904 412.7027 417.0931 379.4657 363.4415 -4.3856 412.5242 416.9098 379.2559 365.0555 -4.3832 412.3410 416.7242 379.0681 366.6545 -4.3776 412.1500 416.5276 378.8674 368.2684 -4.3738 411.9851 416.3590 378.6600 369.8670 -4.3690 411.8122 416.1812 378.4755 371.4808 -4.3655 411.6269 415.9924 378.2851 373.0958 -4.3614 411.4308 415.7922 378.0651 374.6958 -4.3552 411.2497 415.6050 377.8689 376.2956 -4.3537 411.0678 415.4215 377.6811 377.9083 -4.3493 410.8838 415.2331 377.4781 379.5000 -4.3462 410.7132 415.0595 377.2818 381.1060 -4.3420 410.5220 414.8640 377.0984 382.6961 -4.3362 410.3444 414.6806 376.8977 384.3121 -4.3317 410.1563 414.4880 376.6833 385.9041 -4.3287 409.9774 414.3061 376.4923 387.5118 -4.3264 409.8007 414.1271 376.2891 389.1056 -4.3216 409.6090 413.9307 376.0808 390.7130 -4.3164 409.4378 413.7541 375.8788 392.3228 -4.3124 409.2526 413.5650 375.6541 393.9188 -4.3082 409.0508 413.3590 375.4584 395.5316 -4.3049 408.8717 413.1766 375.2383 397.1613 -4.2970 408.6808 412.9778 375.0274 398.8045 -4.2948 408.4836 412.7784 374.8075 400.4035 -4.2911 408.2989 412.5900 374.6078 402.0025 -4.2849 408.1070 412.3919 374.3803 403.6164 -4.2808 407.9377 412.2185 374.1857 405.2301 -4.2759 407.7507 412.0267 373.9681 406.8299 -4.2711 407.5699 411.8410 373.7590 408.4436 -4.2665 407.3777 411.6442 373.5749 410.0426 -4.2634 407.1809 411.4443 373.3426 411.6716 -4.2591 406.9947 411.2538 373.1350 413.2709 -4.2538 406.8062 411.0600 372.9323 414.8866 -4.2502 406.6086 410.8588 372.7455 416.4856 -4.2459 406.4231 410.6691 372.5473 418.0846 -4.2398 406.2301 410.4698 372.3343 419.7144 -4.2351 406.0430 410.2780 372.1231 421.3285 -4.2309 405.8510 410.0819 371.9475 422.9275 -4.2300 405.6755 409.9055 371.7468 424.5415 -4.2237 405.4825 409.7062 371.5366 426.1555 -4.2197 405.2810 409.5008 371.3386 427.7705 -4.2173 405.0903 409.3076 371.1521 429.3708 -4.2131 404.9024 409.1155 370.9532 430.9860 -4.2079 404.7152 408.9231 370.7517 432.5861 -4.2047 404.5338 408.7385 370.5400 434.3253 -4.1996 404.3246 408.5242 370.3102 436.0146 -4.1964 404.1126 408.3090 370.1056 437.6286 -4.1919 403.9329 408.1248 369.8942 439.2276 -4.1878 403.7460 407.9339 369.6852 440.8415 -4.1810 403.5429 407.7239 369.4618 442.4520 -4.1781 403.3472 407.5253 369.2543 444.0589 -4.1722 403.1591 407.3313 369.0393 445.6508 -4.1683 402.9775 407.1458 368.8241 447.2429 -4.1620 402.7736 406.9356 368.5923 448.8359 -4.1579 402.5762 406.7341 368.3988 450.4595 -4.1509 402.3850 406.5359 368.1640 452.0670 -4.1488 402.2039 406.3527 367.9492 453.6596 -4.1401 402.0013 406.1414 367.7475 455.2691 -4.1345 401.8137 405.9482 367.5260 456.8638 -4.1331 401.6204 405.7535 367.3227 458.4760 -4.1287 401.4033 405.5319 367.1082 460.0888 -4.1220 401.2176 405.3396 366.9026 461.6870 -4.1194 401.0257 405.1451 366.6963 463.2856 -4.1145 400.8362 404.9507 366.4850 465.0171 -4.1075 400.6370 404.7445 366.2681 466.7068 -4.1026 400.4169 404.5195 366.0584 468.3208 -4.0953 400.2270 404.3223 365.8584 469.9196 -4.0906 400.0371 404.1278 365.6500 471.5185 -4.0830 399.8314 403.9144 365.4387 473.1478 -4.0783 399.6483 403.7266 365.2262 474.7466 -4.0730 399.4622 403.5353 365.0371 476.3455 -4.0702 399.2484 403.3186 364.8346 477.9595 -4.0624 399.0377 403.1001 364.6356 479.5585 -4.0590 398.8538 402.9128 364.4597 481.1878 -4.0525 398.6592 402.7117 364.2434 482.8035 -4.0459 398.4526 402.4985 364.0312 484.4023 -4.0409 398.2709 402.3118 363.8323 486.0196 -4.0349 398.0620 402.0969 363.6471 487.6345 -4.0305 397.8606 401.8911 363.4507 489.2498 -4.0255 397.6656 401.6911 363.2314 490.8496 -4.0191 397.4650 401.4841 363.0380 492.4490 -4.0138 397.2706 401.2844 362.8248 494.0643 -4.0094 397.0845 401.0939 362.6081 495.6964 -4.0030 396.8772 400.8802 362.3806 497.2706 -3.9979 396.6741 400.6720 362.1773 498.9004 -3.9923 396.4882 400.4805 361.9649 500.5004 -3.9872 396.2755 400.2627 361.7603 502.1145 -3.9850 396.0825 400.0675 361.5352 503.7139 -3.9768 395.8872 399.8640 361.3275 505.3480 -3.9732 395.6757 399.6489 361.1029 506.9436 -3.9680 395.4851 399.4531 360.8771 508.5361 -3.9627 395.2728 399.2355 360.6802 510.1274 -3.9587 395.0801 399.0388 360.4721 511.7491 -3.9530 394.8949 398.8479 360.2631 513.3419 -3.9484 394.6922 398.6407 360.0488 514.9498 -3.9429 394.4841 398.4270 359.8399 516.5436 -3.9383 394.2896 398.2280 359.6259 518.1604 -3.9327 394.0879 398.0206 359.4327 519.7550 -3.9282 393.8830 397.8112 359.2236 521.3668 -3.9224 393.6904 397.6128 359.0055 522.9656 -3.9163 393.4960 397.4123 358.7910 524.5948 -3.9131 393.2931 397.2062 358.5841 526.1780 -3.9076 393.0960 397.0036 358.3968 527.8058 -3.9030 392.9001 396.8031 358.1576 529.4046 -3.8980 392.6850 396.5830 357.9576 531.0035 -3.8896 392.4989 396.3885 357.7590 532.6025 -3.8858 392.2919 396.1777 357.5531 534.2316 -3.8838 392.0925 395.9763 357.3565 535.8456 -3.8784 391.8911 395.7695 357.1579 537.4455 -3.8702 391.6968 395.5670 356.9372 539.0445 -3.8649 391.5002 395.3651 356.7399 540.6585 -3.8586 391.3017 395.1603 356.5385 542.2730 -3.8573 391.0985 394.9559 356.3363 543.8870 -3.8518 390.8942 394.7460 356.1304 545.4870 -3.8484 390.6972 394.5456 355.9372 547.0879 -3.8433 390.4968 394.3401 355.7411 548.7026 -3.8397 390.3084 394.1480 355.5413 550.3166 -3.8332 390.1030 393.9362 355.3437 551.9161 -3.8283 389.8986 393.7269 355.1361 553.5464 -3.8221 389.6923 393.5145 354.9043 555.1456 -3.8167 389.4957 393.3123 354.6980 556.7595 -3.8128 389.3030 393.1158 354.4996 558.3585 -3.8090 389.0967 392.9058 354.2743 559.9731 -3.8032 388.9108 392.7140 354.0679 561.5875 -3.7988 388.6869 392.4856 353.8512 563.2016 -3.7941 388.4866 392.2807 353.6361 564.8011 -3.7884 388.2955 392.0839 353.4109 566.4153 -3.7825 388.0824 391.8649 353.1971 568.0265 -3.7775 387.8736 391.6512 352.9870 569.6261 -3.7725 387.6879 391.4604 352.7686 571.2539 -3.7662 387.4759 391.2421 352.5656 572.8456 -3.7620 387.2693 391.0314 352.3347 574.4383 -3.7570 387.0826 390.8396 352.1213 576.0455 -3.7495 386.8751 390.6247 351.9205 577.6378 -3.7439 386.6787 390.4226 351.7105 579.2448 -3.7406 386.4755 390.2161 351.5059 580.8529 -3.7345 386.2747 390.0092 351.2892 582.4628 -3.7290 386.0729 389.8019 351.0814 584.0585 -3.7255 385.8737 389.5992 350.8814 585.6543 -3.7180 385.6695 389.3875 350.6768 587.2709 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256.7943 258.0054 222.4442 1600.4900 -1.2066 256.6016 257.8081 222.2499 1602.0985 -1.2035 256.4093 257.6129 222.0557 1603.6910 -1.2030 256.2143 257.4173 221.8828 1605.3150 -1.2018 256.0006 257.2024 221.6958 1606.9079 -1.1954 255.8130 257.0084 221.5200 1608.5015 -1.1923 255.6185 256.8108 221.3361 1610.1126 -1.1933 255.4181 256.6114 221.1463 1611.8349 -1.1945 255.1958 256.3902 220.9327 1613.5371 -1.1921 254.9846 256.1767 220.7517 1615.1341 -1.1874 254.7964 255.9837 220.5651 1616.7316 -1.1827 254.5902 255.7729 220.3855 1618.3306 -1.1806 254.3850 255.5655 220.2110 1619.9446 -1.1748 254.1874 255.3622 220.0304 1621.5588 -1.1723 253.9873 255.1597 219.8322 1623.1728 -1.1699 253.8015 254.9714 219.6474 1624.7716 -1.1737 253.6003 254.7740 219.4685 1626.3706 -1.1697 253.3992 254.5689 219.2895 1627.9845 -1.1648 253.2057 254.3705 219.1134 1629.5986 -1.1622 253.0007 254.1629 218.9260 1631.2125 -1.1604 252.8019 253.9623 218.7402 1633.0141 -1.1548 252.5808 253.7357 218.5499 1634.6135 -1.1498 252.3945 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