DTA measure 1Pb_gyors_fel_le Date: 20241210:1221 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 744.36 s Mass = 100.000 mg data_number = 1841 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.7600 -1.5786 237.5955 239.1740 262.3704 1.1235 -1.5780 237.6575 239.2354 262.3501 1.4880 -1.5752 237.6901 239.2653 262.3354 1.9720 -1.5735 237.7452 239.3187 262.3468 2.3360 -1.5746 237.7890 239.3635 262.3369 2.7000 -1.5764 237.8340 239.4103 262.3377 3.1240 -1.5743 237.8862 239.4605 262.3334 3.5480 -1.5715 237.9258 239.4973 262.3156 3.9120 -1.5703 237.9627 239.5330 262.3094 4.3360 -1.5672 238.0274 239.5946 262.3109 4.7600 -1.5654 238.0832 239.6486 262.3080 5.1240 -1.5674 238.1476 239.7150 262.3115 5.4880 -1.5652 238.1835 239.7487 262.3007 5.9725 -1.5640 238.2432 239.8072 262.3057 6.3360 -1.5640 238.2948 239.8588 262.3124 6.7000 -1.5634 238.3309 239.8943 262.3033 7.1840 -1.5641 238.3784 239.9425 262.3101 7.5480 -1.5629 238.4253 239.9882 262.3160 7.9120 -1.5609 238.4715 240.0323 262.3307 8.3365 -1.5602 238.5355 240.0957 262.3630 8.7610 -1.5589 238.5989 240.1578 262.3537 9.1250 -1.5547 238.6430 240.1977 262.3544 9.4890 -1.5533 238.6907 240.2440 262.3558 9.9735 -1.5538 238.7291 240.2829 262.3684 10.3390 -1.5550 238.7895 240.3446 262.3765 10.7030 -1.5540 238.8446 240.3986 262.3909 11.1870 -1.5531 238.9060 240.4591 262.4176 11.5520 -1.5536 238.9285 240.4820 262.4359 11.9160 -1.5529 238.9757 240.5285 262.4580 12.3405 -1.5524 239.0413 240.5937 262.4830 12.7650 -1.5543 239.0957 240.6500 262.4995 13.1290 -1.5514 239.1457 240.6971 262.5198 13.5530 -1.5513 239.1921 240.7434 262.5732 13.9775 -1.5470 239.2422 240.7892 262.5910 14.3420 -1.5491 239.2807 240.8298 262.6078 14.7060 -1.5495 239.3280 240.8775 262.6361 15.1900 -1.5506 239.3820 240.9326 262.6852 15.5550 -1.5510 239.4185 240.9695 262.7129 15.9190 -1.5521 239.4725 241.0246 262.7496 16.4030 -1.5502 239.5113 241.0615 262.8028 16.7680 -1.5495 239.5650 241.1144 262.8258 17.1320 -1.5489 239.6022 241.1511 262.8662 17.5570 -1.5450 239.6450 241.1900 262.9091 17.9825 -1.5435 239.6975 241.2411 262.9666 18.3480 -1.5444 239.7356 241.2799 263.0309 18.7735 -1.5423 239.8053 241.3476 263.0841 19.1985 -1.5414 239.8558 241.3972 263.1427 19.5630 -1.5422 239.9100 241.4522 263.1986 19.9275 -1.5413 239.9703 241.5116 263.2302 20.4135 -1.5432 240.0474 241.5906 263.2968 20.7795 -1.5376 240.0795 241.6171 263.3565 21.1455 -1.5392 240.1071 241.6464 263.4185 21.5715 -1.5400 240.1639 241.7039 263.4808 21.9975 -1.5423 240.2079 241.7503 263.5499 22.3635 -1.5431 240.2489 241.7920 263.6059 22.7895 -1.5420 240.3005 241.8425 263.6624 23.2155 -1.5433 240.3455 241.8889 263.7274 23.5815 -1.5442 240.3890 241.9333 263.8049 23.9885 -1.5422 240.4379 241.9800 263.8744 24.3555 -1.5416 240.4896 242.0312 263.9481 24.8415 -1.5416 240.5467 242.0884 264.0248 25.2075 -1.5430 240.5792 242.1222 264.0593 25.5735 -1.5449 240.6323 242.1773 264.1419 25.9995 -1.5454 240.6725 242.2179 264.2212 26.4250 -1.5470 240.7343 242.2813 264.2924 26.7910 -1.5477 240.7815 242.3292 264.3775 27.1575 -1.5458 240.8175 242.3632 264.4406 27.6435 -1.5429 240.8739 242.4168 264.5460 28.0090 -1.5446 240.9340 242.4786 264.6408 28.3745 -1.5446 240.9757 242.5204 264.7179 28.8615 -1.5473 241.0427 242.5899 264.8176 29.2265 -1.5453 241.0813 242.6266 264.8921 29.5925 -1.5471 241.1252 242.6723 264.9526 30.0190 -1.5459 241.1743 242.7202 265.0301 30.4450 -1.5444 241.2215 242.7658 265.1517 30.8105 -1.5433 241.2633 242.8066 265.2366 31.1765 -1.5445 241.3030 242.8474 265.3029 31.6635 -1.5445 241.3858 242.9303 265.4295 32.0285 -1.5445 241.4254 242.9699 265.5148 32.3945 -1.5458 241.4527 242.9985 265.5928 32.8815 -1.5487 241.5141 243.0628 265.6871 33.2465 -1.5522 241.5766 243.1289 265.7757 33.6125 -1.5518 241.6209 243.1727 265.8635 34.0415 -1.5490 241.6713 243.2203 265.9558 34.4715 -1.5485 241.7316 243.2801 266.0285 34.8365 -1.5517 241.7678 243.3195 266.1265 35.2025 -1.5537 241.8088 243.3625 266.2211 35.6895 -1.5538 241.8671 243.4209 266.3469 36.0545 -1.5558 241.8864 243.4422 266.4205 36.4205 -1.5576 241.9350 243.4926 266.5029 36.8470 -1.5571 241.9951 243.5523 266.5883 37.2730 -1.5572 242.0805 243.6377 266.7009 37.6385 -1.5577 242.1224 243.6800 266.7915 38.0650 -1.5561 242.1644 243.7206 266.8740 38.4910 -1.5593 242.2141 243.7734 266.9848 38.8565 -1.5618 242.2578 243.8197 267.0648 39.2225 -1.5598 242.3002 243.8601 267.1370 39.7095 -1.5594 242.3368 243.8962 267.2527 40.0745 -1.5621 242.3858 243.9479 267.3441 40.4405 -1.5691 242.4381 244.0072 267.4364 40.9275 -1.5665 242.4950 244.0614 267.5508 41.2925 -1.5658 242.5387 244.1045 267.6249 41.6585 -1.5670 242.5926 244.1596 267.7160 42.0850 -1.5682 242.6518 244.2200 267.8217 42.5110 -1.5693 242.6995 244.2688 267.9172 42.8765 -1.5703 242.7491 244.3194 268.0072 43.2425 -1.5705 242.7866 244.3571 268.0728 43.7295 -1.5698 242.8559 244.4258 268.1796 44.0945 -1.5712 242.8954 244.4666 268.2712 44.4605 -1.5695 242.9432 244.5127 268.3269 44.9470 -1.5723 243.0040 244.5763 268.4178 45.3125 -1.5759 243.0734 244.6494 268.5127 45.6785 -1.5775 243.1247 244.7022 268.5985 46.1045 -1.5788 243.1482 244.7270 268.6901 46.5315 -1.5786 243.1719 244.7506 268.7931 46.8975 -1.5802 243.2424 244.8226 268.8635 47.2635 -1.5827 243.2796 244.8623 268.9260 47.7495 -1.5833 243.3509 244.9342 269.0344 48.1155 -1.5887 243.4076 244.9963 269.1028 48.4815 -1.5881 243.4454 245.0335 269.1727 48.9675 -1.5858 243.5037 245.0895 269.2757 49.3335 -1.5845 243.5415 245.1259 269.3561 49.6995 -1.5890 243.5919 245.1809 269.4297 50.1255 -1.5894 243.6512 245.2405 269.5065 50.5520 -1.5913 243.6870 245.2784 269.5795 50.9195 -1.5923 243.7446 245.3368 269.6434 51.2855 -1.5933 243.7915 245.3848 269.7358 51.7715 -1.5967 243.8509 245.4476 269.8290 52.1375 -1.6012 243.8949 245.4961 269.9011 52.5035 -1.5998 243.9480 245.5478 269.9592 52.9895 -1.5988 244.0002 245.5990 270.0492 53.3555 -1.5997 244.0372 245.6369 270.1051 53.7215 -1.6006 244.0942 245.6948 270.1825 54.1475 -1.6006 244.1485 245.7490 270.2731 54.5735 -1.6034 244.2029 245.8064 270.3554 54.9395 -1.5979 244.2569 245.8548 270.3986 55.3055 -1.5996 244.2980 245.8976 270.4651 55.7915 -1.6010 244.3671 245.9681 270.5442 56.1575 -1.6047 244.3920 245.9967 270.6183 56.5235 -1.6067 244.4436 246.0503 270.6833 57.0095 -1.6061 244.5146 246.1207 270.7652 57.3755 -1.6074 244.5517 246.1591 270.8307 57.7415 -1.6099 244.5863 246.1962 270.8882 58.1675 -1.6102 244.6495 246.2598 270.9673 58.5935 -1.6096 244.7206 246.3302 271.0371 58.9595 -1.6113 244.7779 246.3891 271.0901 59.3850 -1.6119 244.8238 246.4357 271.1563 59.8110 -1.6149 244.8628 246.4777 271.2289 60.1765 -1.6151 244.9090 246.5241 271.2805 60.5425 -1.6216 244.9628 246.5844 271.3536 61.0295 -1.6209 245.0243 246.6452 271.4319 61.3945 -1.6198 245.0660 246.6859 271.4924 61.7605 -1.6208 245.1000 246.7208 271.5390 62.1870 -1.6220 245.1602 246.7822 271.6131 62.6135 -1.6208 245.2245 246.8453 271.6770 62.9795 -1.6252 245.2791 246.9043 271.7358 63.3455 -1.6271 245.3249 246.9520 271.7964 63.8325 -1.6297 245.3850 247.0146 271.8448 64.1975 -1.6310 245.4266 247.0575 271.8903 64.5610 -1.6329 245.4774 247.1103 271.9612 65.0485 -1.6311 245.5431 247.1742 272.0536 65.4130 -1.6330 245.5810 247.2140 272.0993 65.7770 -1.6321 245.6466 247.2788 272.1377 66.2010 -1.6341 245.6831 247.3172 272.1855 66.6250 -1.6336 245.7467 247.3803 272.2231 66.9890 -1.6358 245.7946 247.4304 272.2925 67.3530 -1.6367 245.8446 247.4814 272.3490 67.8350 -1.6409 245.8984 247.5392 272.4138 68.2010 -1.6430 245.9392 247.5822 272.4468 68.5650 -1.6437 245.9802 247.6239 272.5110 68.9870 -1.6434 246.0311 247.6744 272.5591 69.4130 -1.6449 246.0997 247.7446 272.6084 69.7770 -1.6449 246.1364 247.7813 272.6565 70.2015 -1.6484 246.1755 247.8238 272.7158 70.6250 -1.6468 246.2401 247.8870 272.7884 70.9890 -1.6483 246.2864 247.9347 272.8367 71.3530 -1.6503 246.3271 247.9774 272.8697 71.8380 -1.6533 246.3854 248.0387 272.9193 72.2020 -1.6530 246.4380 248.0910 272.9724 72.5660 -1.6529 246.5175 248.1704 273.0333 72.9905 -1.6537 246.5681 248.2219 273.0885 73.4140 -1.6556 246.6143 248.2698 273.1417 73.7780 -1.6563 246.6663 248.3226 273.2090 74.2025 -1.6577 246.7113 248.3690 273.2596 74.6260 -1.6591 246.7620 248.4211 273.3112 74.9975 -1.6602 246.8163 248.4765 273.3720 75.3700 -1.6616 246.8477 248.5093 273.4009 75.7945 -1.6636 246.8936 248.5571 273.4512 76.2190 -1.6632 246.9470 248.6102 273.5042 76.5830 -1.6640 246.9911 248.6551 273.5424 77.0075 -1.6626 247.0647 248.7273 273.6038 77.4315 -1.6628 247.1193 248.7821 273.6758 77.7960 -1.6621 247.1808 248.8429 273.7276 78.1600 -1.6639 247.2054 248.8693 273.7808 78.6450 -1.6636 247.2665 248.9301 273.8362 79.0090 -1.6655 247.3123 248.9778 273.8718 79.3730 -1.6676 247.3570 249.0246 273.9073 79.8590 -1.6681 247.4015 249.0696 273.9621 80.2230 -1.6698 247.4581 249.1279 274.0076 80.5870 -1.6689 247.5362 249.2052 274.0650 81.0125 -1.6701 247.6010 249.2710 274.1348 81.4370 -1.6701 247.6529 249.3229 274.2050 81.8020 -1.6711 247.6898 249.3609 274.2692 82.2265 -1.6721 247.7395 249.4116 274.3137 82.6520 -1.6733 247.7856 249.4589 274.3570 83.0175 -1.6735 247.8467 249.5202 274.3980 83.3825 -1.6740 247.8900 249.5639 274.4559 83.8695 -1.6772 247.9368 249.6139 274.5041 84.2345 -1.6785 247.9694 249.6478 274.5670 84.6005 -1.6812 248.0520 249.7332 274.6248 85.0270 -1.6839 248.1071 249.7910 274.6753 85.4530 -1.6836 248.1594 249.8429 274.7450 85.8185 -1.6868 248.2149 249.9017 274.8221 86.1845 -1.6881 248.2617 249.9498 274.8728 86.6715 -1.6890 248.3324 250.0214 274.9420 87.0365 -1.6901 248.3869 250.0770 274.9716 87.4025 -1.6898 248.4325 250.1223 275.0125 87.8290 -1.6868 248.4649 250.1517 275.0869 88.2550 -1.6870 248.5251 250.2121 275.1624 88.6205 -1.6904 248.5646 250.2550 275.2007 89.0470 -1.6889 248.6219 250.3108 275.2660 89.4730 -1.6897 248.6876 250.3773 275.3162 89.8385 -1.6910 248.7349 250.4259 275.3727 90.2045 -1.6913 248.7768 250.4680 275.4285 90.6910 -1.6930 248.8562 250.5492 275.5009 91.0565 -1.6961 248.8962 250.5924 275.5512 91.4225 -1.6942 248.9329 250.6270 275.6091 91.8490 -1.6932 248.9633 250.6565 275.7092 92.2750 -1.6958 249.0341 250.7299 275.7731 92.6405 -1.6981 249.0913 250.7893 275.8325 93.0065 -1.7000 249.1391 250.8391 275.8643 93.4925 -1.7007 249.2011 250.9017 275.9333 93.8585 -1.7028 249.2608 250.9636 276.0017 94.2245 -1.6996 249.3041 251.0037 276.0561 94.7110 -1.7016 249.3824 251.0840 276.1247 95.0765 -1.7042 249.4332 251.1375 276.1785 95.4425 -1.7062 249.4807 251.1869 276.2438 95.8685 -1.7046 249.5218 251.2265 276.2977 96.2950 -1.7071 249.5901 251.2972 276.3772 96.6605 -1.7085 249.6376 251.3461 276.4330 97.0265 -1.7080 249.6680 251.3760 276.5125 97.5125 -1.7096 249.7395 251.4491 276.5833 97.8785 -1.7115 249.7859 251.4973 276.6501 98.2445 -1.7118 249.8307 251.5425 276.7182 98.6705 -1.7132 249.8943 251.6075 276.7747 99.0965 -1.7110 249.9534 251.6644 276.8602 99.4625 -1.7134 249.9994 251.7128 276.9294 99.8885 -1.7160 250.0595 251.7755 277.0097 100.3145 -1.7174 250.1099 251.8273 277.0633 100.6805 -1.7182 250.1536 251.8718 277.1167 101.0465 -1.7173 250.2050 251.9224 277.1852 101.5325 -1.7201 250.2687 251.9888 277.2682 101.8985 -1.7217 250.3179 252.0396 277.3474 102.2645 -1.7224 250.3480 252.0704 277.4118 102.6905 -1.7236 250.4026 252.1263 277.4847 103.1165 -1.7268 250.4475 252.1742 277.5568 103.4825 -1.7273 250.5229 252.2503 277.6303 103.9085 -1.7287 250.5780 252.3068 277.7099 104.3345 -1.7300 250.6573 252.3873 277.7614 104.7005 -1.7267 250.6898 252.4165 277.8278 105.0665 -1.7270 250.7294 252.4564 277.8912 105.5525 -1.7283 250.8124 252.5406 277.9905 105.9185 -1.7286 250.8410 252.5696 278.0691 106.2845 -1.7294 250.8794 252.6088 278.1312 106.7105 -1.7316 250.9285 252.6600 278.2070 107.1365 -1.7379 250.9956 252.7336 278.2846 107.5025 -1.7388 251.0545 252.7933 278.3498 107.9285 -1.7382 251.1142 252.8524 278.4341 108.3545 -1.7358 251.1571 252.8929 278.4940 108.7195 -1.7343 251.2110 252.9453 278.5624 109.0855 -1.7304 251.2699 253.0003 278.6248 109.5725 -1.7277 251.3162 253.0440 278.7239 109.9375 -1.7271 251.3595 253.0866 278.7754 110.3035 -1.7248 251.4101 253.1349 278.8497 110.7325 -1.7240 251.4749 253.1989 278.9038 111.1600 -1.7247 251.5453 253.2700 278.9648 111.5255 -1.7287 251.5954 253.3241 279.0547 111.9520 -1.7331 251.6229 253.3560 279.1338 112.3780 -1.7379 251.6799 253.4178 279.2237 112.7435 -1.7439 251.7202 253.4641 279.2889 113.1095 -1.7493 251.7788 253.5281 279.3619 113.5965 -1.7508 251.8472 253.5980 279.4498 113.9615 -1.7500 251.9094 253.6595 279.5051 114.3275 -1.7524 251.9705 253.7229 279.5887 114.7540 -1.7551 252.0191 253.7742 279.6585 115.1800 -1.7561 252.0649 253.8210 279.7438 115.5455 -1.7582 252.1148 253.8729 279.8041 115.9720 -1.7585 252.1975 253.9560 279.8736 116.3980 -1.7599 252.2351 253.9950 279.9485 116.7635 -1.7654 252.2724 254.0378 280.0121 117.1295 -1.7659 252.3328 254.0987 280.0851 117.6165 -1.7659 252.3900 254.1560 280.1681 117.9815 -1.7691 252.4493 254.2184 280.2505 118.3475 -1.7729 252.4944 254.2673 280.3038 118.8345 -1.7717 252.5788 254.3505 280.3967 119.2005 -1.7732 252.6224 254.3956 280.4591 119.5665 -1.7730 252.6504 254.4234 280.5223 119.9925 -1.7748 252.7110 254.4858 280.5884 120.4190 -1.7764 252.7817 254.5581 280.6550 120.7845 -1.7779 252.8286 254.6064 280.7269 121.1505 -1.7798 252.8695 254.6493 280.7928 121.6370 -1.7811 252.9415 254.7226 280.8769 122.0025 -1.7823 252.9911 254.7734 280.9444 122.3685 -1.7826 253.0301 254.8127 280.9883 122.8550 -1.7840 253.0932 254.8772 281.0976 123.2205 -1.7882 253.1485 254.9367 281.1221 123.5865 -1.7905 253.1914 254.9818 281.1800 124.0125 -1.7915 253.2477 255.0392 281.2689 124.4390 -1.7935 253.3298 255.1233 281.3411 124.8045 -1.7944 253.3800 255.1744 281.3929 125.1705 -1.7945 253.4026 255.1971 281.4527 125.6565 -1.7960 253.4761 255.2721 281.5356 126.0225 -1.7951 253.5278 255.3229 281.6022 126.4285 -1.7939 253.5827 255.3765 281.6671 126.7945 -1.7965 253.6305 255.4269 281.7187 127.2805 -1.7983 253.7277 255.5260 281.8044 127.6465 -1.8017 253.7782 255.5799 281.8536 128.0125 -1.8027 253.8163 255.6190 281.8962 128.4385 -1.8043 253.8753 255.6796 281.9892 128.8630 -1.8061 253.9322 255.7383 282.0683 129.2280 -1.8072 253.9941 255.8013 282.1264 129.5930 -1.8083 254.0359 255.8442 282.1942 130.0740 -1.8116 254.0883 255.8999 282.2579 130.4410 -1.8166 254.1414 255.9579 282.3271 130.8050 -1.8160 254.1928 256.0088 282.3682 131.2290 -1.8136 254.2589 256.0725 282.4337 131.6530 -1.8139 254.3049 256.1188 282.4883 132.0170 -1.8158 254.3600 256.1759 282.5296 132.4410 -1.8158 254.4042 256.2200 282.6088 132.8650 -1.8171 254.4688 256.2859 282.6760 133.2290 -1.8180 254.5145 256.3325 282.7295 133.5930 -1.8200 254.5633 256.3833 282.8072 134.0770 -1.8211 254.6303 256.4513 282.8670 134.4410 -1.8225 254.6947 256.5171 282.9128 134.8050 -1.8234 254.7466 256.5700 282.9542 135.2890 -1.8215 254.8090 256.6306 283.0083 135.6540 -1.8271 254.8528 256.6799 283.0792 136.0180 -1.8281 254.9135 256.7416 283.1570 136.4420 -1.8273 254.9797 256.8070 283.2337 136.8665 -1.8266 255.0234 256.8499 283.2811 137.2310 -1.8289 255.0661 256.8950 283.3321 137.5950 -1.8321 255.1148 256.9468 283.3730 138.0790 -1.8320 255.1739 257.0059 283.4387 138.4440 -1.8341 255.2407 257.0747 283.4938 138.8080 -1.8354 255.2985 257.1339 283.5564 139.2920 -1.8324 255.3533 257.1857 283.6351 139.6560 -1.8358 255.4014 257.2372 283.6852 140.0200 -1.8379 255.4440 257.2819 283.7359 140.4445 -1.8384 255.5064 257.3448 283.7880 140.8695 -1.8430 255.5739 257.4169 283.8806 141.2350 -1.8436 255.6263 257.4700 283.9403 141.6590 -1.8417 255.7017 257.5434 283.9703 142.0835 -1.8446 255.7486 257.5932 284.0361 142.4480 -1.8469 255.7958 257.6428 284.0907 142.8125 -1.8474 255.8514 257.6988 284.1509 143.2975 -1.8482 255.9200 257.7682 284.2095 143.6630 -1.8496 255.9784 257.8280 284.2817 144.0285 -1.8540 256.0230 257.8771 284.3413 144.4545 -1.8505 256.0753 257.9258 284.4065 144.8805 -1.8509 256.1425 257.9934 284.4636 145.2460 -1.8521 256.2011 258.0532 284.5167 145.6705 -1.8517 256.2441 258.0958 284.5743 146.0965 -1.8545 256.2892 258.1437 284.6399 146.4615 -1.8551 256.3288 258.1839 284.6993 146.8265 -1.8581 256.3807 258.2388 284.7635 147.3125 -1.8602 256.4572 258.3174 284.8323 147.6785 -1.8623 256.5154 258.3777 284.8734 148.0445 -1.8664 256.5627 258.4291 284.9379 148.4705 -1.8666 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