DTA measure 1Pb_gyors_le Date: 20241210:149 Lower limit = 220.0 C Upper limit = 440.0 C Rate = 8.00 C/min Mtime = 1647.79 s Mass = 957.200 mg data_number = 1023 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4493 -6.4951 361.0345 367.5296 405.8980 4.0566 -6.4059 361.6235 368.0294 405.9480 5.6479 -6.3255 362.2175 368.5430 406.0078 7.2554 -6.2497 362.8199 369.0695 406.1218 8.8638 -6.1733 363.2875 369.4608 406.0795 10.4710 -6.1115 363.7986 369.9102 406.2049 12.0596 -6.0422 364.3822 370.4244 406.1529 13.6601 -5.9669 364.9165 370.8834 406.2192 15.2681 -5.9099 365.4156 371.3255 406.1325 16.8911 -5.8501 365.9178 371.7679 406.0899 18.4836 -5.7887 366.4313 372.2200 406.0464 20.0936 -5.7449 366.9887 372.7337 405.9175 21.6910 -5.6919 367.5334 373.2253 405.7870 23.3049 -5.6300 368.1321 373.7621 405.6772 24.9194 -5.5780 368.5119 374.0899 405.5069 26.5203 -5.5226 369.0390 374.5616 405.4104 28.1208 -5.4705 369.5660 375.0365 405.1736 29.7348 -5.4282 369.9357 375.3638 404.9676 31.3346 -5.3687 370.4235 375.7922 404.8227 32.9514 -5.3194 370.7577 376.0771 404.5075 34.5676 -5.2986 371.3703 376.6689 404.2383 36.1665 -5.2548 371.7964 377.0512 404.0262 37.7661 -5.2215 372.0957 377.3172 403.8063 39.3805 -5.1695 372.4766 377.6461 403.5447 40.9945 -5.1339 372.8695 378.0034 403.3823 42.6089 -5.1061 373.3926 378.4987 403.0115 44.2085 -5.0528 373.8168 378.8696 402.8071 45.8225 -5.0187 374.1661 379.1848 402.5832 47.4233 -4.9850 374.6646 379.6496 402.2753 49.0381 -4.9443 375.0026 379.9469 402.1117 50.6519 -4.9020 375.4481 380.3501 401.8894 52.2515 -4.8638 375.7627 380.6265 401.6665 53.8669 -4.8208 376.0493 380.8701 401.4423 55.4658 -4.7983 376.4181 381.2164 401.2483 57.0816 -4.7552 376.7630 381.5182 401.0262 58.6959 -4.7256 377.2867 382.0123 400.8391 60.3096 -4.6879 377.5356 382.2235 400.6375 61.9088 -4.6594 377.8593 382.5187 400.4692 63.4968 -4.6339 378.2404 382.8742 400.3954 65.1071 -4.6037 378.5333 383.1370 400.1337 66.7140 -4.5793 378.8781 383.4574 399.9831 68.3210 -4.5517 379.1874 383.7391 399.8935 69.9131 -4.5204 379.5510 384.0714 399.7055 71.5071 -4.5009 379.8167 384.3177 399.5583 73.1148 -4.4818 380.0938 384.5756 399.5008 74.7240 -4.4549 380.3779 384.8328 399.3323 76.3333 -4.4340 380.7237 385.1577 399.1701 77.9259 -4.4056 381.0712 385.4767 398.9462 79.5336 -4.3892 381.2770 385.6662 398.7601 81.1418 -4.3591 381.6053 385.9644 398.6041 82.7508 -4.3506 381.9042 386.2548 398.4456 84.3605 -4.3194 382.1459 386.4653 398.3243 85.9575 -4.3081 382.3425 386.6506 398.0670 87.5573 -4.2902 382.6832 386.9734 397.9629 89.1866 -4.2544 382.9092 387.1636 397.7191 90.7865 -4.2523 383.1182 387.3705 397.6327 92.3859 -4.2334 383.3820 387.6154 397.4545 94.0036 -4.2122 383.6116 387.8237 397.2693 95.6045 -4.1840 383.8656 388.0496 397.1000 97.2034 -4.1733 384.0759 388.2492 396.8379 98.8334 -4.1587 384.3165 388.4751 396.6998 100.4318 -4.1372 384.5345 388.6718 396.5848 102.0358 -4.1319 384.6921 388.8240 396.3871 103.6354 -4.0998 384.8650 388.9648 396.1516 105.2498 -4.0921 385.1138 389.2059 395.9777 106.8656 -4.0793 385.3037 389.3829 395.8079 108.4799 -4.0650 385.5182 389.5832 395.5970 110.0794 -4.0508 385.6931 389.7440 395.4721 111.6796 -4.0368 385.8194 389.8562 395.1876 113.2936 -4.0253 386.1223 390.1475 394.9618 114.9169 -3.9980 386.2752 390.2731 394.8162 116.5195 -3.9940 386.3648 390.3589 394.6422 118.1215 -3.9932 386.6350 390.6282 394.4373 119.7355 -3.9682 386.6901 390.6584 394.2486 121.3345 -3.9524 386.9175 390.8699 394.0782 122.9344 -3.9341 387.0856 391.0197 393.8427 124.5635 -3.9161 387.2348 391.1509 393.6072 126.1738 -3.9281 387.4175 391.3456 393.4502 127.7646 -3.8953 387.4968 391.3921 393.2724 129.3571 -3.8781 387.6679 391.5460 393.1423 130.9490 -3.8664 387.7727 391.6391 392.9990 132.5568 -3.8563 387.8838 391.7401 392.7843 134.1630 -3.8469 387.9927 391.8397 392.5599 135.7549 -3.8342 388.2296 392.0638 392.3680 137.3630 -3.8109 388.3885 392.1995 392.1292 138.9539 -3.7964 388.4301 392.2265 392.0066 140.5756 -3.7746 388.6061 392.3807 391.7804 142.1829 -3.7734 388.6526 392.4260 391.5972 143.7753 -3.7637 388.7783 392.5420 391.3886 145.3754 -3.7506 388.9159 392.6665 391.2050 146.9735 -3.7402 388.9269 392.6671 390.9796 148.6003 -3.7289 389.0056 392.7345 390.8496 150.1991 -3.7115 389.0867 392.7982 390.6519 151.7978 -3.7124 389.2253 392.9377 390.4390 153.4118 -3.7092 389.2562 392.9654 390.2059 155.0115 -3.6847 389.4031 393.0878 390.0886 156.6108 -3.6711 389.5379 393.2090 389.8930 158.2410 -3.6570 389.5232 393.1802 389.7586 159.8401 -3.6401 389.5892 393.2293 389.6205 161.4406 -3.6284 389.6302 393.2587 389.4303 163.0546 -3.6201 389.6898 393.3099 389.2383 164.6554 -3.6186 389.8327 393.4512 389.0025 166.2623 -3.6139 389.8526 393.4664 388.8556 167.8915 -3.5972 389.9176 393.5148 388.6355 169.4913 -3.5658 390.0579 393.6237 388.4155 171.0915 -3.5687 390.1152 393.6839 388.2078 172.6918 -3.5608 390.1016 393.6624 388.1483 174.3065 -3.5455 390.1300 393.6755 387.8990 175.9373 -3.5444 390.1062 393.6506 387.7280 177.5369 -3.5147 390.2260 393.7407 387.5820 179.1368 -3.5125 390.2690 393.7815 387.3444 180.7508 -3.5031 390.3295 393.8326 387.1060 182.3505 -3.4974 390.3073 393.8047 386.9473 183.9800 -3.4790 390.2848 393.7638 386.8431 185.5795 -3.4672 390.3684 393.8356 386.5792 187.1798 -3.4674 390.3781 393.8455 386.3577 188.7938 -3.4602 390.3328 393.7930 386.1232 190.3906 -3.4443 390.4483 393.8926 385.9658 192.0121 -3.4341 390.4628 393.8969 385.7334 193.6038 -3.4270 390.4098 393.8368 385.6021 195.1961 -3.4211 390.4189 393.8400 385.4087 196.8026 -3.4073 390.4499 393.8572 385.1696 198.3964 -3.4111 390.5105 393.9216 385.0158 200.0191 -3.3832 390.4616 393.8448 384.8322 201.6114 -3.3800 390.4845 393.8645 384.5978 203.2185 -3.3744 390.5123 393.8867 384.3974 204.8105 -3.3616 390.4341 393.7957 384.1618 206.4329 -3.3516 390.4746 393.8261 383.9963 208.0431 -3.3321 390.4376 393.7698 383.7717 209.6360 -3.3263 390.4544 393.7807 383.6556 211.2301 -3.3263 390.4404 393.7667 383.4301 212.8408 -3.3171 390.4275 393.7446 383.2103 214.4678 -3.3025 390.3696 393.6721 383.1935 216.0690 -3.2992 390.3997 393.6989 382.8723 217.6749 -3.2820 390.3338 393.6159 382.6274 219.2739 -3.2754 390.3570 393.6324 382.4362 220.8738 -3.2621 390.3011 393.5631 382.2334 222.4885 -3.2622 390.3544 393.6165 382.1536 224.1043 -3.2557 390.2488 393.5046 381.9027 225.7185 -3.2377 390.1878 393.4255 381.6836 227.3186 -3.2387 390.1627 393.4013 381.4947 228.9190 -3.2185 390.1568 393.3754 381.3147 230.5328 -3.2232 390.0886 393.3117 381.1142 232.1469 -3.1913 390.0465 393.2378 380.8796 233.7609 -3.1922 389.9653 393.1575 380.7771 235.3598 -3.1970 390.0357 393.2328 380.5135 236.9838 -3.1760 389.9054 393.0814 380.2950 238.5710 -3.1871 389.8845 393.0716 380.1091 240.1858 -3.1779 389.7867 392.9646 379.9288 241.8000 -3.1671 389.7617 392.9288 379.7017 243.4155 -3.1525 389.6877 392.8403 379.4931 245.0145 -3.1265 389.6353 392.7618 379.3149 246.6149 -3.1371 389.6340 392.7711 379.0940 248.2295 -3.1340 389.5880 392.7220 378.8559 249.8436 -3.1236 389.4673 392.5909 378.6681 251.4585 -3.1153 389.4286 392.5439 378.5146 253.0579 -3.1003 389.3980 392.4983 378.3189 254.6566 -3.0943 389.3337 392.4279 378.1701 256.2619 -3.0942 389.2321 392.3264 377.9863 257.8706 -3.0872 389.1788 392.2659 377.7631 259.4649 -3.0714 389.0814 392.1528 377.5977 261.0563 -3.0661 389.0128 392.0790 377.2826 262.6628 -3.0528 388.9986 392.0514 377.1563 264.2550 -3.0560 388.9481 392.0041 376.9607 265.8620 -3.0439 388.8090 391.8530 376.8767 267.4569 -3.0275 388.6541 391.6816 376.6890 269.0749 -3.0166 388.6471 391.6637 376.4128 270.6671 -3.0121 388.5834 391.5955 376.2148 272.2741 -3.0068 388.5371 391.5439 375.9292 273.8815 -3.0046 388.3830 391.3876 375.7509 275.4891 -2.9953 388.4073 391.4026 375.6331 277.0844 -2.9892 388.2983 391.2876 375.4442 278.6960 -2.9882 388.1770 391.1652 375.2172 280.2953 -2.9860 388.0554 391.0415 375.0363 281.8969 -2.9698 387.9848 390.9546 374.8525 283.5119 -2.9596 387.9419 390.9015 374.7113 285.1259 -2.9528 387.8138 390.7666 374.4641 286.7258 -2.9547 387.7338 390.6885 374.2830 288.3258 -2.9513 387.5489 390.5002 374.0591 289.9254 -2.9416 387.4644 390.4060 373.7413 291.5546 -2.9301 387.3069 390.2370 373.5394 293.1535 -2.9156 387.2685 390.1840 373.3532 294.7675 -2.9120 387.1966 390.1086 373.0970 296.3666 -2.9087 387.0894 389.9981 373.0055 297.9668 -2.8907 386.9751 389.8658 372.7943 299.5995 -2.8814 386.8695 389.7508 372.6124 301.2014 -2.8776 386.8635 389.7411 372.4844 302.8040 -2.8762 386.7138 389.5900 372.2897 304.4185 -2.8764 386.5795 389.4559 372.0352 306.0175 -2.8547 386.3955 389.2503 371.8796 307.6460 -2.8725 386.3164 389.1889 371.7626 309.2459 -2.8748 386.2457 389.1204 371.5604 310.8598 -2.8502 386.0982 388.9485 371.4564 312.4588 -2.8455 385.9952 388.8407 371.1989 314.0578 -2.8433 385.9556 388.7988 370.9906 315.6869 -2.8197 385.7616 388.5812 370.8420 317.2878 -2.8123 385.7133 388.5255 370.6942 318.9090 -2.8000 385.6342 388.4343 370.3838 320.4991 -2.8115 385.5653 388.3769 370.1554 322.0910 -2.7871 385.4048 388.1919 370.0899 323.6831 -2.7971 385.2471 388.0442 369.9183 325.3509 -2.8005 385.0775 387.8781 369.6604 326.9445 -2.7786 384.9604 387.7390 369.4704 328.5384 -2.7737 384.8880 387.6617 369.1872 330.1601 -2.7670 384.7168 387.4838 369.0519 331.7684 -2.7530 384.6590 387.4120 368.7416 333.3603 -2.7489 384.5150 387.2639 368.5171 334.9676 -2.7435 384.3929 387.1364 368.2656 336.5756 -2.7335 384.2842 387.0177 368.1421 338.1838 -2.7382 384.1109 386.8491 367.7952 339.7926 -2.7291 384.0492 386.7782 367.6713 341.3885 -2.7082 383.8647 386.5729 367.4988 342.9876 -2.7204 383.7556 386.4760 367.1252 344.6166 -2.7011 383.5712 386.2723 367.0100 346.2165 -2.7062 383.4416 386.1477 366.7630 347.8155 -2.6965 383.2633 385.9598 366.4918 349.4336 -2.6969 383.0917 385.7887 366.4212 351.0225 -2.6852 383.0330 385.7182 366.1110 352.6365 -2.6817 382.9134 385.5951 365.8779 354.2523 -2.6702 382.8071 385.4773 365.7836 355.8521 -2.6578 382.6367 385.2945 365.4986 357.4673 -2.6660 382.4689 385.1349 365.3271 359.0658 -2.6568 382.4062 385.0630 365.1055 360.6655 -2.6570 382.3350 384.9919 364.9638 362.2959 -2.6443 382.0311 384.6753 364.7211 363.8968 -2.6355 381.8841 384.5196 364.5614 365.5108 -2.6335 381.8476 384.4811 364.4295 367.1104 -2.6369 381.6083 384.2452 364.1978 368.7098 -2.6359 381.5055 384.1414 363.9830 370.3210 -2.6068 381.3501 383.9569 363.6385 371.9459 -2.6142 381.2608 383.8750 363.5110 373.5456 -2.6086 381.0494 383.6580 363.3886 375.1450 -2.6036 380.9447 383.5484 363.2247 376.7595 -2.5984 380.8319 383.4303 362.9986 378.3585 -2.5952 380.6598 383.2549 362.7141 379.9734 -2.5901 380.4652 383.0553 362.7366 381.5878 -2.5832 380.3241 382.9073 362.3820 383.1841 -2.5778 380.2014 382.7792 362.2479 384.7910 -2.5651 380.1131 382.6782 362.0263 386.3826 -2.5710 379.9799 382.5509 361.8582 387.9890 -2.5764 379.7531 382.3295 361.7278 389.5953 -2.5483 379.6256 382.1739 361.4913 391.1911 -2.5374 379.5215 382.0589 361.2877 392.7914 -2.5287 379.3746 381.9033 361.1294 394.4009 -2.5362 379.1141 381.6504 360.8718 395.9945 -2.5252 378.9937 381.5189 360.7456 397.6016 -2.5112 378.8873 381.3984 360.5454 399.2089 -2.5178 378.7214 381.2392 360.3473 400.8163 -2.5128 378.6128 381.1256 360.1472 402.4084 -2.5058 378.4496 380.9555 359.9009 404.0040 -2.5099 378.2916 380.8015 359.6859 405.6295 -2.5022 378.0744 380.5766 359.4831 407.2264 -2.4884 377.9153 380.4037 359.3612 408.8408 -2.4870 377.8001 380.2871 359.1619 410.4398 -2.4859 377.6344 380.1203 358.9034 412.0388 -2.4800 377.5716 380.0515 358.6954 413.6529 -2.4822 377.3646 379.8468 358.5473 415.2671 -2.4700 377.1816 379.6515 358.2065 416.8668 -2.4681 376.9970 379.4650 358.0641 418.4668 -2.4577 376.8380 379.2957 357.9167 420.0816 -2.4478 376.6961 379.1439 357.6564 421.6949 -2.4340 376.5949 379.0289 357.4781 423.2890 -2.4481 376.3395 378.7876 357.2830 424.9185 -2.4458 376.2269 378.6728 357.0770 426.5179 -2.4362 376.0773 378.5135 356.8700 428.1175 -2.4272 375.8872 378.3144 356.6123 429.7166 -2.4137 375.8015 378.2151 356.4066 431.3305 -2.4126 375.6712 378.0839 356.2031 432.9454 -2.4051 375.4765 377.8816 356.0200 434.5595 -2.3922 375.2354 377.6276 355.8290 436.1586 -2.4049 375.0943 377.4993 355.6146 437.7571 -2.3976 374.9307 377.3283 355.4937 439.3708 -2.3844 374.7639 377.1483 355.1979 440.9849 -2.3832 374.6056 376.9889 355.0472 442.5839 -2.3824 374.4725 376.8548 354.8708 444.1978 -2.3703 374.2602 376.6305 354.6000 445.7981 -2.3650 374.1226 376.4877 354.3617 447.3945 -2.3496 373.8636 376.2132 354.1949 449.0014 -2.3426 373.7282 376.0708 353.9480 450.6078 -2.3461 373.4821 375.8282 353.7327 452.2001 -2.3390 373.3498 375.6888 353.5622 453.8061 -2.3538 373.1319 375.4857 353.2984 455.3999 -2.3362 372.9983 375.3345 353.0752 457.0080 -2.3335 372.8289 375.1624 353.0348 458.6155 -2.3250 372.5988 374.9239 352.7755 460.2096 -2.3256 372.5255 374.8511 352.6144 461.8181 -2.3165 372.3504 374.6669 352.3246 463.4106 -2.3135 372.1717 374.4852 352.0962 465.0336 -2.2991 372.0271 374.3262 351.9169 466.6305 -2.3104 371.9332 374.2436 351.7798 468.2421 -2.3022 371.6908 373.9930 351.5363 469.8389 -2.2886 371.6015 373.8901 351.3523 471.4370 -2.2928 371.4624 373.7552 351.1434 473.0553 -2.2860 371.1738 373.4598 350.8456 474.6595 -2.2789 371.1183 373.3972 350.5915 476.2736 -2.2698 371.0266 373.2964 350.4699 477.8725 -2.2773 370.7391 373.0164 350.3182 479.4715 -2.2694 370.5248 372.7942 350.2099 481.0855 -2.2525 370.4324 372.6849 349.8782 482.6853 -2.2656 370.2290 372.4946 349.6206 484.3145 -2.2449 370.0310 372.2760 349.4443 485.9140 -2.2351 369.9031 372.1382 349.2555 487.5130 -2.2410 369.6533 371.8943 349.1199 489.1268 -2.2393 369.6016 371.8409 348.8990 490.7258 -2.2167 369.4949 371.7116 348.7000 492.3401 -2.2231 369.2597 371.4828 348.5354 493.9499 -2.2104 368.9584 371.1689 348.3217 495.5639 -2.2110 368.8370 371.0480 348.2120 497.1634 -2.2195 368.6669 370.8864 347.9949 498.7638 -2.2126 368.5054 370.7180 347.7924 500.3776 -2.1983 368.2316 370.4299 347.5492 501.9918 -2.1965 368.0490 370.2455 347.3234 503.6084 -2.1869 367.9841 370.1709 347.2169 505.2093 -2.1892 367.7767 369.9659 346.9577 506.8095 -2.1894 367.6303 369.8196 346.7553 508.4235 -2.1727 367.3891 369.5618 346.4738 510.0376 -2.1672 367.1592 369.3265 346.2779 511.6363 -2.1712 366.9958 369.1670 346.0482 513.2441 -2.1562 366.7370 368.8932 345.7921 514.8360 -2.1535 366.6490 368.8025 345.5790 516.4285 -2.1552 366.4468 368.6020 345.3575 518.0501 -2.1480 366.2333 368.3813 345.0965 519.6436 -2.1491 366.0652 368.2144 344.9712 521.2533 -2.1508 365.9244 368.0752 344.7772 522.8475 -2.1296 365.6915 367.8211 344.6260 524.4453 -2.1312 365.4521 367.5833 344.3741 526.0694 -2.1277 365.3754 367.5032 344.1971 527.6638 -2.1180 365.2124 367.3304 343.9778 529.2731 -2.1174 364.9215 367.0389 343.7508 530.8660 -2.0985 364.8588 366.9573 343.5530 532.4756 -2.0958 364.6372 366.7329 343.3659 534.0893 -2.1014 364.4918 366.5931 343.2084 535.7018 -2.0914 364.3160 366.4074 342.9714 537.3008 -2.0939 364.0872 366.1811 342.7633 538.8998 -2.0948 363.8711 365.9659 342.4981 540.4995 -2.0872 363.8045 365.8917 342.3501 542.1289 -2.0747 363.6527 365.7274 342.1014 543.7320 -2.0734 363.4226 365.4960 341.9740 545.3400 -2.0627 363.3413 365.4040 341.7043 546.9398 -2.0617 363.0181 365.0798 341.5485 548.5538 -2.0672 362.7272 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214.1895 1599.6519 -0.2231 237.3824 237.6054 214.0175 1601.2658 -0.2152 237.2312 237.4464 213.8769 1602.8653 -0.2135 236.9813 237.1948 213.7617 1604.4608 -0.2093 236.8335 237.0428 213.5272 1606.0689 -0.2106 236.7122 236.9228 213.4537 1607.6754 -0.2090 236.5742 236.7832 213.2684 1609.2703 -0.2026 236.3101 236.5127 213.1082 1610.8668 -0.2115 236.1216 236.3331 212.9496 1612.4743 -0.2107 235.9633 236.1741 212.8480 1614.0684 -0.2101 235.8037 236.0138 212.7042 1615.6914 -0.2047 235.6260 235.8307 212.5015 1617.2854 -0.2041 235.4118 235.6159 212.3686 1618.8930 -0.2007 235.2716 235.4723 212.1667 1620.4901 -0.2130 235.0350 235.2480 212.0538 1622.0999 -0.2048 234.8885 235.0934 211.8427 1623.7096 -0.2120 234.7243 234.9362 211.7591 1625.3074 -0.2166 234.5415 234.7582 211.5555 1626.9195 -0.1908 234.4761 234.6669 211.3657 1628.5178 -0.1921 234.2524 234.4445 211.2440 1630.1354 -0.1961 234.0629 234.2590 211.0604 1631.7256 -0.2063 233.8471 234.0533 210.9548 1633.3546 -0.1988 233.6900 233.8888 210.7599 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