DTA measure 1VFGHE) Pb(3) Date: 2024925:924 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 960.28 s Mass = 958.800 mg data_number = 1192 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2968 -0.1447 238.9973 239.1420 266.1215 2.0585 -0.1398 239.1640 239.3038 266.1120 2.8808 -0.1357 239.3727 239.5084 266.1322 3.6420 -0.1329 239.5491 239.6820 266.1550 4.5038 -0.1309 239.7490 239.8800 266.1881 5.2955 -0.1273 239.9457 240.0731 266.2094 6.0875 -0.1273 240.1117 240.2391 266.2250 6.9095 -0.1304 240.3195 240.4498 266.2515 7.6715 -0.1279 240.4953 240.6232 266.2738 8.5235 -0.1170 240.6714 240.7884 266.3165 9.3155 -0.1149 240.8463 240.9611 266.3628 10.1085 -0.1110 241.0447 241.1557 266.4179 10.9305 -0.1050 241.2140 241.3190 266.4857 11.6925 -0.1017 241.3734 241.4751 266.5538 12.5445 -0.0972 241.5811 241.6783 266.6417 13.3065 -0.0930 241.7637 241.8567 266.7288 14.1283 -0.0911 241.9343 242.0253 266.8165 14.9503 -0.0871 242.1165 242.2035 266.9145 15.7115 -0.0806 242.2825 242.3631 267.0230 16.5640 -0.0730 242.4943 242.5673 267.1528 17.3255 -0.0850 242.6437 242.7286 267.2654 18.1485 -0.1616 242.8480 243.0095 267.3906 18.9708 -0.1915 243.0160 243.2075 267.5199 19.7325 -0.1693 243.1757 243.3450 267.6473 20.5848 -0.0847 243.3721 243.4567 267.7909 21.3765 -0.0652 243.5539 243.6191 267.9464 22.1655 -0.0581 243.7124 243.7705 268.0772 22.9825 -0.0539 243.8892 243.9431 268.2199 23.7508 -0.0514 244.0562 244.1076 268.3889 24.5730 -0.0521 244.2361 244.2882 268.5494 25.3610 -0.0493 244.4110 244.4603 268.6996 26.1790 -0.0487 244.6031 244.6517 268.8715 26.9670 -0.0482 244.7745 244.8227 269.0379 27.7850 -0.0486 244.9359 244.9845 269.2074 28.5730 -0.0478 245.1204 245.1682 269.3660 29.3620 -0.0443 245.2919 245.3363 269.5441 30.1800 -0.0433 245.4585 245.5019 269.7110 30.9680 -0.0452 245.6195 245.6647 269.8645 31.7868 -0.0463 245.7942 245.8404 270.0203 32.5763 -0.0438 245.9619 246.0057 270.1749 33.3650 -0.0466 246.1195 246.1661 270.3327 34.2135 -0.0426 246.3139 246.3564 270.4977 34.9728 -0.0440 246.4631 246.5071 270.6296 35.7935 -0.0452 246.6546 246.6998 270.7734 36.5848 -0.0429 246.8365 246.8795 270.9199 37.3765 -0.0422 246.9903 247.0325 271.0628 38.1983 -0.0444 247.1645 247.2089 271.2007 38.9905 -0.0437 247.3460 247.3897 271.3433 39.8125 -0.0446 247.5239 247.5685 271.4832 40.6038 -0.0466 247.6906 247.7372 271.6081 41.3955 -0.0458 247.8529 247.8987 271.7486 42.2175 -0.0458 248.0212 248.0671 271.8854 42.9795 -0.0463 248.1788 248.2251 272.0055 43.8315 -0.0462 248.3682 248.4144 272.1508 44.5823 -0.0406 248.5247 248.5653 272.2759 45.4405 -0.0396 248.7088 248.7484 272.3952 46.2025 -0.0414 248.8576 248.8989 272.5448 47.0245 -0.0426 249.0406 249.0832 272.6682 47.8465 -0.0423 249.2007 249.2430 272.7974 48.6085 -0.0605 249.3467 249.4072 272.9149 49.4605 -0.0855 249.5360 249.6215 273.0507 50.2225 -0.0706 249.7000 249.7706 273.1755 51.0440 -0.0572 249.8728 249.9300 273.2976 51.8360 -0.0532 250.0327 250.0860 273.4224 52.6275 -0.0523 250.2028 250.2552 273.5482 53.4798 -0.0519 250.3796 250.4315 273.6866 54.2418 -0.0508 250.5360 250.5869 273.8010 55.0638 -0.0481 250.7055 250.7536 273.9239 55.8558 -0.0409 250.8625 250.9034 274.0495 56.6475 -0.0431 251.0449 251.0880 274.1685 57.4998 -0.0520 251.2252 251.2772 274.2794 58.2615 -0.0547 251.3841 251.4387 274.4041 59.0838 -0.0513 251.5347 251.5860 274.5343 59.8758 -0.0454 251.7182 251.7636 274.6711 60.6675 -0.0479 251.8836 251.9316 274.7946 61.5203 -0.0610 252.0532 252.1142 274.9472 62.2825 -0.0597 252.2130 252.2727 275.0580 63.1048 -0.0601 252.3682 252.4283 275.1844 63.8965 -0.0648 252.5429 252.6077 275.2908 64.6993 -0.0748 252.7140 252.7888 275.4235 65.5125 -0.0784 252.8628 252.9411 275.5549 66.3045 -0.0815 253.0375 253.1189 275.6858 67.1265 -0.0847 253.1891 253.2739 275.8267 67.8885 -0.0841 253.3657 253.4499 275.9393 68.7405 -0.0853 253.5369 253.6222 276.0819 69.5325 -0.0890 253.7017 253.7907 276.2106 70.3245 -0.0911 253.8428 253.9339 276.3667 71.1465 -0.0935 254.0149 254.1084 276.5091 71.9083 -0.0974 254.1770 254.2744 276.6376 72.7603 -0.1003 254.3550 254.4552 276.7770 73.5523 -0.1025 254.5043 254.6068 276.9245 74.3445 -0.1031 254.6819 254.7850 277.0799 75.1670 -0.1048 254.8532 254.9580 277.2192 75.9285 -0.1084 254.9920 255.1004 277.3558 76.7808 -0.1111 255.1487 255.2597 277.5306 77.5425 -0.1120 255.3097 255.4216 277.6464 78.3648 -0.1153 255.4769 255.5922 277.7937 79.1870 -0.1163 255.6421 255.7585 277.9426 79.9495 -0.1196 255.8123 255.9318 278.0747 80.8023 -0.1227 255.9783 256.1009 278.2207 81.5645 -0.1257 256.1190 256.2447 278.3561 82.3868 -0.1296 256.2898 256.4194 278.5048 83.1785 -0.1325 256.4615 256.5940 278.6386 83.9705 -0.1351 256.6217 256.7568 278.7666 84.8228 -0.1355 256.8018 256.9373 278.8925 85.5880 -0.1394 256.9355 257.0749 279.0129 86.3885 -0.1430 257.0974 257.2404 279.1379 87.1770 -0.1465 257.2518 257.3983 279.2630 88.0250 -0.1496 257.4184 257.5680 279.4010 88.7830 -0.1513 257.5821 257.7334 279.5166 89.6020 -0.1526 257.7430 257.8957 279.6420 90.3900 -0.1566 257.9043 258.0609 279.7613 91.1790 -0.1554 258.0646 258.2200 279.8794 92.0273 -0.1595 258.2291 258.3885 280.0101 92.7860 -0.1616 258.3789 258.5405 280.1247 93.6048 -0.1652 258.5434 258.7086 280.2477 94.3945 -0.1708 258.6898 258.8607 280.3618 95.1903 -0.1732 258.8469 259.0201 280.4672 95.9815 -0.1770 259.0178 259.1947 280.5801 96.8308 -0.1774 259.1842 259.3616 280.7135 97.5900 -0.1802 259.3376 259.5178 280.8259 98.4098 -0.1805 259.4945 259.6750 280.9573 99.2295 -0.1827 259.6729 259.8556 281.1176 99.9903 -0.1833 259.8147 259.9980 281.2404 100.8408 -0.1959 259.9903 260.1862 281.3505 101.6015 -0.2150 260.1437 260.3586 281.4941 102.4233 -0.2043 260.3053 260.5096 281.6347 103.2145 -0.2002 260.4530 260.6532 281.7448 104.0063 -0.1998 260.5985 260.7983 281.8862 104.8575 -0.2028 260.7653 260.9681 282.0389 105.6070 -0.2092 260.9206 261.1297 282.1649 106.4223 -0.2141 261.0869 261.3010 282.2911 107.2443 -0.2171 261.2556 261.4727 282.4444 108.0363 -0.2191 261.4005 261.6196 282.5748 108.8278 -0.2225 261.5539 261.7764 282.7064 109.6800 -0.2274 261.7345 261.9619 282.8650 110.4415 -0.2313 261.8838 262.1151 282.9952 111.2638 -0.2348 262.0378 262.2726 283.1293 112.0560 -0.2418 262.1866 262.4284 283.2732 112.8478 -0.2576 262.3240 262.5816 283.4158 113.6708 -0.2489 262.4907 262.7396 283.5532 114.4625 -0.2446 262.6501 262.8947 283.6772 115.2848 -0.2459 262.8108 263.0568 283.8172 116.0513 -0.2456 262.9616 263.2072 283.9722 116.8778 -0.2504 263.1133 263.3637 284.1144 117.6695 -0.2569 263.2896 263.5465 284.2359 118.5218 -0.2560 263.4572 263.7132 284.3966 119.2835 -0.2601 263.5964 263.8566 284.5148 120.1058 -0.2629 263.7508 264.0137 284.6433 120.8975 -0.2679 263.9150 264.1829 284.7710 121.6895 -0.2719 264.0729 264.3448 284.9087 122.5415 -0.2757 264.2342 264.5099 285.0481 123.3035 -0.2822 264.3798 264.6620 285.1756 124.1255 -0.2864 264.5339 264.8204 285.3328 124.9475 -0.2938 264.6988 264.9925 285.4578 125.7095 -0.2965 264.8397 265.1362 285.5864 126.5615 -0.2990 265.0065 265.3055 285.7329 127.3535 -0.2969 265.1719 265.4688 285.8662 128.1455 -0.3052 265.3343 265.6395 285.9986 128.9675 -0.3089 265.4853 265.7942 286.1274 129.7293 -0.3085 265.6175 265.9260 286.2540 130.5813 -0.3105 265.7844 266.0949 286.3970 131.3735 -0.3166 265.9305 266.2471 286.5345 132.1648 -0.3198 266.0901 266.4099 286.6567 132.9870 -0.3229 266.2492 266.5722 286.7958 133.7785 -0.3308 266.4125 266.7433 286.9209 134.6015 -0.3319 266.5630 266.8949 287.0711 135.3938 -0.3306 266.7119 267.0425 287.1972 136.1855 -0.3310 266.8784 267.2094 287.3251 136.9878 -0.3329 267.0401 267.3729 287.4608 137.8098 -0.3398 267.1997 267.5395 287.5919 138.6318 -0.3410 267.3440 267.6849 287.7319 139.3935 -0.3443 267.4877 267.8321 287.8722 140.2458 -0.3465 267.6588 268.0053 287.9905 141.0378 -0.3515 267.8082 268.1598 288.1326 141.8295 -0.3538 267.9628 268.3166 288.2527 142.6518 -0.3595 268.1214 268.4809 288.3950 143.4135 -0.3611 268.2647 268.6258 288.5245 144.2655 -0.3677 268.4234 268.7911 288.6557 145.0575 -0.3701 268.5736 268.9437 288.7825 145.8495 -0.3720 268.7323 269.1043 288.9223 146.6715 -0.3749 268.8858 269.2607 289.0453 147.4635 -0.3809 269.0472 269.4280 289.1782 148.2855 -0.3816 269.1974 269.5790 289.3039 149.0775 -0.3843 269.3604 269.7447 289.4343 149.8680 -0.3897 269.5010 269.8907 289.5642 150.6860 -0.3935 269.6604 270.0539 289.7038 151.4735 -0.3963 269.8042 270.2005 289.8171 152.2928 -0.4001 269.9668 270.3670 289.9551 153.0810 -0.4017 270.1236 270.5252 290.0911 153.8688 -0.4065 270.2599 270.6664 290.2243 154.6870 -0.4077 270.4322 270.8400 290.3471 155.4750 -0.4133 270.5809 270.9942 290.4609 156.2938 -0.4150 270.7352 271.1502 290.5942 157.0418 -0.4191 270.8715 271.2907 290.7205 157.9113 -0.4203 271.0386 271.4589 290.8641 158.6698 -0.4238 271.1743 271.5981 290.9829 159.4885 -0.4274 271.3305 271.7579 291.1174 160.2770 -0.4301 271.4884 271.9185 291.2392 161.0655 -0.4359 271.6260 272.0618 291.3660 161.9145 -0.4376 271.8002 272.2379 291.5071 162.6730 -0.4403 271.9602 272.4005 291.6399 163.4940 -0.4463 272.1270 272.5733 291.7603 164.2845 -0.4491 272.2684 272.7174 291.8918 165.0755 -0.4510 272.4068 272.8578 292.0177 165.8960 -0.4565 272.5678 273.0243 292.1532 166.6870 -0.4582 272.7119 273.1700 292.2798 167.5088 -0.4615 272.8702 273.3316 292.4011 168.3003 -0.4645 273.0260 273.4905 292.5206 169.0915 -0.4704 273.1626 273.6330 292.6556 169.9138 -0.4719 273.3258 273.7976 292.7910 170.6755 -0.4752 273.4756 273.9508 292.9121 171.5280 -0.4780 273.6460 274.1240 293.0397 172.2895 -0.4804 273.7769 274.2573 293.1691 173.1118 -0.4846 273.9169 274.4015 293.3149 173.9038 -0.4876 274.0755 274.5631 293.4313 174.6955 -0.4916 274.2172 274.7089 293.5402 175.5478 -0.4966 274.3729 274.8695 293.6781 176.3095 -0.5000 274.5426 275.0426 293.8056 177.1343 -0.5046 274.6856 275.1902 293.9253 177.9170 -0.5032 274.8453 275.3485 294.0623 178.7388 -0.5046 274.9842 275.4888 294.1812 179.5305 -0.5100 275.1340 275.6440 294.2941 180.3225 -0.5164 275.2767 275.7931 294.4058 181.1445 -0.5180 275.4241 275.9421 294.5383 181.9365 -0.5206 275.5886 276.1092 294.6687 182.7585 -0.5247 275.7621 276.2868 294.7889 183.5505 -0.5250 275.9120 276.4369 294.9136 184.3425 -0.5268 276.0542 276.5810 295.0500 185.1645 -0.5277 276.1953 276.7230 295.1848 185.9265 -0.5327 276.3427 276.8754 295.3002 186.7785 -0.5381 276.4986 277.0367 295.4378 187.5705 -0.5394 276.6482 277.1877 295.5785 188.3623 -0.5429 276.7932 277.3361 295.7211 189.1845 -0.5471 276.9454 277.4926 295.8589 189.9463 -0.5590 277.0941 277.6532 295.9934 190.7980 -0.5601 277.2635 277.8236 296.1407 191.5900 -0.5686 277.4162 277.9848 296.2765 192.3815 -0.5749 277.5530 278.1279 296.4156 193.2048 -0.5761 277.7068 278.2829 296.5692 193.9665 -0.5810 277.8652 278.4462 296.7212 194.8190 -0.5850 278.0179 278.6030 296.8566 195.5805 -0.5893 278.1778 278.7671 296.9854 196.4028 -0.5965 278.3113 278.9078 297.1261 197.2250 -0.6031 278.4695 279.0726 297.2533 198.0090 -0.6038 278.6152 279.2191 297.3862 198.8188 -0.6056 278.7803 279.3859 297.5513 199.6105 -0.6078 278.9071 279.5149 297.6875 200.4328 -0.6146 279.0667 279.6813 297.8230 201.1945 -0.6180 279.2003 279.8183 297.9683 202.0465 -0.6138 279.3744 279.9882 298.1141 202.8385 -0.6180 279.5119 280.1299 298.2521 203.6305 -0.6234 279.6622 280.2856 298.3988 204.4528 -0.6267 279.8231 280.4498 298.5352 205.2455 -0.6304 279.9671 280.5975 298.6713 206.0675 -0.6331 280.1314 280.7645 298.8180 206.8595 -0.6406 280.2682 280.9087 298.9678 207.6515 -0.6442 280.4155 281.0597 299.1125 208.4478 -0.6463 280.5464 281.1927 299.2651 209.2615 -0.6516 280.6991 281.3508 299.3928 210.0535 -0.6549 280.8628 281.5177 299.5011 210.9050 -0.6559 281.0357 281.6916 299.6540 211.6670 -0.6633 281.1766 281.8399 299.7732 212.4888 -0.6680 281.3304 281.9984 299.8919 213.3110 -0.6646 281.4770 282.1416 300.0313 214.0703 -0.6648 281.6033 282.2681 300.1366 214.9185 -0.6662 281.7788 282.4450 300.2792 215.6760 -0.6649 281.9063 282.5712 300.4034 216.4940 -0.6663 282.0794 282.7457 300.4963 217.3125 -0.6690 282.2240 282.8930 300.6211 218.0713 -0.6721 282.3607 283.0329 300.7482 218.8715 -0.6784 282.5112 283.1896 300.8743 219.7220 -0.6715 282.6679 283.3394 300.9858 220.4803 -0.6693 282.8138 283.4831 301.0743 221.3000 -0.6830 282.9617 283.6447 301.1965 222.1180 -0.6943 283.1138 283.8081 301.3316 222.8760 -0.6938 283.2493 283.9432 301.4536 223.7240 -0.6992 283.4134 284.1126 301.5796 224.5123 -0.7020 283.5585 284.2604 301.7206 225.3010 -0.7054 283.7102 284.4156 301.8304 226.1203 -0.7129 283.8697 284.5826 301.9594 226.8790 -0.7144 284.0112 284.7256 302.0803 227.7285 -0.7182 284.1664 284.8846 302.2391 228.5178 -0.7224 284.3030 285.0254 302.3719 229.3085 -0.7197 284.4580 285.1777 302.5192 230.1300 -0.7177 284.6235 285.3412 302.6507 230.8910 -0.7202 284.7543 285.4745 302.7763 231.7428 -0.7273 284.8948 285.6221 302.9330 232.5345 -0.7287 285.0508 285.7794 303.0490 233.3265 -0.7315 285.2048 285.9363 303.1795 234.1485 -0.7391 285.3601 286.0991 303.3199 234.9105 -0.7383 285.4993 286.2376 303.4487 235.7625 -0.7248 285.6394 286.3642 303.5981 236.5545 -0.7286 285.7917 286.5203 303.7295 237.3465 -0.7438 285.9533 286.6971 303.8686 238.1685 -0.7502 286.1048 286.8549 304.0075 238.9435 -0.7582 286.2378 286.9960 304.1319 239.7795 -0.7626 286.3893 287.1519 304.2653 240.5415 -0.7551 286.5375 287.2926 304.4245 241.3935 -0.7583 286.6902 287.4485 304.5589 242.1555 -0.7601 286.8270 287.5871 304.6727 242.9775 -0.7675 286.9785 287.7460 304.8135 243.7995 -0.7765 287.1484 287.9249 304.9561 244.5615 -0.7891 287.2887 288.0778 305.0981 245.4135 -0.7878 287.4454 288.2333 305.2150 246.2055 -0.7901 287.5805 288.3706 305.3562 246.9975 -0.7907 287.7272 288.5179 305.5031 247.8193 -0.7961 287.8792 288.6753 305.6409 248.5810 -0.8082 288.0194 288.8277 305.7554 249.4330 -0.8145 288.1843 288.9988 305.9068 250.2250 -0.8245 288.3336 289.1580 306.0438 251.0165 -0.8327 288.4623 289.2950 306.1709 251.8390 -0.8363 288.6097 289.4459 306.3116 252.6005 -0.8405 288.7564 289.5969 306.4314 253.4528 -0.8418 288.9155 289.7573 306.5857 254.2448 -0.8454 289.0655 289.9109 306.7231 255.0365 -0.8506 289.2123 290.0629 306.8555 255.8588 -0.8523 289.3600 290.2123 306.9920 256.6205 -0.8514 289.4935 290.3449 307.1114 257.4728 -0.8554 289.6496 290.5051 307.2505 258.2648 -0.8603 289.7988 290.6591 307.3817 259.0565 -0.8639 289.9561 290.8199 307.5197 259.8543 -0.8663 290.1001 290.9663 307.6708 260.6765 -0.8671 290.2579 291.1249 307.8034 261.4688 -0.8717 290.3895 291.2612 307.9220 262.2615 -0.8768 290.5357 291.4125 308.0386 263.1140 -0.8785 290.7043 291.5828 308.1790 263.8765 -0.8809 290.8370 291.7179 308.3005 264.6985 -0.8831 290.9783 291.8614 308.4468 265.4905 -0.8860 291.1367 292.0227 308.5806 266.2825 -0.8892 291.2890 292.1782 308.6924 267.1345 -0.8916 291.4588 292.3504 308.8347 267.8965 -0.8979 291.5926 292.4906 308.9574 268.7183 -0.8995 291.7545 292.6540 309.0952 269.5103 -0.9009 291.8755 292.7764 309.2318 270.3025 -0.9017 292.0309 292.9325 309.3577 271.1550 -0.9055 292.1803 293.0858 309.4905 271.9165 -0.9117 292.3234 293.2351 309.6026 272.7395 -0.9142 292.4757 293.3899 309.7370 273.5318 -0.9180 292.6110 293.5290 309.8626 274.3235 -0.9185 292.7441 293.6627 309.9821 275.1758 -0.9222 292.9178 293.8400 310.1386 275.9375 -0.9252 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